Search Results (160)

Durum wheat (Triticum durum) is one of the main raw materials in the food industry, used primarily in the production of pasta. During milling, semolina and flour are obtained with different size distributions, and different compositional and functional characteristics, which influence processes such as gelatinization, retrogradation and the final texture of the products. Understanding these changes is essential for optimizing the technological quality and shelf life of processed foods. The aim was to evaluate how particle size, composition, temperature, and treatment time affect gelatinization, retrogradation, and gel texture. Samples included common wheat flour (control), durum wheat semolina, durum wheat flour, and re-milled semolina (<180 μm). Hydrothermal tests were conducted at 95 °C with varying holding times, and at 140 °C with extended cooling to observe retrogradation. Composition and particle size were found to determine rheological behavior. Semolina showed higher retrogradation and produced firmer gels, while durum wheat flour, with higher protein and ash content, showed atypical profiles and less consistent gels. Increased temperature and time enhanced breakdown and reduced final viscosity, indicating starch thermal degradation. A correlation was observed between final viscosity and gel hardness. This study provides information useful for optimizing the milling, cooking, and development of durum wheat-based products with improved texture and shelf life. Full article

The valorization of agricultural by-products such as beetroot stalks (BSs) offers a sustainable strategy for reducing food waste while enhancing nutritional value of staple foods. This study investigates the incorporation of BS powder, an agricultural waste rich in phenolics, betalains, and dietary fibers, into durum wheat semolina pasta. Pasta containing 5–20% BS were evaluated for bioactive compounds, cooking performance parameters, texture, color, and sensory acceptance. Enrichment increased total phenolics, antioxidant activity, and betalain concentration in a dose-dependent manner, with 20% BS pasta reaching 2.24 mg gallic acid equivalents/g phenolics and 1.53 mg/g betalains. Although drying and boiling reduced bioactive retention, enriched pasta maintained up to eightfold higher antioxidant activity than the control. Cooking performance showed increased water uptake and swelling index at higher substitution levels, while texture analysis revealed reduced hardness and cohesiveness above 15% BS substitution. Color analysis confirmed intense red hues from betalain pigments, enhancing consumer perception. Sensory evaluation indicated that control pasta was preferred for flavor and texture, but 10–15% BS samples were well accepted for their appealing color and mild vegetal notes. Overall, BS powder demonstrates strong potential for upcycling agricultural waste into functional, sustainable pasta with enhanced nutritional quality and alignment with circular economy practices. Full article

Aqueous semolina suspensions were reacted with spherical gold nanoparticles (AuNPs, nominal diameter, 20 nm) to assess the accessibility of cysteine thiols in durum wheat proteins, focusing on network-forming gluten proteins. Unlike small thiol reagents, covalent bond formation between gold ions on the AuNPs surface and protein thiols was greatly facilitated by the addition of 1% sodium dodecyl sulfate (SDS). SDS weakens non-covalent hydrophobic interactions within and among proteins, increasing the exposure of buried thiols without altering disulfide bonds. MS/MS analysis of proteolytic fragments from the isolated AuNP-protein covalent complexes allowed identification of the bound proteins. Proteomics data suggests that AuNPs also associate with gluten proteins lacking free thiols in their native structure, which are bound to AuNPs by forming disulfide bonds with other gluten proteins containing accessible thiols, via thiol-disulfide exchange reactions. This implies that thiol-disulfide reshuffling among gluten proteins occurs already in the grain, enabling proteins without free thiols to become part of AuNP-bound assemblies and revealing specific protein species involved in these early interactions. These observations highlight the role of thiol–disulfide exchange within the grain matrix, elucidating how such molecular rearrangements influence the topology and strength of protein networks in food and in related biopolymeric systems. Results of this exploratory study are discussed for their molecular relevance and for the potential use of size-based analytical and structural approaches in other biological contexts. Full article

Ancient wheats can be understood as dynamic populations of historically cultivated wheat, which, unlike modern varieties, have not been developed through organised genetic improvement programmes, but rather through traditional farmer selection and local adaptation over centuries. Recently, ancient wheats have enjoyed renewed popularity, particularly in Italy, due to their wide genetic diversity and the significant role of wheat and its derivatives (e.g., bread, pasta, and baked goods) in the country’s culinary and cultural heritage. However, information on the characteristics of Italian ancient wheats remains limited and fragmented. Therefore, this review aims to collect, organise and compare the available evidence on the historical, agronomic, economic and sustainability parameters of ancient wheats, in order to provide an overall assessment of these varieties. The results showed that 34 Italian ancient wheats were studied, mainly from Tuscany and Sicily. With plant heights of up to 180 cm and yields of 1.4–4.8 t/ha, ancient wheats are characterised by greater height but lower productivity compared to modern wheats. They demonstrate good adaptability to poor soils and climatic stress, natural competitiveness with weeds and potential resistance to pathogens, rendering them suitable for sustainable, low-input agricultural systems. Furthermore, ancient wheat flours cost more than twice as much as commercial flours, with average prices of €3.00–5.10/kg, mainly due to artisanal production methods and belonging to short or niche supply chains. Finally, considerable variability in test weight (TW) and thousand kernel weight (TKW) could negatively affect flour or semolina yields. In conclusion, despite their low productivity, ancient wheats could offer significant opportunities in terms of environmental sustainability and biodiversity conservation, proving to be a strategic resource for more resilient and sustainable agriculture. Full article

Durum wheat (Triticum durum Desf.) underpins semolina value chains in water-limited regions, yet Peru remains import-dependent due to constrained local adaptation. We evaluated eleven elite lines plus the commercial variety ‘INIA 412 Atahualpa’ across three contrasting semi-arid sites in Arequipa (Santa Elena, San Francisco de Paula, Santa Rita) during 2023–2024 to identify genotypes maximizing performance and stability. Grain yield, thousand-kernel weight (TKW), hectoliter weight, and plant height were analyzed with combined analysis of variance (ANOVA), the additive main effects and multiplicative interaction (AMMI) and genotype and genotype-by-environment (GGE) biplots, complemented by AMMI stability value (ASV) and weighted average of absolute scores and best yield index (WAASBY). Grain yield and hectoliter weight showed significant genotype × environment (G × E) interaction, while plant height was driven mainly by genotype and environment with limited interaction. For grain yield, AMMI (PC1: 55.2%) and GGE (PC1 + PC2: 90.2%) revealed crossover responses and three practical mega-environments: TD-053 “won” at San Francisco de Paula, TD-037 at Santa Elena, and TD-033 at Santa Rita. Additionally, WAASBY-integrated rankings favored TD-033 (93.7%) and TD-014 (84.72%), followed by TD-026/TD-020 (>57%), whereas TD-062 (9.1%) and TD-043/TD-061 underperformed. Quality traits highlighted TD-044 and TD-014 for high hectoliter weight and TD-014/TD-062 for high TKW with contrasting stability. Overall, TD-033 and TD-014 were adaptable across environments, providing selection guidance to strengthen Peru’s durum breeding pipeline under climate variability. Full article

The global trend toward sustainable and health-promoting foods has encouraged the reformulation of meat products that strategically incorporate high-quality animal proteins and functional compounds derived from plants. This study focuses on a complex food concept: meat-based pasta formulated from pork, semolina, and dietary fibers (apple and sugar beet). The quality attributes and the effects of different formulations were evaluated in comparison with a control sample. The findings show that the addition of dietary fibers significantly impacted the chemical composition, lowered the pH and increased water activity. The incorporation of the apple and sugar beet fibers increased the total dietary fiber content from 2.94% (control) to 9.59% and 11.15%, respectively, at the highest level of inclusion. Moreover, texture profile analysis of the raw samples revealed an enhancement in hardness (from 8.01 N in the control to maximum values of 21.23 N and 26.37 N), gumminess (from 3.28 N to 10.43 N and 12.36 N), and slight improvements in cohesiveness (from 0.41 to maximum values of 0.49 and 0.51) with the addition of apple and sugar beet fibers, respectively. The color parameters (L*, a*, b*) varied depending on the fiber source, with beet fiber imparting higher lightness and redness, while apple fiber contributed to darker tones. An initial consumer acceptability test revealed a positive perception of the innovative product, particularly for formulations with low and medium percentages of fiber addition. Overall, the results demonstrate that meat-based pasta can be successfully formulated with dietary fibers, providing an innovative and feasible alternative that meets current consumer expectations for novel, healthy, and sustainable foods. Full article

Thirteen genotypes of durum wheat were grown in two different environments in Portugal. Grain and ash mineral profile, as well as protein content, test weight, and grain ash content were evaluated. Genotype, environment, and their interaction explains the variation in the quality traits, with the environment having the highest influence. Mineral profile analysis was performed by the μ-EDXRF system: macroelements (K, P, Ca, Cl, and S) represented 99% of the total concentration detected in the grain samples, while microelements represented up to 2% of the total concentration when analyzing the ash samples (Fe, Mn, Zn, Cu, Si, Rb, Sr, and Ti). Almost every element found in the grain and ash analysis was affected by the environment. Only K and Ca in the grain had higher concentrations in the environment with water scarcity, while the concentrations of all the detected elements except for Si and Sr were higher in the ashes in this environment. Regarding the genotype, P, S, and Cu grain concentrations were not affected by the environment. The highest grain mineral concentration was found for Gingão, suggesting a better mineral uptake and/or translocation-to-grain capacity. However, regarding the technological quality, most of the genotypes presented ash content values above the maximum specified threshold. Full article

In recent years, pulse flours have gained attention in baked goods for their nutritional value. This study evaluated the effects of incorporating common bean, yellow pea, and grass pea flours (20%, 30%, 40%) into durum wheat semolina on the technological, physical, and rheological properties of flours, doughs, and breads. Combining pulse flours with durum wheat semolina allows for improved dough handling and processing performance, leveraging the functional properties of both ingredients. Water absorption increased with pulse flour addition (average 1.90 g H₂O/g dry matter), though higher levels of yellow pea and grass pea reduced it. Color changes were most evident with common bean flour. Leavening rates varied, reaching 144% after 60 min with 30% yellow pea and 68.75% after 40 min with 30% common bean. Rheological results indicated longer dough development and stability times but reduced strength and extensibility, with higher tenacity. Bread volume decreased from 276.25 cm³ (control) to 208.75 cm³ (40% common bean). Crumb porosity declined, particularly with common bean flour, producing smaller pores. Grass pea flour promoted browning, enhancing color contrast. Texture analysis showed harder, more gum-like breads with higher chew resistance: hardness ranged from 15.85 N (20% common bean) to 30.45 N (40% yellow pea). Gumminess and chewiness increased, while cohesiveness decreased. Overall, pulse flour integration alters bread quality, yet represents a promising approach to creating healthier, functional, baked products. Full article

This study investigates the properties of biopolymer films derived from semolina and farina, focusing on the effect of varying concentrations of glycerol as a plasticizer. The research fills a gap in the study of grains such as semolina and farina, which have the potential to expand the range of biodegradable materials. Mechanical tests revealed significant differences between the two film types. Farina-based films were notably more ductile, exhibiting an elongation at break of up to two times their original length, but with a low tensile strength of only 1–2 MPa. In contrast, semolina-based films were significantly stiffer, with a maximum elongation at break of 10%. A notable exception was the semolina film with a 25% glycerol concentration, which displayed an exceptionally high tensile strength of 17 MPa. This is a significant improvement over the typical potato starch-based film tested, which breaks at 5 MPa under static tearing. Furthermore, the study examined the films’ morphology, color, SFE, and surface roughness. Free surface energy ranged from 40 to 60 mJ/m² in the tests, where the influence of the plasticizer was significant. Color tests clearly show yellow discoloration. Full article

The study aimed to produce semolina pasta enriched with walnut or hazelnut oil cake and to investigate its nutritional and technological properties. The pasta was prepared by substituting 10% of semolina with walnut or hazelnut oil cakes. The chemical composition, antioxidant properties, and culinary characteristics of the pasta were determined. Additionally, the texture and color of uncooked and cooked pasta were examined using instrumental techniques. The enriched pastas showed higher protein, fat, ash, and dietary fiber contents compared to standard pasta (SP). Walnut oil cake pasta (WOCP) had the highest protein content, amounting to 15.8 g/100 g dry weight (d.w.), while hazelnut oil cake pasta (HOCP) had the highest dietary fiber content (6.75 g/100 g d.w.). Moreover, the enriched pastas showed significantly higher antioxidant potential and total phenolic content, both before and after cooking. The total phenolic content (TPC) of cooked pasta ranged from 88.85 mg GAE/100 g d.w. (SP) to 145.48 mg GAE/100 g d.w. (WOCP). Compared to SP, the developed pastas required cooking times of 2–3 min longer and showed higher water absorption, accompanied by increased cooking losses. They were characterized by a specific, dark color and showed reduced hardness and lower elasticity after cooking compared to SP. Pasting properties further suggested that starch swelling was restricted by the nut oil cakes. Overall, incorporating walnut and hazelnut oil cakes enhanced the nutritional profile and imparted notable health-promoting attributes to the pasta, underscoring the potential of these by-products as functional ingredients in pasta formulations. Full article

This study aimed to valorize underutilized local ingredients by developing nutritionally enhanced pasta products enriched with sorghum and cork oak flours. The resulting pasta samples were characterized by their chemical composition, color attributes, functional properties, texture, microstructure, and antioxidant capacity. Semolina-based pasta showed higher protein content, while cork oak flour contributed significantly to lipid content, and sorghum flour was notably rich in fiber and minerals. Colorimetric analysis quantified visible differences in appearance, depending on the type of flour used. Functional assessment showed comparable water absorption indices across all samples; however, sorghum-enriched pasta exhibited significantly higher water solubility. Textural analysis indicated that sorghum reduced pasta adhesiveness and cohesiveness, whereas cork oak flour increased hardness, gumminess, and adhesiveness—likely due to its high fiber content, contributing to a stickier mouthfeel. Microstructural observations confirmed a denser and more compact matrix in pasta formulated with cork oak flour. Antioxidant analysis revealed that cork oak flour imparted the highest antioxidant potential, followed by sorghum and semolina. HPLC/ESI-TOF-MS profiling demonstrated a rich and diverse polyphenolic composition in the enriched samples. These formulations not only enhance the functional and nutritional profile of traditional pasta but also align with the increasing consumer demand for low-carbohydrate, fiber-rich foods. Full article

Surplus bread accounts for a significant proportion of food waste in many countries. The focus of this study was twofold: firstly, to investigate the use of carasau bread residue as a sourdough substrate, and secondly, to reuse this sourdough into a new carasau baking process. Selected lactic acid bacteria (Lactiplantibacillus plantarum) and yeast strains (Saccharomyces cerevisiae and Wickerhamomyces anomalus) were used to inoculate three substrates: bread residue (S1), bread residue supplemented with durum wheat middlings (S2), and semolina (S3). Sourdoughs were refreshed for five days by backslopping, and microbiological and physicochemical analyses were performed. Results indicated that incorporating wheat middlings into bread residue enhanced microbial performance, as evidence by a decrease in pH from 6.0 to around 4.5 compared to using bread residue alone as a substrate. Carasau bread produced with the sourdough derived from bread residue and wheat middlings exhibited comparable physicochemical properties to commercial baker’s yeast carasau bread, but had better sensory properties, scoring a mean acceptability of 7.0 versus 6.0 for baker’s yeast bread. These results show that bread residue supplemented with wheat middlings can serve as a sourdough substrate, allowing its reuse in the baking process to produce high-quality carasau bread and promote the circular economy. Full article

The aim of this study was to develop and characterize antioxidant-active films for potential food packaging applications. The films were produced by casting aqueous solutions containing semolina flour (6% w/w), pectin extracted from passion fruit (1% w/w), inverted sugar (1% w/w), and sucrose (1% w/w), incorporating hydroalcoholic extracts from jatoba stem bark (X₁) and pods (X₂) at concentrations ranging from 0 to 1% (w/w). The films were characterized in terms of their functional, physical, chemical, structural, and degradation properties. The formulation that showed the best performance, referred to as the optimized formulation (FO), contained 0.5% X₁ and 0.5% X₂, presenting a high phenolic compound content (8.80 mg GAE/g), strong antioxidant activity as determined by the DPPH method (75.28%) and FRAP assay (6.02 mmol FeSO₄/g), good thermal stability (350 °C), and a high soil degradation rate (83.47% in 15 days). These results indicate that the FO film has potential application as a primary packaging material with antioxidant function for oxidation-sensitive foods, meeting the demand for biodegradable and environmentally sustainable solutions in the food industry. Full article

This study explores the application of three fermented plant materials—wheat, acorns, and sorghum—in couscous preparation, as well as their impact on its properties. A survey was conducted in some localities in Algeria. The aim is to reproduce the diagrams for the manufacture of different types of couscous incorporated with fermented materials and to evaluate the pasting properties, culinary qualities, and microstructure of each type of couscous produced. The survey identified four couscous formulations made with durum wheat semolina: couscous 1 (4% sorghum, 4% wheat, 8% acorns), couscous 2 (8% acorns), couscous 3 (0.8% sorghum, 6% acorns), and couscous 4 (4% wheat, 4% acorns). A comparative study of the four types of couscous showed significant differences in their physicochemical and microstructural properties. Formulations C3 and C4 showed the best functional performance among all the couscous samples studied. In terms of the swelling index, measured at 25 °C and 95 °C, C3 reached 131.11% and 165.55%, respectively, while C4 recorded 124.9% and 157.0%. Furthermore, these two formulations had the highest viscosity values: initial viscosity of 25 mPas (C3) and 27 mPas (C4), maximum viscosity of 31 mPas (C3) and 30 mPas (C4), and final viscosity of 49 mPas (C3) and 46 mPas (C4). Analysis of the cooking loss revealed higher values for couscous 1 and 2. The microstructure of couscous 2 revealed the presence of native starch particles, open porosity, and a state of partial gelatinization. The study revealed that formulations C3 and C4 significantly (p < 0.05) impact couscous structure by enhancing functionality while preserving quality. It also maintained ancestral knowledge and offered valuable insights for future industrial applications. Full article

This study evaluated the potential of three ancient Sicilian tetraploid wheat genotypes—‘Margherito’, ‘Perciasacchi’, and ‘Russello’—for organic pasta production, compared to the national variety ‘Cappelli’. Significant variations in particle size distribution were found, with ‘Russello’ exhibiting the highest proportion of fine particles and the greatest protein content (14.30% d.m.). ‘Perciasacchi’ displayed the highest gluten index (81.26%). ‘Margherito’ and ‘Cappelli’ had the highest antioxidant activity, with ‘Margherito’ showing elevated levels of lutein and total carotenoids. Rheological analysis revealed differences in dough properties. ‘Perciasacchi’ exhibited the highest dough stability and P/L ratio (6.57), whereas ‘Russello’ showed the lowest values for both. Additionally, ‘Russello’ had lower consistency (12 B.U.), reduced gel stability, and limited water retention in the visco-amylographic analysis. Pasta quality was evaluated based on cooking time, water absorption, and texture. Cooking time ranged from 10 to 12 min, with ‘Russello’ and ‘Margherito’ showing lower water absorption. Texture analysis indicated that ‘Margherito’ pasta was the least firm, while ‘Russello’ showed the greatest loss of consistency when overcooked. From a sensory perspective, ‘Russello’ had lower firmness, but a stronger semolina flavor and surface roughness. ‘Cappelli’ had the most intense cooked pasta odor, while ‘Perciasacchi’ was the hardest and least sticky, though less flavorful. The results support the use of ancient tetraploid wheat genotypes as valuable resources for sustainable, high-quality pasta production. Full article