An Efficient Approach to Address Issues of Graphene Nanoplatelets (GNPs) Incorporation in Aluminium Powders and Their Compaction Behaviour
by
Zeeshan Baig 1, Othman Mamat 1,*, Mazli Mustapha 1, Asad Mumtaz 2, Mansoor Sarfraz 3 and Sajjad Haider 4
Zeeshan Baig 1, Othman Mamat 1,*, Mazli Mustapha 1, Asad Mumtaz 2, Mansoor Sarfraz 3 and Sajjad Haider 4
1
Department of Mechanical Engineering, Universiti Teknologi PETRONAS, 32610 Bandar Seri Iskandar, Perak, Malaysia
2
Department of Fundamental and Applied Sciences, Universiti Teknologi PETRONAS, 32610 Bandar Seri Iskandar, Perak, Malaysia
3
Sustainable Energy Technologies Center, College of Engineering, King Saud University, Riyadh 11421, Saudi Arabia
4
Department of Chemical Engineering, College of Engineering, King Saud University, Riyadh 11421, Saudi Arabia
*
Author to whom correspondence should be addressed.
Metals 2018, 8(2), 90; https://doi.org/10.3390/met8020090
Received: 12 October 2017 / Revised: 31 December 2017 / Accepted: 22 January 2018 / Published: 25 January 2018
(This article belongs to the Special Issue Metallic Materials and Manufacturing)
The exceptional potential of the graphene has not been yet fully translated into the Al matrix to achieve high-performance Al nanocomposite. This is due to some critical issues faced by graphene during its processing such as the dispersion uniformity, structure damage, compatibility/wettability, and low graphene embedding content in Al matrix. In the present work, a new integrative method was adopted and named as “solvent dispersion and ball milling” (SDBM) to address the issues above efficiently in a single approach. This strategy involves effective graphene nanoplatelets (GNPs) solvent dispersion via surfactant decoration and solution ball milling employed to polyvinyl alcohol (PVA) coated Al with various GNPs content (0.5, 1 and 1.5 wt. %). Flaky Al powder morphology attained by optimizing ball milling parameters and used for further processing with GNPs. Detailed powders characterizations were conducted to investigate morphology, graphene dispersion, group functionalities by FTIR (Fourier transform infrared spectroscopy) spectroscopy and crystallinity by powder XRD (X-ray diffraction)analysis. Compaction behaviour and spring back effect of the GNPs/Al powders was also investigated at different compaction pressure (300 to 600 Mpa) and varying GNPs fractions. In response, green and sintered relative density (%) along with effect on the hardness of the nanocomposites samples were examined. Conclusively, in comparison with the unreinforced Al, GNP/Al nanocomposite with 1.5 wt. % GNPs exhibited the highest hardness gives 62% maximum increase than pure Al validates the effectiveness of the approach produces high fraction uniformly dispersed GNPs in Al matrix.
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Keywords:
graphene; dispersion; powder processing; ball milling; aluminium nanocomposite
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MDPI and ACS Style
Baig, Z.; Mamat, O.; Mustapha, M.; Mumtaz, A.; Sarfraz, M.; Haider, S. An Efficient Approach to Address Issues of Graphene Nanoplatelets (GNPs) Incorporation in Aluminium Powders and Their Compaction Behaviour. Metals 2018, 8, 90.
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