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Molbank 2008, 2008(1), M561;

Microwave Synthesis of (4-hydroxy Phenyl) 3-oxo butanoate

Applied Chemistry and Environement Laboratory, Faculty of Sciences, Univerity Mohamed 1st, Oujda, Marocco
Author to whom correspondence should be addressed.
Received: 2 May 2007 / Revised: 20 November 2007 / Accepted: 15 January 2008 / Published: 25 March 2008
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The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of the total reactants) [2,3] was placed in a pyrex tube which was then introduced into a Maxidigest MX 350 Prolabo microwave monomode reactor fitted with a rotational system [4]. View Full-Text
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Ramdani, M.; Benchat, N.-E.; Anaflous, A.; El Kalai, F. Microwave Synthesis of (4-hydroxy Phenyl) 3-oxo butanoate. Molbank 2008, 2008, M561.

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