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17 pages, 4972 KB  
Article
Effect of Automated Multi-Pass MAG Welding Parameters on the Fracture Toughness and Hydrogen Embrittlement Susceptibility of API 5L X70 Pipeline Steel
by Danko Ćorić, Kristijan Jurgec, Ivica Garašić and Maja Remenar
Processes 2026, 14(7), 1069; https://doi.org/10.3390/pr14071069 - 27 Mar 2026
Viewed by 307
Abstract
Welded joints in API 5L X70 pipeline steel represent critical locations for pipelines intended for hydrogen service because welding can create microstructural inhomogeneity, stress concentrations, and uneven mechanical properties that can promote hydrogen-assisted degradation. In hydrogen-containing environments, these effects may manifest as reduced [...] Read more.
Welded joints in API 5L X70 pipeline steel represent critical locations for pipelines intended for hydrogen service because welding can create microstructural inhomogeneity, stress concentrations, and uneven mechanical properties that can promote hydrogen-assisted degradation. In hydrogen-containing environments, these effects may manifest as reduced ductility, loss of fracture resistance, and increased cracking susceptibility, particularly in the weld metal and heat-affected zone. Therefore, welding procedures for X70 intended for hydrogen applications must be evaluated using systematic mechanical testing and microstructural characterization under defined hydrogen exposure conditions. The study investigates the detrimental effects of hydrogen on the mechanical integrity of pipeline materials, focusing on welded joints of the API 5L X70 steel, a candidate material for use in hydrogen-containing environments. The weldability and structural performance of the X70 pipeline steel joints in hydrogen environments, produced using automated multi-pass metal active gas (MAG) welding, was experimentally studied. Welding was performed on a DN800 pipe with precise control over welding parameters. Comprehensive analyses were conducted on the welded joints, including microstructure examinations, hardness measurements, slow strain rate testing in high-pressure gaseous H2 with a N2 baseline and fracture toughness testing. In high-pressure hydrogen SSRT showed a moderate reduction in ductility relative to nitrogen, with reduction of area decreasing from 81.2% (N2) to 69.1 and 71.5% (H2), while time-to-failure remained comparable (475 min in N2 vs. 497 and 496 min in H2) Ultimate tensile strength was not reduced (579 MPa in N2 vs. 609 and 597 MPa in H2). Secondary surface cracks were observed only on specimens tested in hydrogen. Fracture mechanics testing after hydrogen exposure yielded KIH values of 58–59 MPa√m in the weld metal and 57–61 MPa√m in the HAZ, exceeding the 55 MPa√m acceptance threshold applied in this study. The results highlight the necessity of optimized welding techniques and targeted material analyses to ensure the safety and durability of pipelines in hydrogen-rich environments, thereby contributing to the development of reliable infrastructure for sustainable energy systems. Full article
(This article belongs to the Section Materials Processes)
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24 pages, 11341 KB  
Article
An RSM-Based Investigation on the Process–Performance Correlation and Microstructural Evolution of Friction Stir Welded 7055 Al/2195 Al-Li Dissimilar T-Joints
by Binbin Lin, Yanjie Han, Duquan Zuo, Nannan Wang, Yuanxiu Zhang, Haoran Fu and Chong Gao
Materials 2026, 19(6), 1260; https://doi.org/10.3390/ma19061260 - 23 Mar 2026
Viewed by 360
Abstract
Friction stir welding (FSW) is a key technology for manufacturing T-shaped thin-walled structures and avoiding fusion welding defects. However, the quantitative relationship between its process parameters and the microstructure properties of the joint remains unclear. To address this, this study established regression models [...] Read more.
Friction stir welding (FSW) is a key technology for manufacturing T-shaped thin-walled structures and avoiding fusion welding defects. However, the quantitative relationship between its process parameters and the microstructure properties of the joint remains unclear. To address this, this study established regression models via response surface methodology (RSM) relating rotational speed (w), welding speed (v), and plunge depth (h) to the mechanical properties of T-joints. The optimal process parameters (400 rpm, 60 mm/min, 0.21 mm) were determined, under which the ultimate tensile strength (UTS) and weld nugget hardness (WNH) of the joint reached 74.1% (377 MPa) and 94.4% (153 Hv) of the base materials (BM) respectively, with v showing the most significant influence on joint mechanical properties. Microstructural observations revealed that from the BM to the stirring zone (SZ), the grains underwent a continuous evolution from coarsening, partial recrystallization to complete dynamic recrystallization (DRX). In the SZ, due to severe plastic deformation and high heat input, the continuous dynamic recrystallization (CDRX) was the dominant mechanism, and the grain was significantly refined. The heat input in the thermomechanical affected zone (TMAZ) is relatively low, mainly geometric dynamic recrystallization (GDRX). DRX-driven grain refinement was the primary strengthening factor in the joint, with hardness closely related to grain size. However, thermal cycling induced softening in the heat-affected zone (HAZ) and promoted the precipitation of brittle compounds such as Al3Mg2 and MgZn2, which caused crack initiation exhibiting intergranular brittle fracture. Subsequently, under stress drive, it extends to SZ, mainly characterized by ductile fracture. Full article
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23 pages, 3484 KB  
Article
A Predictive Crater-Overlap Model for EDM Finishing Relevant to AISI 304 Welded Joints
by Mohsen Forouzanmehr, Mohammad Reza Dashtbayazi and Mahmoud Chizari
J. Manuf. Mater. Process. 2026, 10(2), 75; https://doi.org/10.3390/jmmp10020075 - 21 Feb 2026
Viewed by 538
Abstract
Electrical Discharge Machining (EDM) enables precision post-weld finishing of AISI 304 stainless steel, but stochastic spark overlaps make the fatigue-critical maximum peak-to-valley height (Rmax) difficult to predict. This study develops a validated physics-based framework quantifying how crater overlap governs R [...] Read more.
Electrical Discharge Machining (EDM) enables precision post-weld finishing of AISI 304 stainless steel, but stochastic spark overlaps make the fatigue-critical maximum peak-to-valley height (Rmax) difficult to predict. This study develops a validated physics-based framework quantifying how crater overlap governs Rmax evolution. Experiments on unwelded AISI 304 cylinders—proxying weld metal while excluding heat-affected zone (HAZ) effects—used Central Composite Design (20 trials, 900–9380 μJ discharge energies). Profilometry and scanning electron microscopy (SEM) correlated the crater size, overlap intensity, micro-cracking, and Rmax escalation from 18 to 85 μm. Primary and secondary crater formation under minimum and maximum overlap configurations were simulated using a 2D axisymmetric finite element model with Gaussian heat flux and temperature-dependent thermophysical properties. The predictive metric Rmax,num = (dinitial + dsecondary)/2 achieved 11–19% average error against the experimental Rmax,exp, with complementary valley depth (Rv) validation at 13% error. The Specimen 7 outlier (~50% error) reveals the limitations of deterministic modelling under stochastic debris accumulation and plasma instability at intermediate energies. Crater overlap generates secondary dimples, sharp inter-crater peaks, and rim micro-crack networks, driving the 4.7-fold Rmax increase—approaching International Institute of Welding (IIW) fatigue thresholds (<25 μm for high-cycle categories). The framework explicitly links the discharge energy, plasma channel radius (Rpc), and overlap geometry to surface topography, enabling process optimization (I·ton < 60 A·s maintains Rmax < 25 μm). Mesh independence (<2.5% convergence) and six centre-point replicates (CV = 4.2%) confirm robustness. This validated upper-bound Rmax predictor supports the digital co-optimization of welding and EDM parameters for aerospace/energy applications, with planned extensions to stochastic 3D models incorporating adaptive remeshing and real weld topographies. Full article
(This article belongs to the Special Issue Recent Advances in Welding and Joining Metallic Materials)
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13 pages, 3064 KB  
Article
Investigation of Weld Formation, Microstructure and Mechanical Properties of Small Core Diameter Single Mode Fiber Laser Welding of Medium Thick 6061 Aluminum Alloy
by Binyan He, Guojin Chen, Jianming Zheng and Pu Huang
Photonics 2025, 12(12), 1204; https://doi.org/10.3390/photonics12121204 - 7 Dec 2025
Viewed by 713
Abstract
In this study, a small core diameter single mode fiber laser was applied to weld an 8 mm thick plate of 6061-T6 aluminum alloy. The microstructural evolution and mechanical properties of the laser welded aluminum alloy specimens were investigated in detail. The results [...] Read more.
In this study, a small core diameter single mode fiber laser was applied to weld an 8 mm thick plate of 6061-T6 aluminum alloy. The microstructural evolution and mechanical properties of the laser welded aluminum alloy specimens were investigated in detail. The results indicated that fully penetrated welded specimens, free of welding defects like porosity, melt sagging, and hot cracking could be achieved by optimizing the processing parameters through response surface methodology. The upper part of the fusion zone consisted mainly of fine equiaxed dendrites, with secondary dendrite arm spacing (SDAS) of approximately 3–5 μm. While the lower region of the fusion zone exhibited pronounced microstructural coarsening, made up mostly of coarse columnar grains, along with some localized equiaxed grains, and an SDAS ranging from 8 to 12 μm. Both the fusion zone and heat affected zone (HAZ) were characterized by a “softened” hardness profile. The fusion zone featured a narrow region with the lowest microhardness across the welded joint with the microhardness value reducing to ~72% of the base metal (BM). Meanwhile, the microhardness of the HAZ was ~87.4% of the BM. The ultimate tensile strength of laser welded specimens was ~243.6 MPa, amounting to approximately 78.3% of the base metal. This study provides a fresh approach for welding medium-thick aluminum alloy plate using a high-quality laser beam, even at the kilowatt level with a fiber laser, and it shows a strong promise for applications in light-alloy manufacturing sectors such as automotive, rail transportation, aerospace, and beyond. Full article
(This article belongs to the Special Issue Laser Processing and Modification of Materials)
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18 pages, 6345 KB  
Article
Comparative Analysis of the Structure, Properties and Internal Stresses of MAG Welded Joints Made of S960QL Steel Subjected to Heat Treatment and Pneumatic Needle Peening
by Jacek Górka, Mateusz Przybyła and Bernard Wyględacz
Materials 2025, 18(23), 5363; https://doi.org/10.3390/ma18235363 - 28 Nov 2025
Viewed by 463
Abstract
The aim of the research was to analyse the impact of peening each of the beads on the properties of a butt joint made of S960QL steel welded with ceramic backing on a robotic workstation using the 135 (MAG) method, and to determine [...] Read more.
The aim of the research was to analyse the impact of peening each of the beads on the properties of a butt joint made of S960QL steel welded with ceramic backing on a robotic workstation using the 135 (MAG) method, and to determine the impact of pneumatic needle peening on the stress level. This analysis was based on a comparison of three butt joints: in the as-welded state, with each weld bead peened and post-weld heat treatment—stress relief annealing—performed. High-frequency peening (90 Hz) of each weld was performed to reduce stresses in the welded joint by introducing tensile stresses into it. A Weld Line 10 pneumatic hammer from PITEC GmBH was used for this purpose. The test joints obtained were tested in accordance with the requirements of EN ISO 15614-1. In order to determine the state of residual stresses, stress measurements were carried out using the Barkhausen effect based on the testing procedure of the technology supplier, NNT. This meter measures the intensity of the Barkhausen effect using a standard probe (with a single core). In order to verify the stress measurement using the Barkhausen method, stress measurements were performed using the XRD sin 2ψ technique based on the X’Pert Stress Plus program, which contains a database of material constants necessary for calculations. Structural studies, including phase analysis and crystallographic grain orientation, were performed using the backscattered electron diffraction method with a high-resolution scanning electron microscope and an EBSD (Electron Backscatter Diffraction) detector, as well as EDAX OIM analysis software. In addition, X-ray diffraction testing was performed on a Panalytical X’Pert PRO device using filtered cobalt anode tube radiation (λ = 1.79021 A). Qualitative X-ray phase analysis of the tested materials was performed in a Bragg–Brentano system using an Xcelerator strip detector. The tests showed that the high-frequency peening of each bead did not cause negative results in the required tests during qualification of the S960QL plate-welding technology compared to the test plates in the as-welded and post-stress-relief heat treatment states. Interpass peening of the weld face and HAZ resulted in a reduction in residual stresses after welding at a distance of 15 mm from the joint axis compared to the stress measurement result for the sample in the as-welded condition. This allows for a positive assessment of peening in terms of reducing the crack initiator in the form of the concentration of tensile stresses in the area of the fusion line and HAZ. Full article
(This article belongs to the Special Issue Fusion Bonding/Welding of Metal and Non-Metallic Materials)
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11 pages, 9420 KB  
Article
Microstructure Evolution and Toughening Mechanisms in the Nugget Zone of Friction-Stir-Welded X80 Pipeline Steel
by Miaoye Han, Min Yang, Yinhui Rao, Xiong Luo, Ruihai Duan, Sheng Guo, Ying Dong and Shujin Chen
Coatings 2025, 15(12), 1384; https://doi.org/10.3390/coatings15121384 - 26 Nov 2025
Viewed by 469
Abstract
Coarse grains and blocky M-A constituents are often generated in the heat-affected zone (HAZ) of fusion welded pipeline steel joints owing to high heat input, causing a significant deterioration of toughness. This study demonstrated the effect of heat input in friction stir welding [...] Read more.
Coarse grains and blocky M-A constituents are often generated in the heat-affected zone (HAZ) of fusion welded pipeline steel joints owing to high heat input, causing a significant deterioration of toughness. This study demonstrated the effect of heat input in friction stir welding (FSW) on the microstructure and toughness of the nugget zone (NZ), elucidating the microstructure evolution and toughening mechanism. The results revealed a marked reduction in effective grain size within the NZ at low heat input (LHI) and a significant increase in the ratio of the refined M-A constituent. Furthermore, the decreased heat input leads to weak texture components (D1, D2, and F) accompanied by a decrease in the kernel average misorientation (KAM) value. This microstructural optimization clearly enhances toughness, and an excellent toughness value of 200 J, representing 95.3% of the basal metal (BM), was achieved in the NZ at LHI. The primary reason for this improvement is the refinement of effective grains and M-A constituents resulting from reduced heat input. During crack propagation, the high proportion of effective grain boundaries and fine M-A constituents acts as a barrier, arresting and deflecting cracks and thereby enhancing toughness. Full article
(This article belongs to the Special Issue Research in Laser Welding and Surface Treatment Technology)
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22 pages, 9034 KB  
Article
Laser Beam Welding of IN625 Alloy with Equiaxed Grains: Influence of Process Parameters
by Giuliano Angella, Fabio Bergamini, Francesco Cognini, Alessandra Fava, Paolo Ferro, Alessandra Palombi, Maria Richetta and Alessandra Varone
Metals 2025, 15(12), 1296; https://doi.org/10.3390/met15121296 - 25 Nov 2025
Viewed by 756
Abstract
Ni-based superalloys, known for their excellent mechanical strength and corrosion resistance at high temperature, are widely used in aeronautic, aerospace, and energy industries. Since both the materials and manufacturing processes required to produce high-performance components made of these alloys are expensive, the welding [...] Read more.
Ni-based superalloys, known for their excellent mechanical strength and corrosion resistance at high temperature, are widely used in aeronautic, aerospace, and energy industries. Since both the materials and manufacturing processes required to produce high-performance components made of these alloys are expensive, the welding repair of damaged components plays a crucial role in industrial applications. High energy density welding techniques, such as laser beam welding (LBW) and electron beam welding (EBW), are the most promising to achieve high-quality welds. Nevertheless, welding processes significantly affect the microstructure and mechanical properties of both the melted zone (MZ) and the heat-affected zone (HAZ). This may result in alloying element segregation, precipitation of undesired secondary phases, and the presence of residual stresses that can lead to crack formation. Therefore, a comprehensive investigation of the effects of process parameters on weld seam properties is essential to maintain high performance standards. In this work, LBW was employed to join 2.5 mm thick plates of equiaxed IN625 superalloy. The seams were produced by varying three parameters: the two characteristic parameters of LBW, i.e., laser power (P = 1700, 2000, 2300 W) and welding speed (v = 15, 20, 25 mm/s), alongside power modulation (Γ = Pmin/Pmax = 0.6, 0.8, 1). The scope of this work is to evaluate the effect of the combined variation of all these welding parameters on the final characteristics of welded seams. The resulting microstructures were characterized by using digital radiography, Light Microscopy (LM), Scanning Electron Microscopy (SEM), and X-ray Diffraction (XRD). Vickers microhardness measurements were performed across the weld seams to evaluate the mechanical properties in the MZ and HAZ. The optimal set of welding parameters, producing defect-free seams without cracks and pores, was identified as P = 2000 W, v = 25 mm/s, and Γ = 0.6. Full article
(This article belongs to the Special Issue Weldability and Reparability of Nickel-Base Alloys)
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13 pages, 5096 KB  
Article
Microstructure and Mechanical Properties of Friction Stir Welded the Novel Al-Mg-Zn-Si Alloy
by Junzhe Huang, Ying Li, Xiwu Li, Hongwei Yan, Lizhen Yan, Kai Wen, Yanan Li, Guanjun Gao, Kai Zhu, Mingyang Yu, Yongan Zhang and Baiqing Xiong
Materials 2025, 18(23), 5269; https://doi.org/10.3390/ma18235269 - 21 Nov 2025
Viewed by 835
Abstract
The high-Mg-content Al-Mg-Zn-Si alloy, as a novel aluminum alloy, exhibits excellent strength, toughness, and corrosion resistance, demonstrating significant application potential in lightweight structural components for aerospace, weapon systems, rail transportation, and other fields. In this study, friction stir welding was employed to weld [...] Read more.
The high-Mg-content Al-Mg-Zn-Si alloy, as a novel aluminum alloy, exhibits excellent strength, toughness, and corrosion resistance, demonstrating significant application potential in lightweight structural components for aerospace, weapon systems, rail transportation, and other fields. In this study, friction stir welding was employed to weld the high-Mg-content Al-Mg-Zn-Si alloy. Subsequent aging treatment was applied to establish the relationship between the mechanical properties and microstructural characteristics of the welded joint, aiming to elucidate the strengthening mechanisms of the new alloy and provide insights for achieving high-quality welds. The results indicate that the microhardness profile of the as-welded joint exhibited a “W” shape, with overall low hardness values and minor differences between zones. After the aging treatment, the microhardness increased significantly in the base material (BM), the thermo-mechanically affected zone (TMAZ), and the stir zone (SZ), whereas the heat-affected zone (HAZ) adjacent to the SZ exhibited only a marginal increase, making it the softest region in the aged joint. The yield strength and ultimate tensile strength of the aged joint increased to 327 MPa and 471 MPa, respectively. The enhancement in microhardness and strength after aging treatment was attributed to the precipitation of numerous nano-sized T-phase particles within grains. Interestingly, the tensile samples of the aged joint fractured in the high-hardness SZ instead of the low-hardness HAZ. This fracture behavior was primarily attributed to continuous grain boundary precipitates, which reduced intergranular cohesion. In contrast, the elongated grain structure in the HAZ more effectively resisted intergranular crack propagation compared to the equiaxed grains in the SZ. Full article
(This article belongs to the Section Metals and Alloys)
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14 pages, 22611 KB  
Article
The Strain Evolution and Fracture of GH3535 Alloy Welded Joint Characterized by DIC at Different Temperatures
by Qingchun Zhu, Yucheng Zhu, Jie Wang, Li Jiang and Zhijun Li
Crystals 2025, 15(11), 916; https://doi.org/10.3390/cryst15110916 - 24 Oct 2025
Cited by 1 | Viewed by 689
Abstract
Welding is widely employed in manufacturing processes, with the mechanical properties of welded joints being a primary focus of welding technology research. However, distinct regions of welded joints—including the base metal (BM), heat-affected zone (HAZ), and deposited metal (DM)—exhibit divergent deformation behaviors, which [...] Read more.
Welding is widely employed in manufacturing processes, with the mechanical properties of welded joints being a primary focus of welding technology research. However, distinct regions of welded joints—including the base metal (BM), heat-affected zone (HAZ), and deposited metal (DM)—exhibit divergent deformation behaviors, which collectively influence the fracture behavior of the joints. In this study, the specific locations of strain concentration and fracture in GH3535 alloy welded joints (fabricated using ERNiMo-2 welding wire) were investigated during tensile tests at room temperature (RT) and 700 °C. Characterizations were performed via digital image correlation (DIC), electron backscatter diffraction (EBSD), and transmission electron microscopy (TEM). Results revealed that during RT tension, strain was concentrated in the deposited metal adjacent to the fusion line (FL) which is 200% higher than BM, where cracks also initiated. At 700 °C, strain was mainly concentrated in the deposited metal, where the maximum strain concentration was approximately three times that in the base metal, and fracture also occurred in this region. It has been confirmed through in-suit observations that during high-temperature deformation, the deposited metal of the GH3535 alloy is more prone to strain concentration and simultaneously exhibits lower plasticity. This study advances the understanding of the deformation behavior of GH3535 alloy welded joints through in-suit observation results, and indicates that strengthening the deposited metal (i.e., the region more prone to strain concentration) is a more effective approach to improve the mechanical properties of such welded joints. Full article
(This article belongs to the Special Issue Microstructure and Mechanical Properties of Alloys and Composites)
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34 pages, 18226 KB  
Article
The Vanadium Micro-Alloying Effect on the Microstructure of HSLA Steel Welded Joints by GMAW
by Giulia Stornelli, Bryan Ramiro Rodríguez-Vargas, Anastasiya Tselikova, Rolf Schimdt, Michelangelo Mortello and Andrea Di Schino
Metals 2025, 15(10), 1127; https://doi.org/10.3390/met15101127 - 10 Oct 2025
Cited by 1 | Viewed by 1264
Abstract
Structural applications that use High-Strength Low-Alloy (HSLA) steels require detailed microstructural analysis to manufacture welded components that combine strength and weldability. The balance of these properties depends on both the chemical composition and the welding parameters. Moreover, in multi-pass welds, thermal cycling results [...] Read more.
Structural applications that use High-Strength Low-Alloy (HSLA) steels require detailed microstructural analysis to manufacture welded components that combine strength and weldability. The balance of these properties depends on both the chemical composition and the welding parameters. Moreover, in multi-pass welds, thermal cycling results in a complex Heat-Affected Zone (HAZ), characterized by sub-regions with a multitude of microstructural constituents, including brittle phases. This study investigates the influence of Vanadium addition on the microstructure and performance of the HAZ. Multi-pass welded joints were manufactured on 15 mm thick S355 steels with different Vanadium contents using a robotic GMAW process. A steel variant containing both Vanadium and Niobium was also considered, and the results were compared to those of standard S355 steel. Moving through the different sub-regions of the welded joints, the results show a heterogeneous microstructure characterized by ferrite, bainite and martensite/austenite (M/A) islands. The presence of Vanadium reduces carbon solubility during the phase transformations involved in the welding process. This results in the formation of very fine (average size 11 ± 4 nm) and dispersed precipitates, as well as a lower percentage of the brittle M/A phase, in the variant with a high Vanadium content (0.1 wt.%), compared to the standard S355 steel. Despite the presence of the brittle phase, the micro-alloyed variants exhibit strengthening without loss of ductility. The combined presence of both hard and soft phases in the HAZ provides stress-damping behavior, which, together with the very fine precipitates, promises improved resistance to crack propagation under different loading conditions. Full article
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21 pages, 8060 KB  
Article
Enhanced Microstructural and Mechanical Properties of Mig Welded Al 7075 Alloy Under Longitudinal Vibrations
by Teodor Machedon-Pisu and Mihai Machedon-Pisu
Materials 2025, 18(18), 4281; https://doi.org/10.3390/ma18184281 - 12 Sep 2025
Cited by 1 | Viewed by 780
Abstract
In many areas such as the automotive, aircraft, and building industries, the high-strength aluminum alloy Al 7075 is frequently used due to its appropriate properties as a lightweight structural material. However, due to modest weldability, it is challenging to obtain high-quality welds with [...] Read more.
In many areas such as the automotive, aircraft, and building industries, the high-strength aluminum alloy Al 7075 is frequently used due to its appropriate properties as a lightweight structural material. However, due to modest weldability, it is challenging to obtain high-quality welds with suitable mechanical properties, as cracks are generated while welding. Moreover, in order to avoid post-welding heat treatments and the use of complex welding equipment, in this paper the Al 7075 alloy is welded with MIG under longitudinal vibrations by using the Al 4043 alloy as filler material. As a consequence of strengthening the HAZ through precipitation, the mechanical and structural properties of the welded joints can be improved. These are investigated both under longitudinal forced vibrations at 50 Hz and without such vibrations. The results reveal improvements in terms of reducing the risk of hot cracking, obtaining a band structure free of porosity of the welds, improving the hardness of the welds under vibrations by 8.7% to 12.5%, and improving the tensile strength of the plates welded under vibrations by 12 to 15.5% in comparison to no vibrations. In relation to other welding procedures, the proposed procedure is more cost-effective and the weld quality is improved during the welding process. Full article
(This article belongs to the Section Metals and Alloys)
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24 pages, 9894 KB  
Article
Effects of Multiple Welding Thermal Cycles on Stress Corrosion of L360N Steel in a Simulated Shale Gas Gathering Environment Containing Sulfate-Reducing Bacteria
by Jie Xiao, Shouxi Wang, Yong Xu, Kexi Liao, Guiyang Wu, Jing Yan, Yongbo Wang, Lincai Peng and Puzhi Li
Materials 2025, 18(18), 4255; https://doi.org/10.3390/ma18184255 - 11 Sep 2025
Viewed by 675
Abstract
The combined effect of sulfate-reducing bacteria (SRB) and a microstructure on the stress corrosion behavior of heat-affected zones (HAZs) in pipeline steel for shale gas field applications was investigated. The results show that when the peak heating temperature reached 1020 °C, a coarse [...] Read more.
The combined effect of sulfate-reducing bacteria (SRB) and a microstructure on the stress corrosion behavior of heat-affected zones (HAZs) in pipeline steel for shale gas field applications was investigated. The results show that when the peak heating temperature reached 1020 °C, a coarse microstructure formed during multiple thermal cycles (MTCs), and Widmanstätten structures appeared in the HAZ. In the simulated environment, SRB intensified localized pitting corrosion of both the base metal and the HAZ. The welding HAZ was softened by the MTCs, and significant microcrack growth was observed in the presence of SRB. Among all subzones, the coarse-grained HAZ (CGHAZ) was the most susceptible to stress corrosion cracking (SCC) under shale gas service conditions. Cracks initiated at the metal surface and propagated vertically into the material. SRB activity further increased the SCC sensitivity of the CGHAZ. Full article
(This article belongs to the Special Issue Microstructure Engineering of Metals and Alloys, 3rd Edition)
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19 pages, 11731 KB  
Article
Effect of Post-Weld Heat Treatment on Microstructure and Hardness Evolution of the Martensitic Hardfacing Layers for Hot Forging Tools Repair
by Marzena Lachowicz, Marcin Kaszuba, Paweł Widomski and Paweł Sokołowski
Materials 2025, 18(17), 4214; https://doi.org/10.3390/ma18174214 - 8 Sep 2025
Cited by 1 | Viewed by 1101
Abstract
The study investigates the influence of post-weld heat treatment (PWHT) on the microstructure and hardness of hardfacing layers applied to hot forging tools. The research focuses on three tool steels (55NiCrMoV7, X37CrMoV5-1, and a modified X38CrMoV5-3) and uses robotized gas metal arc welding [...] Read more.
The study investigates the influence of post-weld heat treatment (PWHT) on the microstructure and hardness of hardfacing layers applied to hot forging tools. The research focuses on three tool steels (55NiCrMoV7, X37CrMoV5-1, and a modified X38CrMoV5-3) and uses robotized gas metal arc welding (GMAW) with DO015 filler material. It examines the structural and mechanical differences in the hardfaced layers before and after heat treatment involving quenching and tempering. The findings reveal that PWHT significantly improves microstructural homogeneity and hardness distribution, especially in the heat-affected zone (HAZ), mitigating the risk of crack initiation and tool failure. The study shows that untempered as-welded layers exhibit microstructural inhomogeneity and extreme hardness gradients, which negatively impact tool durability. PWHT leads to tempered martensite formation, grain refinement, and a more stable hardness profile across the joint. These improvements are critical for extending the service life of forging tools. The results underscore the importance of customizing PWHT parameters according to the specific material and application to optimize tool performance. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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17 pages, 5136 KB  
Article
Laser Welding of Metal–Polymer–Metal Composites: Enhancing Energy Control
by Serguei P. Murzin and Heinz Palkowski
Processes 2025, 13(9), 2774; https://doi.org/10.3390/pr13092774 - 29 Aug 2025
Cited by 1 | Viewed by 1440
Abstract
This study investigates two-sided pulsed-periodic laser welding of three-layer metal–polymer–metal (MPM) composite sheets composed of galvanized dual-phase steel (DPK 30/50+ZE) as outer layers and a polypropylene–polyethylene (PP–PE) core. Welding was performed using a Rofin StarWeld Performance pulsed Nd:YAG laser with controlled parameters: pulse [...] Read more.
This study investigates two-sided pulsed-periodic laser welding of three-layer metal–polymer–metal (MPM) composite sheets composed of galvanized dual-phase steel (DPK 30/50+ZE) as outer layers and a polypropylene–polyethylene (PP–PE) core. Welding was performed using a Rofin StarWeld Performance pulsed Nd:YAG laser with controlled parameters: pulse energy (30–32 J), duration (6–8 ms), and frequency (up to 1 Hz). High-quality welds were achieved with penetration depths reaching 70% of the outer metal layer thickness and minimal defects. Microscopic analysis revealed distinct fusion and heat-affected zones (HAZ) with no evidence of cracks or porosity, indicating stable thermal conditions. Mechanical testing showed that the welded joints attained a tensile strength of approximately 470 MPa, about 80% of the ultimate tensile strength of the base metal, with an average elongation of 0.6 mm. These results confirm the structural integrity of the joints. The observed weld morphology and microstructural features suggest that thermal conditions during welding significantly affect joint quality and HAZ formation. The study demonstrates that strong, defect-free joints can be produced using basic beam-shaping optics and outlines a pathway for further improvement through the integration of diffractive optical elements (DOEs) to enhance spatial-energy control in multilayer structures. Full article
(This article belongs to the Special Issue Progress in Laser-Assisted Manufacturing and Materials Processing)
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24 pages, 5715 KB  
Article
Distribution of Residual Stresses in Dissimilar Ferritic Steel Weld Joints and Their Modification via Mechanical Hammer Peening
by Zhiyong Hu, Enyu Shi, Yanan Cui, Jiexin Hu and Liangyun Lan
Metals 2025, 15(9), 961; https://doi.org/10.3390/met15090961 - 29 Aug 2025
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Abstract
Dissimilar steel welding is a necessary means for engineering structures to meet complex service conditions. However, residual stress becomes a challenge for the service properties of dissimilar welded joints (DWJs), as it can reduce fatigue strength and trigger cracking in welded components. Therefore, [...] Read more.
Dissimilar steel welding is a necessary means for engineering structures to meet complex service conditions. However, residual stress becomes a challenge for the service properties of dissimilar welded joints (DWJs), as it can reduce fatigue strength and trigger cracking in welded components. Therefore, accurately estimating the distribution of residual stress and efficiently eliminating it is of great importance. This study investigated the evolution of residual stress during the welding process of two commonly used ferritic steels through experimental and numerical analyses. The results show that different thermal cycle behaviors between DWJs have a significant impact on the formation of residual stress. Longitudinal tensile residual stress is predominant in the weld and heat-affected zone (HAZ), with higher longitudinal tensile and compressive stresses in the Q390 side than in the Q690 side, while the maximum transverse tensile stress occurs in the HAZ of the Q690 side. Hammer peening shows excellent ability to eliminate residual stress after welding, with a maximum elimination rate of approximately 62%, and converts the stress state from tensile to compressive at a certain welding depth. The analysis of process parameters reveals that peening velocity is the most influential factor. Under the present experimental configuration, the peening velocity should be set between 4.5 m/s and 5.5 m/s. Full article
(This article belongs to the Special Issue Metal Forming and Additive Manufacturing)
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