Fibers, Volume 10, Issue 3 (March 2022) – 9 articles

This study investigates the physical and mechanical properties of short Entada mannii- glass fiber polypropylene hybrid composites. The polymeric hybrid composite was produced by combining different ratios of Entada mannii fiber (EMF)/glass fiber (GF) using the compression molding technique. The tensile properties, compressive strength, impact strength and hardness were evaluated while the fracture surface morphology was examined using the scanning electron microscope (SEM). It further evaluates the moisture absorption and percentage void content of the developed composites. The experimental results show that tensile, compressive, impact and hardness properties of all the hybrid composites were significantly improved as compared with single reinforced composites. Specifically, hybrid composites (EMF/GF5) revealed an overall tensile strength of 41%, hardness of 51% and compressive strength of 47% relative to single reinforced composites, which can be ascribed to enhanced fiber–matrix bonding. The chemical treatment enhanced the EMF fiber surface and promoted good adhesion with the polypropylene (PP) matrix. Moisture absorption properties revealed that the addition of EMF/GF reduces the amount of moisture intake of the hybrid composites attributed to good cementing of the fiber–matrix interface. Morphological analysis revealed that single reinforced composites (EMF1 and GF2) were characterized by fiber pullout and deposition of voids in the composite as compared with the hybrid composites. Full article

This study aimed to reveal the influence of the draw ratio and take-up speed on the pore size distribution and morphology of the hollow fiber ultrafiltration membrane selective layer. To this end, spinnerets with ring ducts of 1.8 and 1.3 mm were employed, whereas the external diameter of the obtained fiber was kept equal. Atomic force microscopy and scanning electron microscopy were employed to study the morphology of the selective layer. Liquid–liquid displacement porosimetry was used to determine the limiting pore size distribution. The produced polyethersulfone ultrafiltration membranes had a robust, sponge-like porous structure, permeance 1000 L/(m²·h·bar), smooth selective layer, and mean pore size 25 nm. It was found that limiting pore sizes are affected more by the change in the take-up speed, whereas the surface pore sizes, roughness, and morphology are controlled by the draw ratio. It was shown that excessive draw causes the selective layer stretching and crop-up of the porous sublayer. Consequently, the diameters of the spinneret ring duct and the bore needle should match the hollow fiber outer and lumen diameters, respectively. Full article

The use of the innovative material of Carbon Fiber-Reinforced (C-FRP) ropes as external near surface mounted reinforcement for the strengthening of reinforced concrete beam-column joints is studied. The ropes are diagonally applied forming external X-type reinforcements on both sides of the joint body. The efficiency of the technique is mainly based on the assumption that the confinement of the joint body due to the applied X-shaped ropes and the contribution of the ropes as shear reinforcement are efficient enough to reduce the shear deformations observed in the joint core during the seismic excitation. Thereof the experimental measurements of the shear deformations of nine full scale beam-column joints tested in cyclic deformations are elaborated and presented herein. The specimens are sorted in two groups. Specimens of group A have been designed in the way that damage is mainly expected in the beam. On the other hand, in order to investigate the efficacy of the use of the ropes for substandard joints the group B specimens have been designed in the way that cracks and some damages are expected to develop in the joint body. Systematic and extended comparative presentations for specimens with and without ropes proved in all the examined cases that the externally mounted C-FRP ropes kept the joint body intact and substantially reduced the shear deformations especially in high drifts. Moreover, the influence of the externally mounted X-shaped C-FRP ropes on the seismic behaviour of these specimens is also examined in terms of the developing principal tensile stresses inside the joint body. From the comparisons of the principal stresses developing in specimens with and without X-form C-FRP ropes it became quite obvious that the ropes kept the joint body intact and allowed the development of higher values of principal stresses comparing with the stresses developing in specimens without ropes. Full article

This paper reviews Fibre Reinforced Polymer (FRP) composites in Civil Engineering applications. Three FRP types are used in Structural Engineering: FRP profiles for new construction, FRP rebars and FRP strengthening systems. Basic materials (fibres and resins), manufacturing processes and material properties are discussed. The focus of the paper is on all-FRP new-build structures and their joints. All-FRP structures use pultruded FRP profiles. Their connections and joints use bolting, bonding or a combination of both. For plate-to-pate connections, effects of geometry, fibre direction, type and rate of loading, bolt torque and bolt hole clearance, and washers on failure modes and strength are reviewed. FRP beam-columns joints are also reviewed. The joints are divided into five categories: web cleated, web and flange cleated, high strength, plate bolted and box profile joints. The effect of both static and cyclic loading on joints is studied. The joints’ failure modes are also discussed. Full article

This study investigates the effectiveness of hybrid fibers (steel and macro-synthetic) on the shear behavior of prestressed concrete beams. The hybrid fiber combination was selected to avoid workability issues at high volume dosages and ensure effective crack arresting over the crack opening range. Fracture studies included testing notched concrete prisms to identify the role of hybrid fibers in the crack bridging mechanism. Seven hybrid fiber reinforced prestressed concrete (HFRPC) beams were tested at a low shear span (a) to depth (d) ratio of 2.4. The effects of hybrid fibers on load–deflection behavior and strain in the strand are reported. Similarly, the crack opening, crack slip and crack angle variation regarding applied shear were investigated using the digital image correlation (DIC) technique. Test results of HFRPC beams showed considerable improvements in peak load and the post-peak response with a higher hybrid fiber dosage. The crack opening and crack slip measurement across the major shear crack revealed continuous dilatant behavior. The kinematic response of critical shear crack reflects the sustained dilation response up to the ultimate load, which depends on the critical shear crack angle of the tested beams. As the fiber dosage increases, the shear crack slip and width are reduced, indicating the roles of hybrid fibers in improving ductility and the change in failure mode from brittle shear tension to relatively ductile shear tension. Full article

The sustainable management of waste from agricultural crops represents an urgent challenge. One possible solution considers waste as possible secondary raw materials for specific uses. Among these, the use of agricultural waste as a product for the assembly of panels for the sound absorption of living environments represents a particularly suitable solution. In this study, the acoustic properties of the cocoa pod husk were evaluated, using silicone as a binder. Different proportions of materials and thicknesses were evaluated. A Support Vector Machine (SVM)-based model with a Gaussian kernel was then used to predict the acoustic performance of composite materials. The results obtained suggest the adoption of this material for the acoustic correction of living environments and this methodology for the prediction of the acoustic behavior of materials. Full article

The aim of this work is to explore the manufacturing of insulation structures using fused filament deposition of biosourced materials. The approach considers printing of Polylactic acid (PLA) and PLA-flax (PF) structures using varied infill density and printing temperatures. Differential Scanning Calorimetry and Thermal Gravimetry analysis are performed to study thermal behaviour of PLA and PF and derive weight content of fibres within PF. Thermal measurements show a strong dependence of thermal conductivity with infill density and slightly improved thermal insulation of PF compared to PLA. Moreover, both PF and PLA show a hydrophobic behaviour unlike conventional green concretes based on hemp or flax. In addition, both scanning electron and optical microscopies show marked morphological changes induced by the laying down process for PF. This latter exhibits a more complex and tortuous microstructure compared to PLA marked by the presence of inter-filament porosity. This work concludes with superior hygrothermal properties of PLA and PF compared to other biosourced materials such as hemp or flax concrete. This work also concludes with the beneficial role of flax fibres that provides better hygrothermal properties to the printed structures as well as on the need to optimize the infill characteristics including density and cell morphology density. Full article

Tissue Engineering is considered a promising route to address existing deficits of autografts and permanent synthetic prostheses for tendons and ligaments. However, the requirements placed on the scaffold material are manifold and include mechanical, biological and degradation-related aspects. In addition, scalable processes and FDA-approved materials should be applied to ensure the transfer into clinical practice. To accommodate these aspects, this work focuses on the high-scale fabrication of high-strength and highly oriented polycaprolactone (PCL) fibers with adjustable cross-sectional geometry and degradation kinetics applying melt spinning technology. Four different fiber cross-sections were investigated to account for potential functionalization and cell growth guidance. Mechanical properties and crystallinity were studied for a 24-week exposure to phosphate-buffered saline (PBS) at 37 °C. PCL fibers were further processed into scaffolds using multistage circular braiding with three different hierarchical structures. One structure was selected based on its morphology and scaled up in thickness to match the requirements for a human anterior cruciate ligament (ACL) replacement. Applying a broad range of draw ratios (up to DR9.25), high-strength PCL fibers with excellent tensile strength (up to 69 cN/tex) could be readily fabricated. The strength retention after 24 weeks in PBS at 37 °C was 83–93%. The following braiding procedure did not affect the scaffolds’ mechanical properties as long as the number of filaments and the braiding angle remained constant. Up-scaled PCL scaffolds resisted loads of up to 4353.88 ± 37.30 N, whilst matching the stiffness of the human ACL (111–396 N/mm). In conclusion, this work demonstrates the fabrication of highly oriented PCL fibers with excellent mechanical properties. The created fibers represent a promising building block that can be further processed into versatile textile implants for tissue engineering and regenerative medicine. Full article

This article proposes an advanced algorithm for the numerical solution of a coupled nonlinear Schrödinger equations system describing the evolution of a high-power femtosecond optical pulse in a single-mode polarization-maintaining optical fiber. We use the algorithm based on a variant of the split-step method with the Madelung transform to calculate the complex amplitude when executing a nonlinear operator. In contrast to the known solution, the proposed algorithm eliminates the need to numerically solve differential equations directly, concerning the phase of complex amplitude when executing the nonlinear operator. This made it possible, other things being equal, to reduce the computation time by more than four times. Full article