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22 pages, 1438 KB  
Article
Analysis of 3D-Printed Cycloidal Gear Degradation in a Run-to-Failure Test
by Krzysztof Olejarczyk, Marcin Wikło and Miroslaw Rucki
Appl. Sci. 2026, 16(6), 2866; https://doi.org/10.3390/app16062866 - 16 Mar 2026
Abstract
The paper presents results of a degradation analysis of polyamide 12 reinforced with carbon fibers used for additive manufacturing of cycloidal gear. Both FEM simulation and a fatigue test indicated the ability of the material to withstand loads during the work of cycloidal [...] Read more.
The paper presents results of a degradation analysis of polyamide 12 reinforced with carbon fibers used for additive manufacturing of cycloidal gear. Both FEM simulation and a fatigue test indicated the ability of the material to withstand loads during the work of cycloidal transmission. However, a run-to-failure (RTF) test revealed critical failure after 105 cycles, with displacement and damage of the material in the area close to bearing instead of expected areas of teeth being in friction with pins. Acceleration analysis with time synchronous averaging (TSA) confirmed rapid degradation of the material’s strength at the end of the RTF test. It was found that the PA12 cycloidal gear damage was a result of fatigue accelerated by the temperature increase under the cyclic loads that took place during the RTF test. In particular, displacement of 0.2 mm did not appear in the specimens tested at 27 °C even after 105 cycles, while at 140 °C this value was reached almost immediately. At 70 °C and 90 °C, plastic deformation of 0.2 mm was reached after 30,000 and 5000 cycles, respectively. The finding can be used in a predictive maintenance system of such cycloidal transmission with 3D-printed polymer gears. Full article
15 pages, 4853 KB  
Article
Microstructural Evolution Governing the Creep Resistance of Grade 92 Steel Under Wide-Temperature Heat Treatment: From Ferrite Recovery to Dynamic Precipitation Strengthening
by Yinsheng He, Hongyu Zhou, Liming Xu and Keesam Shin
Materials 2026, 19(6), 1101; https://doi.org/10.3390/ma19061101 - 12 Mar 2026
Viewed by 81
Abstract
Thermal excursions during post-weld heat treatment (PWHT) and on-site fabrication frequently compromise the integrity of Grade 92 steel. While hardness fluctuations are documented, the correlation between initial properties and long-term creep stability remains controversial. This study aims to evaluate the relationship between thermal [...] Read more.
Thermal excursions during post-weld heat treatment (PWHT) and on-site fabrication frequently compromise the integrity of Grade 92 steel. While hardness fluctuations are documented, the correlation between initial properties and long-term creep stability remains controversial. This study aims to evaluate the relationship between thermal history and subsequent creep performance. Heat treatments of T92 steel across a wide temperature range (760–1000 °C) were performed, followed by creep tests at 600 °C/130 MPa and microstructural characterization. Results reveal a non-monotonic evolution of hardness and strength, reaching a minimum at 850 °C due to martensitic lath recovery into ferrite, but nearly doubling the as-received (AR) values above 900 °C due to fresh martensite formation. Creep life drops to a minimum at 850 °C and recovers to the AR level at 950 °C. A significant “decoupling” occurs at 1000 °C, where the sample possesses the highest hardness but only exhibits one-fourth the life of the 950 °C sample. Superior performance stems from the retained M23C6 and its dynamic precipitation, which pins dislocations to form micro-lath structures. Conversely, 1000 °C facilitates full carbide dissolution, accelerating dislocation recovery. These findings emphasize precise PWHT control and demonstrate that a 950 °C rejuvenation treatment can restore over-tempered or damaged components. Full article
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13 pages, 18880 KB  
Article
Microstructure and Mechanical Properties of ZM6 Cast Magnesium Alloy with Through-Hole Defects Repaired by Ultrasonic-Assisted TIG Welding
by Faming Shen, Zhien Chen, Ming Che, Zhaoxiang Chang, Xin Qiao, Yongjun Li, Guihua Li, Mingyue Zhao, Yunhao Xia and Sanbao Lin
Crystals 2026, 16(3), 182; https://doi.org/10.3390/cryst16030182 - 9 Mar 2026
Viewed by 131
Abstract
This study addresses the challenge of through-hole defects in ZM6 cast magnesium alloy components by proposing an innovative repair strategy using ultrasonic-assisted Tungsten Inert Gas (U-TIG) welding. The microstructure and mechanical properties of the repaired joint were systematically characterized through optical microscopy, scanning [...] Read more.
This study addresses the challenge of through-hole defects in ZM6 cast magnesium alloy components by proposing an innovative repair strategy using ultrasonic-assisted Tungsten Inert Gas (U-TIG) welding. The microstructure and mechanical properties of the repaired joint were systematically characterized through optical microscopy, scanning electron microscopy (SEM), X-ray diffraction (XRD), and room-temperature tensile testing. The results indicate that, assisted by the ultrasonic energy field, the repair zone successfully reconstitutes a typical and optimized triple-phase microstructure: (1) the matrix: α-Mg solid solution (dark gray), supersaturated with Nd and Zr; (2) the strengthening phase: a eutectic Mg12Nd phase (light gray), rich in Nd, distributed along grain boundaries acting as the primary strengthening component; (3) the grain refiner: dispersed Zr-rich particles (bright white spots), which effectively pin grain boundaries. Crucially, the application of ultrasound significantly refined the α-Mg grains and transformed the continuous network of the Mg12Nd phase into a more fragmented and uniform dispersion. This refined microstructure synergistically integrates the strengthening mechanisms of solid solution, precipitation hardening, and grain refinement. Consequently, the repaired joint exhibits excellent mechanical properties, achieving over 90% of the base metal’s tensile strength and elongation at room temperature. This work not only validates the feasibility of U-TIG welding for repairing ZM6 alloys but also provides a solid theoretical foundation and a promising technical pathway for the in-service repair and remanufacturing of high-performance magnesium alloy components. Full article
(This article belongs to the Section Crystalline Metals and Alloys)
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17 pages, 1925 KB  
Article
Simplified Point-of-Care Testing for Human Pythiosis: Development of a Whole-Blood-Based Lateral Flow Immunoassay
by Jidapa Szekely, Kitti Saelai, Sirida Youngchim, Siriporn Chongkae, Pornchanan Chanchay, Wiraphan Rakchang, Paramaporn Rattanaphan and Narongdet Kositpantawong
Diagnostics 2026, 16(5), 652; https://doi.org/10.3390/diagnostics16050652 - 24 Feb 2026
Viewed by 261
Abstract
Background/Objectives: Human pythiosis, caused by Pythium insidiosum, is associated with severe morbidity and high mortality when diagnosis is delayed. Culture-based diagnosis is time-consuming and may be insensitive in clinical specimens, highlighting the need for rapid point-of-care serodiagnostic tools. Here, we developed [...] Read more.
Background/Objectives: Human pythiosis, caused by Pythium insidiosum, is associated with severe morbidity and high mortality when diagnosis is delayed. Culture-based diagnosis is time-consuming and may be insensitive in clinical specimens, highlighting the need for rapid point-of-care serodiagnostic tools. Here, we developed and clinically evaluated the Anti-Pin Antibody Test Strip, a whole-blood-compatible lateral flow immunoassay (LFIA) for detecting anti-P. insidiosum antibodies. Methods: Secretory protein antigens of P. insidiosum were prepared and conjugated to gold nanoparticles for LFIA development. Analytical performance was assessed by determining the limit of detection (LOD) using serial dilutions of pythiosis serum and by evaluating cross-reactivity with sera from patients with other infections. Interference testing examined common anticoagulants and adverse sample conditions (hemolysis, lipidemia, and icterus). Clinical performance was evaluated using 258 serum samples, comprising 48 pythiosis-positive and 210 pythiosis-negative specimens confirmed by immunoblotting and/or culture. Test results were read at 5 min. Results: The assay LOD was a serum titer of 1:1000. No cross-reactivity was observed across the tested infectious and immunologic panels, and no interference was detected from anticoagulants or adverse sample conditions. Whole-blood testing showed no red blood cell interference. In clinical evaluation, sensitivity was 100.00% (48/48), specificity was 95.24% (200/210), and accuracy was 96.12%, with a PPV of 82.76% and an NPV of 100.00%. Conclusions: The Anti-Pin Antibody Test Strip provides rapid (5 min), operationally simple serodiagnosis and may support screening/triage of suspected pythiosis, particularly where laboratory methods are limited. Full article
(This article belongs to the Special Issue Advances in Infectious Disease Diagnosis Technologies)
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22 pages, 8223 KB  
Article
Tribological Properties of AISI 420 ESR Stainless Steel Modified by Sequential Boriding and Nitriding
by Melvyn Alvarez Vera, Rafael Carrera Espinoza, Valeria López López, Marc Wettlaufer, Stefan Barth, Juan Carlos Díaz Guillén, Héctor Manuel Hernández García, Rita Muñoz Arroyo, Javier A. Ortega, Pablo Moreno Garibaldi and Marco A. Cruz-Gómez
Coatings 2026, 16(2), 263; https://doi.org/10.3390/coatings16020263 - 21 Feb 2026
Viewed by 333
Abstract
This study investigates the effects of surface thermochemical treatments using boriding, nitriding, and boronitriding on the microstructure and mechanical properties of martensitic stainless steel AISI 420 ESR. Powder-pack boriding, gas nitriding, and sequential boronitriding processes were applied to enhance surface hardness, wear resistance, [...] Read more.
This study investigates the effects of surface thermochemical treatments using boriding, nitriding, and boronitriding on the microstructure and mechanical properties of martensitic stainless steel AISI 420 ESR. Powder-pack boriding, gas nitriding, and sequential boronitriding processes were applied to enhance surface hardness, wear resistance, and adhesion. The microstructural and mechanical properties of the surface samples were analyzed using scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction, microhardness, and nanoindentation testing. Tribological behavior was analyzed using a pin-on-disk tribometer under dry-sliding wear conditions, with applied normal loads of 5 N and 10 N and a sliding distance of 1000 m. The results showed that the borided samples exhibited the highest surface hardness, up to 1182 HV0.05, as well as brittle fracture and spallation with poor adhesion, while the boronitrided layer offered excellent adhesion. The boronitriding condition demonstrated a synergistic balance, combining high wear resistance (5.92 × 10−7 mm3N−1m−1 and 4.96 × 10−7 mm3N−1m−1) and reduced friction (~0.78 and ~0.67) for loads of 5 N and 10 N, respectively, without brittle fractures on the coating layer. These results confirm that duplex coating treatment is an effective strategy for improving the surface performance of AISI 420 ESR components subjected to severe operating conditions. Full article
(This article belongs to the Special Issue Advances in Protective Coatings for Metallic Surfaces)
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14 pages, 1239 KB  
Article
Reliable Belt-Style Depositor Design in a Food Processing Plant
by Tyler F. Baker, Wolday Desta Abrha and Erkan Kaplanoglu
Appl. Sci. 2026, 16(4), 1855; https://doi.org/10.3390/app16041855 - 12 Feb 2026
Viewed by 224
Abstract
Considering consumer health, consistency in processes, and developing trust among the public, food manufacturing facilities are expected to adhere to strict regulatory policies. Along with these expectations, machinery capabilities, especially considering reliability, maintainability, and hygienic designs, would play a significant role in delivering [...] Read more.
Considering consumer health, consistency in processes, and developing trust among the public, food manufacturing facilities are expected to adhere to strict regulatory policies. Along with these expectations, machinery capabilities, especially considering reliability, maintainability, and hygienic designs, would play a significant role in delivering quality products and developing efficient processes. This paper focuses on a belt-style depositor machine, whose primary purpose is to deposit product pieces onto product passing below it. First, the key issues with the current machine are pinpointed. Next, alternative designs are provided aimed at testing, evaluating, and building belt-driven depositing machines. The original design experienced persistent belt tracking issues, frequent maintenance interruptions, and sanitation concerns due to its complex, heavy components. The project applied the Define, Measure, Analyze, Design, and Verify (DMADV) framework to test alternative belt configurations and implement improvements that significantly reduced maintenance time, improved tracking reliability, and enhanced hygienic design. Lab and real-world tests compared three prototypes, namely the V-Rib, Crowned Roller, and Pin Drive. The prototypes were compared against defined performance targets. The final system, built around a self-tracking V-Rib belt with modular components and reduced tool disassembly, demonstrated a 75% reduction in belt change time, and improved product consistency and compliance with sanitation standards. This redesign offers a replicable model for upgrading depositor systems across production lines. Full article
(This article belongs to the Special Issue Industrial System Reliability Modeling and Optimization)
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16 pages, 1150 KB  
Article
Does Stimulation of Plantar Mechanoreceptors Alter Visual Spatial Localization?
by Philippe Villeneuve, Frédéric Viseux, Rodolfo Parreira and Maria Pia Bucci
J. Funct. Morphol. Kinesiol. 2026, 11(1), 74; https://doi.org/10.3390/jfmk11010074 - 12 Feb 2026
Viewed by 373
Abstract
Objectives: Few studies have previously shown an interaction between feet and gaze in postural control. The aim of the current study is to more specifically examine how vertical heterophoria (VH) varies with stimulation of the mechanoreceptors in the foot sole. A new method [...] Read more.
Objectives: Few studies have previously shown an interaction between feet and gaze in postural control. The aim of the current study is to more specifically examine how vertical heterophoria (VH) varies with stimulation of the mechanoreceptors in the foot sole. A new method is proposed for fast assessment of minimum VH, especially when values are less than 1/2 diopter (pD). Methods: The Maddox rod test was used to assess VH with a new device made of a small point source of light located in the center of a circular box that enables the measurement of minimum VH. The VH assessment was based on a group of 95 adults in upright posture on different subtle plantar stimulations (with and without pins and on foam). Results: Almost half of the subjects exhibited minimum heterophoria with vertical deviations less than 1 pD, most of them (96%) with a VH ≤ 1/2 pD (small heterophoria). For the latter, a subtle plantar foot change induced by pins (1 mm high) or foam (4 mm high) can have different effects on ortho- and heterophoria. Orthophoric subjects became heterophoric with foam and pins, while heterophoric subjects became orthophoric with foam and pins, which can increase or decrease their phorias depending on the foam or pins and the type of HV. Using the new circular box makes it fast and easy to highlight even the smallest of heterophorias. We suggest that clinicians use this device to assess the effects of postural interventions, even though it has not yet proven its validity. The findings of the current study highlight the interrelation between gaze and foot systems, while the importance of the plantar mechanoreceptors is demonstrated. Full article
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19 pages, 12818 KB  
Article
Mechanical Stability of Amorphous Silicon Thin-Film Devices on Polyimide for Flexible Sensor Platforms
by Giulia Petrucci, Fabio Cappelli, Martina Baldini, Francesca Costantini, Augusto Nascetti, Giampiero de Cesare, Domenico Caputo and Nicola Lovecchio
Sensors 2026, 26(3), 1026; https://doi.org/10.3390/s26031026 - 4 Feb 2026
Viewed by 336
Abstract
Hydrogenated amorphous silicon (a-Si:H) is a mature thin-film technology for large-area devices and thin-film sensors, and its low-temperature growth via Plasma-Enhanced Chemical Vapor Deposition (PECVD) makes it particularly suitable for biomedical flexible and wearable platforms. However, the reliable integration of a-Si:H sensors on [...] Read more.
Hydrogenated amorphous silicon (a-Si:H) is a mature thin-film technology for large-area devices and thin-film sensors, and its low-temperature growth via Plasma-Enhanced Chemical Vapor Deposition (PECVD) makes it particularly suitable for biomedical flexible and wearable platforms. However, the reliable integration of a-Si:H sensors on polymer substrates requires a quantitative assessment of their electrical stability under mechanical stress, since bending-induced variations may affect sensor accuracy. In this work, we provide a quantitative, direction-dependent evaluation of the static-bending robustness of both single-doped a-Si:H layers and complete p-i-n junction stacks on polyimide (Kapton®), thereby linking material-level strain sensitivity to device-level functionality. First, n- and p-doped a-Si:H layers were deposited on 50 µm thick Kapton® and then structured as two-terminal thin-film resistors to enable resistivity extraction under bending conditions. Electrical measurements were performed on multiple samples, with the current path oriented either parallel (longitudinal) or perpendicular (transverse) to the bending axis, and resistance profiles were determined as a function of bending radius. While n-type layers exhibited limited and mostly gradual variations, p-type layers showed a stronger sensitivity to mechanical stress, with a critical-radius behavior under transverse bending and a more progressive evolution in the longitudinal one. This directional response identifies a practical bending condition under which doped layers, particularly p-type films, are more susceptible to strain-induced degradation. Subsequently, a linear array of a-Si:H p-i-n sensors was fabricated on Kapton® substrates with two different thicknesses (25 and 50 µm thick) and characterized under identical bending conditions. Despite the increased strain sensitivity observed in the single-layers, the p-i-n diodes preserved their rectifying behavior down to the smallest radius tested. Indeed, across the investigated radii, the reverse current at −0.5 V remained consistent, confirming stable junction operation under bending. Only minor differences, related to substrate thickness, were observed in the reverse current and in the high-injection regime. Overall, these results demonstrate the mechanical robustness of stacked a-Si:H junctions on polyimide and support their use as sensors for wearable biosensing architectures. By establishing a quantitative, orientation-aware stability benchmark under static bending, this study supports the design of reliable a-Si:H flexible sensor platforms for curved and wearable surfaces. Full article
(This article belongs to the Special Issue Recent Innovations in Wearable Sensors for Biomedical Approaches)
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27 pages, 5961 KB  
Article
Experimental Study of the Effect of Surface Texture in Sliding Contacts Using Infrared Thermography
by Milan Omasta, Tomáš Knoth, Petr Šperka, Michal Hajžman, Ivan Křupka, Pavel Polach and Martin Hartl
Lubricants 2026, 14(2), 64; https://doi.org/10.3390/lubricants14020064 - 31 Jan 2026
Viewed by 450
Abstract
This study investigates the influence of surface texturing on temperature distribution in lubricated sliding contacts using infrared thermography. The work addresses the broader challenge of understanding thermal effects in conformal hydrodynamic contacts, where localized heating and viscosity variations can significantly affect tribological performance. [...] Read more.
This study investigates the influence of surface texturing on temperature distribution in lubricated sliding contacts using infrared thermography. The work addresses the broader challenge of understanding thermal effects in conformal hydrodynamic contacts, where localized heating and viscosity variations can significantly affect tribological performance. A pin-on-disc configuration was employed, featuring steel pins with laser-etched micro-dimples that slid against a sapphire disc, allowing for thermal imaging of the contact zone. A dual-bandpass filter infrared thermography technique was developed and rigorously calibrated to distinguish between the temperatures of the steel surface and the lubricant film. Friction measurements and laser-induced fluorescence were used in parallel to assess contact conditions and the behavior of the lubricant film. The results show that surface textures can alter local frictional heating and contribute to non-uniform temperature distributions, particularly in parallel contact geometries. Lubricant temperature was consistently higher than the surface temperature, highlighting the role of shear heating within the fluid film. However, within the tested parameter range, no unambiguous viscosity-wedge signature was identified beyond the dominant temperature-driven viscosity reduction captured by the in situ correction. The method provides a novel means of experimentally resolving temperature fields in sliding textured contacts, offering a valuable foundation for validating thermo-hydrodynamic models in lubricated tribological systems. Full article
(This article belongs to the Special Issue Mechanical Tribology and Surface Technology, 2nd Edition)
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9 pages, 1634 KB  
Proceeding Paper
Integrated Strategies for Structural, Thermal, and Fire Failure Mitigation in Lightweight TRC/CLCi Composite Facade Panels
by Pamela Voigt, Mario Stelzmann, Robert Böhm, Lukas Steffen, Hannes Franz Maria Peller, Matthias Tietze, Miguel Prieto, Jan Suchorzewski, Dionysios Kolaitis, Andrianos Koklas, Vasiliki Tsotoulidi, Maria Myrto Dardavila and Costas Charitidis
Eng. Proc. 2025, 119(1), 56; https://doi.org/10.3390/engproc2025119056 - 29 Jan 2026
Viewed by 230
Abstract
The thermally efficient and lightweight TRC/CLCi composite panels for functional and smart building envelopes, funded by the iclimabuilt project (Grant Agreement no. 952886), offer innovative solutions to sustainably address common failure risks in facade systems. This work specifically emphasizes strategies for mitigating structural, [...] Read more.
The thermally efficient and lightweight TRC/CLCi composite panels for functional and smart building envelopes, funded by the iclimabuilt project (Grant Agreement no. 952886), offer innovative solutions to sustainably address common failure risks in facade systems. This work specifically emphasizes strategies for mitigating structural, thermal, and fire-related failures through targeted material selection, advanced design methodologies, and rigorous validation protocols. To effectively mitigate structural failures, high-pressure concrete (HPC) reinforced with carbon fibers is utilized, significantly enhancing tensile strength, reducing susceptibility to cracking, and improving overall durability. To counteract thermal bridging—a critical failure mode compromising energy efficiency and structural integrity—the panels employ specially designed glass-fiber reinforced pins connecting HPC outer layers through the cellular lightweight concrete (CLC) insulation core that has a density of around 70 kg/m3 and a thermal conductivity in the range 35 mW/m∙K comparable to those of expanded polystyrene and Rockwool. These connectors ensure effective load transfer and maintain optimal thermal performance. A central focus of the failure mitigation strategy is robust fire behavior. The developed panels undergo rigorous standardized fire tests, achieving an exceptional reaction to fire classification of A2. This outcome confirms that HPC layers maintain structural stability and integrity even under prolonged fire exposure, effectively preventing catastrophic failures and ensuring occupant safety. In conclusion, this work highlights explicit failure mitigation strategies—reinforced concrete materials for structural stability, specialized glass-fiber connectors to prevent thermal bridging, rigorous fire behavior protocols, and comprehensive thermal performance validation—to produce a facade system that is robust, energy-efficient, fire-safe, and sustainable for modern buildings. Full article
(This article belongs to the Proceedings of The 8th International Conference of Engineering Against Failure)
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19 pages, 13479 KB  
Article
Friction and Wear of Extrusion Dies Under Extreme Transient High-Temperature Conditions in the Extrusion of a Novel Nickel-Based High-Temperature Powder Alloy
by Baizhi Sun, Jinhui Wang, Yanzhuo Liu, Kongyan Zhang, Yuhua Zhang, Zifeng Liu, Falin Zhang, Guangyun Duan, Hongqiang Du, Yongsheng Wei, Yingnan Shi and Xinmei Hou
Lubricants 2026, 14(2), 55; https://doi.org/10.3390/lubricants14020055 - 27 Jan 2026
Viewed by 492
Abstract
During the extrusion of novel nickel-based powder superalloy bars, the die is subjected to elevated temperatures, high pressures, and severe friction, which readily lead to abrasive wear and thermal-fatigue damage. These failures deteriorate the quality of the extruded products and significantly shorten the [...] Read more.
During the extrusion of novel nickel-based powder superalloy bars, the die is subjected to elevated temperatures, high pressures, and severe friction, which readily lead to abrasive wear and thermal-fatigue damage. These failures deteriorate the quality of the extruded products and significantly shorten the service life of the die. Frequent repair and replacement of the tooling ultimately increase the overall manufacturing cost. This study investigates the friction and wear behavior of H13 and 5CrNiMo hot-work tool steels under extreme transient high-temperature conditions by combining finite element simulation with tribological testing. The temperature and stress distributions of the billet and key tooling components during extrusion were analyzed using DEFORM-3D. In addition, pin-on-disk friction and wear tests were conducted at 1000 °C to examine the friction coefficient, wear morphology, and subsurface grain structural evolution under various loading conditions. The results show that the extrusion die and die holder experience the highest loads and most severe wear during the extrusion process. For 5CrNiMo tool steel, the wear mechanism under low loads is dominated by mild abrasive wear and oxidative wear, whereas increasing the load causes a transition toward adhesive wear and severe oxidative wear. In contrast, H13 tool steel exhibits a transition from abrasive wear to severe oxidative wear. In 5CrNiMo steel, friction-induced recrystallization, grain refinement, and softening lead to the formation of a mechanically mixed layer, which, together with a stable third-body layer, markedly reduces and stabilizes the friction coefficient. H13 steel, however, undergoes surface strain localization and spalling, resulting in persistent fluctuations in the friction coefficient. The toughness and adhesion of the oxide film govern the differences in wear mechanisms between the two steels. Owing to its higher Cr, V, and Mo contents, H13 forms a dense but highly brittle oxide scale dominated by Cr and Fe oxides at 1000 °C. This oxide layer readily cracks and delaminates under frictional shear and thermal cycling. The repeated spalling exposes the fresh surface to further oxidation, accompanied by recurrent adhesion–delamination cycles. Consequently, the subsurface undergoes alternating intense shear and transient load variations, leading to localized dislocation accumulation and cracking, which suppresses the progression of continuous recrystallization. Full article
(This article belongs to the Special Issue Friction and Wear Mechanism Under Extreme Environments)
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8 pages, 3364 KB  
Proceeding Paper
Effect of Stirring Efficiency on Fatigue Behavior of Graphene Nanoplatelets-Reinforced Friction Stir Spot Welded Aluminum Sheets
by Amir Alkhafaji and Daniel Camas
Eng. Proc. 2026, 124(1), 6; https://doi.org/10.3390/engproc2026124006 - 23 Jan 2026
Viewed by 217
Abstract
Friction stir spot welding (FSSW) is a novel variant of Friction Stir welding (FSW), developed by Mazda Motors and Kawasaki Heavy Industries to join similar and dissimilar materials in a solid state. It is an economic and environmentally friendly alternative to resistance spot [...] Read more.
Friction stir spot welding (FSSW) is a novel variant of Friction Stir welding (FSW), developed by Mazda Motors and Kawasaki Heavy Industries to join similar and dissimilar materials in a solid state. It is an economic and environmentally friendly alternative to resistance spot welding (RSW). The FSSW technique, however, includes some structural defects imbedded within the weld joint, such as keyhole formation, hook crack, and bond line oxidation challenging the joint strength. The unique properties of nanomaterials in the reinforcement of metal matrices motivated researchers to enhance the FSSW joints’ strength. Previous studies successfully fabricated nano-reinforced FSSW joints. At different volumetric ratios of nano-reinforcement, nanoparticles may agglomerate due to inefficient stirring of the welding tool pin, forming stress concentration sites and brittle phases, affecting tensile and fatigue strength under static and cyclic loading conditions, respectively. This work investigated how the welding tool pin affects stirring efficiency by controlling the distribution of a nano-reinforcing material within the joint stir zone (SZ), and thus the tensile and fatigue strength of the FSSW joints. Sheets of AA6061-T6 of 1.8 mm thickness were used as a base material. In addition, graphene nanoplatelets (GNPs) with lateral sizes of 1–10 µm and thicknesses of 3–9 nm were used as nano-reinforcements. GNP-reinforced FSSW specimens were prepared and successfully fabricated. Optical microscope (OM) and field emission scanning electron microscope (FE-SEM) methods were employed to visualize the GNPs’ incorporation into the SZs of the FSSW joints. Micrographs of as-welded specimens showed lower formations of scattered, clustered GNPs achieved by the threaded pin tool compared to continuous agglomerations observed when the cylindrical pin tool was used. Tensile test results revealed a significant improvement of about 30% exhibited by the threaded pin tool compared to the cylindrical pin tool, while fatigue test showed an improvement of 46–24% for the low- and high-cycle fatigue, respectively. Full article
(This article belongs to the Proceedings of The 6th International Electronic Conference on Applied Sciences)
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19 pages, 5147 KB  
Article
The Influence of Applying PVD Coatings on Adhesion Wear Resistance of Quenching and Tempering Steels
by Ivica Kladarić, Stjepan Golubić, Danko Ćorić and Andrijana Milinović
Metals 2026, 16(2), 130; https://doi.org/10.3390/met16020130 - 23 Jan 2026
Viewed by 260
Abstract
The article examines the effect of different types of two-layer nanostructured coatings (cVIc and nACVIc) deposited on three types of steel substrates, 45S20, C45E, and 42CrMo4, to determine the resistance to adhesive wear of the substrate/coating system. The samples underwent different heat treatments, [...] Read more.
The article examines the effect of different types of two-layer nanostructured coatings (cVIc and nACVIc) deposited on three types of steel substrates, 45S20, C45E, and 42CrMo4, to determine the resistance to adhesive wear of the substrate/coating system. The samples underwent different heat treatments, including normalising, quenching, and quenching and tempering, followed by PVD (physical vapour deposition) treatment at temperatures of 450 °C (cVIc) and 460 °C (nACVIc). The thickness of the cVIc layers for all three steels ranged from 0.9 to 3.4 μm, while the thickness of the nACVIc layers on all steels was slightly greater, ranging from 1.9 to 3.1 μm. Tribological tests were conducted using the pin-on-disc method, and the results were statistically analysed. Results indicate that steel grade, heat treatment, and PVD coating significantly affect adhesive wear resistance, with the type of PVD coating showing the strongest influence. For all three steels, quenched and uncoated samples exhibited the lowest adhesion wear index values. Normalised and quenched with or without tempering steels coated with cVIc layer exhibit higher resistance to adhesive wear due to better adhesion of the layer compared to the nACVIc coating. Full article
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20 pages, 2130 KB  
Article
Microstructural, Hardness, and Abrasive Wear Properties of Functionally Graded Al/ZrB2 Composites Produced by In Situ Centrifugal Casting
by İbrahim Güney, Ömer Faruk Demirok, Yunus Emre Benkli, Çağlar Yüksel and Ömer Savaş
Metals 2026, 16(1), 125; https://doi.org/10.3390/met16010125 - 21 Jan 2026
Viewed by 329
Abstract
Functionally graded aluminum matrix composites are of interest for applications requiring region-dependent mechanical and tribological performance. In this study, the micro-structure, hardness, and abrasive wear properties of functionally graded Al/ZrB2 compo-site materials produced by an in situ centrifugal casting method were investigated. [...] Read more.
Functionally graded aluminum matrix composites are of interest for applications requiring region-dependent mechanical and tribological performance. In this study, the micro-structure, hardness, and abrasive wear properties of functionally graded Al/ZrB2 compo-site materials produced by an in situ centrifugal casting method were investigated. The ZrB2 reinforcement phase was synthesized in situ within the molten aluminum matrix, and functional grading was achieved through the action of centrifugal force during solidification. Samples taken from cylindrical castings were characterized using optical microscopy, scanning electron microscopy (SEM), X-Ray diffraction (XRD), density measurements, Brinell hardness testing, and abrasive wear experiments. Phase analyses con-firmed the successful in situ formation of ZrB2 and verified that the phase distribution in-creased toward the direction of centrifugal force. Hardness increased with reinforcement content, rising from approximately 28 HB in the matrix-rich region to 68 HB and 72 HB in regions reinforced with 12% and 15% ZrB2, respectively. Abrasive wear behavior was evaluated using the pin-on-disk method, and a Taguchi L (35) orthogonal array was employed for experimental design. Statistical analyses showed that the composite region was the most influential parameter affecting wear performance, followed by abrasive particle size and applied load, while sliding distance and sliding speed were not statistically significant. These findings demonstrate that in situ centrifugal casting is an effective approach for producing functionally graded Al/ZrB2 composites with improved hardness and wear resistance. Full article
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23 pages, 5255 KB  
Article
Analysis of Wear Behavior Between Tire Rubber and Silicone Rubber
by Juana Abenojar, Miguel Angel Martínez and Daniel García-Pozuelo
Appl. Sci. 2026, 16(2), 878; https://doi.org/10.3390/app16020878 - 14 Jan 2026
Cited by 1 | Viewed by 628
Abstract
Vulcanized NR-SBR is widely used in vehicle components; however, its irreversible crosslinking limits recyclability and contributes to the large number of tires discarded annually worldwide, and in this context, this work presents an experimental comparative assessment of the tribological behavior of conventional tire [...] Read more.
Vulcanized NR-SBR is widely used in vehicle components; however, its irreversible crosslinking limits recyclability and contributes to the large number of tires discarded annually worldwide, and in this context, this work presents an experimental comparative assessment of the tribological behavior of conventional tire rubber and silicone VMQ, motivated by a wheel concept based on a detachable tread aimed at improving durability and sustainability rather than proposing an immediate material substitution. Wear and friction behavior were investigated under abrasive and self-friction conditions using pin-on-disk testing with an abrasive counterpart representative of asphalt, supported by optical and scanning electron microscopy. The results show that NR-SBR undergoes severe abrasive and erosive wear, characterized by deep and irregular wear tracks, pronounced fluctuations in the dynamic friction coefficient, and strong sensitivity to load and sliding speed, particularly during the initial stages of track formation. In contrast, VMQ exhibits mild abrasive wear dominated by viscoelastic deformation, leading to shallow and stable wear tracks, lower friction coefficients, and significantly reduced material loss once the contact track is fully developed. These differences are attributed to the distinct mechanical responses of the elastomers, as the higher hardness and limited strain capacity of rubber promote micro-tearing and unstable material removal, while the high elasticity of silicone enables stress redistribution and stable contact conditions under abrasive loading. UV aging increases stiffness of rubber, resulting in reduced wear and friction, while silicone remains largely unaffected after 750 h due to the stability of its Si–O–Si backbone. Self-friction tests further indicate that smooth silicone sliding against rubber yields the lowest friction values, highlighting a favorable material pairing for detachable tread concepts. Factorial design analysis confirms material type as the dominant factor influencing both wear and friction. Overall, for the specific materials and operating conditions investigated, VMQ demonstrates higher durability, greater tribological stability, and improved aging resistance compared to NR-SBR, providing experimental evidence that supports its potential for long-life, more sustainable detachable tread applications. Full article
(This article belongs to the Section Materials Science and Engineering)
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