A Comprehensive Review on Sensor-Based Electronic Nose for Food Quality and Safety
Abstract
1. Introduction
- Ensuring food quality and safety: E-noses help detect spoilage, contamination, and adulteration in food products, ensuring freshness and quality control.
- Advancing medical diagnostics: E-noses are used in disease detection by analyzing breath, sweat, or urine to identify biomarkers associated with conditions like diabetes, cancer, and infections.
- Enhancing environmental monitoring: E-noses detect pollutants, hazardous gases, and air quality changes, aiding in environmental protection and public health.
- Improving industrial process control: E-noses help monitor manufacturing processes, detect leaks, and ensure consistent product quality in industries such as pharmaceuticals, perfumes, and beverages.
- Strengthening security and defense: E-noses are used in explosive and drug detection, helping in law enforcement and military and border security operations.
- Boosting agriculture and farming: E-noses assist in monitoring soil conditions, plant health, and pest infestations by detecting VOCs released by plants to improve crop yields and reduce reliance on harmful pesticides.
- Ensuring workplace safety: E-noses help prevent occupational hazards by detecting toxic or flammable gases in industrial and laboratory environments.
1.1. Research Questions and Contributions
1.1.1. Research Questions
- Research Question 1 (RQ1): What are the state-of-the-art research results over the last decade in the field of e-nose systems aimed at food quality and safety?
- Research Question 2 (RQ2): What lessons have been learned from the design and deployment of e-nose systems in laboratory and industrial settings?
- Research Question 3 (RQ3): What research gaps exist in the application of e-noses for food quality and safety, and what are the future research directions that we must explore to address these gaps?
1.1.2. Research Contributions
- We present an in-depth analysis of research results over the past decade in the e-nose field designed for food quality and safety. We concluded the analysis based on a proposed taxonomy, which we developed through a comprehensive examination of peer-reviewed research papers from three scientific databases. We highlight key technological advances, practical implementations, and performance results obtained across various food sectors.
- We identify critical lessons learned, such as the importance of e-nose components selection (sensors, signal processing unit, data pattern recognition model) according to the type of food and the need to develop suitable data pattern recognition models, as well as new sensors tailored to food quality and safety assessment.
- We identify current research gaps, such as the lack of real-world validation and limited sensor sensitivity, and we discuss future research opportunities that will improve the reliability, scalability, and industrial applicability of e-nose technologies in food systems.
1.1.3. Organization of This Paper
2. E-Nose Components
- Conductometric sensors, including conducting polymer (CP) sensors [12], alter their conductivity in the presence of gas molecules.
- Electrochemical sensors [15] convert chemical reactions at the electrode surface into electrical signals.
- Optical sensors [16] monitor changes in light absorption, fluorescence, or scattering in response to gas exposure.
- Bioelectronic sensors [19] integrate biological recognition elements to selectively detect specific VOCs.
3. Review Methodology
3.1. Criteria for Selecting Relevant Research Papers Used in This Review
- In the first stage, we used the Scopus, IEEE Xplore, and Web of Science (WoS) electronic databases to search for final peer-review English-language documents published between 2014 and 2025. We considered only documents of type articles, reviews, and conference papers. We conducted the search using the following words appearing in the title or abstract of the documents: electronic nose, e-nose, artificial nose, bioelectronic nose, food quality, food safety, and food freshness.
- In the second stage, we reviewed the titles of the documents retrieved from the search query to remove duplicates.
- In the third stage, we thoroughly reviewed the full text of the remaining documents (after removing duplicates) before making the final selection, excluding unrelated studies, highlighting the key sections relevant to our review, and identifying the taxonomy of the research literature on the development of e-nose technology/applications in the field of food quality and safety.
3.2. Preliminary Results Obtained
3.3. Final List of Selected Papers and Taxonomy of the Research Literature on E-Nose for Food Quality and Safety
4. Analysis of the Research Works from the Final List of Selected Publications
4.1. Reviews
4.1.1. Reviews on Advancements in Electronic Nose Systems for Food Industry Applications
4.1.2. Reviews on Sensor Development and Pattern Recognition Techniques in Electronic Nose Systems
4.1.3. Reviews on Recent Sensing Technologies for Food Quality Assessment
4.1.4. Our Review on Sensor-Based Electronic Nose for Food Quality and Safety
- Development and application of a unique taxonomy ensuring broad coverage and reduced selection bias: We conducted an extensive analysis of peer-reviewed studies across three major scientific databases, the taxonomy. The taxonomy enables a systematic evaluation of technological advancements (both sensors and pattern recognition techniques), practical implementations, and performance outcomes across the following food and beverage sectors: meat, seafood, vegetables and fruits, spices, oils, coffee, tea, diary, and alcoholic beverages.
- Decade-long coverage of research results: By capturing trends over an extended period, our review offers an up-to-date perspective on technological evolution and trends.
- Lessons-learned synthesis: Our review identifies critical lessons learned from the existing literature in each category from the taxonomy we developed. The lessons learned will help guide both future academic research and practical development of e-nose systems for food quality and safety.
- Identification of unresolved research gaps: Our review reveals notable gaps that must be addressed in the future. These gaps include the lack of e-nose real-world validation, limitations in sensor sensitivity and stability, challenges in achieving miniaturize and portable e-noses, lack of standardized testing protocols, limited real-time processing capabilities, and insufficient support for user-friendly visualization of odor classification and identification outcomes.
4.2. Electronic Nose Systems for Food Quality and Safety
Lessons Learned
- Cost: The sensors used in the experiments belong to the cheap components’ class, usually included in gas measurement systems, where their main feature is the detection of the presence of a certain gas component. Another characteristic of such systems is the low manufacturing cost. The documentation that comes with the sensors used is brief, containing little relevant information, omitting aspects like the manufacturer-recommended schematics, calibration and compensation methods depending on temperature and relative humidity values, or formulas for converting the voltage or resistance measured by the microcontroller back into the actual physical quantity measured by the sensor. In many cases, the datasheets do not include important characteristics such as precision, accuracy, repeatability, stability over time, or startup periods. Most sensors used are analog, and they do not integrate calibration circuits, drift, compensation or control mechanisms, or an ADC within the same package. As a result, their overall measurement performance is typically poor, and they are further affected by the required external electronics. The BME688 [125] sensor used in [124,152] stands out in a positive way because it includes important circuitry besides the sensing element, which supports advanced functions such as filtering, signal conditioning, the ADC, the compensation table and algorithm, and digital communication with the processing unit, ESP32. The BME688 development kit uses eight sensors instead of one to form a sensor array, which enhances detection performance, especially for low-cost setups. Though calibrated, sensors differ slightly, and tracking signal trends over time across multiple sensors improve reliability. Additionally, free gas flow causes variations in individual sensor responses before steady state, making arrays beneficial.
- Power usage: The energy consumption required by the sensors used is high, and they are suitable for integration with systems powered permanently from the main power outlet. Sensors with heaters that are common in most studies have long response times, between 10 and 300 s, and operate at 200–400 °C. This leads to high power consumption unsuitable for portable devices and faster aging that requires frequent recalibrations. The recommended preheating time, or sensor warm-up time, until the first correct measurements can be extensively long, up to 2 to 7 days in some cases. The power consumed during measurement ranges from 0.3 to 1.0 W, and the continuous operation of the heating element in some sensors makes them unsuitable for use in portable electronic nose systems.
- Data collection: The data acquisition platforms are not designed for instrumentation systems. Most of the proposed solutions use low-resolution ADCs (10- or 12-bit), typically with a 0 to 5 V input range. This leads to an effective resolution per bit of 5 to 10 mV. Temperature and relative humidity compensation are generally based on low-accuracy T and RH sensors (±1 °C for temperature and ±4% for relative humidity), with a few exceptions. In platforms based on ESP32, measurement performance in terms of used digits is further limited by the built-in ADC, which typically offers an effective resolution of only 8 bits. Some proposed electronic nose systems utilize industrial-grade measurement platforms (i.e., PCI6035E, AD7606) and compensation sensors (sensors helping in adjusting the measurement depending on ambient parameters such as temperature, humidity, or pressure) for temperature and relative humidity (i.e., SHT15), which outperform those commonly used in standard gas detectors.
- Portability: Very few papers focus on low-power or portable systems. However, the question of whether a measurement system can be powered from the main outlet is a valid one. In this case, what are the time and logistical efforts required to make the system operational at a different location? For example, when considering the BME688 sensor, a system using it requires 30 min to reach maximum accuracy after power cycling. Other manufacturers do not specify this time requirement, but in some cases, it could require days.
- Data processing: Generally, the accuracy of measurement data is verified through thousands of hours of operation and repeated measurements, ideally conducted on multiple similar devices operating in parallel. Some past research solutions [103,115,119,138,141,163] used professional techniques (i.e., Gas Chromatography–Mass Spectrometry (GC–MS) [176]) to compare their experimental results with reference ones. In all the papers that we reviewed, the number of samples collected by the sensor arrays and used by the machine learning algorithms is rather small (<300 samples). In these conditions, expecting authors to validate their work with equipment that has been running for a full year is not feasible. This raises questions regarding the performance metrics obtained. To validate the results obtained, standard test/evaluation scenarios should be run, not just particular test sets created by the authors of the papers.
4.3. Food Analysis Based on Previously Developed/Commercial Electronic Nose Systems
4.3.1. Commercial Electronic Nose Systems
4.3.2. Electronic Noses Developed by Academic Research Groups
Lessons Learned
- To apply well-known pattern recognition techniques to assess the quality and safety of different types of food: Studies such as [178,188,194,195,196] used PEN3, Fox 3000, and Fox 4000 commercial electronic noses to apply algorithms such as PCA, Random Forest, and ANNs to evaluate the quality of various food categories (meat, fruits, jams, milk). In [186,189,197], the researchers applied well-known pattern recognition techniques (PCA, PLS-DA, Partial Least Squares regression) to both e-nose data (PEN3, Fox 4000) and chromatography analysis results (GC–MS), leveraging the complementary strengths of these methods in chemical analysis and pattern recognition.
- To develop novel models or algorithms for odor identification and classification: Studies such as [183,191,193,202] used data collected from commercial electronic nose devices (PEN3, Cyranose@ 320) to develop novel data models for the identification and classification of odors, demonstrating strong performance.
- To confirm the ability of commercial e-noses to recognize and classify aromas: Studies such as [199,200] proved that the FOODsniffer e-nose can accurately classify meat based on its data analysis, with results validated against GC–MS analysis and physicochemical measurements. The authors of [201] validated NeOse Pro to evaluate the quality of the plant-based beverage by applying PCA and LDA to the e-nose data and comparing the results with those obtained using the same algorithms on GC–MS data.
4.4. Gas Sensors for Electronic Nose Systems
Lessons Learned
4.5. Food-Related Datasets and Algorithms/Techniques for Pattern Recognition Used on Them
Lesson Learned
- Public datasets provide a valuable foundation for developing and testing new models or algorithms for odor identification and classification.
- Public datasets accelerate comparative research. The availability of well-structured datasets has enabled researchers to benchmark different models, promoting transparency and repeatability. As Table 11 shows, deep learning models outperform traditional classifiers in some cases. Additionally, approaches that combine multiple classifiers tend to boost accuracy and model stability. Such comparisons are possible because the researchers employed the same dataset.
- Diverse model strategies provide complementary insights. The use of a wide range of algorithms across datasets shows that no single approach performs best across all datasets and applications. Different algorithms excel under specific data characteristics and task requirements.
- Model performance is dataset dependent. Even if the authors of the cited research efforts reported high accuracies, these are heavily influenced by the specific dataset, number of classes, sensor types, and experimental conditions.
5. Research Gaps and Future Research Opportunities
- Sensor technology: We must develop novel gas-sensitive materials with enhanced selectivity and sensitivity for food VOCs, new gas sensors with fast response time, adaptive calibration methods, and sensor baseline correction techniques to improve the stability of the gas sensors and integrate bio-inspired or biomimetic sensors.
- Data processing: We must implement deep learning algorithms for pattern recognition and VOC classification. We must develop and implement efficient multi-sensor (e-nose, e-tongue, e-eye) data fusion algorithms for a more holistic food profiling approach. Additionally, we must also develop standardized odor databases and reference libraries and real-time data analysis platforms for on-site decision making.
- Miniaturization and portability: We must integrate micro-electro-mechanical systems/ nano-electro-mechanical systems technology for compact and low-power devices. We must also develop reliable wireless and IoT-enabled e-noses for remote monitoring.
- Standardization: We must develop standardized testing protocols across different food types and storage conditions.
6. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
Abbreviations
ADC | analog-to-digital converters |
ANNs | artificial neural networks |
CNN | Convolutional Neural Network |
CNT | carbon nanotube |
CP | conducting polymer |
GC–IMS | Gas Chromatography with Ion Mobility Spectrometry |
GC–MS | Gas Chromatography–Mass Spectrometry |
KNNs | k-nearest neighbors |
LDA | linear discriminant analysis |
LSTM | Long Short-Term Memory |
MLP | Multilayer Perceptron |
MOS | metal oxide semiconductor |
MSE | Mean Squared Error (MSE) |
PCA | principal component analysis |
PIC | Programmable Interface Controller |
PLS-DA | Partial Least Squares-Discriminant Analysis |
PNN | Probabilistic Neural Network |
PPM | Parts per Million |
QCM | quartz crystal microbalance |
R2 | R-squared |
RMSE | Root Mean Square Error |
SAW | surface acoustic wave |
SVMs | support vector machines |
SVR | Support Vector Machine Regression Technique |
VOCs | volatile organic compounds |
WoS | Web of Science |
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Type of Sensor | Advantages | Application Sector |
---|---|---|
Chemiresistive sensors: MOS | High sensitivity, high selectivity, durability, long lifespan, fast response time | Air quality monitoring, food freshness detection, industrial gas sensing, medical diagnostic |
Chemiresistive sensors: CNT | Ultra-high sensitivity, fast response time, low power consumption, miniaturization potential | Breath analysis for disease detection, air quality monitoring, workspace safety |
Conductometric sensors: CP | Fast response time, low power consumption, tunable sensitivity | Medical diagnostics, food quality assessment, environmental monitoring |
Mass-sensitive sensors: QCM | High sensitivity, ability to detect low-concentration gases | Breath analysis, detection of toxic substances, fragrance quality control |
Mass-sensitive sensors: SAW | Fast response time, small size, high ruggedness | Explosive and drug detection, environmental monitoring, workspace safety |
Electrochemical sensors | High selectivity in terms of the electrochemical properties of target VOCs, low power consumption, reliable detection of specific gases | Toxic gas detection, breath analysis, air quality monitoring |
Optical sensors | Non-contact sensing, high specificity in terms of the chemical identity of VOCs, fast response time | Industrial gas detection, medical diagnostics, hazardous material monitoring, food quality assessment |
FET sensors | High sensitivity, fast response time, compatibility with nanomaterials and 2D materials, fast electronic response | Medical diagnostics, food quality assessment, environmental monitoring, industrial process control, security and defense |
Bioelectronic sensors | High specificity in terms of molecular recognition of target VOCs, biomimetic functionality, potential for personalized diagnostics | Disease detection, food quality monitoring |
Pattern Recognition Technique | Advantages | Type of Sensor | Application Sector |
---|---|---|---|
PCA |
| MOS, CP, QCM, SAW, CNT, optical sensors, electrochemical sensors | Food quality control, medical diagnostics, environmental monitoring, industrial process control |
LDA |
| MOS, CP, QCM, SAW, optical sensors, electrochemical sensors | Medical diagnostics, food quality control, environmental monitoring, security and defense |
ANNs |
| MOS, CP, QCM, SAW, CNT, bioelectronic sensors | Medical diagnostics, food quality control, environmental monitoring, security and defense |
SVM |
| MOS, CP, QCM, SAW, CNT | Medical diagnostics, food quality control, environmental monitoring, security and defense, workspace safety |
KNN |
| MOS, CP, QCM, SAW, CNT | Food quality monitoring, environmental monitoring, medical diagnostics, industrial process control |
6 March 2025 | Journal/ Magazine Articles | Reviews | Conference Papers | Total |
---|---|---|---|---|
Scopus | 40 | 11 | 18 | 69 |
IEEE Xplore | 21 | 2 | 94 | 117 |
WoS | 298 | 120 | 47 | 465 |
Total | 359 | 133 | 159 | 651 |
Total without duplicates | 314 | 122 | 113 | 549 |
6 March 2025 | Journal/ Magazine Articles | Reviews | Conference Papers | Total |
---|---|---|---|---|
Scopus | 3 | 2 | 6 | 11 |
IEEE Xplore | 5 | 0 | 35 | 40 |
WoS | 233 | 78 | 35 | 346 |
Final total | 241 | 80 | 76 | 397 |
Paper | Design Architecture | Data Analysis Techniques | Evaluation and Performance Metrics | Application Area |
---|---|---|---|---|
Electronic Nose Systems for Meat Quality and Safety | ||||
[76] | Sensor array: MQ-137, MQ-136 [77], TGS2602 [78]; Signal processing unit: Arduino Uno R3 | PCA | Accuracy: 94.9% (fresh/spoiled/rotten) | Beef quality assessment |
PCA + Probabilistic Neural Network (PNN) [79] | Accuracy: 100% (fresh/spoiled) | |||
[80] | IoT-enabled e-nose; Sensor array: AM2302 [81], one optical sensor from Winsen Electronics Technology Co., Zhengzhou, China, MH-Z19C [82], ZE03-NH3, ZE03-C2H4 [83]; Signal processing unit: ESP32-S3 controller [84] | Linear Regression [85] | Aerobic bacteria and Pseudomonas species play a crucial role in the production of VOCs in beef | Beef quality monitoring and spoilage detection |
[86] | Sensor array: MQ-2, MQ-3, MQ-4, MQ-6, MQ-7, MQ-8, MQ-9, MQ-135 [77]; Signal processing unit: Arduino Mega 2560 microcontroller [87], Raspberry Pi 4 [88] | PCA + SVM | Accuracy: 98.49% (healthy/ compromised) | Chicken meat quality assessment |
[89] | Sensor array: MQ-2, MQ-3, MQ-6, MQ-7, MQ-9, MQ-135, DHT22 [90]; Signal processing unit: Arduino Uno microcontroller | SVM, Linear Regression, KNN, Random Forest [91] | Best accuracy: 100% for Random Forest with random split data; 69% for Random Forest with non-randomly split data; 78.5% for SVM with group split data (fresh/semi-fresh/spoiled) | Chicken meat quality assessment |
[92] | Sensor array: HGS1000, HGS1001, HGS1002, HGS1007 [93]; Signal processing unit: 12-bit ADC with four channels of input data; heating voltage can be set between 0 and 2.4V | Convolutional Neural Network (CNN) CNN [94] + time series feature extraction [95] | Accuracy: 92.1% (fresh/sub-fresh/spoiled) Accuracy: 98.4% (fresh/sub-fresh/spoiled) | Pork, beef, mutton, chicken, crab, shrimp, fish meat quality assessment |
[96] | Sensor array: MQ-2, MQ-4, MQ-6, MQ-9, MQ-135, MQ-136, MQ-137, MQ-138,DHT22; Signal processingunit: N/A | KNN | Accuracy rates between 97% and 100% (variations of meat with ratio 0%, 10%, 50%, 90%, 100%) | Authenticity of beef and pork meat |
SVM | Accuracy rates between 81.5% and 99.5% (variations of meat with ratio 0%, 10%, 50%, 90%, 100%) | |||
Electronic Nose Systems for Seafood Quality and Safety | ||||
[97] | Sensor array: MQ-136, MQ-137, MQ-5, MQ-8; Signal processing unit: N/A | Support Vector Machine Regression Technique (SVR) [98] | R-squared (R2): 0.981; Root Mean Square Error (RMSE): 0.012 | Estimation of the microbial population in seafood |
[99] | IoT-enabled e-nose with image processing capabilities; Sensor array: N/A; Signal processing unit: N/A | A nonparametric kernel-based modeling + hidden Markov model | Quality model indices closely align with the manual results provided by quality assurance experts | Fish origin verification, fish quality assessment |
[100] | Sensor array: MQ-1, MQ-2 and two MQ-135; Signal processing unit: ESP32 microcontroller | KNN | Accuracy: 98% (fresh/less fresh/ not fresh) | Freshness and quality of crabs |
Naïve Bayes [101] | Accuracy: 91% (fresh/less fresh/ not fresh) | |||
SVM | Accuracy: 87% for SVM (fresh/less fresh/not fresh) | |||
[102] | Sensor array: TGS2620, TGS2611, TGS822, TGS832, TGS2602, TGS2600, TGS826, TGS825; Signal processing unit: N/A; Preheating process before using the sensors | PCA | Cumulative variance of the principal component: 95% (fresh/contaminated) | Tuna quality assessment (Pseudomonas aeruginosa bacteria) |
SVM | Accuracy: 99% (fresh/contaminated) | |||
[103] | Sensor array: MQ-2, MQ-3, MQ-4, MQ-5, MQ-6, MQ-7, MQ-8, MQ-9; Signal processing unit: N/A | Linear Regression | R2: 0.98; Accuracy: 93.75% | Prawn quality assessment |
Electronic Nose Systems for Vegetables and Fruits Quality and Safety | ||||
[104,105] | Sensor array: MQ-3, MQ-6, MQ-8, MQ-135; Signal processing unit: ADC for Raspberry Pi 4/ Raspberry Pi 3 | CNN | Accuracy: 86% (ripe/not ripe/unknown) | Identification of the ripening stage of tomato fruits |
[106] | Sensor array: MQ-135, MQ-136, TGS822, TGS2600, TGS2602, TGS2603, TGS2610, TGS2611, DHT22; Signal processingunit: N/A | Random Forest | Accuracy: 94% (good/good/fair/ poor) | Identification of the ripening stage of tomato fruits |
KNN | Accuracy: 83% (good/good/fair/ poor) | |||
ANNs | Accuracy: 79% (good/good/fair/ poor) | |||
SVM | Accuracy: 64% (good/good/fair/ poor) | |||
[107,108] | Sensor array: MQ-135, MQ-4; Signal processing unit: Gizduino micro- controller [109] | ANNs | Accuracy: 93.33% (not spoiled/ partially spoiled/ spoiled) | Tomato puree quality assessment |
Fuzzy logic technique [110] | Accuracy: 90% (not spoiled/ partially spoiled/ spoiled) | |||
[111] | Sensor array: TGS2620, TGS823, DHT22; Signal processing unit: Arduino microcontroller | PCA + t-distributed Stochastic Neighbor Embedding [112] + k-Means [113] + Long Short-Term Model [114] | Accuracy: 99.46% (fresh/half-spoiled/spoiled) | Broccoli quality assessment |
[115] | Sensor array: TGS880, TGS822, TGS826, TGS2602, TGS2600; Signal processing unit: ATmega8 [116] microcontroller with an integrated ADC | PCA + Centroid link- and completely-link cluster analyses | Similarity levels >93% for of the samples tested (fresh/half/ completely contaminated) | Broccoli quality assessment (Staphylococcus, Salmonella and Shigella) |
[117] | Sensor array: MQ-2, DHT11; Signal processing unit: Arduino Uno microcontroller and Node MCU [118] IoT platform | Linear Regression, Random Forest, SVR | Best performance with a value of Mean Squared Error (MSE): 0.1207 for Random Forest | Banana freshness assessment |
[119] | Sensor array: TGS2600, TGS2602,TGS2603, TGS2610, TGS2611, TGS2612, TGS2620; Signal processing unit: NI DAQ card, USB-6009 [120] | PCA + KNN | Accuracy: 98.10% (unripe/half-ripe/fully ripe/overripe) | Identification of the ripening stage of banana |
PCA + SVM | Accuracy: 95.24% (unripe/half-ripe/fully ripe/overripe) | |||
LDA + KNN | Accuracy: 90.48% (unripe/half-ripe/fully ripe/overripe) | |||
LDA + SVM | Accuracy: 86.67% (unripe/half-ripe/fully ripe/overripe) | |||
[121] | Sensor array: MQ-2, MQ-3, MQ-4, MQ-5, MQ-7, MQ-8, MQ-135 sensors; Signal processing unit: Arduino Due [122] microcontroller | SVM | Accuracy: 99% (rotten/fresh) | Avocado fruits quality assessment |
[123] | Sensor array: MQ-136, MQ-4, MQ-137, MQ-3, MQ-2, MQ-135, MQ-131, MQ-8, MQ-9; Signal processing unit: Raspberry Pi computer | PCA + KNN | Accuracy: 92% (spoiled/not spoiled) | Fruits (banana, pechay, carrot, grape) quality assessment |
[124] | Sensor array: eight BME688 gas sensors [125]; Signal processing unit: Adafruit Huzzah32 (ESP32) development board [126] | Neural Networks [127] | Accuracy: 76% (spoiled/not spoiled) | Fruits and vegetables quality assessment |
Electronic Nose Systems for Spices’ Quality and Safety | ||||
[128,129] | Sensor array: TGS800, TGS813, TGS823, TGS2602, TGS2610, TGS2611, TGS2620, MQ-135; Signal processing unit: ADCs of a Programmable Interface Controller (PIC) microcontroller | Random Forest | Accuracy: 100% (nutmeg/ clove/cinnamon) | Identification of nutmeg, clove, and cinnamon |
[130] | Sensor array: TGS2600, TGS2602, TGS2610, TGS813, TGS822, MQ-138, MQ-2 MQ-8; Signal proc. unit: AD7606 analog-to- digital data acquisition system [131] and S3C6410-based Linux platform [132] | PCA + SVM | Accuracy: 95% | Authenticity of star anise |
Electronic Nose Systems for Oils’ Quality and Safety | ||||
[133] | Sensor array: eight TGS and MQ sensors, and one temperature and relative humidity sensor; Signal proc. unit: RPi computer | Clustering technique [134] | Identification of three classes of palm oil: never heated/heated for 10 to 30 h/heated for 40 to 60 h | Palm oil quality assessment |
[135] | Sensor array: MICS-6814 MOS sensor [136], MCP9700 temperature sensor [137]; Signal processing unit: ADS1015, PIC18F45K22, FT230XS USB/UART converter | ANNs | Accuracy: 99.49% (degummed/extraction/filtered/marketed) | Sunflower oil quality assessment |
[138] | Sensor array: MQ-3, MQ-4, MQ-7, MQ-8, MQ-135, MQ-137, MQ-138, MG-811; Signal processing unit: N/A | ANNs (classification) | Accuracy: 86.5% | Extra-virgin olive oil quality assessment |
ANNs (regression) | Correlation coefficient: 0.93; Slope 0.90 | |||
[139] | Sensor array: MQ-2, MQ-3, MQ-4, MQ-5, MQ-7, MQ-8, MQ-9, MQ-135; Sensor processing unit: Arduino Nano microcontroller | Discrete Fourier transform data analysis [140] | Accuracy: 91% (extra virgin/virgin); Accuracy: between 67% and 77% (extra virgin/virgin/blend /pomace/fresh air) | Olive oil quality assessment |
[141] | Sensor array: MQ-3, TGS822, MQ-136, MQ-9, TGS813, MQ-135, TGS2602, TGS2620; Sensor processingunit: N/A | PCA | Total variance of the data for distilled water extracts from mint plants: 95%; Total variance of the data for mint essential oil: 89% | Mint essential oil and mint distilled water extracts quality assessment |
LDA | Accuracy for the classification of mint essential oil: 91.33%; Accuracy for mint distilled water extracts: 86.67% | |||
ANNs | Accuracy for the classification of distilled water extracts 100%; Accuracy for the classification of mint essential oil 96.7% | |||
[142] | Sensor array: MQ-9, MQ-4, MQ-135, MQ-8, TGS2620, MQ-136, TGS813, TGS822, MQ-3; Signal proc. unit: N/A | PCA | Accuracy: 98% | Identification of essential oils from herbs and fruits |
LDA and Quadratic Discriminant Analysis | Accuracy: 100% (essential oil emissions from herbal leaves/fruits); Accuracy: 100% for Quadratic Discriminant Analysis and 98.9% for LDA (mango/lemon/orange /mint/tarragon/thyme) | |||
SVM | Accuracy: 100% (essential oil emissions from herbal leaves/fruits); Accuracy: 98.9% (mango/lemon/orange /mint/tarragon/thyme) | |||
[143] | Sensor array: six different polymeric gas sensors (polymeric nanocom- posites of polyaniline with multiwalled carbon nanotubes and graphene oxide); Signal processing unit: N/A | PCA | Accuracy: 99.85% | Authenticity of clove oil |
Interactive Document Map multivariate projection techniques | Accuracy: 99.81% | |||
LDA | Accuracy: 98.30% | |||
Electronic Nose Systems for Coffee and Tea Quality and Safety | ||||
[144] | Sensor array: MQ-7, MQ-3, MQ-135, TGS2600, TGS2602, TGS2610, TGS2611, TGS2620, DHT22; Signal processing unit: N/A | Extreme Gradient Boosting [145] | Accuracy rates between 82% and 95% (sixteen classes of coffee) | Authenticity of coffee |
SVM | Accuracy rates between 81% and 95% (sixteen types of coffee) | |||
CNN | Accuracy rates between 86% and 98% (sixteen types of coffee) | |||
CNN + Long Short-Term Memory (LSTM) [146] | Accuracy rates between 83% and 98% (sixteen types of coffee) | |||
[147] | Sensor array: carbon nanotube-based multichannel with 64 interdigital electrodes; Sensor processing unit: N/A | LDA | Accuracy: 97.4% (three different coffee aromas) | Authenticity of coffee |
[148] | Sensor array: four sensors (SnO2_bs1, ZH0504, SnO2 Au_bs2, SU0303) and two nanowire sensors (Sn-NW1, Sn-NW2); Sensor processing unit: N/A | PCA | N/A (four classes of roasted coffee beans) | Analysis of different methods of coffee roasting |
[149] | Sensor array: TGS821, TGS2444, TGS823, TGS2600, TGS2602, TGS2610, TGS826, TGS2620; Signal processing unit: NI DAQ card, USB-6009 | PCA | Accuracy: 95% (four acidity levels of coffee drinks) | Coffee drinks quality assessment |
Radial Basis Function Neural Network [150] | Accuracy: 94.75% (to predict the scores of acidity level) | |||
[151] | Sensor array: six sensing units (nanocomposites that stem from the combination of ZnO, In2O3, and ZnO/In2O3 nanoparticles with polypyrrole and poly(styrenesulfonate)); Signal processing unit: N/A | PCA + Euclidean distances by dendrograms | N/A (seventeen classes of coffee) | Authenticity of coffee |
[152] | Sensor array: eight BME688 sensors; Signal processing unit: Adafruit Huzzah32 (ESP32) development board | Random Forest | MSE: 0.062 | Authenticity of coffee |
Stochastic Gradient Descent [153] | Accuracy: 70.10% (two classes of coffee) | |||
Adam Optimizer [154] | Accuracy: 67.70% (two classes of coffee) | |||
[155] | Sensor array: TGS832, TGS823, TGS2600, TGS2610, TGS2611; Signal processing unit: PCI6035E data acquisition card [156] | Bayesian classification [157] | Classification error in percentage 30.91% (four classes of tea) | Black tea quality assessment |
Electronic Nose Systems for Diary Quality and Safety | ||||
[158] | Sensor array: TGS2600, TGS822, TGS2611, TGS826, TGS2602, TGS832, TGS2620; Signal processing unit: Arduino microcontroller | PCA + LDA + SVM | Accuracy: 85% | Identification of milk source |
PCA + LDA + Logistic Regression [159] | Accuracy: 81.50% | |||
PCA + LDA + Random Forest | Accuracy: 80.50% | |||
Electronic Nose Systems for Alcoholic Beverage Quality and Safety | ||||
[160] | Sensor array: MQ-2, MQ-135, TGS825, WSP-2110, MP-503, TGS2602, WSP-1110, MQ-138, MQ-137, MQ-136; Sensor processing unit: N/A | Convolution Dot-Product Attention Mechanism [160], Residual network (ResNet50 mode) [161] | Accuracy: 98.47% (ten production origins of rice wines) | Identification of the origins of rice wines |
[162] | Sensor array: TGS2600, TGS2602, TGS2603, TGS2610, TGS2611, TGS2620, TGS813, TGS822; Sensor processing unit: N/A | LDA + PCA + CNN-LSTM | Accuracy: 98% (whiskey/brandy /gin/vodka/tequila) | Identification of various types of spirit samples |
[163] | Sensor array: TGS2600, TGS2603, TGS2610D, TGS2611C, TGS2620; Signal processing unit: N/A | Linear Discriminant | Accuracy: 69.23% (six brands of whiskey); Accuracy: 100% (whiskey regions of origin) | Authenticity of whiskey |
SVM | Accuracy: 82.05% (six brands of whiskey); Accuracy: 98.72% (whiskey regions of origin) | |||
KNN | Accuracy: 61.54% (six brands of whiskey); Accuracy: 92.31% (whiskey regions of origin) | |||
Bagged Tree [91] | Accuracy: 74.36% (six brands of whiskey); Accuracy: 94.87% (whiskey regions of origin) | |||
Subspace Discriminant [164] | Accuracy: 70.51% (six brands of whiskey); Accuracy: 100% (whiskey regions of origin) | |||
[165] | Sensor array: TGS2600, TGS2602, TGS2603, TGS2610, TGS2611, TGS2620, TGS813, TGS822, DHT22; Signal processing unit: N/A; | CNN-LSTM | Accuracy: 93% (three whiskey types) | Authentication of whiskey |
CNN | Accuracy: 91% (three different types of whiskey) | |||
LSTM | Accuracy: 91% (three different types of whiskey) | |||
Recurrent Neural Networks [166] | Accuracy: 89% (three whiskey types) | |||
[167] | Sensor array: eight MOS sensors with two different types of copper oxide heterojunctions, ZnO–CuO and NiO–CuO; Signal processing unit: N/A | Hierarchical Clustering Analysis [168] | Euclidean distance: 0.5 (four samples of Chinese Jing Wine) | Identification of the same liquors manufactured in different years |
[169] | Sensor array: TGS825, TGS821, TGS826, TGS822, TGS842, TGS813, TGS2610, TGS2201; Signal processing unit: N/A | PCA + Signal-to-Noise Ratio | First two principal components captured 92.47% of data variance (thirteen varieties of Chinese liquor) | Identification of several types of liquors |
[170] | Sensor array: MQ-3, MQ-6, MQ-9, MQ-135, MQ-136, MQ-137, MQ-138, MQ-139, SHT15 [171]; Signal processing unit: NI DAQ card, USB-6009 | PCA + Multi-Layer Perceptron (MLP) [172] | Accuracy: 100% (three distinct local Thai spirits) | Identification of local Thai craft spirits |
PCA + k-Means | Accuracy: 72.23% (three distinct local Thai spirits) | |||
[173] | Sensor array: MQ-3, MQ-4, MQ-7, MQ-8, MQ-135, MQ-136, MQ-137, MQ-138, MG811 [174], AM2320 [175]; Signal processing unit: microcontroller with an onboard ADC | ANNs | Correlation coefficient: 0.97 (to predict seventeen volatile aromatic compounds) | Beer quality assessment |
# | Sensor | Target Gas | Detection Range [ppm] | Response and Resume Time [s] | Heater Consumption [mW] | Preheat Time [min/h/day] |
---|---|---|---|---|---|---|
1 | BME688 | IAQ, bVOC, eCO2 bVOC: (5 ppm Ethane, 10 ppm Isoprene/2-methyl-1,3 Butadiene, 10 ppm Ethanol, 50 ppm Acetone, 15 ppm Carbon monoxide) | 0–500 (IAQ), bVOC, CO2 P: 300–100 hPa, H: 0–100% T: −40–85 °C | 1/3/300 | 0.16–21.6 | 30 min |
2 | MQ-2 | Flammable gas, smoke | 300–10,000 ppm (Flammable gas) | 60 | 950 | 48 h |
3 | MQ-3 | Alcohol, Benzine | 0.05–10 mg/L Alcohol | - | 750 | 24 h |
4 | MQ-4 | Methane | 300–10,000 ppm (CH4) | 60 | 950 | 48 h |
5 | MQ-5 | Liquefied petroleum gas, Methane | 300–10,000 ppm (CH4, C3H8) | 60 | 950 | 48 h |
6 | MQ-6 | Liquefied petroleum gas | 300–10,000 ppm (Propane) | 60 | 950 | 48 h |
7 | MQ-7 | Carbon monoxide | 20–2000 ppm (CO) | 60 | 350 | 48 h |
8 | MQ-8 | Hydrogen gas | 100–1000 ppm (H2 gas) | 60 | 950 | 48 h |
9 | MQ-9 | Carbon monoxide and Combustible gas (Methane and Liquefied petroleum gas) | 10–1000 ppm (CO) 100–10,000 ppm (Combustible gas) | 60 | 350 | 48 h |
10 | MQ-131 | Ozone | 10–1000 ppm (O3) | 110 | 950 | 48 h |
11 | MQ-135 | Ammonia gas, Sulfide, Benzene series steam | 10–1000 ppm (Ammonia gas, Toluene, Hydrogen, smoke) | 60 | 950 | 48 h |
12 | MQ-136 | Hydrogen sulfide gas | 1–200 ppm (H2S gas) | 60 | 950 | 48 h |
13 | MQ-137 | Ammonia gas | 5–500 ppm (NH3 gas) | 60 | 900 | 48 h |
14 | MQ-138 | Toluene, acetone, alcohol, hydrogen | 5–500 ppm | 60 | 900 | 48 h |
15 | MQ-139 | Freon | 10–1000 ppm | 180–300 | 900 | 48 h |
16 | ZE03-NH3 | CO, O2, NH3, H2S, NO2, O3, SO2, CL2, HF | 0–1000 ppm (CO), 0–25% vol (O2), 0–100 ppm (NH3), 0–100 ppm (H2S), 0–20 ppm (NO2), 0–10 ppm (HF), 0–20 ppm (SO2), 0–10 ppm (CL2), 0–20 ppm (O3) | 15–150 | 20 | - |
17 | ZE03-C2H4 | CO, O2, NH3, H2S, NO2, O3, SO2, CL2, HF, H2, PH3, HCL, C2H4 | - | 15–150 | 20 | - |
18 | MICS-6814 | Carbon monoxide, Nitrogen dioxide, Ethanol, Hydrogen, Ammonia, Methane, Propane, Iso-butane | 1–1000 ppm (CO), 0.05–10 ppm (NO2), 10–500 ppm (C2H5OH), 1–1000 ppm (H2), 1–500 ppm (NH3), CH4 > 1000 ppm, C3H8 > 1000 ppm, C4H10 > 1000 ppm | - | 43–76 | - |
19 | TGS2201 | Diesel exhaust, Gasoline exhaust | 0.1–10 ppm (NO, NO2) 10–1000 ppm (CO, H2, HC) | - | 505 | 7 d |
20 | TGS2444 | Ammonia gas, Hydrogen sulfide gas, Ethanol | 10–300 ppm of NH3, 10–100 ppm of H2S, 300–1000 ppm of Ethanol | 60–180 | 56 | 48 h |
21 | TGS2600 | Hydrogen, Ethanol | 1–30 ppm of H2 | - | 210 | 7 d |
22 | TGS2602 | VOCs, Ammonia, Hydrogen sulfide gas | 1–30 ppm of EtOH | - | 280 | 7 d |
23 | TGS2603 | Trimethylamine, Methyl mercaptan | 1–30 ppm of EtOH | - | 240 | 96 h |
24 | TGS2610 | Butane, Liquefied petroleum gas | 1–25 % LEL | - | 280 | 7 d |
25 | TGS2611 | Methane, Natural gas | 500–10,000 ppm | - | 280 | 7 d |
26 | TGS2612 | Methane, Propane, Iso-butane | 1–25 % LEL of each gas | - | 280 | 7 d |
27 | TGS2620 | Alcohol, Organic solvent vapors | 50–5000 ppm EtOH | - | 210 | 7 d |
28 | TGS800 | General air contaminants | 1–30 ppm | - | 660 | - |
29 | TGS813 | Combustible gases | 500–10,000 ppm of Methane | - | 835 | - |
30 | TGS821 | Hydrogen | 30–1000 ppm of H2 | - | 660 | - |
31 | TGS822/823 | Alcohol, Organic solvents | 50–5000 ppm of Ethanol | - | 660 | - |
32 | TGS825 | Hydrogen sulfide gas | 5–100 ppm of (H2) | - | 660 | - |
33 | TGS826 | Ammonia gas | 30–300 ppm of NH3 | - | 835 | - |
34 | TGS832 | R-134a | 100–3000 ppm of R-134a | - | 835 | - |
35 | TGS842 | Methane natural gas | 500–10,000 ppm of CH4 | - | 835 | - |
36 | TGS880 | Fumes from food (alcohol, odor) | 10–1000 ppm (Air and Ethanol) | - | 835 | - |
37 | WSP1110 Obsolete | NO2 sensor | 0.1–10 ppm NO2 | - | - | - |
38 | WSP2110 | Toluene, Methanal, Benzene, Alcohol, Acetone | 1–50 ppm NO2 | 70 | 300 | 120 h |
39 | MP503 | Alcohol, Smoke, Iso-butane, Methanal | 10–1000 ppm (Alcohol) | 60 | 300 | 48 h |
40 | MG811 | Carbon dioxide | 350–10,000 ppm (CO2) | 20 | 1200 | - |
Commercial E-Nose | Paper | Data Analysis Techniques | Evaluation and Performance Metrics | Application Area |
---|---|---|---|---|
PEN3: A sensor array of ten different metal oxides single thick film sensors [177] | [183] | Recurrent Criss-Cross Attention Network [184] | Accuracy: 98% | Peanuts quality assessment |
[185] | Statistical analysis on data collected by PEN3 (weight loss measurements and firmness analysis also performed) | Prove that ilmenite-grafted graphene oxide coating reduces postharvest losses | Postharvest preservation of fruits (bananas) | |
[186] | PCA (e-nose and Headspace-Gas Chromatography-Ion Mobility Spectrometry) | Accuracy: 100% (genuine/fake) | Amomi fructus authenticity | |
Partial Least Squares-Discriminant Analysis (PLS-DA) [187] (e-nose and Headspace-Gas Chromatography-Ion Mobility Spectrometry) | Accuracy: 97.96% (origin identification) | Amomi fructus origin identification | ||
[188] | PCA + ANNs | Accuracy: 99% | Milk safety assessment | |
[189] | Solid-Phase Microextraction [190] coupled with GC–MS and e-nose analysis | Not discussed | Development of structured lipids with enhanced flavor profiles for dairy products and functional food | |
[191] | Dung Beetle Optimizer algorithm [192] combined with 10 different machine learning methods | Coefficient of determination > 0.895 | Prediction of the electronic sensory characteristics of fermented milk | |
[193] | Proposed data augmentation model (e-nose + e-tongue) + CNN | Accuracy: 95.34% (four types of mixed solution); Accuracy: 97.78% (five brands of beer); Accuracy: 97.37% (five kinds of apple) | Quality of different food | |
Fox 3000: Two sensor chambers equipped with twelve MOS sensors [178] | [178] | Random Forest | Accuracy: 95.30% | Mandarin orange quality assessment |
Fox 4000: An injection system, sensor chambers with eighteen MOS sensors, a mass flow controller, and a micro-controller acquisition board [179] | [194] | PCA | Discrimination index: 93 (seven batches of hydrolysate) | Quality of baked goods (effects of enzymatic hydrolysis on soy protein concentrate) |
[195] | PCA | PCA1: 94.54%, PCA2: 3.38% of the total variance (untreated sample/pasteurized sample/treated sample/sterilized sample in 0, 30 and 60 days of storage) | Shelf life of chicken products quality assessment | |
[196] | PCA | Discrimination index: 90 (eight types of plum jam samples) | Evaluation of the characteristics of sugar-free plum jams | |
[197] | PCA + CA + Partial Least Squares regression [198] (GC–MS and e-nose data) | Correlation coefficients > 0.98 (for 14 characteristic aroma-active compounds) | Mitten crab quality assessment | |
FOODsniffer [180] | [199] | E-nose data analysis compared with microbiological and GC–MS analyses | FOODsniffer can anticipate the unacceptability conditions of salmon (at 22 °C, 10% of samples are `Not satisfactory’ when FOODSniffer is `Green’) | Salmon fillet and burger quality and safety assessment |
[200] | E-nose data analysis (PCA) compared with physicochemical measurements of meat quality | PC1–71.13%, PC2: 83.70% of total variance | Meat quality assessment | |
NeOse Pro: A gold-layer-based optoelectronic sensor array featuring sixty-three non-specific peptides [181] | [201] | PCA + Gas Chromatography with Ion Mobility Spectrometry (GC–IMS) | Completely separate one sample | Plant-based beverage quality assessment |
PCA + e-nose | Completely separate seven samples | |||
LDA + GC–IMS | Accuracy between 15.4% and 100% | |||
LDA + e-nose | Accuracy between 96.2% and 100% | |||
Cyranose@ 320: An array of thirty-two nanocomposite sensors [182] | [202] | Proposed e-nose pattern recognition algorithm | Accuracy: 80% at room temperature | Identification of Terfezia arenaria truffle |
E-Nose | Paper | Data Analysis Techniques | Evaluation and Performance Metrics | Application Area |
---|---|---|---|---|
LibraNose: An array of eight QCM non-selective sensors coated with different polypyrrole derivatives—University of Rome Tor Vergata, Italy [203] | [209] | E-nose data analysis (PCA + Random Forest regression) | Accuracy: 92.8% (for predictions of B. thermosphacta) | Meat quality assessment |
High Performance Liquid Chromatography + Random Forest regression | Accuracy: 100% (for predictions of Lactobacilli) | |||
GC–MS + Random Forest regression | Accuracy: 93.9% (for predictions of Enterobacteriaceae) | |||
GC–MS + kNN-R | Accuracy: 96.0% (for predictions of Pseudomonads) | |||
[210] | PCA + Proposed data model based on Adaptive Fuzzy Logic System | Accuracy: 94.28% (fresh/semi-fresh/spoiled) | Monitoring of meat spoiling during storage | |
[211] | PCA + Proposed Multi-Input Multi-Output Clustering-based Fuzzy Wavelet Neural Network model | Accuracy: 95.71% (fresh/semi-fresh/spoiled); RMSE: 0.2969 to predict the microbial load on meat surface | Meat quality assessment | |
[212] | Proposed model based on ensemble-based (Bagging and Boosting) SVM | Accuracy: 84.1% (fresh/semi-fresh/spoiled) | Meat quality assessment | |
Proposed model based on ensemble-based (Bagging and Boosting) SVM-regression | Accuracy: 85% to predict bacterial species counts | |||
E-nose with an array of twelve QCM sensors—University of Rome Tor Vergata, Italy [204] | [204] | PLS-DA | 94% of the original data’s variation can be represented in a reduced-dimensional space; Accuracy: 100% (five different classes of sparkling wines) | Identification of rosé sparkling wines |
[213] | PLS-DA | 85% of the original data’s variation can be represented in a reduced-dimensional space; Accuracy between 60% and 100% for the first stages of Botrytis cinerea infection (1, 2, 3 days) | Identification of noble rot (a fungus also known as Botrytis cinerea) in postharvest wine grapes | |
E-nose with an array of eight QCM sensors—University of Rome Tor Vergata, Italy [205] | [205] | PCA + LDA | Accuracy: 71.4% (Aspergillus niger/ Aspergillus fumigatus/ Aspergillus flavus) | Identification of Aspergillus Species |
E-nose with four gas sensors (BME680 [214], SGP30 [215], CCS811 [216], iAQ-Core [217]) —Industrial Engineering School of the University of Extremadura, Spain [206] | [206] | E-nose data analysis (PCA + PLS-DA) compared with GC–MS | PC1–83.5%, PC2–12.3% of the total variance; Accuracy: 100% (six classes of roasted coffee beans exposed to different heat treatment conditions) | Roasted coffee quality assessment |
[218] | PCA + PLS-DA | Whole roasted almonds–R2: 0.89 for acrylamide and furfural, R2: 0.83 for hydroxymethylfurfural Ground roasted almonds–R2: 0.99 for acrylamide, R2: 0.98 for hydroxymethylfurfural, R2: 0.88 for furfural | Prediction of contaminants in roasted almonds | |
Agrinose: An array of eight MOS sensors (AS-MLV-P2 [219], TGS2602, TGS2600, TGS2603, TGS2610, TGS2611, TGS8100 [220], TGS2620) —Institute of Agrophysics IA PAS, Poland [207] | [221] | Proposed model based on a three-parameter method based on the impregnation time, cleaning time, and maximum response of chemically sensing sensors + PCA compared with GC–MS | PC1 + PC2 describe 72.64% of the total variance and enable clear separation of different sample classes | Assessment of the suitability of bread for consumption after storage |
[222] | Proposed model based on a three-parameter method based on the impregnation time, cleaning time, and maximum response of chemically sensing sensors + PCA compared with Fourier Transform Infrared Spectroscopy [223] and GC–MS | PC1 + PC2 describe 79.25% of the total variance and enable clear separation of different sample classes | Identification of rapeseed spoilage | |
E-nose with nine MOS sensors (MQ-2, MQ-3, MQ-4, MQ-5, MQ-6, MQ-7, MQ-8, MQ-9, MQ-135)—Department of Biosystems Engineering, Bu-Ali Sina University, Iran [208] | [224] | PCA | Included 55%, 75%, 47%, and 53% of data for unprocessed whole/dried slices/powder/tablet | Garlic quality assessment |
LDA | Accuracy: 90%, 93.33%, 88.89%, 60% (unprocessed whole/dried slices/powder/tablet) | |||
SVM | Accuracy: 72.22%, 80.00%, 75.55%, 40% (unprocessed whole/dried slices/powder/tablet) | |||
Backpropagation Neural Network [225] | Accuracy: 100%, 97.80%, 92.2%, 77.78% (unprocessed whole/dried slices/powder/tablet) |
# | Sensor | Target Gas | Detection Range [ppm] | Response and Resume Time [s] | Heater Consumption [mW] | Preheat Time [min/h/Day] |
---|---|---|---|---|---|---|
1 | BME688 | IAQ, bVOC, eCO2 bVOC: (5 ppm Ethane, 10 ppm Isoprene/2-methyl-1,3 Butadiene, 10 ppm Ethanol, 50 ppm Acetone, 15 ppm Carbon monoxide) | 0–500 (IAQ), bVOC, CO2 P: 300–1100 hPa, H: 0–100% T: −40–85°C | 1/3/300 | 0.16–21.6 | 30 min |
2 | SGP30 End of life | VOC, eCO2, Ethanol, Hydrogen sulfide gas | 0–60,000 ppb (VOC), 400–60,000 ppm (eCO2) 0– 1000 ppm (Ethanol, H2S) | 1 | 86.4 | 24 h |
3 | CCS811 | TVOC, eCO2 | 0–1187 ppb (TVOC), 400–8192 ppm (eCO2) | 0.25/1/10/60 | 1.2–46 | 48 h |
4 | iAQ-Core Obsolete | eCO2, TVOC | 450–2000 ppm (eCO2), 125–600 ppb (TVOC ) | 1/11 | 9–69 | - |
5 | AS-MLV-P2 Obsolete | CO, Butane, Methane, Ethanol, Hydrogen | 30–500 ppm (CO), 15–150 ppm (Butane), 250–4500 ppm (CH4), 10–200 ppm (Ethanol), 25–500 ppm (H) | 1/10 | 50 | 5 d |
6 | TGS8100 | Methane, Iso-butane, CO, Hydrogen, Ethanol | 1–100 ppm, 1–30 ppm (H2) | - | 15 | >1 h |
Reference and Sensor Type/Technology | Target Compounds/ Application | Data Analysis Techniques | Key Features/Results |
---|---|---|---|
[226]: Silicon NanoWires + multi-walled carbon nanotube | Essential oils, alcoholic beverages, general food | PCA | Fast response time (20–30 s), high selectivity, dual surface, and chemical modification |
[227]: Graphene junctions | Aflatoxin B1 | N/A | 1.2 V bias yields >3 µA current change; suitable for rapid e-nose integration |
[228]: Plasmonic arrays + chemometrics + machine learning | Multiple VOCs in food | PCA + LDA | Uses Surface-Enhanced Raman Spectroscopy, mimics animal olfaction; machine learning enables multi-analyte detection |
[229]: Memristor-based in-memory computing + MOS sensor array | Various gases (15 sensors) | CNN | 94% classification accuracy; 20.2 mW power; fast response time (<0.4 ms inference time); compact processing scheme |
[230]: Graphene + Metal Phthalocyanines | Ammonia gas, interfering gases | PCA | 5-sensor array (Co-Pc, Ni-Pc, Zn-Pc, Fe-Pc, pristine); promising for food quality monitoring |
[231]: Film Bulk Acoustic Resonator sensors | General gases; example: banana freshness | Real-time signal processing and pre-processing + Discriminative analysis | Miniaturized portable e-nose; 6–8× more sensitive than polymer-coated Film Bulk Acoustic Resonator; drift-compensated |
[232]: Colorimetric Fe(II) complex | Ammonia gas | PCA + Hierarchical cluster analysis, SVM | Detects 105 ppb at room temp; reusable; no external energy needed |
[233]: CNT + olfactory receptor (ODR-10) | Diacetyl in alcoholic beverages | Sensitivity and selectivity analysis | Detection limit of 10 fM; better than fluorescence assays and GC–IMS in classification |
Dataset | Description | Paper | Data Analysis Techniques | Evaluation and Performance Metrics |
---|---|---|---|---|
[234,235] | 2220 sensor signal responses collected from twelve cuts of beef samples in four different degrees of freshness using eleven gas sensors | [236] | Proposed model based on 1D-CNN | Accuracy: 97.22% (excellent/good/ acceptable/spoiled) |
[237] | ANNs | Accuracy: 99.9% (excellent/good/ acceptable/spoiled) | ||
Linear Regression | Accuracy: 98.9% (excellent/good/ acceptable/spoiled)) | |||
KNN | Accuracy: 98.8% (excellent/good/ acceptable/spoiled) | |||
[238] | Proposed MLP model on Field Programmable Gate Array | Accuracy: 92.72% (excellent/good/ acceptable/spoiled) | ||
[239] | Proposed approach based on Single Plurality Voting System model + Decision Tree | Accuracy: 91.13% (excellent/good/ acceptable/spoiled) | ||
Proposed approach based on Single Plurality Voting System model + KNN | Accuracy: 88.69% (excellent/good/ acceptable/spoiled) | |||
Proposed approach based on Single Plurality Voting System model + LDA | Accuracy: 80.73% (excellent/good/ acceptable/spoiled) | |||
[240] | 420 samples for seven different mixtures of beef and pork collected from eight gas sensors | [241] | Proposed model based on a conventional Deep Extreme Learning Machine with an autoencoder for feature learning | Accuracy: 99.85% (seven combination mixtures of meat) |
Proposed model based on SVM with a Radial Basis Function kernel | Accuracy: 93.48% (seven combination mixtures of meat) | |||
Proposed model based on a conventional Deep Extreme Learning Machine with PCA for feature learning | Accuracy: 99.97% (seven combination mixtures of meat) | |||
Proposed model based on PCA + SVM with a Radial Basis Function kernel | Accuracy: 96.88% (seven combination mixtures of meat) | |||
[242,243] | Time series data for 235 wine samples collected from six gas sensors | [244] | Proposed model based on CNN | Accuracy: 99.2% (low quality/average quality/high quality) |
[245] | 48,846 rows for rice quality acquired from nine gas sensors and four other sensors for related data | [245] | Proposed model based on KNN | R2: 0.7217; RMSE: 3.8043 |
[246] | Gradient Tree Boosting | Accuracy: 96% (expired/non-expired) | ||
[247] | Complement Naïve Bayes classifier | Accuracy: 98% (expired/non-expired) | ||
Multinomial Naïve Bayes classifier | Accuracy: 97% (expired/non-expired) | |||
Gaussian Naïve Bayes classifier | Accuracy: 82% (expired/non-expired) | |||
Bernoulli Naïve Bayes classifier | Accuracy: 52% (expired/non-expired) | |||
[248] | MLP | Accuracy: 99.84% (expired/non-expired) |
Identified Gap | Recommended Solution in This Review |
---|---|
Low real-world deployment despite high lab accuracy | Provide case studies and benchmarking tables to bridge lab-to-field gaps |
Sensor selectivity and sensitivity challenges | Develop gas-sensitive materials with enhanced selectivity and sensitivity for food VOCs, or design bio-inspired or biomimetic sensors that mimic natural senses to improve detection accuracy in food analysis |
Sensor response time challenges | Design gas sensors with fast response times |
Sensor drift and calibration challenges | Introduce adaptive/recalibrating machine learning models and emphasize real-time feedback control |
Black-box nature of machine learning models used in classification | Recommend interpretable machine learning models and alignment with food safety regulations (i.e., Codex/ISO) |
Lack of efficient multi-sensor (e-nose, e-tongue, e-eye) data fusion algorithms results in incomplete food profiling | Develop advanced data fusion frameworks using machine learning, hybrid fusion techniques, and synchronized pre-processing |
Miniaturization and portability challenges | Recommend integration of micro-electro-mechanical systems/ nano-electro-mechanical systems technologies for compact, low-power devices |
Lack of standardization in methodology and validation | Recommend universal protocols for data collection, validation, and sensor benchmarking |
Lack support in user-friendly visualization of the odor classification and identification results | Introduce real-time data analysis platforms for on-site decision making |
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Sanislav, T.; Mois, G.D.; Zeadally, S.; Folea, S.; Radoni, T.C.; Al-Suhaimi, E.A. A Comprehensive Review on Sensor-Based Electronic Nose for Food Quality and Safety. Sensors 2025, 25, 4437. https://doi.org/10.3390/s25144437
Sanislav T, Mois GD, Zeadally S, Folea S, Radoni TC, Al-Suhaimi EA. A Comprehensive Review on Sensor-Based Electronic Nose for Food Quality and Safety. Sensors. 2025; 25(14):4437. https://doi.org/10.3390/s25144437
Chicago/Turabian StyleSanislav, Teodora, George D. Mois, Sherali Zeadally, Silviu Folea, Tudor C. Radoni, and Ebtesam A. Al-Suhaimi. 2025. "A Comprehensive Review on Sensor-Based Electronic Nose for Food Quality and Safety" Sensors 25, no. 14: 4437. https://doi.org/10.3390/s25144437
APA StyleSanislav, T., Mois, G. D., Zeadally, S., Folea, S., Radoni, T. C., & Al-Suhaimi, E. A. (2025). A Comprehensive Review on Sensor-Based Electronic Nose for Food Quality and Safety. Sensors, 25(14), 4437. https://doi.org/10.3390/s25144437