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Polymers
Volume 17
Issue 12
10.3390/polym17121597
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This is an early access version, the complete PDF, HTML, and XML versions will be available soon.
Article

AI-Aided Crystallization Elution Fractionation (CEF) Assessment of Polyolefin Resins

by
Lorenzo Brighel
1,2,
Gabriella Maria Lucia Scuotto
1,
Giuseppe Antinucci
1,2,
Roberta Cipullo
1,2 and
Vincenzo Busico
1,2,*
1
Department of Chemical Sciences, Federico II University of Naples, via Cinthia, 80126 Napoli, Italy
2
DPI, 5600 AX Eindhoven, The Netherlands
*
Author to whom correspondence should be addressed.
Polymers 2025, 17(12), 1597; https://doi.org/10.3390/polym17121597 (registering DOI)
Submission received: 2 May 2025 / Revised: 30 May 2025 / Accepted: 6 June 2025 / Published: 7 June 2025
(This article belongs to the Special Issue Scientific Machine Learning for Polymeric Materials)
Versions Notes

Abstract

Artificial Intelligence (AI) tools and methods are dramatically innovating the application protocols of most polymer characterization techniques. In this paper, we demonstrate that, with the aid of custom-made and properly trained machine learning algorithms, analytical Crystallization Elution Fractionation (aCEF) can be changed from an ancillary to a standalone approach usable to identify and categorize commercially relevant polyolefin materials without any prior information. The proposed protocols are fully operational for monomaterials, whereas for multimaterials, integration with AI-aided 13C NMR is a realistic intermediate step.
Keywords: crystallization elution fractionation; artificial intelligence; machine learning; polyolefin characterization; mechanical recycling crystallization elution fractionation; artificial intelligence; machine learning; polyolefin characterization; mechanical recycling

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MDPI and ACS Style

Brighel, L.; Scuotto, G.M.L.; Antinucci, G.; Cipullo, R.; Busico, V. AI-Aided Crystallization Elution Fractionation (CEF) Assessment of Polyolefin Resins. Polymers 2025, 17, 1597. https://doi.org/10.3390/polym17121597

AMA Style

Brighel L, Scuotto GML, Antinucci G, Cipullo R, Busico V. AI-Aided Crystallization Elution Fractionation (CEF) Assessment of Polyolefin Resins. Polymers. 2025; 17(12):1597. https://doi.org/10.3390/polym17121597

Chicago/Turabian Style

Brighel, Lorenzo, Gabriella Maria Lucia Scuotto, Giuseppe Antinucci, Roberta Cipullo, and Vincenzo Busico. 2025. "AI-Aided Crystallization Elution Fractionation (CEF) Assessment of Polyolefin Resins" Polymers 17, no. 12: 1597. https://doi.org/10.3390/polym17121597

APA Style

Brighel, L., Scuotto, G. M. L., Antinucci, G., Cipullo, R., & Busico, V. (2025). AI-Aided Crystallization Elution Fractionation (CEF) Assessment of Polyolefin Resins. Polymers, 17(12), 1597. https://doi.org/10.3390/polym17121597

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