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Molbank 2018, 2018(4), M1034; https://doi.org/10.3390/M1034

Synthesis and Structure Elucidation of N′-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide

1
National Center for Petrochemicals Technology, King Abdulaziz City for Science and Technology, P.O. Box 6086, Riyadh 11442, Saudi Arabia
2
Department of Chemistry, College of Science and Humanities, Shaqra University, P.O. Box 33, Duwadimi 11911, Saudi Arabia
3
Applied Organic Chemistry Department, National Research Centre, Dokki, Giza 12622, Egypt
4
School of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10 3AT, UK
5
Department of Optometry, College of Applied Medical Sciences, King Saud University, P.O. Box 10219, Riyadh 11433, Saudi Arabia
*
Authors to whom correspondence should be addressed.
Received: 1 November 2018 / Revised: 21 November 2018 / Accepted: 30 November 2018 / Published: 2 December 2018
(This article belongs to the Section Structure Determination)
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Abstract

N′-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide (3) was synthesized in a yield of 88% from an acid-catalyzed reaction of 5-methyl-1-phenyl-1H-1,2,3- triazole-4-carbohydrazide and 4-methoxybenzaldehyde in ethanol under reflux for 2.5 h. The structure of 3 was confirmed by the data obtained from infrared, nuclear magnetic resonance, mass spectroscopy, single crystal X-ray diffraction, and microanalysis. View Full-Text
Keywords: 1,2,3-triazoles; carbohydrazides; single crystal X-ray diffraction; spectroscopic structural analysis; heterocycles 1,2,3-triazoles; carbohydrazides; single crystal X-ray diffraction; spectroscopic structural analysis; heterocycles
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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited (CC BY 4.0).

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Alotaibi, M.H.; Mohamed, H.A.; Abdel-Wahab, B.F.; Hegazy, A.S.; Kariuki, B.M.; El-Hiti, G.A. Synthesis and Structure Elucidation of N′-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide. Molbank 2018, 2018, M1034.

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