Search Results (1,293)

This study systematically investigates 50 μm-diameter 631 stainless steel fine wires subjected to both sequential and simultaneous electrothermomechanical loading to simulate probe spring conditions in microelectronic test environments. Under cyclic current loading (~10⁴ A/cm²), the 50 μm 631SS wire maintained electrical integrity up to 0.30 A for 15,000 cycles. Above 0.35 A, rapid oxide growth and abnormal grain coarsening resulted in surface embrittlement and mechanical degradation. Current-assisted tensile testing revealed a transition from recovery-dominated behavior at ≤0.20 A to significant thermal softening and ductility loss at ≥0.25 A, corresponding to a threshold temperature of approximately 200 °C. These results establish the endurance limit of 631 stainless steel wire under coupled thermal–mechanical–electrical stress and clarify the roles of Joule heating, oxidation, and microstructural evolution in electrical fatigue resistance. A degradation map is proposed to inform design margins and operational constraints for fatigue-tolerant, electrically stable interconnects in high-reliability probe spring applications. Full article

In the framework of hydrogen production and storage for clean energy generation, the resistance to hydrogen embrittlement of a newly developed austenitic stainless steel is presented. Gas-atomized metal powders prepared from secondary-sourced metals were employed to manufacture test specimens with Laser Powder Bed Fusion (LPBF) technology. After machining and exposure to a controlled, pressurized hydrogen atmosphere at high temperature, the effect of hydrogen charging on the mechanical performance under static and dynamic conditions was investigated. The stabilizing effect of the optimized chemical composition is reflected in the absence of degradation effects on Yield Stress (YS), Ultimate Tensile Stress (UTS), and fatigue life observed for specimens exposed to hydrogen. Moreover, despite a moderate reduction in the elongation at fracture observed by increasing the hydrogen charging time, ductility loss calculated as Relative Reduction of Area (RRA) remains substantially unaffected by the duration of exposure to hydrogen and demonstrates that the austenitic steel is capable of resisting hydrogen embrittlement (HE). Full article

The research presented in this paper is based on the need for personalized medical implants, whose serial production is impossible, so the need for production process adjustments is inevitable. Conventional production technologies usually set geometrical limitations and generate a lot of waste material, which leads to great expenses, especially when the material used for production is an expensive Ti alloy. Additive technologies offer the possibility to produce a product almost without waste material and geometrical limitations. Nevertheless, the methods developed for additive production using metal powder are not significantly used in biomedicine because there is insufficient data published regarding the properties of additively produced parts, especially from the fatigue and fracture standpoint. The aim of this research is the experimental determination of fracture mechanics properties of additively produced parts and their comparison with the properties of parts produced by conventional technologies. Drawing is the first production process in the comparison, and the second one is selective laser melting (SLM). The Ti-alloy Ti-6Al-7Nb, used for medical implants, was selected for this research. Experimental testing was performed in order to determine ΔK_th fracture mechanics parameters and resistance curves according to ASTM E1820. Test specimen dimensioning and the experiments were carried out according to the respective standards. For the drawn test specimen, the value obtained was ΔK_th = 3.84 MPam^0.5, and the fracture toughness was K_c = 84 MPam^0.5, while for SLM produced test specimens the values were ΔK_th = 4.53 MPam^0.5, and K_c = 21.9 MPam^0.5. Full article

Selective laser melting (SLM) offers a novel approach for manufacturing intricate structures, broadening the application of titanium alloy parts in the aerospace industry. After the build period, heat treatments of annealing (AT) and hot isostatic pressing (HIP) are often implemented, but a comparison of their mechanical performances based on the specimen orientation is still lacking. In this study, horizontally and vertically built Ti6Al4V SLM specimens that underwent the aforementioned treatments, together with their microstructural and defect characteristics, were, respectively, investigated using metallography and X-ray imaging. The mechanical properties and failure mechanism, via fracture analysis, were obtained. The critical factors influencing the mechanical properties and the correlation of the fatigue lives and failure origins were also estimated. The results demonstrate that the mechanical performances were determined by the α-phase morphology and defects, which included micropores and fewer large lack-of-fusion defects. Following the coarsening of the α phase, the strength decreased while the plasticity remained stable. With the discrepancy in the defect occurrence, anisotropy and scatter of the mechanical performances were introduced, which was significantly alleviated with HIP treatment. The fatigue failure origins were governed by defects and the α colony, which was composed of parallel α phases. Approximately linear relationships correlating fatigue lives with the X-parameter and maximum stress amplitude were, respectively, established in the AT and HIP states. The results provide an understanding of the technological significance of the evaluation of mechanical properties. Full article

The aim of translucency-enhancing liquids (TEL) is to locally influence the phase composition of zirconia in order to increase its translucency. This study aimed to determine the influence of TEL on 3Y- and 4Y-TZP zirconia concerning roughness, hardness, wear, flexural strength, dynamic stability and fracture force of fixed dental prostheses after thermal cycling and mechanical loading. Two zirconia materials (4Y-TZP; 3Y-TZP-LA, n = 8 per material and test) were investigated with and without prior application of TEL. Two-body wear tests were performed in a pneumatic pin-on-block design (50 N, 120,000 cycles, 1.6 Hz) with steatite balls (r = 1.5 mm) as antagonists. Mean and maximum vertical loss as well as roughness (Ra, Rz) were measured with a 3D laser-scanning microscope (KJ 3D, Keyence, J). Antagonist wear was determined as percent area of the projected antagonist area. Martens hardness (HM; ISO 14577-1) and biaxial flexural strength (BFS; ISO 6872) were investigated. The flexural fatigue limit BFSdyn was determined under cyclic loading in a staircase approach with a piston-on-three-ball-test. Thermal cycling and mechanical loading (TCML: 2 × 3000 × 5 °C/55 °C, 2 min/cycle, H₂O dist., 1.2 × 10⁶ force á 50 N) was performed on four-unit fixed dental prostheses (FDPs) (n = 8 per group) and the fracture force after TCML was determined. Statistics: ANOVA, Bonferroni test, Kaplan–Meier survival, Pearson correlation; α = 0.05. TEL application significantly influences roughness, hardness, biaxial flexural strength, dynamic performance, as well as fracture force after TCML in 3Y-TZP. For 4Y-TZP, a distinct influence of TEL was only identified for BFS. The application of TEL on 3Y- or 4Y-TZP did not affect wear. TEL application has a strong effect on the mechanical properties of 3Y-TZP and minor effects on 4Y-TZP. All effects of the TEL application are of a magnitude that is unlikely to restrict clinical application. Full article

This study investigates the mechanical behavior of X52 steel pipes and their weld regions under pure hydrogen transport conditions, with a focus on assessing potential hydrogen embrittlement risks. Through experimental analysis, the research evaluates how different pipeline regions—including the base metal, weld metal, and heat-affected zones—respond to varying hydrogen pressures. Key mechanical properties such as elongation, fracture toughness, and crack growth resistance are analyzed to determine their implications for structural integrity and safety. Based on the findings, this study proposes criteria for the safety evaluation of X52 pipelines operating in hydrogen service environments. The results are intended to inform decisions regarding the repurposing of existing pipelines or the design of new infrastructure dedicated to pure hydrogen transport, offering insights into material performance and critical safety considerations for hydrogen pipeline applications. Full article

Aluminium alloy 6082 is widely used in the automotive and aerospace industries due to its high strength-to-weight ratio. However, its structural integrity can sometimes be affected by an early fatigue failure. This study investigates the fatigue performance of extruded 6082-T6 samples through a series of fatigue tests conducted at varying stress levels. The material showed significant variability under identical fatigue conditions, suggesting the presence of microstructural defects. Scanning electron microscopy with energy-dispersive spectroscopy (SEM/EDS) and scanning transmission electron microscopy (S/TEM) were used to identify the nature and location of the defects and evaluate the underlying mechanisms influencing the fatigue performance. Computer tomography (CT) also confirmed the presence of oxide inclusions on the fracture surface and near the edges of the samples. These oxide inclusions are distributed throughout the material heterogeneously and in the form of broken oxide films, suggesting that they might have originated during the material’s early processing stages. These oxides acted as stress concentrators, initiating microcracks that led to catastrophic and unpredictable early failure, ultimately reducing the fatigue life of micro-oxide-containing samples. These results highlight the need for better casting control and improved post-processing techniques to minimise the effect of oxide presence in the final components, thus enhancing their fatigue life. Full article

Magnesium (Mg) alloys have demonstrated tremendous potential in biomedical applications, emerging as promising metallic biomaterials due to their biocompatibility, degradability, and favorable mechanical properties. However, their practical implementation faces significant limitations stemming from mechanical performance degradation and premature fracture failure caused by complex physiological interactions, including flow erosion, corrosion fatigue, stress coupling effects, and dynamic wear under bodily conditions. Surface coating technology has been recognized as an effective strategy to prevent direct contact between magnesium substrates and corrosive media. This review systematically examines the fundamental degradation mechanisms of magnesium alloys in both vivo and vitro environments, presents recent advances in surface modification coatings for magnesium alloys, and critically analyses the interaction mechanisms between modified layers and electrolyte solutions. Special emphasis is placed on revealing the formation mechanisms, structural characteristics, and fracture behaviors of conversion coatings. Furthermore, the study discusses the current challenges in biomedical surface modification of magnesium alloys, proposes potential solutions to enhance their clinical applicability, and outlines future research directions to fully exploit the development potential of these advanced biomaterials. Full article

In composites, fiber–matrix thermal mismatch induces stress heterogeneity that is beyond the resolution of macroscopic approaches. The asymptotic expansion homogenization method is used to create a multi-scale thermo-mechanical coupling model that predicts the elastic modulus, thermal expansion coefficients, and thermal conductivity of ceramic matrix composites at both the macro- and micro-scales. These predictions are verified to be accurate with a maximum relative error of 9.7% between the measured and predicted values. The multi-scale analysis method is then used to guide the vane’s thermal stress analysis, and a macro–meso–micro multi-scale model is created. The thermal stress distribution and stress magnitudes of the guide vane under a transient high-temperature load are investigated. The results indicate that the temperature and thermal stress distributions of the guide vane under the homogenization and lamination theory models are rather comparable, and the locations of the maximum thermal stress are predicted to be reasonably close to one another. The homogenization model allows for the rapid and accurate prediction of the guide vane’s thermal stress distribution. When compared to the macro-scale stress values, the meso-scale predicted stress levels exhibit excellent accuracy, with an inaccuracy of 11.7%. Micro-scale studies reveal significant stress concentrations at the fiber–matrix interface, which is essential for the macro-scale fatigue and fracture behavior of the guide vane. Full article

This study investigates the mechanical behavior and failure characteristics of chain slings under standard and non-standard fastening methods. Through dimensional inspections, fracture tests, and finite element analysis, we identified critical factors influencing chain failure. Chains exhibiting over 10% diameter reduction or increased pitch exceeded discard criteria and showed significant strength loss. Fracture loads in aged chains dropped by more than 35% compared to standards. Structural analysis revealed that standard fastening (using master links) ensures uniform stress distribution and higher load capacity, whereas non-standard fastening (direct wrapping on eyebolts) caused stress concentration, reduced tensile capacity by over 15%, and led to localized failure near contact areas. These results validate the structural soundness of international standards (DIN EN 818-4, ISO 3056) and highlight the risks of improper fastening. Practical recommendations include strict adherence to standard fastening methods, avoidance of direct wrapping, and implementation of regular inspections. The findings emphasize the need for design considerations regarding fastening geometry and suggest further research into fatigue life prediction and contact condition optimization. Full article

The application of additive manufacturing technology in the field of nuclear power is becoming increasingly promising. The low-cycle fatigue behavior of Z2CN19-10 controlled-nitrogen-content stainless steel (SS) was investigated by fatigue equipment, scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and transmission electron microscopy (TEM), including additive manufactured (AM) and forged materials. The results showed that the microstructure of the AM material exhibited anisotropy for the X, Y, and Z directions. The tensile and impact properties of the X, Y, and Z directions in AM material were similar. The fatigue life (N_f) of X- and Y-direction specimens was better than that of Z-direction specimens. The tensile, impact, and fatigue properties of all AM materials were lower than those of the forged specimens. The Z direction specimens of AM material showed the best plastic strain by the highest transition fatigue life (N_T) during the fatigue strain amplitude at 0.3% to 0.6%. The forged specimens showed the best fatigue properties under the plastic strain amplitude control mode. Fatigue fracture surfaces of AM and forged materials exhibited multi- and single-fatigue crack initiation sites, respectively. This could be attributed to the presence of incompletely melted particles and manufacturing defects inside the AM specimens. The dislocation morphology of AM and forged fatigue specimens was observed to study the low-cycle fatigue behaviors in depth. Full article

With the increasing demand for highway maintenance, enhancing the resource utilization of reclaimed asphalt pavement (RAP) has become an urgent and widely studied issue. Although foam asphalt cold recycling technology offers significant benefits in terms of resource utilization and energy saving, it still faces challenges, particularly the poor stability of foam asphalt mixtures. This study focuses on optimizing the performance of foam asphalt recycled mixtures through interface modification, aiming to promote the widespread application of foam asphalt cold recycling technology. Specifically, the research follows these steps: First, the optimal mix ratio of the recycled mixtures was determined based on the fundamental properties of foam asphalt and RAP. Then, zinc oxide, silane coupling agents, and amine anti-stripping agents were introduced to modify the recycled mixtures. At last, a series of tests were conducted to comprehensively evaluate improvements in road performance. The results indicate that the silane coupling agent enhances the low-temperature performance and fatigue. The fracture energy reached 526.71 J/m². Zinc oxide improves the low-temperature cracking resistance and dry shrinkage performance. Amine anti-stripping agents have minimal impact on the low-temperature performance. The linear shrinkage was reduced by 2.6%. The results of TOPSIS indicated that silane coupling agent modification exhibits superior fatigue resistance and low-temperature performance, achieving the highest comprehensive score of 0.666. Although amine-based anti-stripping agents improve fatigue life, they are not suitable for modifying foamed asphalt mixtures due to their detrimental effects on low-temperature performance and moisture resistance. Full article

The cast nickel-based superalloy K417G exhibits excellent high-temperature strength, but non-equilibrium solidification during casting can cause defects such as irreparable interdendritic microporosity, which significantly degrades its fatigue and creep properties. This study uses hot isostatic pressing (HIP) to eliminate internal flaws such as porosity in the K417G alloy, aiming to improve its mechanical properties. We investigated the microstructure and mechanical properties of K417G under two thermal conditions: solution heat treatment (SHT) and hot isostatic pressing (HIP). The results indicate that HIP significantly reduces microporosity. Compared to SHT, HIP improves the mechanical performance of K417G. The creep fracture mechanism shifts from intergranular brittle fracture (SHT) to ductile fracture (HIP). Consequently, HIP increases the alloy′s creep life approximately threefold and raises its fatigue limit by about 20 MPa. This improvement is attributed to pore density reduction, which decreases stress concentration zones and homogenizes the microstructure, thereby impeding fatigue crack nucleation and extending the crack incubation period. Full article

Hydrogen has gradually become one of the indispensable sources of energy for mankind. Since the discovery of hydrogen embrittlement (hydrogen-induced degradation of material properties) more than 100 years ago, fatigue properties in hydrogen environments have been studied. Fatigue crack growth of materials in a hydrogen environment is a complex process involving the interaction of multiple factors. Hydrogen binds to atoms within the material, leading to diffusion and aggregation of hydrogen atoms, which causes an increase in internal stresses. These stresses may concentrate at the crack tip, accelerating the rate of crack expansion and leading to fatigue fracture of the material. The work of current researchers has summarised a number of fatigue models to help understand this phenomenon. This paper firstly summarises the existing hydrogen embrittlement mechanisms as well as hydrogen embrittlement experiments. It then focuses on the mechanism of fatigue crack propagation in hydrogen environments and related literature. It also analyses and summarises a cluster diagram of the literature generated using CiteSpace. The fatigue life prediction methods for materials in hydrogen environment are then summarised in this paper. It aims to provide some guidance for the selection and design of materials in developing fields such as fatigue materials in hydrogen environment. Finally, challenges in the current research on the fatigue properties of materials under hydrogen embrittlement conditions are pointed out and discussed to guide future research efforts. Full article

The use of adhesive joints in naval applications requires a thorough understanding of their fatigue performance. This paper reports on the fatigue experiments performed on double cantilever beam specimens with thick adhesive bondline manufactured under shipyard conditions. The specimens have an initial crack at the steel–adhesive interface and are tested in unaged, salt-spray-aged and immersion-aged conditions to determine the interface mode I fatigue properties. The strain energy release rate is calculated using the Kanninen–Penado model, and the fatigue crack growth curve is determined using a power law model. The crack growth rate slope for salt-spray-aged specimens is 16.5% lower than for unaged specimens, while that for immersion-aged specimens is 66.1% lower and is shown to be significantly different. The fracture surfaces are analyzed to identify the failure mechanisms and the influence of the aging process on the interface properties. Since the specimens are manufactured under shipyard conditions, the presence of voids and discontinuities in the adhesive bondline is observed and as a result leads to scatter. Hence, Bayesian linear regression is performed in addition to the ordinary least squares regression to account for the scatter and provide a distribution of plausible values for the power law coefficients. The results highlight the impact of aging on the fatigue property, underscoring the importance of considering environmental effects in the qualification of such joints for marine applications. Full article