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19 pages, 2762 KB  
Article
Research on Foam Sand-Flushing Simulation of Coiled Tubing in Shale Gas Horizontal Wells
by Jianian Xu, Huajian Zhang, Ju Deng, Yichen Shao, Zhenjun Zhang and Hongli Liu
Processes 2026, 14(9), 1383; https://doi.org/10.3390/pr14091383 (registering DOI) - 25 Apr 2026
Abstract
To address the issues of easy leakage and low sand-flushing efficiency of coiled tubing working fluid in shale gas horizontal wells, this study investigates the flow behavior of foam fluid in both the coiled tubing and the annulus during foam sand-flushing operations, and [...] Read more.
To address the issues of easy leakage and low sand-flushing efficiency of coiled tubing working fluid in shale gas horizontal wells, this study investigates the flow behavior of foam fluid in both the coiled tubing and the annulus during foam sand-flushing operations, and optimizes operational parameters to enhance sand-flushing efficiency. Considering the dynamic variations in foam fluid properties with temperature and pressure, secondary flow effects in the spiral section, annular eccentricity, wellbore trajectory, and the solid phase in sand-carrying fluid, a one-dimensional steady-state hydraulic model incorporating flow and heat transfer is developed for the entire wellbore. This model covers the spiral, straight, jet, and annular sections of coiled tubing. Using field data from an example well, simulations yield the pressure distribution along the foam circulation path, the total circulation time, and key operational parameters. The feasibility of coiled tubing foam sand-flushing in shale gas horizontal wells is demonstrated, and the optimization of operational parameters to improve sand-flushing efficiency is analyzed. The findings provide important guidance for parameter design and equipment selection for safe and efficient sand-flushing operations in shale gas horizontal wells. Full article
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14 pages, 2036 KB  
Article
Temperature-Driven Transition from Knudsen Diffusion to Viscous Flow in a Macroporous Ceramic Membrane
by Mohammod Hafizur Rahman
Ceramics 2026, 9(5), 46; https://doi.org/10.3390/ceramics9050046 (registering DOI) - 25 Apr 2026
Abstract
Ceramic membranes show potential for high-temperature CO2 extraction from flue gas; nevertheless, their performance under simultaneous heat and pressure stress is not well comprehended. This research addresses the temperature-dependent CO2/N2 separation characteristics of a commercial ceramic membrane (pore size [...] Read more.
Ceramic membranes show potential for high-temperature CO2 extraction from flue gas; nevertheless, their performance under simultaneous heat and pressure stress is not well comprehended. This research addresses the temperature-dependent CO2/N2 separation characteristics of a commercial ceramic membrane (pore size ~0.1–1 µm) utilizing simulated flue gas (11.8% CO2, 74.2% N2, 2.5% O2, remainder CH4) at temperatures ranging from 60 to 140 °C and pressures between 4 and 6 bar. Calibrated GC-TCD was used to quantify permeate compositions across multiple operating valve openings. With a CO2/N2 selectivity (α) of 0.75 at 4 bars, the maximum CO2 enrichment peaked at 80 °C (10.8 mol%), getting close to the Knudsen diffusion limit (0.80). Selectivity decreased dramatically beyond 100 °C—α = 0.61 (100 °C), 0.45 (140 °C)—and CO2 dropped to 5.8% at 4 bar and 2.2% at 6 bars. Viscous flow dominance was shown by the strong pressure amplification—α decreased by more than 60% from 4 to 6 bar at all temperatures. These findings emphasize the possibility of performance collapse in hot, pressured flue streams and identify the limited operating window under which Knudsen-controlled transport can be maintained. The study provides quantitative evidence of a transition in transport regime under mixed flue-gas conditions. Full article
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29 pages, 11894 KB  
Article
Analysis of Vortex-Induced Vibrations in a Test Production Riser Subjected to Internal Multiphase Flow
by Qiang Fu, Liangjie Mao, Yu Chen, Rui Qin and Junlong Zhu
J. Mar. Sci. Eng. 2026, 14(9), 785; https://doi.org/10.3390/jmse14090785 - 24 Apr 2026
Abstract
The natural gas hydrate production riser is the main passage for offshore hydrate production and transport. Its safe operation directly affects the production process. However, current hydrate production methods cannot avoid hydrate decomposition and formation inside the pipe. Hydrate phase change causes internal [...] Read more.
The natural gas hydrate production riser is the main passage for offshore hydrate production and transport. Its safe operation directly affects the production process. However, current hydrate production methods cannot avoid hydrate decomposition and formation inside the pipe. Hydrate phase change causes internal multiphase flow. Together with the external ocean current, it leads to more complex nonlinear vibration of the riser. Based on China’s gas hydrate trial production in the Shenhu area of the South China Sea, this study establishes a dynamic model of a production riser. The model considers hydrate phase change inside the pipe and vortex-induced vibration. It is solved using the Newmark-β method, and its validity is confirmed by CFD simulations. The results show that, under the combined action of ocean currents and internal multiphase flow, the riser exhibits a clear multi-frequency response in vortex-induced vibration. Its spatial trajectory is highly irregular. Specifically, hydrate phase change increases internal gas content and gas slippage, elevating fluid velocity. This reduces the riser’s structural stiffness and effective tension, altering the VIV response. In addition, lower top tension and higher slurry density, flow rate, and outlet backpressure delay hydrate decomposition. These factors also reduce the effective tension along the riser and increase its in-line deformation. Full article
18 pages, 6208 KB  
Article
Enhanced Gas Drainage via Gas Injection Displacement Based on Hydraulic Flushing: Numerical Simulation and Field Test
by Xin Yang, Feiyan Tan and Qingcheng Zhang
Energies 2026, 19(9), 2061; https://doi.org/10.3390/en19092061 - 24 Apr 2026
Abstract
Hydraulic flushing is an effective permeability enhancement technology for coal seams in underground coal mines and has been widely applied in several mining areas in China. However, in low-permeability coal seams, gas drainage from hydraulic flushing boreholes often enters a rapid depletion phase, [...] Read more.
Hydraulic flushing is an effective permeability enhancement technology for coal seams in underground coal mines and has been widely applied in several mining areas in China. However, in low-permeability coal seams, gas drainage from hydraulic flushing boreholes often enters a rapid depletion phase, and achieving secondary enhanced drainage remains a critical challenge. To address this issue, this study investigates a synergistic gas drainage technology that combines gas injection displacement with hydraulic flushing. Taking the No. 3 coal seam in the Lu’an mining area of China as the research object, the optimal process parameters of this synergistic technology are systematically determined through numerical simulation and validated by underground field tests. A fully coupled numerical model incorporating the adsorption–desorption–seepage processes of the CH4/N2/O2 ternary gas system is established. The influences of injection spacing and injection pressure on drainage performance are systematically analyzed. Simulation results identify the optimal process parameters as an injection spacing of 3.5 m and an injection pressure of 1.4 MPa. Under these conditions, the relative coal permeability reaches a maximum of 1.06, the permeability enhancement zone fully covers the region between the injection and drainage boreholes, and the coal seam gas content decreases to the critical threshold of 8 m3/t in approximately 235 days. The model is quantitatively validated using 82-day field monitoring data from the synergistic module, with a relative error of approximately 1.1% between the simulated and field-derived recovery ratios. Subsequently, four sets of underground engineering trials—conventional drainage, gas injection displacement alone, hydraulic flushing alone, and the synergistic technology—are conducted in the target coal seam based on the optimized parameters. Statistical analysis of the 82-day field data shows that the synergistic technology achieves a cumulative pure methane volume of 4.83 m3, outperforming conventional drainage by 85.8% (4.83 m3 compared with 2.60 m3), gas injection alone by 23.5% (4.83 m3 compared with 3.91 m3), and hydraulic flushing alone by 52.4% (4.83 m3 compared with 3.17 m3). The mean flow rate of the synergistic module during the injection phase reaches 0.070 ± 0.012 L/min, significantly higher than that of gas injection alone (0.044 ± 0.011 L/min). This study provides economically feasible theoretical and technical support for efficient gas drainage in low-permeability coal seams in underground mines. Full article
(This article belongs to the Special Issue Petroleum and Natural Gas Engineering: 2nd Edition)
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31 pages, 2177 KB  
Article
Resilient Optimal Dispatch of Ship-Integrated Energy System and Air Lubrication Using an Enhanced Traffic Jam Optimizer
by Wanjun Han, Jinlong Cui, Xinyu Wang and Xiaotao Chen
J. Mar. Sci. Eng. 2026, 14(9), 779; https://doi.org/10.3390/jmse14090779 - 24 Apr 2026
Abstract
With increasingly stringent greenhouse gas emission regulations in the shipping industry, there is an urgent need for an efficient energy management strategy for new energy ship power systems. However, existing dispatch models often overlook the dynamic energy-saving potential of active drag reduction technologies [...] Read more.
With increasingly stringent greenhouse gas emission regulations in the shipping industry, there is an urgent need for an efficient energy management strategy for new energy ship power systems. However, existing dispatch models often overlook the dynamic energy-saving potential of active drag reduction technologies and lack effective optimization algorithms capable of handling high-dimensional, multi-constrained problems. To address these problems, this paper proposes a novel integrated dispatch framework for hybrid energy ship power systems that incorporates air lubrication systems. First, a unified multi-energy dispatch model is established, coupling the dynamic operation of air lubrication systems with electrical, thermal, and propulsion energy flows. Second, an Improved Traffic Jam Optimizer algorithm is proposed, which enhances global exploration and local exploitation through a nonlinear parameter adaptation mechanism, differential mutation strategy, and dynamic hybrid search architecture. Convergence analysis based on Markov chain theory is provided to guarantee algorithmic reliability. Simulation results demonstrate that the proposed algorithm outperforms existing methods in terms of convergence speed, solution accuracy, and stability. Furthermore, integrating air lubrication systems into the ship power system reduces total operating costs and greenhouse gas emissions by up to 20.569% and 6.310%, respectively. Full article
23 pages, 1762 KB  
Article
Comparison of Sampling Systems for Biological Sample Dehumidification Prior to Electronic Nose Analysis
by Ana Maria Tischer, Beatrice Julia Lotesoriere, Stefano Robbiani, Hamid Navid, Emanuele Zanni, Carmen Bax, Fabio Grizzi, Gianluigi Taverna, Raffaele Dellacà and Laura Capelli
Appl. Sci. 2026, 16(9), 4174; https://doi.org/10.3390/app16094174 - 24 Apr 2026
Abstract
It is well known that gas sensor responses are affected by the presence of humidity in the analyzed gas. This is particularly true when dealing with biological fluid samples, whose high moisture content interferes with the adsorption of the trace volatile organic compounds [...] Read more.
It is well known that gas sensor responses are affected by the presence of humidity in the analyzed gas. This is particularly true when dealing with biological fluid samples, whose high moisture content interferes with the adsorption of the trace volatile organic compounds (VOCs) on the sensors’ active layer. To address this challenge, this study focuses on designing and testing a novel sampling system for the dehumidification of biological fluid headspace to be characterized by an electronic nose (e-Nose). Such a system, based on the use of disposable polymeric sampling bags purged with dry air, exploits the polymers’ permeability to water vapor to reduce sample humidity. Tested materials included NalophanTM (20 μm), high-density polyethylene (HDPE, 8, 9, 10 and 11 μm), low-density polyethylene (LDPE, 12 and 50 μm), and biodegradable polyester (Bio-PS, 15 μm). First, dehumidification performance was characterized as a function of dry air flow rate and film type. A purge of 1 L/min accelerated the sample humidity removal compared to passive storage of bags from >2 h to <1 h (from 80% to 20% RH). Second, a mass-balance model was applied to dedicated experiments to decouple water losses due to diffusion and adsorption, showing that diffusion through the polymer wall dominates, while adsorption occurs in the early stages of conditioning. Third, because these materials are not selectively permeable to water, potential loss of water-soluble VOCs during dehumidification was investigated. Pooled urine headspace samples—both raw and spiked with a metabolite mix of VOCs—were dried using each material and analyzed using a photo-ionization detector (PID) and an e-Nose. Results were compared against a NafionTM dryer. Comparison was based on the e-Nose’s ability to discriminate between pooled vs. spiked samples and reveal real-life metabolomic changes. NalophanTM bags and NafionTM dryer provided the highest VOC fingerprint to support discrimination by the e-Nose, while Bio-PS provided the fastest sample dehumidification. The proposed bag-based system offers a cost-effective, disposable, and contamination-free solution to humidity interference in e-Noses. Full article
(This article belongs to the Special Issue State of the Art in Gas Sensing Technology)
16 pages, 1725 KB  
Article
Morphological Shift and Lipid Accumulation in Trichosporon cutaneum B3 Induced by Enhanced Dissolved Oxygen
by Ya Wang, Bin He and Riming Yan
J. Fungi 2026, 12(5), 312; https://doi.org/10.3390/jof12050312 - 24 Apr 2026
Abstract
In oleaginous yeast submerged fermentation, dissolved oxygen (DO) regulates both metabolism and cell morphology. Under oxygen limitation, Trichosporon cutaneum transitions from yeast-form to hyphae-form; the yeast-form morphology is more suitable for lipid production. This study enhanced oxygen transfer via reactor engineering to maintain [...] Read more.
In oleaginous yeast submerged fermentation, dissolved oxygen (DO) regulates both metabolism and cell morphology. Under oxygen limitation, Trichosporon cutaneum transitions from yeast-form to hyphae-form; the yeast-form morphology is more suitable for lipid production. This study enhanced oxygen transfer via reactor engineering to maintain yeast morphology and improve lipid productivity. Three strategies were assessed: increased agitation/aeration, enriched air supply, and microporous ceramic membrane gas distributor (MCMGD). Fermentation kinetics were analyzed alongside computational fluid dynamics (CFD) simulations of volumetric mass transfer coefficient (kLa), gas holdup, bubble diameter, and flow fields. Conventional strategies only partially alleviated oxygen limitation (maximum 4.47 g/L lipid). Enriched air improved lipid content but induced early myceliation. The MCMGD (1.0 vvm, 150 rpm) shortened fermentation from 150 h to 60 h, achieving 12.06 g/L lipid (49.16% content)—a 2.16-fold lipid concentration increase. Mechanistically, it generated smaller bubbles (1.47 mm vs. 2.54 mm) and higher kLa (0.012 s−1 vs. 0.0055 s−1). CFD revealed improved axial flow, reduced dead zones, and uniform gas holdup, suppressing yeast-to-hyphae shift. By enhancing mass transfer under low shear, the MCMGD ensures adequate oxygenation, maintains productive morphology, and significantly improves lipid production—offering a promising strategy for industrial application. Full article
(This article belongs to the Section Fungal Cell Biology, Metabolism and Physiology)
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18 pages, 2362 KB  
Article
Competing Mechanisms and Implications of Rock Physical Property Alteration in Carbonate UGS During Cyclic Operations
by Han Jia, Dongbo He, Meifang Hou, Weijie Wang, Wei Hou, Yixuan Yang, Liao Zhao and Mingjun Chen
Processes 2026, 14(9), 1354; https://doi.org/10.3390/pr14091354 - 23 Apr 2026
Abstract
The multi-cycle high-rate injection and production operations in Underground Gas Storage (UGS) facilities converted from depleted fracture-pore carbonate gas reservoirs induce complex rock–fluid interactions that threaten long-term integrity and performance. This study experimentally investigates the petrophysical responses of the Xiangguosi (XGS) UGS carbonate [...] Read more.
The multi-cycle high-rate injection and production operations in Underground Gas Storage (UGS) facilities converted from depleted fracture-pore carbonate gas reservoirs induce complex rock–fluid interactions that threaten long-term integrity and performance. This study experimentally investigates the petrophysical responses of the Xiangguosi (XGS) UGS carbonate reservoirs in China using multi-cycle stress sensitivity tests, fines migration experiments, and water evaporation–salt precipitation analyses. SEM observations distinguish the contributions of crack closure and matrix compression to permeability evolution. Results show a sharp contrast in mechanical damage: high-quality rocks present negligible permanent deformation (<8% Young’s modulus reduction), whereas poor-quality rocks suffer catastrophic deterioration (>60%). Fines migration exhibits a three-stage behavior under cyclic flow, with water saturation significantly aggravating permeability impairment. A critical salinity threshold (220,000 ppm) is identified for the transition between drying-enhanced storage and salt plugging. Permeability declines sharply despite a slight porosity increase due to selective salt clogging of key pore throats, revealing a clear porosity–permeability decoupling. Salt deposition under movable water conditions can reduce UGS capacity by up to 1.45%. Reservoir heterogeneity, microfractures, karst structures, and initial petrophysical properties dominate the storage and flow space evolution. This work provides a predictive framework for optimizing injection–production strategies and improving the performance of complex carbonate UGS. Full article
(This article belongs to the Special Issue Advanced Strategies in Enhanced Oil Recovery: Theory and Technology)
21 pages, 5697 KB  
Article
Tri-Stage Optimization Framework for Optimal Clustering of Power Distribution Systems into Sustainable Microgrids
by Yahia N. Ahmed, Ahmed Abd Elaziz Elsayed and Hany E. Z. Farag
Energies 2026, 19(9), 2050; https://doi.org/10.3390/en19092050 - 23 Apr 2026
Abstract
Decentralized sustainable microgrids are emerging as a promising approach for addressing the increasing complexity of modern power systems while ensuring reliable and efficient operation. A fundamental driver of this transition is the partitioning of distribution networks into self-sufficient microgrids supported by the effective [...] Read more.
Decentralized sustainable microgrids are emerging as a promising approach for addressing the increasing complexity of modern power systems while ensuring reliable and efficient operation. A fundamental driver of this transition is the partitioning of distribution networks into self-sufficient microgrids supported by the effective integration of Distributed Energy Resources (DERs) and Energy Storage Systems (ESSs), enabling improved power flow management and enhanced voltage stability. In this regard, this paper proposes a tri-stage optimization framework designed to segment power distribution systems into multiple self-sustaining microgrids while maintaining optimal network performance. In the first stage, the distribution grid is partitioned into microgrid clusters based on electrical distance metrics and bus correlation analysis. The second stage focuses on the optimal sizing and operational management of DERs and ESSs within each identified microgrid to ensure energy self-sufficiency and minimize greenhouse gas (GHG) emissions. In the third stage, an optimal resource allocation strategy is implemented, where the resources determined in the previous stage are optimally placed within the distribution network to achieve optimal power flow, reduce system losses, and maintain voltage stability under worst-case operating conditions. The proposed framework is validated using the IEEE 33-bus test system. Simulation results demonstrate its effectiveness in multi-microgrid classification, coordinated planning, and resource allocation, highlighting its superiority in enhancing system performance and resilience. Full article
22 pages, 3671 KB  
Article
The Aerodynamic Drag Coefficient Effect on the Working Area Ventilation Status
by Gulmira Sattarova, Nurbek Spatayev, Marina Ponomareva, Ravil Mussin, Nail Zamaliyev, Denis Akhmatnurov, Nikita Ganyukov, Edvard Reshetnyakov, Shulepin Andrey, Krzysztof Skrzypkowski and Krzysztof Zagórski
Appl. Sci. 2026, 16(9), 4155; https://doi.org/10.3390/app16094155 - 23 Apr 2026
Abstract
In the present-day mining conditions, the ensuring of effective ventilation is the key factor in mine safety and energy efficiency. Calculating the aerodynamic drag of mine workings is the basis for designing and optimizing ventilation systems. Aerodynamic drag is determined by the aerodynamic [...] Read more.
In the present-day mining conditions, the ensuring of effective ventilation is the key factor in mine safety and energy efficiency. Calculating the aerodynamic drag of mine workings is the basis for designing and optimizing ventilation systems. Aerodynamic drag is determined by the aerodynamic drag coefficient, whose values in classical theory do not always correspond to actual mining conditions. This study examines the effect of the working cross-sectional area, the air flow velocity (taking into account leaks through the mined space), the support density, and the presence of reinforcement elements on the aerodynamic drag coefficient. Using statistical analysis, multivariate relationships were obtained for calculating the aerodynamic drag coefficient. The practical significance of the results consists of improving the accuracy of ventilation parameter calculations, optimizing the air flow and ventilation modes, and reducing risks in controlling aero-gas conditions in mining areas. Full article
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14 pages, 1762 KB  
Article
Research on Powder Convergence Characteristics of Powder Feeding Nozzle in Wide-Band Laser Cladding
by Erhao Zhou, Jianjun Peng, Bingjing Guo, Junhua Wang and Xiaojun Yu
Micromachines 2026, 17(5), 515; https://doi.org/10.3390/mi17050515 (registering DOI) - 23 Apr 2026
Abstract
Laser cladding processing efficiency is often limited by low powder utilization. To address this, our study elucidates the mechanism by which powder feeding parameters influence powder stream convergence, aiming to optimize these parameters. A three-dimensional model of a wide-band symmetrical nozzle was developed [...] Read more.
Laser cladding processing efficiency is often limited by low powder utilization. To address this, our study elucidates the mechanism by which powder feeding parameters influence powder stream convergence, aiming to optimize these parameters. A three-dimensional model of a wide-band symmetrical nozzle was developed using a Computational Fluid Dynamics—Discrete Element Method (CFD-DEM) coupling method to simulate the gas–solid flow. Single-factor tests and experimental validation confirmed the model’s reliability. The results identify carrier gas flow as the key parameter controlling the focal length and powder concentration, while the powder feed rate primarily governs the concentration on the focal plane. These findings provide a theoretical foundation for optimizing laser cladding parameters to enhance powder utilization. Full article
(This article belongs to the Special Issue Optical and Laser Material Processing, 2nd Edition)
32 pages, 11317 KB  
Article
Enhanced Quasi-One-Dimensional Modeling and Design Performance Assessment of an ORC with Radial Turbine for Waste Heat Recovery
by Raffaele Carandente, Alessandro di Gaeta, Veniero Giglio and Fabrizio Reale
Energies 2026, 19(9), 2039; https://doi.org/10.3390/en19092039 - 23 Apr 2026
Abstract
Organic Rankine Cycles (ORCs) are widely recognized as an effective solution for Waste heat recovery (WHR). However, the design and optimization of these systems must address the tradeoff between computational efficiency and the need to capture complex component behavior. This requires moving beyond [...] Read more.
Organic Rankine Cycles (ORCs) are widely recognized as an effective solution for Waste heat recovery (WHR). However, the design and optimization of these systems must address the tradeoff between computational efficiency and the need to capture complex component behavior. This requires moving beyond purely energetic 0D modeling approaches to account for constructional, spatial, and operational constraints. This work presents a novel modeling framework with a specific focus on the expansion device. Radial inflow turbine stages are selected for their capability to achieve high pressure ratios while maintaining compactness and high efficiency. Heat exchangers follow a generic one-dimensional counterflow configuration, with a shell-and-tube geometry adopted for sizing purposes. The turbine stages are modeled by resolving several internal sections in order to capture local thermofluid dynamic conditions. The framework predicts turbine efficiency and incorporates a newly developed formulation for shock-induced losses, improving performance prediction under trans-sonic flow conditions. After validation against experimental data, the model is applied to a WHR system integrated with an internal combustion engine fueled by biofuels. The results highlight the existence of optimal operating conditions arising from competing physical mechanisms. The analysis also shows the transition from single-stage to two-stage turbine configurations at high pressure ratios and emphasizes the role of real gas effects in determining stage performance and optimal expansion distribution. The results of simulations carried out for three different working fluids (ethanol, toluene, and R1234ze(E)) highlight that the available mechanical power ranges from 10 to 22 kW for single-stage turbine configurations and from 24 to 36 kW for two-stage configurations, with total system volumes varying between approximately 600 and 9000 L. Among the working fluids considered here, ethanol provides the best overall performance for the present case study. Overall, the proposed approach provides a reliable and computationally efficient tool for the preliminary design and optimization of ORC-based WHR systems. Full article
17 pages, 12346 KB  
Article
Calcium Carbonate Scaling in Pipes in the Presence of CO2: Experimental Evaluation of Deposited Mass and Adhesion
by Luila Abib Saidler, Renato do Nascimento Siqueira, Helga Elisabeth Pinheiro Schluter, Andre Leibsohn Martins and Bruno Venturini Loureiro
Appl. Sci. 2026, 16(9), 4123; https://doi.org/10.3390/app16094123 - 23 Apr 2026
Abstract
Inorganic scale formation in oil wells is a major flow assurance challenge, causing production losses, increased intervention costs and reduced operational efficiency. In Brazil, recent discoveries in pre-salt reservoirs have increased the relevance of calcium carbonate (CaCO3) scaling under high-pressure and [...] Read more.
Inorganic scale formation in oil wells is a major flow assurance challenge, causing production losses, increased intervention costs and reduced operational efficiency. In Brazil, recent discoveries in pre-salt reservoirs have increased the relevance of calcium carbonate (CaCO3) scaling under high-pressure and high-temperature (HPHT) conditions. Experimental data representative of petroleum environments under such conditions, particularly regarding the influence of CO2 and flow conditions, remain limited. In this study, a compact pressurized experimental unit was designed and constructed to investigate the dynamic formation, deposition and adhesion of CaCO3 under conditions close to those encountered in oil production systems. A dedicated experimental methodology was developed to promote controlled mixing of aqueous sodium bicarbonate (NaHCO3) and calcium chloride (CaCl2) solutions and CO2 injection, enabling precise control of pressure, temperature and flow regime. The effects of turbulent flow, expressed by different Reynolds numbers, on the deposited CaCO3 mass and its adhesion to the substrate were systematically evaluated under controlled conditions of 40 °C and a pressure drop of 15 bar was imposed in the control valve in order to promote the flash of CO2 and CaCO3 precipitation. Complementary characterization analyses were performed to assess crystal morphology and adhesion detachment strength. The results provide new experimental insights into CaCO3 scaling mechanisms under CO2-rich flowing conditions, contributing to improved understanding of scale adhesion and the development of mitigation strategies for flow assurance in oil and gas operations. Full article
22 pages, 5570 KB  
Article
Macroscopic Characterization and Microscopic Pore Structure of Permian Shale Reservoirs in Hunan–Guizhou–Guangxi Basin: Insights from NMRC, Fractal and Image-J Methods
by Yue Sun, Yuqiang Jiang, Miao Li, Xiangfeng Wei, Jingyu Hao and Yifan Gu
Fractal Fract. 2026, 10(5), 279; https://doi.org/10.3390/fractalfract10050279 - 23 Apr 2026
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Abstract
Permian shale is the largest and most promising shale gas exploration target in southern China after Silurian shale. The fine evaluation of shale reservoirs is a prerequisite for large-scale exploration and development. Based on the fractal method, this study, through the combined technology [...] Read more.
Permian shale is the largest and most promising shale gas exploration target in southern China after Silurian shale. The fine evaluation of shale reservoirs is a prerequisite for large-scale exploration and development. Based on the fractal method, this study, through the combined technology of nuclear magnetic resonance cryoporometry (NMRC) and Image recognition software (Image-J), clarifies the pore size distribution of Permian shale in the HGG Basin. The purpose of this study is to characterize the macroscopic parameters of Permian shale and reveal the level of reservoir space development in Permian shale. The controlling factors of porosity and pore structure are demonstrated. It is suggested that Permian shales in the HGG Basin have organic carbon contents similar to marine shales. In the favorable interval of the Dalong Formation, the average organic carbon content is comparable to that of the LMX pay zone. The lower Longtan shales have the highest organic carbon and the greatest gas generation potential, followed by the Dalong shales. TOC is the primary control on porosity in the lower Longtan and Dalong formations, whereas clay minerals dominate the control in the upper Longtan. Abundant pores between grains and between layers within clay minerals account for most of the porosity in Upper Longtan shale. In the lower Longtan and Dalong formations, organic pores are pervasive, explaining the difference in the dominant controls on porosity between these intervals. Clay minerals are a key control on the development of Permian shale reservoirs. The fractal dimension of adsorption pores (DA) has no clear relationship with the total clay content, is negatively correlated with the illite content, and shows no clear relationship with the chlorite content. In contrast, the fractal dimension of flow pores (DS) shows a weak positive correlation with the total clay content, a clear positive correlation with the illite content, and a negative correlation with the chlorite content. When illite interacts with water, it tends to break down and plug pores, an effect that is especially pronounced in the smallest pores hosted by organic matter; this accounts for the negative correlation between DA and the illite content. In larger, flow-bearing pores, disintegrated illite roughens otherwise smooth walls between and within grains, increasing structural complexity and raising DS. By contrast, reactions between chlorite and pore fluids tend to smooth the walls of flow pores, reducing structural complexity and lowering DS. Full article
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21 pages, 10271 KB  
Article
Kinetic Uncertainty in Hydrogen Jet Flames Using Lagrangian Particle Statistics
by Shuzhi Zhang, Vansh Sharma and Venkat Raman
Hydrogen 2026, 7(2), 56; https://doi.org/10.3390/hydrogen7020056 - 22 Apr 2026
Viewed by 79
Abstract
Hydrogen-enriched fuel injection in staged gas-turbine combustors is commonly achieved through jet-in-crossflow (JICF) configurations, where flame stabilization is governed by a local balance between flow-induced strain/mixing and chemical reaction rates. This work investigates turbulent reacting JICF relevant to staged combustion conditions using high-fidelity [...] Read more.
Hydrogen-enriched fuel injection in staged gas-turbine combustors is commonly achieved through jet-in-crossflow (JICF) configurations, where flame stabilization is governed by a local balance between flow-induced strain/mixing and chemical reaction rates. This work investigates turbulent reacting JICF relevant to staged combustion conditions using high-fidelity simulations with adaptive mesh refinement (AMR) and differential-diffusion effects together with Lagrangian particle statistics. Chemistry model uncertainties are incorporated by using a projection method that maps uncertainty estimates from detailed mechanisms into the model used in this work. Results show that the macroscopic flame topology remains in a stable two-branch regime (lee-stabilized and lifted) and is primarily controlled by the jet momentum–flux ratio J. Visualization of the normalized scalar dissipation rate reveals that the flame front resides on the low-dissipation side of intense mixing layers, occupying an intermediate region between over-strained and under-mixed regions. While hydrogen content does not significantly change the global stabilization mode for the cases studied, uncertainty analysis reveals composition-dependent differences that are not apparent in the mean behavior alone. In particular, visualization in Eulerian (χ, T) state-space analysis and particle statistics conditioned on the stoichiometric surface demonstrate that higher-hydrogen cases observe a lower scalar dissipation rate and exhibit substantially reduced variability in OH production under kinetic-parameter perturbations, whereas lower-hydrogen blends experience higher dissipation and amplified chemical sensitivity. These findings highlight that, even in globally similar JICF regimes, the hydrogen content can modify the local response of the flame to kinetic-parameter uncertainty, motivating uncertainty-aware interpretation and design for hydrogen-fueled staging systems. Full article
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