Search Results (15)

In this study, high-temperature uniaxial tensile tests were performed on IN718 superalloy samples fabricated using Wire Arc Additive Manufacturing (WAAM) and compared to wrought IN718 superalloy samples. The mechanical properties and Portevin–Le Chatelier (PLC) behavior of WAAM IN718 were analyzed, with particular attention paid to its anisotropy and differences from its wrought counterpart. WAAM specimens were obtained from three distinct orientations within the printed blocks. The results indicated that WAAM IN718 exhibited a higher yield strength but reduced failure elongation compared to wrought IN718. Among the WAAM samples, the yield strength was highest in the transverse direction, followed by the in-depth direction, and lowest in the growth direction. Post-aging treatment significantly increased the yield strength of WAAM IN718. WAAM IN718 showed a larger critical strain for the onset of serrated flow and smaller stress drop amplitudes compared to wrought IN718 under the PLC effect. Furthermore, as the strain rate decreased, PLC serrations in WAAM specimens from the in-depth direction transitioned from type A to type C. Conversely, specimens from the growth direction maintained type B serrations at a strain rate of ${10}^{-4}{\mathrm{s}}^{-1}$. This study also examined potential factors influencing the differences in PLC behavior and conducted an analysis of the fracture surfaces across various specimens. Full article

Death from falls accounts for a significant number of injuries and fatalities globally, often linked to suicides, workplace accidents, or substance abuse, and rarely to homicidal causes. Injuries from falls vary based on height, impact point, and surface struck, with severe trauma often seen, including visceral ruptures, organ lacerations, and complex fractures. Even minimal external injuries can mask severe internal damage, such as multiple organ ruptures, organ tears, and large vessel lacerations. Blunt cardiac injuries, which occur in 5% to 50% of falls, are significant, especially in falls over 6 m. In 70% of the cases, cardiac rupture is observed at the level of the posterior wall of the heart and occurs due to a contusive action on the heart during the diastolic filling phase. We report a case of a 29-year-old man (weight 95 kg) who died from an 11-meter fall. He had a history of cardiac surgery for the transposition of the great vessels, and an autopsy revealed extensive cardiac rupture, likely worsened by fibrotic adhesions anchoring the heart to the pericardium. Toxicological investigations on peripheral blood showed BAC > 2.58 g/L. Heart scars, macro- and microscopically as a deposit of fibrous tissue, due to previous surgery, may have contributed to the extent of the lesion, suggesting the need for further study on post-operative tissue changes and their effects on trauma from falls. Full article

The present study investigates the tensile behavior and microstructure evolution of the 6082 aluminum alloy aged with high temperature. A universal testing machine was applied to explore the tensile behavior, while features of the fracture surface were characterized via scanning electron microscopy (SEM). The microstructural evolution was assessed through optical microscopy (OM) and transmission electron microscopy (TEM). The findings illustrate that the 6082 alloy sheet achieves peak strength following treatment at 180 °C for 8 h for the 0° orientation specimen, with the yield strength and tensile strength reaching 345 MPa and 373 MPa, respectively. An increase in aging temperature results in a decline in strength, accompanied by an improvement in elongation. After the treatment at 330 °C for 0.5 h, the corresponding yield strength falls below 150 MPa, with elongation exceeding 12%. The alloy sheet consistently exhibits ductile fracture characteristics with various aging treatments. The aging processes have no obvious influence on grain morphology. The fibrous grain structure is responsible for the anisotropic mechanical properties. The alloy aged at 180 °C for 8 h demonstrates the greatest precipitate density with the smallest precipitate size. As the aging temperature increases, the precipitate distribution becomes less uniform, and the precipitates grow coarser, leading to a decline in the precipitate density and corresponding strength of the alloy. Furthermore, it is noted that smaller precipitates are more effective in suppressing the mechanical anisotropy of the alloy. Full article

A novel high depth-to-width ratio of 15:1 narrow-gap gas metal arc welding technique was developed for the welding of S500Q steel in a horizontal butt joint. The bead arrangement of the I groove was optimized to produce a high-quality connection with the upper sidewall of the joint. The microstructure and mechanical properties were observed and evaluated by optical microscopy, scanning electron microscopy, tensile testing, and micro-hardness and impact toughness testing at 1/5, 2/5, 3/5, and 4/5 thickness of the joint. The 3/5 T position exhibited the highest strength, which was attributed to the presence of finer carbide precipitates. The highest micro-hardness appeared at 4/5 T. The highest impact toughness appeared at 3/5 T. The formation of coarse granular bainite was the major reason for the decrease in impact toughness in other regions. A microscopic fracture at 1/5 T and 3/5 T was further analyzed. It was observed that the width of the fibrous zone at 3/5 T was significantly larger than that at 1/5 T. The radial zones at 1/5 T were observed to exhibit cleavage, with secondary cracks on the fracture surface. Full article

Background: Osteochondritis dissecans (OCD) is a joint disorder predominantly affecting the knee, elbow, and ankle of children and adolescents. This comprehensive review delves into the epidemiology, etiology, clinical manifestations, diagnostic approaches, and treatment of OCD. Results: The most common cause of OCD is repetitive microtrauma, typically associated with sports activities, alongside other significant factors such as genetic predisposition, ischemia, and obesity. In early stages or when lesions are small, OCD often presents as non-specific, vaguely localized pain during physical activity. As the condition progresses, patients may experience an escalation in symptoms, including increased stiffness and occasional swelling, either during or following activity. These symptom patterns are crucial for early recognition and timely intervention. Diagnosis in most cases is based on radiographic imaging and magnetic resonance imaging. Nonsurgical treatment of OCD in young patients with open growth plates and mild symptoms involves activity restriction, immobilization methods, and muscle strengthening exercises, with a return to sports only after symptoms are fully resolved and at least six months have passed. Surgical treatment of OCD includes subchondral drilling in mild cases. Unstable lesions involve methods like restoring the joint surface, stabilizing fractures, and enhancing blood flow, using techniques such as screws, anchors, and pins, along with the removal of fibrous tissue and creation of vascular channels. The specifics of OCD treatment largely depend on the affected site. Conclusions: This synthesis of current research and clinical practices provides a nuanced understanding of OCD, guiding future research directions and enhancing therapeutic strategies. Full article

The 1100 aluminum alloy has been widely used in many industrial fields due to its high specific strength, fracture toughness, excellent thermal conductivity, and corrosion resistance. In this study, the corrosion behavior of the homogenized and hot-extruded 1100 aluminum alloy in acid salt spray environment for different time was studied. The microstructure of the 1100 aluminum alloy before and after corrosion was characterized by an optical microscope (OM), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and a laser scanning confocal microscope (LSCM). The difference in corrosion resistance between the homogenized and extruded 1100 aluminum alloy was analyzed via the electrochemical method. The results indicate that after hot extrusion at 400 °C, the microstructure of the 1100 aluminum alloy changes from an equiaxed crystal structure with (111) preferentially distributed in a fibrous structure with (220) preferentially distributed. There was no obvious dynamic recrystallization occurring during extrusion, and the second-phase particles containing Al-Fe-Si were coarse and unevenly distributed. With the increase in corrosion time, corrosion pits appeared on the surface of the 1100 aluminum alloy, and a corrosion product layer was formed on the surface of the homogenized 1100 aluminum alloy, which reduced the corrosion rate. After 96 h of corrosion, the CPR of the extruded samples was 0.619 mm/a, and that of the homogenized samples was 0.442 mm/a. The corrosion resistance of the extruded 1100 aluminum alloy was affected by the microstructure and the second phase, and no protective layer of corrosion products was formed on the surface, resulting in a faster corrosion rate and deeper corrosion pits. Full article

Composites of poly(vinyl alcohol) (PVA) in the shape of braids, in combination with crystals of hydroxyapatite (HAp), were analyzed to perceive the influence of this bioceramic on both the quasi-static and viscoelastic behavior under tensile loading. Analyses involving energy-dispersive X-ray spectroscopy (EDS) and scanning electron microscopy (SEM) allowed us to conclude that the production of a homogeneous layer of HAp on the braiding surface and the calcium/phosphate atomic ratio were comparable to those of natural bone. The maximum degradation temperature established by thermogravimetric analysis (TGA) showed a modest decrease with the addition of HAp. By adding HAp to PVA braids, an increase in the glass transition temperature (Tg) is noticed, as demonstrated by dynamic mechanical analysis (DMA) and differential thermal analysis (DTA). The PVA/HAp composite braids’ peaks were validated by Fourier transform infrared (FTIR) spectroscopy to be in good agreement with common PVA and HAp patterns. PVA/HAp braids, a solution often used in the textile industry, showed superior overall mechanical characteristics in monotonic tensile tests. Creep and relaxation testing showed that adding HAp to the eight and six-braided yarn architectures was beneficial. By exhibiting good mechanical performance and most likely increased biological qualities that accompany conventional care for bone applications in the fracture healing field, particularly multifragmentary ones, these arrangements can be applied as a fibrous fixation system. Full article

In the pursuit of sustainability and reduced dependence on new plastic materials, this study explores the upcycling potential of high-density polyethylene (HDPE) milk bottles into high-stiffness, high-heat-distortion-temperature (HDT) composites. Recycled high-density polyethylene (rHDPE) sourced from used milk bottles serves as the composite matrix, while reinforcing fillers are derived from dried pineapple leaves, comprising fibers (PALF) and non-fibrous materials (NFM). A two-roll mixer is employed to prepare rHDPE/NFM and rHDPE/PALF mixtures, facilitating filler alignment in the resulting prepreg. The prepreg is subsequently stacked and pressed into composite sheets. The introduction of PALF as a reinforcing filler significantly enhances the flexural strength and modulus of the rHDPE composite. A 20 wt.% PALF content yields a remarkable 162% increase in flexural strength and a 204% increase in modulus compared to neat rHDPE. The rHDPE/NFM composite also shows improved mechanical properties, albeit to a lesser degree than fiber reinforcement. Both composites exhibit a slight reduction in impact resistance. Notably, the addition of NFM or PALF substantially elevates HDT, raising the HDT values of the composites to approximately 84 °C and 108 °C, respectively, in contrast to the 71 °C HDT of neat rHDPE. Furthermore, the overall properties of both the composites are further enhanced by improving their compatibility through maleic anhydride-modified polyethylene (MAPE) use. Impact fracture surfaces of both composites reveal higher compatibility and clear alignment of NFM and PALF fillers, underscoring the enhanced performance and environmental friendliness of composites produced from recycled plastics reinforced with pineapple leaf waste fillers. Full article

Epoxy matrix composites reinforced with high-performance fibers, such as carbon, Kevlar, and glass, exhibit excellent specific stiffness and strength in many mechanical applications. However, these composites are disappointingly non-recyclable and are usually disposed of in landfill sites, with no realistic prospect for biodegradation in a reasonable time. In contrast, moldable composites with carbonized elastomeric matrices developed in the last decades possess attractive mechanical properties in final net-shape products and can also be incinerated or recycled. Many carbon and inorganic fillers have recently been evaluated to adjust the properties of carbonized elastomeric composites. Renewable organic fillers, such as human or animal hair, offer an attractive fibrous material with substantial potential for reinforcing composites with elastomeric matrices. Samples of unidirectional fiber composites (with hair volume fractions up to 7%) and quasi-isotropic short fiber composites (with hair volume fractions up to 20%) of human hair-reinforced nitrile butadiene rubbers (HH-NBRs) were produced in the peroxide-cured and carbonized states. The samples were characterized using scanning electron microscopy (SEM), Raman spectroscopy, and photoacoustic microscopy. Mechanical tests were performed under tension using a miniature universal testing machine. The expected effect of fiber reinforcement on the overall mechanical performance was demonstrated for both cured and carbonized composites. Considerable enhancement of the elastic modulus (up to ten times), ultimate tensile strength (up to three times), and damage tolerance was achieved. The evidence of satisfactory interfacial bonding between hair and rubber was confirmed via SEM imaging of fracture surfaces. The suitability of photoacoustic microscopy was assessed for 3D reconstructions of the fiber sub-system’s spatial distribution and non-destructive testing. Full article

Unfortunately, most of the previous work studying the fracture toughness of fibrous composites has deliberately ignored bridging the fiber onto the pre-crack/notch surfaces by creating such a crack as a through-thickness crack (TTC). Furthermore, no standard specifications for measuring the fracture toughness of fibrous composites have considered the fiber bridging through the pre-notch. Only a few pieces of research, no more than fingers on one hand, have addressed this problem by creating an actual crack, i.e., a matrix crack (MC) instead of a TTC. The challenge these researchers face is the inability to calculate the fracture toughness directly through the stress intensity factor (SIF) relationship because there is no geometry correction factor equation, f(a/d), for an MC. The main objective of the present work is to calculate f(a/d) and ascertain a relationship between the SIF and crack mouth opening displacement (CMOD) for an MC numerically using 3-D finite element analysis. An experimental program was also conducted to measure the fracture toughness of three types of concrete beams: high-strength concrete (HSC) beams with a TTC, HSC beams with an MC, and fiber-reinforced concrete (FRC) beams with an MC. The results showed that FRC beams with an MC have the highest fracture toughness and, subsequently, the highest resistance to crack growth. The numerical results revealed a suggested relationship between the SIF and CMOD of FRC beams with an MC. This relation was used to predict the fracture toughness of FRC with an MC by the critical value of CMOD measured experimentally. Full article

CoCr_xFeMnNi (x represents the atomic percentage of Cr element, x = 20, 25, 30, and 35, denoted as Cr20, Cr25, Cr30, and Cr35 alloys) high-entropy alloy (HEA) coatings were cladded by plasma arc on the surface of 0Cr13Ni5Mo steel. The effects of Cr elements on the cavitation erosion mechanisms were studied by comparing the differences of microstructure, microhardness, cavitation erosion volume loss (CVL), cavitation erosion volume loss rate (CER), and eroded surface morphologies between the coatings. As the Cr content increased, the microhardness of the coatings increased continuously, and the microstructure transformed into fine dendrites. The microhardnesses of Cr20, Cr25, Cr30, and Cr35 were 223.9 HV, 250.5 HV, 265.2 HV, and 333.7 HV, respectively. With structural change, the slip pattern shifted from uniform distribution to distribution along the grain boundary, increasing slip resistance. Additionally, strain hardening capacity increased with reduced stacking fault energy (SFE). The resistance to cavitation erosion (CR) of the HEA increased with the increase in Cr content. The CVL of 20 h cavitation erosion of Cr35 coating was only 26.84% of that of 0Cr13Ni5Mo steel, and the peak CER was only 28.75% of that of 0Cr13Ni5Mo steel. The fracture damage mechanisms of the four HEA coatings were an obvious lamellar structure and fibrous fracture. Full article

The distribution of surface integrity features directly affects the initiation and propagation of fatigue cracks. In this paper, the surface integrity characteristics changing law of turning and ultrasonic impacting specimens during high cycle fatigue loading has been studied, and the effect of surface modified layer on the fatigue properties of titanium alloy has been revealed. The results showed that the surface roughness increased with the increase of fatigue cycles. The compressive residual stress and its gradient distribution depth decreased continuously. The gradient distribution depth of residual stress in the ultrasonic-impacted surface rapidly decreased by about 50% near the fracture stage. Local cyclic hardening occurred at 20–50 μm from the surface of the specimen in the early stage of fatigue evolution, and then the microhardness continued to decrease. During this process, there were no significant changes in hardened layer depth. The fibrous microstructure of the ultrasonic-impacted surface undergoes a process from coarsening to gradual disintegration during the fatigue process. Its attenuation process needs a longer period of time. The fatigue source of the turned specimen was located at about 320 μm from the surface, and the fatigue source of ultrasonic impact was about 610 μm from the surface. The fatigue striation width of the ultrasonic impact specimen was about 20% narrower than that of the turned specimen. The fatigue life of the ultrasonic impact specimen was increased by 73.9% compared with the turned specimen. The research in this paper is of great significance for exploring the anti-fatigue mechanism and the ability of various surface integrity features. Full article

The performance of Ag-8.5Au-3.5Pd alloy wire after cold deformation and annealing were analyzed by SEM (scanning electron microscope), strength tester and resistivity tester. The processing process and performance change characteristics of Ag-8.5Au-3.5Pd alloy wire were studied. The results show that alloy wire grains gradually form a fibrous structure along with the increase in deformation. The strength of the wire increases with the increase in deformation rate, but the increase trend becomes flat once the deformation rate is higher than 92.78%; the resistivity of Ag-8.5Au-3.5Pd alloy wire decreases with the increase in annealing temperature, reaching minimum (2.395 × 10⁻⁸ Ω·m) when the annealing temperature is 500 °C; the strength of Ag-8.5Au-3.5Pd alloy wire decreases with the increase in annealing temperature. When the annealing temperature is 500 °C, the strength and elongation of the φ0.2070 mm Ag-8.5Au-3.5Pd alloy wire are 287 MPa and 25.7%, respectively; the fracture force and elongation of φ0.020 mm Ag-8.5Au-3.5Pd alloy wire are 0.0876 N and 14.8%, respectively. When the annealing temperature is 550 °C, the metal grains begin to grow and the mechanical performance decrease; the φ0.020 mm Ag-8.5Au-3.5Pd alloy wire have good surface quality when the tension range is 2.5–3.0 g. Full article

Carbon Fibre-Reinforced Polymers (CFRPs) in aerospace applications are expected to operate in moist environments where carbon fibres have high resistance to water absorption; however, polymers do not. To develop a truly optimised structure, it is important to understand this degradation process. This study aims to expand the understanding of the role of water absorption on fibrous/polymeric structures, particularly in a matrix-dominant property, namely interlaminar strength. This work used Acoustic Emission (AE), which could be integrated into any Structural Health Monitoring System for aerospace applications, optical strain measurements, and microscopy to provide an assessment of the gradual change in failure mechanisms due to the degradation of a polymer’s structure with increasing water absorption. CFRP specimens were immersed in purified water and kept at a constant temperature of 90 °C for 3, 9, 24 and 43 days. The resulting interlaminar strength was investigated through short-beam strength (SBS) testing. The SBS values decreased as immersion times were increased; the decrease was significant at longer immersion times (up to 24.47%). Failures evolved with increased immersion times, leading to a greater number of delaminations and more intralaminar cracking. Failure modes, such as crushing and multiple delaminations, were observed at longer immersion times, particularly after 24 and 43 days, where a pure interlaminar shear failure did not occur. The observed transition in failure mechanism showed that failure of aged specimens was triggered by a crushing of the upper surface plies leading to progressive delamination at multiple ply interfaces in the upper half of the specimen. The crushing occurred at a load below that required to initiate a pure shear failure and hence represents an under prediction of the true SBS of the sample. This is a common test used to assess environmental degradation of composites and these results show that conservative knockdown factors may be used in design. AE was able to distinguish different material behaviours prior to final fracture for unaged and aged specimens suggesting that it can be integrated into an aerospace asset management system. AE results were validated using optical measurements and microscopy. Full article

In this study, gas metal arc welding (GMAW) was used to construct a thin wall structure in a layer-by-layer fashion using an AWS ER70S-6 electrode wire with the help of a robot. The Charpy impact test was performed after extracting samples in directions both parallel and perpendicular to the deposition direction. In this study, multiple factors related to the resulting absorbed energy have been discussed. Despite being a layered structure, homogeneous behavior with acceptable deviation was observed in the microstructure, hardness, and fracture toughness of the structure in both directions. The fracture is extremely ductile with a dimpled fibrous surface and secondary cracks. An estimate for fracture toughness based on Charpy impact absorbed energy is also given. Full article