Comparative Analysis of the Structure, Properties and Internal Stresses of MAG Welded Joints Made of S960QL Steel Subjected to Heat Treatment and Pneumatic Needle Peening
Abstract
1. Introduction
2. Methods and Materials
2.1. Welding of the Test Plates
2.2. Interpass Peening
2.3. Post-Weld Stress Relief Heat Treatment
2.4. Acceptance Tests in Accordance with PN-EN ISO 15614-1:2017 [20]
- Tensile test in accordance with PN-EN ISO 4136:2022 [28];
- Transverse bending test in accordance with PN-EN ISO 5173:2023 [29];
- Impact test in accordance with PN-EN ISO 9016:2022 [30];
- Hardness test in accordance with PN-EN ISO 9015-1:2011 [31];
- Macroscopic test in accordance with PN-EN ISO 17639:2022 [32].
2.5. Microstructure Analysis Using Electron Backscatter Diffraction
2.6. Stress Measurement Using Barkhausen Effect
2.7. Quantitative Phase Analysis and Stress Measurements Using X-Ray Diffraction
3. Result and Discussion
3.1. Welding Technology Qualification Test Results
3.2. Joint Microstructure Analysis
3.3. Phase Composition Analysis Using X-Ray Diffraction
3.4. Stress Measurement Analysis
4. Conclusions
- ➢
- Transverse tensile testing of all three test plates showed tensile strength, Rm, results were over the required value of 980 N/mm2;
- ➢
- Transverse bending tests on samples with face tension and edge tension showed no non-conformities and met the ISO 15614-1:2017 requirements;
- ➢
- Impact testing of test plates in the as-welded state and with inter-stitch peening yielded similar results, and in the case of samples taken from the welded joints in the post-heat treatment state, the test results from the heat-affected zone were on average about 30J higher than for the other two plates. This may be due to a decrease in hardness in the HAZ as a result of stress relief annealing, which was confirmed during the test.
- ➢
- The hardness test of the welded joint in the as-welded condition in the parent material area showed an average value of 356 HV10; for the fusion zone, it was 345 HV10, and for the heat-affected zone, it was 315 HV10. In the case of the test plate after stress relief annealing, the values were as follows: parent material—357 HV10, fusion zone—365 HV10, and HAZ—307 HV10. In the case of the test plate after peening, the values were as follows: parent material—352 HV10, fusion zone—337 HV10, and HAZ—328 HV10. There is a noticeable increase in hardness in the HAZ area that has been peened.
- ➢
- Observation with a light microscope showed that in the HAZ area directly below the plate surface, the microstructure is fragmented, which is most likely caused by intense plastic deformation during the HFMI process and the resulting deformation. The observation of the microstructure under a light microscope was supplemented by EBSD analysis, which confirmed differences in grain size in the zone directly below the surface.
- ➢
- Phase composition analysis using X-ray diffraction, as well as EBSD analysis, showed that the fusion zone contains approximately 4% Fe-γ austenite by volume. This is due to the increased nickel content in the electrode wire used to weld these samples (2.24% by weight).
- ➢
- Both tested treatments resulted in significant improvement in HAZ stresses, with PWHT achieving better improvement. Both of the tested treatments did not negatively impact mechanical properties in any significant manner. While PWHT looks like a more promising technology, it possesses significant downsides vs. HFMI, mainly a higher cost.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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| Plate | Element Concentration, wt% | |||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| C | Mn | Si | P | S | Cr | Mo | Ni | V | Cu | Al | Ti | Nb | As | |
| S960QL | 0.12 | 1.42 | 0.47 | 0.008 | 0.003 | 0.59 | 0.56 | 0.79 | 0.05 | 0.11 | 0.007 | 0.005 | 0.02 | 0.002 |
| Wire | Element Concentration, wt% | |||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| C | Mn | Si | P | S | Cr | Ni | V | Cu | Al | Mo | Ti + Zr | |
| ED-FK | 0.11 | 1.75 | 0.81 | 0.007 | 0.009 | 0.36 | 2.24 | 0.002 | 0.009 | 0.005 | 0.57 | 0.08 |
| Sample Designation | Bead No | Interpass Temperature [°C] | Average Welding Current [A] | Average Arc Voltage [V] | Welding Time [min] | Linear Energy [kJ/mm] |
|---|---|---|---|---|---|---|
| S960QL as welded | 1 | 28.6 | 201 | 23.9 | 2:35 | 1.07 |
| 2 | 82.5 | 203 | 27.0 | 1:27 | 0.70 | |
| 3 | 104.5 | 255 | 26.3 | 2:42 | 1.35 | |
| S960QL + HMFI | 1 | 47.5 | 200 | 23.8 | 2:38 | 1.04 |
| 2 | 89.6 | 202 | 27.1 | 1:29 | 0.71 | |
| 3 | 114.5 | 255 | 26.3 | 2:31 | 1.34 | |
| S960QL + PWHT | 1 | 36.0 | 202 | 24.0 | 2:51 | 1.06 |
| 2 | 92.4 | 202 | 27.0 | 1:27 | 0.71 | |
| 3 | 119.7 | 254 | 26.4 | 2:29 | 1.37 |
| Test Type | Sample | Result | Sample | Result | |||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| S960QL as welded | |||||||||||||||||||
| Transverse tensile test | TT-1 | 1007 MPa | TT-2 | 1011 MPa | |||||||||||||||
| Transverse bending tests | TFBB1 | positive | TRBB1 | positive | |||||||||||||||
| TFBB2 | positive | TRBB2 | positive | ||||||||||||||||
| Charpy impact testing | VWT 0/2 | 58.9 J | VHT 0/2 | 82.4 J | |||||||||||||||
| VWT 0/2 | 54.9J | VHT 0/2 | 79.5 J | ||||||||||||||||
| VWT 0/2 | 59.8 J | VHT 0/2 | 74.6 J | ||||||||||||||||
| Hardness testing | Ma-1 HV10 | L1 | 367 | 370 | 356 | 313 | 301 | 335 | 341 | 331 | 330 | 352 | 285 | 334 | 365 | 353 | 357 | ||
| L2 | 350 | 351 | 345 | 279 | 290 | 334 | 366 | 349 | 356 | 349 | 316 | 279 | 340 | 359 | 356 | ||||
| S960QL peened | |||||||||||||||||||
| Transverse tensile test | TT-1 | 1011 MPa | TT-2 | 989 MPa | |||||||||||||||
| Transverse bending tests | TFBB1 | positive | TRBB1 | positive | |||||||||||||||
| TFBB2 | positive | TRBB2 | positive | ||||||||||||||||
| Charpy impact testing | VWT 0/2 | 58.9 J | VHT 0/2 | 66.7 J | |||||||||||||||
| VWT 0/2 | 58.9 J | VHT 0/2 | 70.6 J | ||||||||||||||||
| VWT 0/2 | 58.9 J | VHT 0/2 | 68.7 J | ||||||||||||||||
| Hardness testing | Ma-1 HV10 | L1 | 355 | 366 | 362 | 303 | 360 | 326 | 326 | 370 | 361 | 365 | 385 | 327 | 315 | 355 | 360 | ||
| L2 | 356 | 341 | 334 | 282 | 278 | 356 | 336 | 320 | 309 | 326 | 334 | 295 | 316 | 353 | 356 | ||||
| S960QL PWHT | |||||||||||||||||||
| Transverse tensile test | TT-1 | 998 MPa | TT-2 | 992 MPa | |||||||||||||||
| Transverse bending tests | TFBB1 | positive | TRBB1 | positive | |||||||||||||||
| TFBB2 | positive | TRBB2 | positive | ||||||||||||||||
| Charpy impact testing | VWT 0/2 | 52.0 J | VHT 0/2 | 117.7 J | |||||||||||||||
| VWT 0/2 | 96.1 J | VHT 0/2 | 116.7 J | ||||||||||||||||
| VWT 0/2 | 101.0 J | VHT 0/2 | 100.0 J | ||||||||||||||||
| Hardness testing | Ma-1 HV10 | L1 | 360 | 361 | 370 | 300 | 319 | 328 | 334 | 355 | 349 | 307 | 290 | 310 | 338 | 344 | 347 | ||
| L2 | 356 | 354 | 344 | 292 | 288 | 345 | 371 | 387 | 398 | 330 | 300 | 294 | 327 | 329 | 344 | ||||
| Mean Stress [MPa] | |||
|---|---|---|---|
| Test Sample | Fusion Zone | HAZ | Parent Material |
| S960QL as welded | −170 | +180 | −40 |
| S960QL peened | −150 | +30 | −65 |
| S960QL PWHT | −170 | −90 | −140 |
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Górka, J.; Przybyła, M.; Wyględacz, B. Comparative Analysis of the Structure, Properties and Internal Stresses of MAG Welded Joints Made of S960QL Steel Subjected to Heat Treatment and Pneumatic Needle Peening. Materials 2025, 18, 5363. https://doi.org/10.3390/ma18235363
Górka J, Przybyła M, Wyględacz B. Comparative Analysis of the Structure, Properties and Internal Stresses of MAG Welded Joints Made of S960QL Steel Subjected to Heat Treatment and Pneumatic Needle Peening. Materials. 2025; 18(23):5363. https://doi.org/10.3390/ma18235363
Chicago/Turabian StyleGórka, Jacek, Mateusz Przybyła, and Bernard Wyględacz. 2025. "Comparative Analysis of the Structure, Properties and Internal Stresses of MAG Welded Joints Made of S960QL Steel Subjected to Heat Treatment and Pneumatic Needle Peening" Materials 18, no. 23: 5363. https://doi.org/10.3390/ma18235363
APA StyleGórka, J., Przybyła, M., & Wyględacz, B. (2025). Comparative Analysis of the Structure, Properties and Internal Stresses of MAG Welded Joints Made of S960QL Steel Subjected to Heat Treatment and Pneumatic Needle Peening. Materials, 18(23), 5363. https://doi.org/10.3390/ma18235363

