Search Results (306)

As the demand for sustainable construction materials grows, wood ash and nanosilica have emerged as promising components for eco-friendly mortars, whose optimization requires advanced analytical techniques capable of capturing their complex linear and nonlinear interactions, making frameworks such as response surface methodology and artificial neural networks essential for effective mix design. This study examines the mechanical performance of eco-friendly mortar incorporating wood ash (WA) as a partial cement replacement and nanosilica solution (NSS) as a strength-enhancing additive, with the aim of optimizing compressive and flexural behaviour. Wood ash was substituted at levels of 5–25%, while NS (0.265 moL⁻¹) was substituted at levels of 0–1.7%. Twenty-one mortar samples were produced and tested at multiple curing ages. Two modelling techniques, response surface methodology (RSM) and artificial neural networks (ANNs), were employed to evaluate the individual and interactive effects of WA and NSS on strength development at curing ages of 28 and 180 days. While RSM provided insight into factor significance and linear interactions, ANN more effectively captured nonlinear behaviour, achieving superior predictive accuracy (R² = 1.000 for 28-day strength). Experimental results revealed that nanosilica substantially enhanced strength up to an optimal dosage of approximately 2.5 g, beyond which performance declined due to particle agglomeration or matrix over-refinement. In contrast, higher WA contents produced strength reductions attributable to dilution effects. Optimization showed that mixtures containing low WA (≤30 g) combined with moderate NSS (2.0–2.5 g) exhibited the highest mechanical performance. Collectively, the findings confirm that ANN-based models outperform RSM and multilinear regression, underscoring their effectiveness for mix design optimization and performance forecasting in sustainable cementitious systems. Full article

Fibre-reinforced polymer composites incorporating synthetic reinforcements such as glass and carbon fibres are widely used due to their superior mechanical performance. However, their energy-intensive production and end-of-life disposal contribute to an increased carbon footprint and significant environmental burden. Natural fibre-reinforced composites have emerged as promising low impact alternatives, but variability in their mechanical performance and the lack of controlled comparative studies limit their structural application. This study presents a controlled experimental comparison of alkaline-treated unidirectional flax/epoxy and hemp/epoxy composites fabricated using the vacuum-assisted resin infusion moulding (VARIM) process. Alkali treatment was employed to enhance the fibre–matrix interfacial bonding. Mechanical characterization was conducted through tensile, flexural, impact, interlaminar shear strength (ILSS), and Vickers microhardness testing in accordance with relevant ASTM and ISO standards. The flax/epoxy composites exhibited superior in-plane mechanical performance including, 9.1% higher tensile modulus, 13.8% higher flexural strength and 20.5% higher flexural modulus compared to hemp/epoxy composites. A significant improvement was observed in impact performance, with hemp composites showing 87.4% higher impact strength, indicating enhanced resistance to dynamic loading. Conversely, hemp/epoxy composites demonstrated a 10.6% higher ILSS, suggesting improved interfacial shear resistance and fibre interlocking. These findings confirm that the fibre type significantly influences composite performance, with flax fibres providing superior stiffness and strength, while hemp fibres offer better interlaminar shear behaviour and impact strength. Scanning Electron Microscopy (SEM) fractographic analysis was additionally conducted on fracture surfaces to characterize failure mechanisms and fibre–matrix interfacial morphology. The present study provides a reliable comparative framework for material selection and demonstrates the potential of flax- and hemp-based composites as sustainable alternatives for lightweight structural applications. This study supports the development of sustainable composite materials and contributes to the United Nations Sustainable Development Goals (SDGs), particularly SDG 12 (Responsible Consumption and Production), SDG 13 (Climate Action), and SDG 11 (Sustainable Cities and Communities). Full article

This study investigates the effects of polypropylene fibre content on the workability and compressive strength of recycled aggregate concrete (RAC), as well as the flexural behaviour of RAC beams. The results indicate that recycled aggregates adversely affect the mechanical properties of concrete and reduce the crack resistance, stiffness retention, and crack-control capacity of concrete beams. Although polypropylene fibres reduce mixture workability, they improve the mechanical properties of recycled concrete and enhance the flexural behaviour of recycled concrete beams. The contribution of polypropylene fibres is mainly reflected in improved crack control and post-peak behaviour, whereas their effect on ultimate load-bearing capacity remains relatively limited. In addition, the improvement provided by the fibres does not increase proportionally with fibre dosage. A moderate fibre content can effectively balance load-bearing capacity, deformation capacity, and crack control, whereas excessive fibre addition may weaken the reinforcement effect because of poor fibre dispersion and reduced matrix uniformity. These findings provide useful guidance for evaluating the flexural performance and potential engineering applications of fibre-reinforced recycled aggregate concrete beams. Full article

The aim of this study was to evaluate the influence of artificial saliva ageing and cyclic hydrothermal loading on the mechanical properties of dental composite materials. Two commercial composites (Filtek Z550 and Filtek Ultimate Flow) and two experimental materials representing flow-type and hybrid composites were investigated. SENB specimens were prepared in accordance with ASTM E399, together with flat specimens intended for impact strength testing using the Dynstat method. All samples were aged in artificial saliva for approximately one month at 37 ± 1 °C, and subsequently, half of the specimens were subjected to thermocycling in the temperature range of 10–65 °C for 10,000 cycles. Static mechanical tests, including three-point bending (TFS), biaxial flexural strength (BFS), and compression strength (CS), were performed before and after thermocycling. In addition, impact strength and fracture toughness expressed by the stress intensity factor K_IC were determined. The results were analyzed in terms of the residual work of fracture (WOF), while the durability of the materials was evaluated using Weibull distribution parameters. The experimental analysis was complemented by SEM observations of the microstructure. The obtained results demonstrated a pronounced deterioration of mechanical properties after hydrothermal loading. The average impact strength after artificial saliva ageing reached 11.69 J/mm² for Filtek Z550, 11.57 J/mm² for Ex-hyb(P), 16.39 J/mm² for Filtek Ultimate Flow, and 10.27 J/mm² for Ex-flow(P), whereas after thermocycling, these values decreased to 5.38 J/mm², 8.86 J/mm², 4.55 J/mm², and 4.39 J/mm², respectively. A similar trend was observed for the fracture toughness parameter KIC, which decreased considerably after thermocycling for all investigated materials. The analysis of the residual work of fracture revealed the influence of thermocycling on the energy-related parameters of the composites. In the case of TFS, the average WOF decreased, among others, from 13.65·10⁻³ J to 1.90·10⁻³ J for Filtek Ultimate Flow and from 4.76·10⁻³ J to 2.37·10⁻³ J for Filtek Z550. For BFS, a noticeable decrease in WOF was also observed, particularly for Ex-flow(P) and Filtek Ultimate Flow. In the compression tests (CS), the changes were less unambiguous, and some materials exhibited an increase in WOF after thermocycling. Furthermore, changes in the scale and shape parameters of the Weibull distribution were identified, indicating degradation of composite durability under hydrothermal loading. The results confirmed that cyclic hydrothermal loading exerts a greater influence on impact strength and fracture toughness than on static flexural strength. While all investigated materials exhibited degradation, the extent of changes was material-dependent, and compression behaviour showed non-uniform responses. Weibull analysis confirmed reduced reliability and increased heterogeneity of the composites after ageing, indicating that hydrothermal fatigue is a dominant factor governing long-term mechanical deterioration of dental resin-based composites. Full article

The modal behaviour of the wooden bridge over the Rhine described by Julius Cæsar in the De Bello Gallico is analysed by a simple analytical model, i.e., a Kirchhoff–Love (KL) plate. The overall structure is indeed modelled as a thin plate, representing the walking surface, resting on elastic supports that approximate the compliance of the underlying structure. Firstly, these elastic constraints are represented by linear springs; in a refined step, beam elements with equivalent stiffness and mass are adopted. The system complexity arises from the consequent non-trivial boundary conditions and is tackled by selecting suitable auxiliary functions to operate with discretised equations of motion, in a Galërkin-like approach. MATLAB helped to develop in-house scripts capable of reconstructing the flexural behaviour as the governing parameters vary, without repeated experimental tests. The analytical results are compared with theoretical predictions and between the two assumed elastic supports, allowing verification of model consistency and explanation of differences in the bridge behaviour. The ease of implementation of these codes also enables the evaluation of the structural potential of historical constructions, the investigation of modular characteristics and connections between subcomponents, and the assessment of the effects of external loads. The study of historical structure dynamics is thus relevant not only for reconstruction, but also for modern mechanical design, with potential applications in civil, mechanical, materials, and naval engineering. Full article

Low tensile strength (brittleness) is a significant drawback of lightweight aggregate concrete, as it significantly limits its application. The parameters can be improved by using dispersed reinforcement. For the purpose of the study, two fractions of high-strength lightweight aggregate were used. It was produced by sintering waste material from power plants and cogeneration plants (e.g., fly ash). Hook-shaped steel fibres were used as the reinforcement. The presented tension test results apply to lightweight fibre-reinforced concrete, i.e., flexural tensile strength, splitting tensile strength and residual flexural tensile strength compared to lightweight non-reinforced concrete. It also refers to the analysis of fibre distribution using computer tomography and the microstructure of the fibre–cement slurry contact zone. The test results revealed that steel fibres are distributed correctly in lightweight concrete, creating effective reinforcement for the brittle cement matrix. The experimental work was supported by numerical simulations based on the Finite Element Method (FEM). A lightweight concrete structure with volumetric content and steel fibre distribution identical to those used in the experiment was modelled. This way, the numerical simulations were verified. The confirmation of the numerical model’s reliability shall help engineers develop the material’s strength at the product design stage. The optimisation shall be possible owing to the easy application of the fibres’ variable configuration, given their share and orientation. As a result of combining experimental tests with numerical simulations, the paper evaluates the influence of steel fibres on the strength of lightweight concrete. Ansys Workbench software was used to model a three-point bending test on lightweight concrete beams. A Menetrey–Willam constitutive model was selected to represent the mechanical behaviour of fibre-reinforced concrete; the model assumed material hardening/softening. Simulations yielded numerical responses similar to the experimental results, confirming the model’s ability to capture the fibre reinforcement’s influence on the forms of destruction. Full article

This study examines the effects of graphene oxide (GO) on the hydration behaviour, microstructure, and mechanical properties of Portland cement-based materials. Cement pastes and mortars incorporating GO at dosages of 0.0005%, 0.005%, and 0.05% by weight of cement were analysed through thermogravimetric analysis (TGA), X-ray diffraction (XRD), scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy (SEM/EDS), and mechanical strength testing. TGA results indicate that GO exerts a time-dependent influence on cement hydration. At early ages, GO slightly retards hydration, evidenced by lower C–S–H and CH content in GO-containing samples at 2 and 7 days, attributed to water adsorption by its oxygen-containing functional groups. At later curing ages (28–90 days), TGA results show greater C–S–H and CH weight losses in GO-modified samples compared to the reference, consistent with GO acting as a water reservoir and nucleation site. XRD and SEM results confirm that GO incorporation leads to a reduction in CH crystal size, a denser and more homogeneous microstructure, and fewer pores and microcracks. Mechanical tests revealed that GO contents of 0.0005% and 0.05% produced the most significant improvements, with increases of up to 9% in compressive strength and 16% in flexural strength at 90 days compared with the control specimens. In summary, the incorporation of low GO dosages effectively refines cement microstructure, enhances long-term hydration, and improves mechanical performance, demonstrating GO’s potential as a strength- and durability-enhancing nanomaterial for cementitious composites. Full article

The durability of cementitious mortars exposed to freeze–thaw (F/T) cycles and abrasion remains a challenge in sustainable infrastructure, motivating the exploration of alternative fiber reinforcements with lower environmental impact. There is a notable gap in understanding the behavior of natural-fiber-reinforced composites, particularly their response to freeze–thaw cycles and abrasion. Additionally, data on the physical and mechanical properties of mortars that use sheep wool and Spanish broom fibers as cement composite reinforcement remain limited. This study investigates the influence of industrially produced fibers (polypropylene and glass) and natural fibers (sheep wool and Spanish broom, with different treatments) on the F/T cycles and abrasion resistance of cement mortars. Six mixtures were prepared, including a reference and five fiber-reinforced mortars (FRM) with 0.5% fiber content by binder mass. The workability of fresh mortar, abrasion resistance, flexural strength, compressive strength, and specific fracture energy were evaluated at the age of 56 days and after 56 F/T cycles. Results indicate that fiber addition reduced workability and compressive strength and no FRM has increased flexural strength at 56 days. Polypropylene- and NaOH-treated Spanish broom fibers improved flexural performance after FT exposure, exceeding the reference mortar flexural strength by up to 23%. All FRMs have significantly enhanced fracture energy, with increases up to 2.6 times compared to the reference mortar, and maintained improved values after F/T cycling. For the selected amount of fiber, abrasion resistance remained within the same performance class for all mixtures. Polypropylene and hydroxide treated Spanish broom FRMs demonstrated the highest potential for improving F/T resistance and toughness, while FRM with untreated or seawater-treated natural fibers require further optimization for durability in alkaline environments. Understanding the behaviour of local natural fibers under extreme conditions is essential for developing durable, sustainable construction materials. Full article

Hybrid polymeric woven composites (HPWCs) are increasingly important in automotive, aerospace, and renewable energy structures where low weight, impact tolerance, damage containment, and superior mechanical properties are required. By combining dissimilar fibres within woven architectures, HPWCs can achieve a more favourable balance of stiffness, strength, and energy absorption than single-fibre woven systems; however, experimental evidence and predictive modelling remain insufficiently integrated, particularly under dynamic and post-impact loading. This systematically searched critical review provides an HPWC-focused synthesis that links architecture-driven mechanical behaviour, damage development, and multiscale numerical simulation within a single framework. The effects of reinforcement architecture, fibre pairing, and matrix selection on tensile, flexural, compressive, interlaminar, strain rate-dependent, and impact responses are examined, with particular emphasis on barely visible impact damage and post-impact residual strength. Macroscale, mesoscale, and microscale finite element strategies are critically compared in terms of predictive fidelity, computational cost, and suitability for design-orientated assessment. The main contribution of this review lies in integrating experimental characterisation with modelling limitations, validation requirements, and industrial relevance, thereby clarifying where current approaches are effective and where critical gaps remain. Practical implications for lightweight structural design, impact-resistant components, and future validation-driven research are highlighted. Full article

Intralayer hybridisation provides a powerful strategy for tailoring the stiffness–strength–ductility balance of fibre-reinforced composites through architecture control. This study investigates the flexural behaviour of carbon/glass intralayer hybrid composites with varying carbon-to-glass (C:G) ratios and degrees of dispersion using a finite element modelling framework supported by experimental validation against published flexural test data. Four hybrid ratios (C:G = 2:1, 1:1, 1:2, and 1:4) and multiple dispersion levels were examined under three-point bending to quantify the effects of intralayer architecture on flexural strength, modulus, and strain to failure. The results show that carbon-rich hybrids retain high flexural stiffness and strength while achieving substantial improvements in failure strain and damage tolerance compared with pure carbon laminates. In these systems, flexural strength is strongly influenced by dispersion, with moderate-to-high dispersion improving strain compatibility, delaying tensile-side carbon fibre fracture, and enhancing strength. In contrast, glass-dominated hybrids exhibit flexural behaviour that is largely insensitive to dispersion, with strength and modulus following near rule-of-mixtures trends and failure governed by progressive glass fibre and matrix damage. Across all hybrid ratios, flexural modulus is controlled primarily by fibre volume fraction, whereas flexural strength and failure strain depend sensitively on intralayer architecture when carbon fibres remain the dominant load-bearing phase. These findings clarify the respective roles of hybrid ratio and dispersion in governing flexural performance and extend recent studies by demonstrating a systematic transition from dispersion-dominated to ratio-dominated behaviour as glass content increases. The results provide mechanistic insight and practical design guidance for optimising intralayer hybrid composites for lightweight, damage-tolerant structural applications. Full article

Alkali-activated concrete can reduce reliance on Portland cement by valorizing industrial by-products. This study evaluates slag-based alkali-activated concretes incorporating natural diatomaceous earth (M2, M3) and residual diatomaceous earth from industrial filtration (V6–V7), benchmarked against an OPC reference. The experimental program measures compressive, tensile and flexural strengths and elastic modulus, and examines steel–concrete bond behavior through bond stress–slip response at multiple slip levels. Member-level performance is assessed using reinforced beams tested under four-point bending, and cracking is compared in the constant-moment region using crack number and average spacing derived from post-test observations. Results show that diatom-based alkali-activated mixtures can achieve mechanical performance comparable to OPC concrete, with clear dependence on diatom source and mixture design. Bond response is markedly mixture-dependent and cannot be inferred from compressive strength alone. All beams exhibited flexural behavior suitable for structural applications, with the RV6 mixture providing the most favorable overall response among the tested members. These findings support the feasibility of residual diatomaceous earth as a viable component in structural alkali-activated concretes. Full article

This study investigates the effect of metakaolin (MK) as a partial replacement of cement (CEM I) in high-workability mortars, with emphasis on fresh-state behaviour, mechanical properties, microstructural development, and carbon footprint implications. Mortars were produced with MK replacement levels ranging from 0 to 50% by mass of binder, under a constant water-to-binder ratio and fixed superplasticiser amount. Fresh-state results showed that increasing MK content reduced flowability due to its high fineness; however, high workability was maintained for replacement levels up to 20%. At 28 days, MK replacement up to 10% retains approximately 90–95% of the control compressive and flexural strength, whereas higher replacement levels lead to gradual strength reductions (to ~55–60% at 50% MK), despite comparable early-age strength gains across all mixes. Durability-related indicators demonstrated reduced water absorption and capillary uptake at moderate MK contents (approximately 20–30%), indicating refined pore structure and reduced pore connectivity. Microstructural analyses using SEM, TGA, and XRD confirmed effective portlandite consumption and the formation of dense C–A–S–H-type hydration products at moderate MK replacement levels, whereas excessive MK contents resulted in unreacted MK. A comparative carbon footprint assessment showed that MK incorporation leads to proportional reductions in embodied CO₂ emissions, with replacement levels of 10–20% providing the most favourable balance between mechanical performance, durability, and environmental benefit. Therefore, the results demonstrate that MK can be used as a supplementary cementitious material for producing low-carbon, high-workability mortars. Full article

Mycelium-based composites (MBCs) are gaining attention as sustainable alternatives to conventional materials because they are grown biologically rather than produced through resource-intensive extraction and processing. This study evaluates MBCs for non-load-bearing wall panels and environmentally responsible substitutes for traditional building materials. A reproducible manufacturing process is presented, and heat-pressed panels are characterised for physical, mechanical, and chemical performance. Novelty lies in species-driven evaluation using rice-husk waste as the sole lignocellulosic substrate and a Queensland-native Amauroderma species. Five fungal species, Trametes hirsuta, Ganoderma sp., Amauroderma sp., Pycnoporus coccineus and Trametes versicolor, were cultivated on rice husks and compared under identical processing conditions. Statistical analysis showed species selection significantly influenced tensile strength, whereas flexural and compressive performance showed no significant interspecies differences. Panels achieved tensile, compressive, and flexural strengths up to approximately 0.47, 0.35, and 1.35 MPa, respectively, with Amauroderma exhibiting the highest stiffness and compressive performance. Composites from four of the five species showed low moisture sensitivity and favourable thermal behaviour relative to previously reported mycelium materials. These results demonstrate that fungal species selection is a key design lever and supports rice-husk-derived MBCs as sustainable insulation and non-load-bearing construction materials. Full article

This study presents a comprehensive numerical investigation into the combined bending–shear behaviour of hollow-flanged cold-formed steel (HFCFS) beams filled with lightweight concrete (LWC). Although previous research has independently examined the pure bending and pure shear responses of these composite members, their structural performance under simultaneous bending and shear remains unexplored. In this work, advanced three-dimensional finite element (FE) models were developed in ABAQUS to simulate the nonlinear behaviour of LWC-filled HFCFS beams subjected to various shear-span ratios. The modelling approach was validated using published experimental data and extended through a systematic parametric study that considered three beam geometries, two steel yield strengths (350 MPa and 450 MPa), two lightweight-concrete strengths (30 MPa and 50 MPa), and aspect ratios ranging from 1.5 to 3.5. The results demonstrated a clear progression of governing failure modes, from web shear buckling at low aspect ratios to combined shear–flexure interaction at intermediate spans and flexural-dominated failure at larger spans. Normalised shear and bending demand–capacity ratios (V/Vu and M/Mu) were used to identify the dominant limit state, revealing a predictable transition from shear-controlled to flexure-controlled behaviour. The findings enhance the understanding of composite thin-walled steel–concrete systems under combined actions and highlight the need for dedicated design rules for CF-HFCFS beams operating within the bending–shear interaction domain. Full article

The concept of self-healing polymers has been prevalent over the last few decades. However, their performance and behaviour in structural applications in the form of layered composites have not been studied extensively. In this study, an attempt has been made to evaluate the recovery of the mechanical properties of Carbon Fibre-Reinforced Polymer composites (CFRPs) with an intrinsically healable polymeric resin system. Destructive tests, including static tensile, compression, and flexural tests, are carried out to evaluate their ability to recover mechanical compliance after healing. Nondestructive tests based on the Acousto-Ultrasonic (AU) approach are carried out to establish and distinguish the state of these composites. The results show that the tested self-healing CFRPs can recover their mechanical properties, particularly their flexural and compressive properties, after unstable matrix damage. On the other hand, the AU approach, supported by Machine Learning (ML) models, demonstrates that the damaged states and the heal states of these composites can be distinguished from the virgin state. Full article