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14 pages, 11137 KB  
Article
Ultra-Precision Turning of Ferrous and Non-Ferrous Material by Sapphire Tool
by Chung Chi Chiu, Yintian Xing, Wai Sze Yip and Suet To
Micromachines 2026, 17(6), 641; https://doi.org/10.3390/mi17060641 - 22 May 2026
Abstract
Ultra-precision machining of ferrous alloys remains challenging because conventional diamond tools suffer severe thermochemical wear, whereas ultrasonic vibration-assisted cutting requires complex and costly equipment. This study investigates single-crystal sapphire as an alternative cutting-tool material for ultra-precision machining of both non-ferrous and ferrous metals. [...] Read more.
Ultra-precision machining of ferrous alloys remains challenging because conventional diamond tools suffer severe thermochemical wear, whereas ultrasonic vibration-assisted cutting requires complex and costly equipment. This study investigates single-crystal sapphire as an alternative cutting-tool material for ultra-precision machining of both non-ferrous and ferrous metals. A sapphire tool was fabricated from a polished wafer, laser-shaped into an equilateral triangular insert, vacuum-brazed onto a tungsten carbide carrier, and finished by ultra-fine grinding to yield a well-defined cutting edge. Ultra-precision turning experiments were conducted on copper and 420 stainless steel using a Moore Nanotech 350FG lathe, and the performance of the sapphire tool was benchmarked against conventional diamond (copper) and cubic boron nitride (CBN) tools (stainless steel) under comparable cutting conditions. Surface roughness (Ra) and topography were characterized using an optical surface profiler, while scanning electron microscopy and atomic force microscopy were employed to assess tool wear and cutting-edge geometry. The sapphire tool produced mirror-like surfaces with average surface roughness (Ra) values of 6.4 nm on copper and 39.1 nm on 420 stainless steel, compared with 1.3 nm for diamond on copper and 92.9 nm for CBN on stainless steel. Across both materials, sapphire generated regular, stable tool marks and exhibited minimal wear, with no catastrophic edge degradation or clear evidence of severe chemical interaction with the steel workpiece. These results demonstrate that sapphire is a viable tool material for extending diamond turning-level surface quality to stainless steel without ultrasonic assistance. Full article
(This article belongs to the Section D:Materials and Processing)
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19 pages, 3133 KB  
Article
Microstructure Evolution and Thermal Performance Enhancement of Ultrasonically Brazed Cu/Al Composite Heat Sinks via Gradient Heat Treatment
by Ming-Jun Xie, Peng-Fei Wang, Lin Gao, Yan-Fei Bian and Zhi Cheng
Metals 2026, 16(5), 517; https://doi.org/10.3390/met16050517 - 11 May 2026
Viewed by 203
Abstract
Aiming at the urgent heat dissipation demands of high-power, high-integration electronic devices, Cu/Al composite heat sinks combine the high thermal conductivity of copper and the lightweight advantage of aluminum, becoming a mainstream solution for advanced thermal management systems. The significant physicochemical differences between [...] Read more.
Aiming at the urgent heat dissipation demands of high-power, high-integration electronic devices, Cu/Al composite heat sinks combine the high thermal conductivity of copper and the lightweight advantage of aluminum, becoming a mainstream solution for advanced thermal management systems. The significant physicochemical differences between Cu and Al, however, make high-quality joining a technical bottleneck. In this study, flux-free ultrasonic brazing with a Zn-based filler metal was used to join 6061 aluminum alloy and industrial pure copper. Gradient heat treatment (55–300 °C) was subsequently applied to systematically investigate its effect on the microstructure, microhardness, and thermal properties of the joints. The results show that the as-brazed joint exhibited excellent bonding (97.3% bonding rate) and shear strength (95.24 MPa). The weld seam consisted of Zn solid solution, Cu solid solution, and Al-Cu-Zn ternary compounds. Heat treatment did not induce new phases but led to the coarsening of Zn-Al-Cu compounds and aggregation of the eutectic structure, reducing grain boundaries. Consequently, the microhardness at the weld center varied non-monotonically, and the thermal conductivity of the joint showed an overall increasing trend with rising heat treatment temperature. This enhancement is attributed to reduced phonon scattering at diminished grain boundaries. This study clarifies the heat treatment–microstructure–thermal properties relationship, providing important guidance for the thermal performance optimization of Cu/Al composite heat sinks. Full article
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25 pages, 1286 KB  
Review
Progress and Challenges in Joining for Precision Endoscope Fabrication
by Peiquan Xu, Xiaohao Zheng, Leijun Li and Ziyi Wang
Sensors 2026, 26(9), 2828; https://doi.org/10.3390/s26092828 - 1 May 2026
Viewed by 710
Abstract
This review summarizes the base materials, joining methods, filler materials, and principal technical challenges in endoscope joining fabrication, and proposes practical strategies to improve joint reliability under clinical constraints. We conducted a comprehensive search in multiple databases, including Web of Science, Google Scholar, [...] Read more.
This review summarizes the base materials, joining methods, filler materials, and principal technical challenges in endoscope joining fabrication, and proposes practical strategies to improve joint reliability under clinical constraints. We conducted a comprehensive search in multiple databases, including Web of Science, Google Scholar, patent databases, Scopus databases, and Medline (via PubMed), for articles on the joining for precision endoscope fabrication, covering the period from 1950 to 2026. We employed the combinations of keywords, “endoscopy”, “minimally invasive surgery”, “welding”, “joining”, “sealing”, “soldering”, “bonding”, and “brazing”. Approximately 500 references were retrieved. After excluding duplicates and irrelevant studies, 158 publications met the inclusion criteria. Data on base materials, joining, processes, filler materials, and technical issues related to sterilization, corrosion, and microstructural evolution were extracted and analyzed. Endoscopes are multi-material systems, involving metallic biomaterials (stainless steels (SSs), titanium alloys, nickel-based alloys, etc.), optical functional materials (glass, sapphire, quartz, etc.), engineering plastics, ceramics, composite materials, and coatings. Joining, sealing, and functional integration have been achieved via adhesive bonding, laser soldering, laser brazing, wave soldering, reflow soldering, fusion welding, and other joining techniques. The main challenges include how to reliably join highly mismatched dissimilar materials, how to fabricate low-residual-stress joints, and how to increase the long-term resistance to sterilization-induced degradation and thermal aging over repeated 100–200 °C thermal cycles. Conventional joining techniques struggle to balance mechanical integrity, joint hermeticity, and long-term stability under such harsh cyclic conditions. The resulting joints may suffer surface yellowing, interfacial debonding, microcracking, delamination, or progressive property degradation during service. We propose the following three strategies to achieve reliable, low-residual-stress, and sterilization-resistant joining of dissimilar materials for endoscopes: (1) A synergistic design that combines thin-film engineering (including evaporation, sputtering, and electroplating) with silver anti-oxidation layers is proposed to reduce residual stresses and to enhance the joint hermeticity. (2) To develop principles for the selection of multi-joining processes to achieve the multi-material integration and functional assembly of dissimilar material components. (3) To develop the laser-based joining methods (fusion, brazing, or braze-welding) for precision control of heat input, bonding quality, and the least damage to the heat-sensitive components. Full article
(This article belongs to the Section Biomedical Sensors)
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15 pages, 4538 KB  
Article
Microstructure and Processing Performance of Brazed Diamond Micro-Powder Grinding Wheel with Ni-Based Filler Alloy
by Shuyi Wang, Haozhong Xiao and Bing Xiao
Materials 2026, 19(9), 1800; https://doi.org/10.3390/ma19091800 - 28 Apr 2026
Viewed by 266
Abstract
In this study, a brazed diamond micro-powder grinding wheel with Ni-based filler metal was fabricated, which achieved one-step grinding forming of YG-6 cemented carbide rods. The interfacial microstructure, elemental diffusion behavior, and interfacial phases of the brazed diamond micro-powder joint were systematically characterized. [...] Read more.
In this study, a brazed diamond micro-powder grinding wheel with Ni-based filler metal was fabricated, which achieved one-step grinding forming of YG-6 cemented carbide rods. The interfacial microstructure, elemental diffusion behavior, and interfacial phases of the brazed diamond micro-powder joint were systematically characterized. Furthermore, the machining performance of the brazed diamond micro-powder grinding wheel was comprehensively evaluated in combination with its service life and the surface roughness of the machined YG-6 cemented carbide rods. The results show that the Ni-based filler exhibits good wettability to diamond micro-powder particles, and the diamonds have a reasonable protrusion height in the filler layer, with no graphitization observed on the surface of the brazed diamonds. During the brazing process, the active element Cr continuously segregates toward the diamond surfaces and reacts progressively with dissolved C atoms on the diamond surfaces, eventually forming a lath-shaped Cr–C compound layer on the diamond surfaces. XRD results identify this compound as Cr3C2. Elemental diffusion occurs between the filler layer and the steel substrate, forming a Fe–Ni solid solution diffusion zone. Consequently, the Ni-based filler forms a reliable chemical metallurgical bond with both the diamond micro-powder particles and the steel substrate. The as-prepared brazed diamond micro-powder grinding wheel exhibits excellent service life: a single wheel can grind more than 1300 YG-6 cemented carbide rods on average before failure. The surface roughness (Ra) of the machined YG-6 cemented carbide workpieces remains below 1.6 μm throughout all processing stages, which satisfies the requirements for one-step precision grinding. Full article
(This article belongs to the Section Metals and Alloys)
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38 pages, 24690 KB  
Review
Glass-Ceramic Bonding Agents for High-Performance Grinding: A Material Design Framework Based on Multi-System Comparisons
by Yufei Li, Le Tian, Longyao Xu, Mingmin Li, Huaying Bian, Xuetao Wang and Shuanghua Wang
Inorganics 2026, 14(4), 116; https://doi.org/10.3390/inorganics14040116 - 20 Apr 2026
Viewed by 1384
Abstract
This review systematically analyzes the technological progress, structural characteristics, and performance disparities among various diamond grinding wheel bond systems, aiming to establish a unified performance evaluation framework. This framework clarifies material selection criteria and highlights promising research directions. Eight prevalent bond systems are [...] Read more.
This review systematically analyzes the technological progress, structural characteristics, and performance disparities among various diamond grinding wheel bond systems, aiming to establish a unified performance evaluation framework. This framework clarifies material selection criteria and highlights promising research directions. Eight prevalent bond systems are encompassed: resin, metal, ceramic, brazing, electroplating, composite, additive manufacturing, and glass-ceramics. A comparative analysis of these systems is conducted across multiple dimensions. Key evaluation metrics primarily include bond strength, thermal stability, self-sharpening capability, thermal conductivity, and formability. Considerable variations in these indicators are observed across the different bonding agents. Each system presents distinct advantages alongside inherent limitations. Within the constructed multi-metric framework, glass-ceramic bonding agents demonstrate high comprehensive potential in critical aspects such as bond strength and thermal stability, underscoring their research value as a novel high-performance bond system. Current primary challenges focus on the regulation of crystallization kinetics, the design of interfacial reaction layers, and multiscale performance prediction. Future research may advance along several paths. Synergistic design of material composition and microstructure is essential, while in-depth investigation into multiphysics coupling mechanisms remains necessary. Furthermore, data-driven material optimization methods are poised to unlock new possibilities for bond development. These approaches are expected to facilitate the precise design and application of high-performance diamond grinding wheel bonds. Full article
(This article belongs to the Special Issue Novel Ceramics and Refractory Composites)
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23 pages, 11106 KB  
Article
Design of CoNiCrFeCu-xSc High-Entropy Alloy Fillers for Braze-Welding of WC-Co to Steel
by Peiquan Xu, Shicheng Sun, Benben Li and Leijun Li
Materials 2026, 19(8), 1606; https://doi.org/10.3390/ma19081606 - 16 Apr 2026
Viewed by 367
Abstract
Efficient joining of hard metals to steels is crucial for supporting sustainable manufacturing under emissions strategies to minimize CO2. CoNiCrFeCu high-entropy alloy containing scandium (Sc) was designed as a filler for laser braze-welding of WC-Co and steel. The designed compositions with [...] Read more.
Efficient joining of hard metals to steels is crucial for supporting sustainable manufacturing under emissions strategies to minimize CO2. CoNiCrFeCu high-entropy alloy containing scandium (Sc) was designed as a filler for laser braze-welding of WC-Co and steel. The designed compositions with different Sc levels were melted and cast in a high-vacuum non-consumable arc furnace. The results showed that the as-cast microstructure was a complex mixture of a networked Ni2Si, elongated Cr-Fe-Co solid-solution phase, and Fe-Ni-Co-Cu solid-solution phase. Scandium was shown to have formed compounds with nickel/cobalt and copper. The TG-DSC analysis confirmed that the melting points of the designed compositions were between 973.7 °C and 981.5 °C. The maximum spreading area of the CoNiCrFeCu-0.9Sc composition on AISI 1045 steel was 64.83 mm2, and on the WC-Co cermet it was 78.63 mm2. The interface between the fusion zone and AISI 1045 steel exhibited an epitaxial growth of dendrites from the steel base metal. The interface between WC-Co and the fusion zone exhibited a partial penetration of brazing filler into the Co matrix, forming a metallurgical bonding between the dissimilar materials. Sc, as an alloying element in the filler metal, enhanced the bond formation because it decreased the solidus temperature and increased wetting. Full article
(This article belongs to the Section Metals and Alloys)
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19 pages, 8878 KB  
Article
Comparative Performance of Ni- and Fe-Based Mixed Alloy Brazed Coatings via Laser Remelting
by Marco Brand, Mareen Goßling, Ion-Dragoş Uțu and Gabriela Mărginean
Lubricants 2026, 14(4), 142; https://doi.org/10.3390/lubricants14040142 - 29 Mar 2026
Viewed by 612
Abstract
Traditionally, repairing coated substrates requires completely removing damaged, wear-resistant layers before recoating. This process leads to high costs, extended downtime, and material waste. Flexible brazing tapes, which are composed of alloy powder and an organic binder, offer an alternative to full coating removal [...] Read more.
Traditionally, repairing coated substrates requires completely removing damaged, wear-resistant layers before recoating. This process leads to high costs, extended downtime, and material waste. Flexible brazing tapes, which are composed of alloy powder and an organic binder, offer an alternative to full coating removal for targeted repairs. Despite this, the process of vacuum brazing these tapes may lead to the formation of defects, including pores caused by trapped gases or residual binder, which compromise coating durability and corrosion resistance. This study focuses on the utilization of laser remelting as a method for post-processing nickel- and iron-based mixed alloy brazing tapes, with the aim of improving the integrity of the coating. Surface quality was assessed via microscopy and microhardness testing by systematically varying laser power, scanning speed, and hatch distance. Among the parameters studied, the most suitable laser parameter combination was found to be 350 W laser power, 250 mm/s scanning speed, and a hatch distance of 0.02 mm. These parameters yielded crack- and pore-free coatings with a remelting depth of 160.3 ± 17.2 µm and a microhardness of 701 ± 23 HV1, which is an 85% increase over as-brazed samples. Wear testing revealed a reduced coefficient of friction, and electrochemical corrosion tests showed lower corrosion current density and enhanced repassivation behavior in remelted coatings. These improvements demonstrate that laser remelting significantly enhances the microstructure, hardness, wear resistance, and corrosion performance of brazed coatings, providing an effective method for localized repair while minimizing material consumption and processing duration. Full article
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17 pages, 4627 KB  
Article
A Novel Bi2O3-TeO2-B2O3-CuO Glass for Copper Metallization of Si3N4: Wettability, Thermal Stability, and Bonding Performance
by Chaochen Chen, Fang Lei, Shiqing Dang, Hongyang Zhang, Ying Shi and Haohong Chen
Ceramics 2026, 9(4), 37; https://doi.org/10.3390/ceramics9040037 - 26 Mar 2026
Viewed by 684
Abstract
To address the lack of suitable glass systems for silicon nitride (Si3N4) surface metallization, which requires high wettability and thermal stability, and robust bonding between the copper layer and the ceramic substrate, a novel Bi2O3-TeO [...] Read more.
To address the lack of suitable glass systems for silicon nitride (Si3N4) surface metallization, which requires high wettability and thermal stability, and robust bonding between the copper layer and the ceramic substrate, a novel Bi2O3-TeO2-B2O3-CuO glass system was developed. This study systematically investigated the influence of Bi2O3 concentration, glass properties, optimized paste composition, and brazing mechanism using phase analysis, microstructural characterization, particle size statistics, thermal analysis, and tensile testing. An optimal glass composition containing 20 mol% Bi2O3 was identified, exhibiting high thermal stability (ΔT = 224 °C) and a coefficient of thermal expansion of 9.63 × 10−6 °C−1. At a brazing temperature of 750 °C, the glass demonstrated excellent wettability with a contact angle of 27°. A conductive paste comprising 94 wt% Cu and 6 wt% glass yielded a thick film with a minimum resistivity of 6.25 μΩ·cm and a maximum tensile strength of 25.2 MPa. Mechanism analysis revealed that the superior wettability drives the liquid glass phase to form a thin intermediate layer that significantly reinforces adhesion. These findings contribute to the research and development of subsequent novel glass systems with superior performance. Full article
(This article belongs to the Special Issue Advances in Ceramics, 3rd Edition)
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18 pages, 4053 KB  
Article
Effect of Sn/Ni Addition on the Microstructure and Properties of Flux-Cored Brass Filler Metal and Its Brazed Joints
by Wei Liu, Xin Huang, Lijun Ren, Jungang Sun and Yongzhou Bu
Metals 2026, 16(3), 348; https://doi.org/10.3390/met16030348 - 20 Mar 2026
Viewed by 342
Abstract
In this study, Sn and Ni powders were incorporated into the flux core of brass brazing filler metals, with alloying achieved via in situ synthesis during brazing. The effects of Sn/Ni single and composite additions on the microstructure, melting characteristics, wettability on Q235 [...] Read more.
In this study, Sn and Ni powders were incorporated into the flux core of brass brazing filler metals, with alloying achieved via in situ synthesis during brazing. The effects of Sn/Ni single and composite additions on the microstructure, melting characteristics, wettability on Q235 steel, and tensile strength of corresponding brazed joints were systematically investigated. Sn addition increased the β-phase fraction, reduced the solidus temperature, and significantly improved wettability—with a maximum unit spreading area of 4.22 mm2/mg at 20 wt.% Sn (2.85 times that of the Sn/Ni-free baseline). However, coarse β-phase grains and their transformation to brittle β′-phase at room temperature resulted in no enhancement of joint tensile strength. Ni addition expanded the α-phase region, refined grains, and induced solid solution strengthening of the α-phase matrix; joint tensile strength peaked at 501 MPa at 20 wt.% Ni (65% higher than the baseline). Excessive Ni (≥40 wt.%) deteriorated wettability due to reduced molten superheat, and 50 wt.% Ni caused α-phase over-strengthening and embrittlement, leading to a sharp strength drop to 214 MPa. The composite addition of 3 wt.% Sn + 10 wt.% Ni reconstructed the filler metal into a refined, uniform grid-like (α + β) dual-phase structure without new phase formation, realizing synergistic optimization of wettability and mechanical properties. The co-added sample exhibited optimal performance, with a unit spreading area of 4.51 mm2/mg and joint tensile strength of 584 MPa (206% and 93% higher than the baseline, respectively). This improvement was attributed to the coupling of uniform stress dispersion by the grid-like microstructure and dual-element functional complementation (Sn for wettability and β-phase strengthening; Ni for grain refinement and α-phase strengthening). This work provides a feasible alloying modification strategy for brass flux-cored brazing filler metals, and the revealed microstructure-performance regulation mechanism offers a valuable reference for developing high-performance brass brazing filler metals. Full article
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14 pages, 7475 KB  
Article
Microstructure and Properties of a Four-Layer Aluminum Alloy Composite Sheet for Brazed Structural Applications
by Ying Liu, Zhengfu Zhang, Yu Cao, Zhuoqiang Mo, Yuejing Bin and Xiaoping Yang
Metals 2026, 16(3), 344; https://doi.org/10.3390/met16030344 - 19 Mar 2026
Viewed by 502
Abstract
Aluminum alloy composites are widely used in various high-end fields due to their ability to give full play to the advantages of each layer. However, the traditional three-layer aluminum alloy composite sheet cannot meet the current demand. In this study, composite rolling technology [...] Read more.
Aluminum alloy composites are widely used in various high-end fields due to their ability to give full play to the advantages of each layer. However, the traditional three-layer aluminum alloy composite sheet cannot meet the current demand. In this study, composite rolling technology is adopted to combine three different alloys (4045, 3003, and 6061) for fabricating a 2.0 mm thick four-layer aluminum alloy composite sheet (4045/3003/6061/3003). The microstructure and properties of the composite sheet were analyzed by simulating the vacuum brazing process (595 °C/10 min) and artificial aging treatment (175 °C for 12 h), combined with characterization techniques including scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). The results show that the four-layer composite sheet exhibits lower Si diffusion after brazing, where the intermediate 3003 aluminum alloy layers effectively prevent the combination of magnesium (Mg) and the 4045 alloy. Compared with the brazed three-layer composite sheet the ultimate tensile strength and yield strength of the four-layer composite sheet after aging are increased by 139.7% and 326.6%, respectively, indicating significant improvement in its mechanical properties. This study provides a reference for the production of four-layer aluminum alloy composite sheet and contributes to the development of rail transit. Full article
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11 pages, 3320 KB  
Article
Research on the Corrosion Behavior of Zn-2Al Filler Metals
by Yue Zhao, Xuewen Wang, Shirui Guo, Lujun Cui, Yinghao Cui, Yuanxun Shen, Quanbin Lu, Xiaolei Li and Yongqian Chen
Crystals 2026, 16(3), 188; https://doi.org/10.3390/cryst16030188 - 10 Mar 2026
Viewed by 417
Abstract
The performance of flux-cored Zn-Al filler metal is susceptible to corrosion-induced degradation, thereby impairing its brazability. In this study, flux-cored Zn-2Al filler metals are prepared, and the salt spray test is subsequently carried out on the prepared filler metals. Scanning transmission electron microscope [...] Read more.
The performance of flux-cored Zn-Al filler metal is susceptible to corrosion-induced degradation, thereby impairing its brazability. In this study, flux-cored Zn-2Al filler metals are prepared, and the salt spray test is subsequently carried out on the prepared filler metals. Scanning transmission electron microscope is used to identify the phases in filler metals. An electrochemical workstation was employed to test the electrochemical performance of the filler metals. The corrosion pathways and evolution patterns of filler metals are analyzed. The findings demonstrate that the corrosion type of the filler metals is electrochemical corrosion, characterized primarily by the corrosion modes of pitting corrosion and intergranular corrosion. The cathode is the α-Al phase, which undergoes an oxygen-absorption corrosion reaction, while the anode is the η-Zn phase, which experiences corrosion and subsequent dissolution. The continuously distributed α-Al phase bands and discontinuously distributed large-sized rod-like α-Al phases accelerate the corrosion rate, and the corrosion propagation rate along the extrusion direction is higher than that in the radially inward direction. After 15 days of salt spray corrosion, the tensile strength of filler metals decreases by 16.2%, and the elongation rate decreases to 3.73%. Full article
(This article belongs to the Section Crystalline Metals and Alloys)
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13 pages, 6394 KB  
Article
Effect of Rapid Solidification on the Structure and Properties of Ag–Cu–(Ti,Zr) Brazing Alloys for Metal–Ceramic Joining
by Sofya Terekhova, Alexander Ivannikov, Anton Abramov, Veronika Kirillova, Vladimir Mikhalchik, Alexander Bazhenov, Pavel Morokhov, Ivan Fedotov, Ivan Klyushin, Nikita Popov and Oleg Sevryukov
J. Manuf. Mater. Process. 2026, 10(3), 90; https://doi.org/10.3390/jmmp10030090 - 3 Mar 2026
Viewed by 690
Abstract
Four compositions of rapidly quenched ribbon brazing alloys based on Ag–Cu–Ti (Ag–26.5Cu–1.5Ti, Ag–25Cu–5Ti) and Ag–Cu–Zr (Ag–26.5Cu–1.5Zr, Ag–25Cu–5Zr) systems were produced. Initial ingots were synthesized by arc melting. Rapidly solidified ribbons, 50–100 μm thick, were then fabricated from homogenized ingots using a “Crystall-702” facility. [...] Read more.
Four compositions of rapidly quenched ribbon brazing alloys based on Ag–Cu–Ti (Ag–26.5Cu–1.5Ti, Ag–25Cu–5Ti) and Ag–Cu–Zr (Ag–26.5Cu–1.5Zr, Ag–25Cu–5Zr) systems were produced. Initial ingots were synthesized by arc melting. Rapidly solidified ribbons, 50–100 μm thick, were then fabricated from homogenized ingots using a “Crystall-702” facility. A comparative analysis of the microstructure and phase composition of both the ingots and ribbons was conducted using scanning electron microscopy and X-ray diffraction. The analysis revealed the presence of Cu4Ti and CuTi intermetallic compounds in the Ag–Cu–Ti alloys, and AgCu4Zr and Zr2Cu in the Ag–Cu–Zr alloys. Rapid quenching was found to produce metastable structures and significantly refine the intermetallic phases. Microhardness measurements of the ingot and ribbon states demonstrated a substantial influence of the processing route on the mechanical properties. The tensile strength of the ingots was also evaluated. The wetting angles of the rapidly quenched alloy melts on 99% Al2O3 (alumina) ceramic substrates under vacuum were determined. All produced ribbons, except for the Ag–26.5Cu–1.5Zr composition, demonstrated adequate wettability. Thus, these materials are considered promising for further research into heat-resistant metal–ceramic joints. Full article
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77 pages, 14413 KB  
Review
Welding Techniques and Microstructural Control for Dissimilar Cu/Al Joints
by Dong Jin, Juan Pu, Xiaohui Shi, Xiangping Xu, Zhaoqi Zhang and Fei Long
Crystals 2026, 16(3), 172; https://doi.org/10.3390/cryst16030172 - 2 Mar 2026
Viewed by 1332
Abstract
Welding copper (Cu) and aluminum (Al) is highly demanded for lightweight and cost-effective manufacturing. However, it faces significant challenges. First, substantial differences in physical properties may lead to high residual stresses and distortion. Second, brittle intermetallic compounds (IMCs) readily form at the interface, [...] Read more.
Welding copper (Cu) and aluminum (Al) is highly demanded for lightweight and cost-effective manufacturing. However, it faces significant challenges. First, substantial differences in physical properties may lead to high residual stresses and distortion. Second, brittle intermetallic compounds (IMCs) readily form at the interface, severely compromising the joint’s mechanical properties and electrical conductivity. Third, the native oxide film on Al impedes effective wetting and bonding. Therefore, effective control over the interfacial microstructure of the welded joint is essential. This review provides a critical analysis and comparison of several typical welding techniques, including laser welding (LW), friction stir welding (FSW), ultrasonic welding (UW), brazing and soldering, and welding–brazing. These analyses focus on their process characteristics, joint microstructures, and corresponding formation mechanisms. Furthermore, this review synthesizes key strategies for enhancing joint quality, including process parameter optimization, introduction of functional interlayers, and external assistance, aimed at optimizing joint microstructure and minimizing defects. Based on the analysis, this work provides comparative insights into process selection and microstructure control, and highlights future directions: advancing novel methods such as magnetic pulse welding and transient liquid phase bonding; developing intelligent real-time process control to suppress brittle IMCs and associated defects; promoting sustainable practices and establishing standardized performance evaluation; and systematically investigating long-term reliability to support the industrial application of robust Cu/Al joints. Full article
(This article belongs to the Special Issue Surface Modification Treatments of Metallic Materials (2nd Edition))
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16 pages, 9682 KB  
Article
Quasi-Static and Fatigue Strength of Copper-Brazed Stainless Steel
by Srečko Glodež, Tonica Bončina, Žan Dvoršak, Branko Nečemer and Franc Zupanič
Appl. Sci. 2026, 16(4), 2160; https://doi.org/10.3390/app16042160 - 23 Feb 2026
Cited by 1 | Viewed by 598
Abstract
This study investigates the quasi-static and fatigue strength of copper-brazed 316L stainless steel. Quasi-static and fatigue tests were conducted at room temperature (20 °C) using a Zwick/Roell Vibrophore 100 testing machine and specially designed copper-brazed specimens. Two types of specimens were prepared—tensile and [...] Read more.
This study investigates the quasi-static and fatigue strength of copper-brazed 316L stainless steel. Quasi-static and fatigue tests were conducted at room temperature (20 °C) using a Zwick/Roell Vibrophore 100 testing machine and specially designed copper-brazed specimens. Two types of specimens were prepared—tensile and shear specimens—to obtain the stress–strain relationships (σ–ε and τ–ε) and the fatigue life (S–N) curves. Based on the experimental results, the quasi-static and fatigue strengths of the copper-brazed joints under external tensile and shear loading were evaluated. The fatigue tests reveal that the shear fatigue strength is significantly lower than the tensile fatigue strength. Furthermore, a comprehensive investigation was conducted, focusing on the metallographic characterisation of the brazed joint and fractographic analyses of fracture surfaces obtained under quasi-static and fatigue loading, with particular emphasis on the shear strength of the investigated brazed joint. The experimental results obtained may be crucial for designing engineering structures (e.g., plate heat exchangers), where copper-brazed joints are the weakest members of the structure. Full article
(This article belongs to the Special Issue Fatigue and Fracture Behavior of Engineering Materials)
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16 pages, 3160 KB  
Article
Mechanical Behavior of a Reinforced Hourglass Lattice Structure
by Chong Liu, Wen Yang, Baifeng Sha, Henghao Zhang, Yongzhao Hou, Cheng Zhong, Meixian Jiang and Yongqiang Ma
Materials 2026, 19(4), 777; https://doi.org/10.3390/ma19040777 - 16 Feb 2026
Viewed by 455
Abstract
Inspired by the networked venation structures, a reinforced hourglass lattice structure is proposed to overcome the insufficient face–core interaction and premature face-sheet buckling that limit the compressive performance of conventional lattice sandwich structures. The reinforced hourglass lattice structure is fabricated using a cutting–interlocking [...] Read more.
Inspired by the networked venation structures, a reinforced hourglass lattice structure is proposed to overcome the insufficient face–core interaction and premature face-sheet buckling that limit the compressive performance of conventional lattice sandwich structures. The reinforced hourglass lattice structure is fabricated using a cutting–interlocking assembly followed by vacuum brazing, enabling enhanced connectivity and increased effective contact area between the lattice core and the face sheets. Quasi-static in-plane and out-of-plane compression experiments, together with finite element simulations and theoretical analysis, are conducted to systematically investigate the compressive behavior of the reinforced hourglass lattice structure. The results demonstrate that the out-of-plane compressive strength of the reinforced hourglass lattice structure exhibits a pronounced dependence on relative density, increasing monotonically with increasing density. Under in-plane compression, comparative studies with conventional hourglass and pyramidal lattice structures reveal that the proposed reinforcement strategy significantly improves face–core load transfer and effectively suppresses local buckling of thin face sheets. As a consequence, the reinforced hourglass lattice structure exhibits higher initial stiffness, enhanced compressive strength, and superior structural stability. These findings indicate that reinforcing the reinforced hourglass core provides an effective design strategy for improving the compressive performance of lattice sandwich structures by strengthening face–core interaction and mitigating face-sheet buckling. Full article
(This article belongs to the Section Materials Simulation and Design)
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