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Synthesis and Structure Elucidation of N′-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide

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National Center for Petrochemicals Technology, King Abdulaziz City for Science and Technology, P.O. Box 6086, Riyadh 11442, Saudi Arabia
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Department of Chemistry, College of Science and Humanities, Shaqra University, P.O. Box 33, Duwadimi 11911, Saudi Arabia
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Applied Organic Chemistry Department, National Research Centre, Dokki, Giza 12622, Egypt
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School of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10 3AT, UK
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Department of Optometry, College of Applied Medical Sciences, King Saud University, P.O. Box 10219, Riyadh 11433, Saudi Arabia
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Authors to whom correspondence should be addressed.
Molbank 2018, 2018(4), M1034; https://doi.org/10.3390/M1034
Received: 1 November 2018 / Revised: 21 November 2018 / Accepted: 30 November 2018 / Published: 2 December 2018
(This article belongs to the Section Structure Determination)
N′-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide (3) was synthesized in a yield of 88% from an acid-catalyzed reaction of 5-methyl-1-phenyl-1H-1,2,3- triazole-4-carbohydrazide and 4-methoxybenzaldehyde in ethanol under reflux for 2.5 h. The structure of 3 was confirmed by the data obtained from infrared, nuclear magnetic resonance, mass spectroscopy, single crystal X-ray diffraction, and microanalysis. View Full-Text
Keywords: 1,2,3-triazoles; carbohydrazides; single crystal X-ray diffraction; spectroscopic structural analysis; heterocycles 1,2,3-triazoles; carbohydrazides; single crystal X-ray diffraction; spectroscopic structural analysis; heterocycles
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MDPI and ACS Style

Alotaibi, M.H.; Mohamed, H.A.; Abdel-Wahab, B.F.; Hegazy, A.S.; Kariuki, B.M.; El-Hiti, G.A. Synthesis and Structure Elucidation of N′-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide. Molbank 2018, 2018, M1034.

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