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15 November 2025

Novel Design of [c2]Daisy-Chain Rotaxane Crosslinkers Bearing Long-Chain Alkenes and Development of Tough Topological Polymer

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Graduate School of Sciences and Technology for Innovation, Yamaguchi University, 2-16-1 Tokiwadai, Ube, Yamaguchi 755-8611, Japan
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Reactions2025, 6(4), 62;https://doi.org/10.3390/reactions6040062 
(registering DOI)

Abstract

To explore new possibilities in topological materials, we designed a tetrafunctional crosslinker composed of a [c2]daisy-chain rotaxane framework. In this study, a novel topological network polymer was successfully synthesized via an addition reaction between 3,6-dioxa-1,8-octanedithiol (DODT) and a tetrafunctional crosslinker, a [c2]daisy-chain rotaxane constructed from dibenzo-24-crown-8 ether (DB24C8) units and bearing long-chain alkenes on its four benzene rings. The resulting network polymer exhibited both high stiffness and toughness, along with excellent shape-memory properties. These characteristics were governed by a balance between plastic and elastic deformation originating from the DODT and rotaxane domains, respectively, highlighting a new design strategy for the creation of advanced topological materials.

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