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Keywords = date palm leaves

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28 pages, 4007 KiB  
Article
Voting-Based Classification Approach for Date Palm Health Detection Using UAV Camera Images: Vision and Learning
by Abdallah Guettaf Temam, Mohamed Nadour, Lakhmissi Cherroun, Ahmed Hafaifa, Giovanni Angiulli and Fabio La Foresta
Drones 2025, 9(8), 534; https://doi.org/10.3390/drones9080534 - 29 Jul 2025
Viewed by 248
Abstract
In this study, we introduce the application of deep learning (DL) models, specifically convolutional neural networks (CNNs), for detecting the health status of date palm leaves using images captured by an unmanned aerial vehicle (UAV). The images are modeled using the Newton–Euler method [...] Read more.
In this study, we introduce the application of deep learning (DL) models, specifically convolutional neural networks (CNNs), for detecting the health status of date palm leaves using images captured by an unmanned aerial vehicle (UAV). The images are modeled using the Newton–Euler method to ensure stability and accurate image acquisition. These deep learning models are implemented by a voting-based classification (VBC) system that combines multiple CNN architectures, including MobileNet, a handcrafted CNN, VGG16, and VGG19, to enhance classification accuracy and robustness. The classifiers independently generate predictions, and a voting mechanism determines the final classification. This hybridization of image-based visual servoing (IBVS) and classifiers makes immediate adaptations to changing conditions, providing straightforward and smooth flying as well as vision classification. The dataset used in this study was collected using a dual-camera UAV, which captures high-resolution images to detect pests in date palm leaves. After applying the proposed classification strategy, the implemented voting method achieved an impressive accuracy of 99.16% on the test set for detecting health conditions in date palm leaves, surpassing individual classifiers. The obtained results are discussed and compared to show the effectiveness of this classification technique. Full article
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17 pages, 1414 KiB  
Article
Comparative Genomics and Draft Genome Assembly of the Elite Tunisian Date Palm Cultivar Deglet Nour: Insights into the Genetic Variations Linked to Fruit Ripening and Quality Traits
by Rahma Zarkouna, Afifa Hachef, Carmine Fruggiero, Gaetano Aufiero, Davide D’Angelo, Hedia Bourguiba, Maha Mezghani-Khemakhem, Nunzio D’Agostino and Salwa Zehdi-Azouzi
Int. J. Mol. Sci. 2025, 26(14), 6844; https://doi.org/10.3390/ijms26146844 - 16 Jul 2025
Viewed by 280
Abstract
The date palm (Phoenix dactylifera L.) is a key crop in the arid regions of North Africa and the Middle East, with substantial socioeconomic value. Although multiple genome assemblies have been generated using next-generation sequencing (NGS) technologies, they primarily focus on Middle [...] Read more.
The date palm (Phoenix dactylifera L.) is a key crop in the arid regions of North Africa and the Middle East, with substantial socioeconomic value. Although multiple genome assemblies have been generated using next-generation sequencing (NGS) technologies, they primarily focus on Middle Eastern cultivars, leaving North African varieties unrepresented. This study aims to address this gap by sequencing and assembling the first genome of a North African date palm using Illumina sequencing technology. We present a draft genome assembly of the elite Tunisian variety Deglet Nour. By comparing it with the Barhee BC4 reference genome, we identify key genetic variants, including single nucleotide polymorphisms (SNPs) and insertions/deletions (INDELs), potentially associated with ripening processes and fruit quality. This work expands the genomic resources for date palm research, particularly for North African cultivars, and provides new insights into the nucleotide-level variability of the genes linked to key agronomic traits. Full article
(This article belongs to the Section Molecular Genetics and Genomics)
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22 pages, 7142 KiB  
Article
Smartphone-Based SPAD Value Estimation for Jujube Leaves Using Machine Learning: A Study on RGB Feature Extraction and Hybrid Modeling
by Qi Wang, Ziyan Shi, Kaiyao Hou, Ning Yan, Cuiyun Wu and Xu Li
Sensors 2025, 25(8), 2545; https://doi.org/10.3390/s25082545 - 17 Apr 2025
Viewed by 450
Abstract
Chlorophyll content in date leaves is critical for fruit quality and yield. Traditional detection methods are usually complex and expensive. This study proposes a rapid detection method for chlorophyll content using smartphone images and machine learning and deep learning models. The SPAD values [...] Read more.
Chlorophyll content in date leaves is critical for fruit quality and yield. Traditional detection methods are usually complex and expensive. This study proposes a rapid detection method for chlorophyll content using smartphone images and machine learning and deep learning models. The SPAD values and RGB images of Xinjiang date palm were collected. The RGB images were preprocessed and their color features were extracted using Python and OpenCV. Through correlation analysis, 21 color features highly correlated with chlorophyll content were selected and downscaled with principal component analysis. Models including SVR, RVM, CNN, CNN-SVR, and CNN-RVM were used for prediction. Among them, the CNN-SVR model showed the most stable performance with R2 values of 72.21% and 77.44% on the training and validation sets, respectively, which outperformed the other models. The proposed method is simple, cost-effective, and highly accurate, providing a novel technical approach for accurate management and health monitoring in the date industry. This method has the potential for wide application. Full article
(This article belongs to the Section Smart Agriculture)
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11 pages, 7413 KiB  
Article
In Vitro Initiation, Regeneration, and Characterization of Plants Derived from Mature Tetraploid Floral Explants of Date Palm (Phoenix dactylifera L.)
by Ahmed Othmani, Amel Sellemi, Monia Jemni, Karim Kadri, Leen Leus and Stefaan P. O. Werbrouck
Horticulturae 2024, 10(11), 1206; https://doi.org/10.3390/horticulturae10111206 - 15 Nov 2024
Viewed by 1234
Abstract
A stable tetraploid date palm mutant with the potential for increased fruit size was recovered from a sectorial di-tetraploid chimera via the in vitro culture of flower explants. Callus was induced using 2,4-D, followed by shoot regeneration on a medium containing NAA and [...] Read more.
A stable tetraploid date palm mutant with the potential for increased fruit size was recovered from a sectorial di-tetraploid chimera via the in vitro culture of flower explants. Callus was induced using 2,4-D, followed by shoot regeneration on a medium containing NAA and BAP and rooting with IBA. Regenerated plantlets, confirmed as tetraploid via flow cytometry, were acclimatized and grown for six years. The leaves of tetraploids exhibited significantly wider petiole bases, thicker rachis and spines, broader leaflets, and a more intense green leaf color compared to diploids. However, leaf length, spine count, and overall leaf number were reduced. This is the first report of successful tetraploid recovery from a chimeric date palm, demonstrating the potential of this technique to generate novel germplasm and highlighting the phenotypic differences associated with tetraploidy in this species. Full article
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22 pages, 5884 KiB  
Article
Application of Anionic Hydrogels from Date Palm Waste for Dye Adsorption in Wastewater Treatment
by Farid Fadhillah, Abdulrahman G. Alhamzani, Khaled Bin Bandar, Abdullah Alshamari, Saad Aljlil, Abdelrahman G. Gadallah, M. A. Habib, Mortaga M. Abou-Krisha and Mona A. Abdel-Fatah
Gels 2024, 10(10), 617; https://doi.org/10.3390/gels10100617 - 26 Sep 2024
Cited by 2 | Viewed by 1590
Abstract
This work aimed to develop an anionic cellulose nanofiber (CNF) bio-adsorbent from date palm tree waste and to investigate its removal efficiency compared to cationic methylene blue dye from contaminated water. Date palm pulp was first prepared from date palm leaves through acid [...] Read more.
This work aimed to develop an anionic cellulose nanofiber (CNF) bio-adsorbent from date palm tree waste and to investigate its removal efficiency compared to cationic methylene blue dye from contaminated water. Date palm pulp was first prepared from date palm leaves through acid hydrolysis using H2SO4, followed by hydrolysis in a basic medium using KOH, in which the process completely removed the components of hemicellulose, lignin, and silica. To obtain anionic CNF, the resulting pulp was further treated with H2SO4, followed by centrifugation. Biogel formation of the CNF suspension was promoted by sonication, where its removal efficiency of methylene blue dye was studied as a function of dye concentration, temperature, contact time, and pH value. In this work, we investigated two isotherms, i.e., Langmuir and Freundlich. The Langmuir model’s consistency with the experimental data suggests that the adsorption of methylene blue dye onto CNF is monolayer and surface-limited. The reported maximum removal efficiency of 5 mg/g at 60 °C indicates the optimal temperature for adsorption in this specific case. Additionally, a pseudo-second-order model and Elovich model were also utilized to obtain a better understanding of the adsorption mechanism, in which we found not just physical adsorption but also an indication of a chemical reaction occurring between methylene blue dye and CNF. According to the results, that pseudo-second-order model’s consistency with the experimental data suggests that the adsorption of methylene blue (MB) onto CNF is rate-limiting step involving chemisorption between the two. The study reveals that CNF adsorbents derived from renewable natural waste sources such as date palm leaves can be effective in removing cationic contaminants such as methylene blue dye. Full article
(This article belongs to the Section Gel Processing and Engineering)
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24 pages, 2934 KiB  
Article
Modeling the Performance Parameters of Pollen Grains of Male Date Palms Using an Artificial Neural Network Based on the Mineral Composition and Morphological Properties of Their Leaves
by Saleh M. Al-Sager, Mahmoud Abdel-Sattar, Rashid S. Al-Obeed, Saad S. Almady and Abdulwahed M. Aboukarima
Horticulturae 2024, 10(7), 741; https://doi.org/10.3390/horticulturae10070741 - 13 Jul 2024
Cited by 1 | Viewed by 1268
Abstract
One of the key factors for sustainability in agricultural systems, particularly, for cultivation of date palms, is the identification of the performance parameters of the pollen grains of male date palms (Phoenix dactylifera L.). This study was carried out to predict the [...] Read more.
One of the key factors for sustainability in agricultural systems, particularly, for cultivation of date palms, is the identification of the performance parameters of the pollen grains of male date palms (Phoenix dactylifera L.). This study was carried out to predict the performance parameters of pollen grains using an artificial neural network (ANN) model. The morphological features of spathe length, spathe weight, number of pinnae per leaf, leaf length, leaf width, length of the pinna part, pinna length, pinna width, length of the spathe stem, and spathe width, as well as the concentrations of minerals such as Mg, N, K, P, and Ca in their leaves were used as inputs to the ANN model. For this purpose, we collected the required data from nine male date palms grown in Saudi Arabia. The ANN model utilized in this work included an input layer with 15 parameters, a hidden layer of 30 neurons, and an output layer with 8 neurons. The ANN model was trained with 27 patterns. Seven patterns were utilized for testing purposes. The coefficient of determination (R2) obtained between the observed and predicted performance parameters’ values using the testing dataset was 0.902 for the number of strands per spathe, 0.967 for strand length, 0.963 for the number of flowers per strand, 0.941 for the number of flowers per spathe, 0.985 for the weight of pollen grains per spathe, 0.810 for the pollen grains’ viability, 0.936 for the pollen grains’ length, and 0.992 for the pollen grains’ width. The length of the spathe stem had the most critical effect on how the ANN model predicted the values of the dependent variables, i.e., the number of strands per spathe, with a percentage of contribution of 17.66%; the weight of pollen grains per spathe, with 17.85%; the pollen grains’ length, with 19.78%, and the pollen grains’ width, with a percentage of contribution of 30.59%. Spathe weight had the most critical influence on strand length and pollen grains’ viability, with percentages of 26.29% and 14.92%, respectively. Leaf width had the most critical effect on the number of flowers per spathe, with a percentage of 12.55%. The elemental concentration of K in the male date palm leaves had the most critical effect on the number of flowers per strand, with a percentage of 13.98%. It was therefore concluded that using a modeling process with the ANN technique can help estimate the performance parameters of male date palms’ pollen grains for different purposes, such as providing a starting point for mathematical analyses associated with the physiological mechanisms of male date palm. Moreover, the outcomes of this research work can be supportive as a practical tool in this field of study. Full article
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15 pages, 4853 KiB  
Article
Experimental Study on the Effect of Date Palm Powder on the Thermal and Physico-Mechanical Properties of Gypsum Mortars
by Mohamed Aymen Kethiri, Noureddine Belghar, Mourad Chikhi, Yousra Boutera, Charafeddine Beldjani and Cristina Tedeschi
Sustainability 2024, 16(7), 3015; https://doi.org/10.3390/su16073015 - 4 Apr 2024
Cited by 2 | Viewed by 2506
Abstract
Date palm leaves have been diachronically applied in building materials in the Middle East and North Africa (MENA) region, so as to enhance specific properties, such as volume stability and strength. This research work concerns an experimental study on the impact of date [...] Read more.
Date palm leaves have been diachronically applied in building materials in the Middle East and North Africa (MENA) region, so as to enhance specific properties, such as volume stability and strength. This research work concerns an experimental study on the impact of date palm leaflet powder (DPLP) on the thermal and physico-mechanical properties of gypsum mortars. A series of mortar compositions were prepared with different proportions of DPLP (0, 1, 3, and 5% w/w of binder) and variant particle size (0.5, 1, and 1.5 mm). The results showed that the mortars containing DPLP exhibited significant changes in their properties due to variations in DPLP concentration and particle size. Increased DPLP led to lower density, higher porosity, and water absorption rate, whereas mechanical strength and thermal conductivity were decreased according to the DPLP proportion and size. This research provides valuable insights into the use of sustainable and renewable building materials, highlighting the benefits of exploiting agricultural waste in the constructional sector. The findings lay the groundwork for future research and innovation in environmentally friendly construction technologies. Full article
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18 pages, 3229 KiB  
Article
Pervious Concrete Made with Recycled Coarse Aggregate and Reinforced with Date Palm Leaves Fibers
by Adil Tamimi, Sami W. Tabsh and Magdi El-Emam
Materials 2023, 16(23), 7496; https://doi.org/10.3390/ma16237496 - 4 Dec 2023
Cited by 8 | Viewed by 2798
Abstract
This study considers 12 pervious concrete mixes incorporating 100% recycled coarse aggregate from old concrete demolition waste and containing various amounts of natural fine aggregate and date palm leaves fibers. First, the properties of the recycled aggregate in terms of their particle size [...] Read more.
This study considers 12 pervious concrete mixes incorporating 100% recycled coarse aggregate from old concrete demolition waste and containing various amounts of natural fine aggregate and date palm leaves fibers. First, the properties of the recycled aggregate in terms of their particle size distribution, abrasion resistance, crushing values, specific gravity and water absorption are obtained. Next, the pervious concrete density, compressive strength, tensile strength, permeability and porosity are determined by experimental testing following the relevant standards. The results are analyzed and compared to determine the influence of using recycled coarse aggregate in the mixtures and the impact of the amount of natural sand and volume fraction of the fibers on the mechanical properties, permeability and porosity of the concrete. Findings of the study showed that the use of recycled coarse aggregate in pervious concrete without fine aggregate reduced the compressive strength by 36% and tensile strength by 57%. Replacing 11.7% of the recycled coarse aggregate with natural sand and adding date palm leaves fibers in an amount equivalent to 0.64% volumetric content to such concrete helped increase the compressive strength by 16.2% and tensile strength by 3.2% above the corresponding strengths of the control mix. There is a clear relationship between permeability and porosity due to their correlation with the density of pervious concrete, and the effect of porosity on tensile strength is more influential than it is on the compressive strength. An equation that can predict the tensile strength of pervious concrete from the compressive strength is proposed, as a function of the natural fine aggregate fraction of the coarse aggregate and volumetric content of natural fibers. Results of the research confirm the feasibility of using recycled aggregate in pervious concrete mixes and the positive impact of natural fibers on the mechanical properties. Full article
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27 pages, 8233 KiB  
Article
Drought-Tolerance Screening of Date Palm Cultivars under Water Stress Conditions in Arid Regions
by Hassan Ali-Dinar, Muhammad Munir and Maged Mohammed
Agronomy 2023, 13(11), 2811; https://doi.org/10.3390/agronomy13112811 - 13 Nov 2023
Cited by 14 | Viewed by 2764
Abstract
Drought stress poses a considerable challenge to agriculture sustainability in arid regions. Water scarcity severely affects date palm growth and productivity in these regions. However, as water resources become increasingly scarce in arid regions, understanding the drought tolerance of date palm cultivars becomes [...] Read more.
Drought stress poses a considerable challenge to agriculture sustainability in arid regions. Water scarcity severely affects date palm growth and productivity in these regions. However, as water resources become increasingly scarce in arid regions, understanding the drought tolerance of date palm cultivars becomes imperative for developing drought-resistant cultivars and optimizing irrigation water usage for sustainable agriculture. This research examines the impact of different drought stress levels based on evapotranspiration (ETc), i.e., 40%, 60%, 80%, and 100% ETc, and time intervals (0, 6, 12, 18, and 24 months) on leaf growth, net photosynthesis, chlorophyll a and b content, and leaf relative water content (LRWC) of four prominent date palm cultivars, Khalas, Barhee, Hilali, and Ashrasee. In addition, the study also examines the effects of drought stress on dry weight, potassium and calcium content of leaf, stem, and root, and proline content in fresh leaves of these four cultivars. A solar-powered drip irrigation system with automated time-based irrigation scheduling was used to accurately control the irrigation water amount. To real-time estimate ETc in the study area, meteorological data were collected using a cloud-based IoT system. The findings of this study revealed that severe drought conditions (40 and 60 % ETc) significantly reduced leaf growth, plant dry biomass, and physiological and biochemical attributes; however, date palm cultivars can be grown under moderate drought conditions (80% ETc) with minimal effect on phenotypic, physiological, and biochemical traits to conserve water. The study also revealed that the drought-related characteristics decreased gradually with an increase in water stress time over 24 months. Comparing the date palm cultivars revealed that the Khalas and Barhee cultivars are more drought-tolerant, followed by Hilali, while Ashrasee is susceptible. The study elucidated a water conservation strategy employed in response to drought-induced stress based on the physiological and morphological parameters of date palm cultivars. It provides valuable insights into irrigation practices in arid regions. However, future studies can be focused on other nondestructive innovative techniques such as pulse-amplitude-modulation (PAM) fluorimetry, infrared radiation (IR), and video imaging system (VIS) methods to identify drought stress in date palms. Full article
(This article belongs to the Special Issue Plant–Water Relationships for Sustainable Agriculture)
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18 pages, 1179 KiB  
Article
Chemical Characterization and Antifungal Activity of Blue Tansy (Tanacetum annuum) Essential Oil and Crude Extracts against Fusarium oxysporum f. sp. albedinis, an Agent Causing Bayoud Disease of Date Palm
by Hajar Ettakifi, Kaoutar Abbassi, Safae Maouni, El Hadi Erbiai, Abderrahmane Rahmouni, Mounir Legssyer, Rabah Saidi, Zouhaire Lamrani, Joaquim C. G. Esteves da Silva, Eugénia Pinto and Abdelfettah Maouni
Antibiotics 2023, 12(9), 1451; https://doi.org/10.3390/antibiotics12091451 - 16 Sep 2023
Cited by 7 | Viewed by 2872
Abstract
Tanacetum annuum L. is a Mediterranean plant, commonly known as Blue Tansy due to its blue colour as an essential oil, which is widely used for medicinal purposes. However, there are no studies on the bioactive compounds (especially, phenolic compounds) and the biological [...] Read more.
Tanacetum annuum L. is a Mediterranean plant, commonly known as Blue Tansy due to its blue colour as an essential oil, which is widely used for medicinal purposes. However, there are no studies on the bioactive compounds (especially, phenolic compounds) and the biological properties of their organic extracts. Herein, the purpose of the present work was to investigate the chemical composition of the essential oil and crude extracts of the T. annuum aerial parts collected from northern Morocco and to evaluate their antioxidant and antifungal activity against Fusarium oxysporum f. sp. albedinis, an agent causing Bayoud disease of the date palm, an important food source and commercial perennial crop in the Sahara and North Africa. Chemically, Folin–Ciocalteu and aluminium chloride colourimetric methods were used to determine the total phenolic (TPC) and total flavonoid (TFC) contents, respectively; polyphenols were characterized using HPLC-MS, while GC-MS was used to analyse the essential oil composition. Moreover, the evaluation of antioxidant and antifungal activities was carried out using the DPPH test and microdilution method, respectively. The results showed that the three T. annuum parts (stems, leaves and flowers) extracts contained important TPC and TFC with values varied between 51.32 and 116.32 mg/g of dry crude extract (DCE). HPLC-MS analysis revealed the identification and quantification of 19 phenolic acids and flavonoids with an emphasis on apigenin 7-glucoside (4540 µg/g of dry weight (DW)), luteolin 7-glucoside (2804 µg/g DW) and salicylic acid (1878 µg/g DW). Additionally, 39 biomolecules were identified in the essential oil using GC-MS, which were predominated by camphor (16.69%), α-pinene (12.37%), bornyl acetate (11.97%) and limonene (11.10%). The methanolic and hydro-methanolic extracts of T. annuum parts demonstrated a strong antioxidant property with IC50 values ranging between 0.22 and 0.65 mg/mL. Concerning antifungal activity, the essential oil and crude extracts of the Moroccan Blue Tansy exhibited a potent capacity against F. oxysporum f. sp. albedinis at low concentrations, with MIC and MFC values of 3.33 and 4.58 µL/mL for the essential oil and values of 3.33 and 9.17 mg/mL for crude extracts, respectively. Overall, these results demonstrated T. annuum as an important source of bioactive compounds and contribute significantly to the potential of using essential oils and extracts for controlling the Bayoud disease of date palms. Moreover, the finding suggests that T. annuum can be highly useful for phytosanitary and pharmaceutical industries. Full article
(This article belongs to the Special Issue Medicinal Plants as a Source of Novel Classes of Antimicrobial Agents)
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18 pages, 3100 KiB  
Article
Preparation, Characterization, and Chemically Modified Date Palm Fiber Waste Biomass for Enhanced Phenol Removal from an Aqueous Environment
by Nadavala Siva Kumar, Mohammad Asif, Anesh Manjaly Poulose, Ebrahim H. Al-Ghurabi, Shaddad S. Alhamedi and Janardhan Reddy Koduru
Materials 2023, 16(11), 4057; https://doi.org/10.3390/ma16114057 - 30 May 2023
Cited by 12 | Viewed by 2247
Abstract
The date palm tree is extensively cultivated in Middle Eastern countries such as Saudi Arabia, generating a large amount of waste in the form of leaves, seeds, and fibrous materials. This study examined the feasibility of using raw date palm fiber (RDPF) and [...] Read more.
The date palm tree is extensively cultivated in Middle Eastern countries such as Saudi Arabia, generating a large amount of waste in the form of leaves, seeds, and fibrous materials. This study examined the feasibility of using raw date palm fiber (RDPF) and NaOH chemically modified date palm fiber (NaOH–CMDPF) obtained from discarded agricultural waste for the removal of phenol in an aqueous environment. The adsorbent characterization was performed by using different techniques, i.e., particle size analysis; elemental analyzer (CHN); and BET, FTIR, and FESEM-EDX analysis. The FTIR analysis revealed the presence of various functional groups on the surface of the RDPF and NaOH–CMDPF. The results showed that chemical modification by NaOH increased the phenol adsorption capacity that was well-fitted by the Langmuir isotherm. Higher removal was obtained with NaOH–CMDPF (86%) than with the RDPF (81%). The RDPF and NaOH–CMDPF sorbents’ maximum (Qm) adsorption capacities were more than 45.62 mg/g and 89.67 mg/g and were comparable to the sorption capacities of various other types of agricultural waste biomass reported in the literature. The kinetic studies confirmed that the adsorption of phenol followed the pseudo-second-order kinetic process. The present study concluded that the RDPF and NaOH–CMDPF were eco-friendly and cost-effective in promoting sustainable management and the reuse of the Kingdom’s lignocellulosic fiber waste material. Full article
(This article belongs to the Special Issue Sustainable Nanocomposites and Technologies for Water Treatment)
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24 pages, 5099 KiB  
Article
Date Palm Tree Leaf-Derived Cellulose Nanocrystal Incorporated Thin-Film Composite forward Osmosis Membranes for Produced Water Treatment
by Asif Saud, Haleema Saleem, Aquib Wakeel Khan, Nazmin Munira, Maryam Khan and Syed Javaid Zaidi
Membranes 2023, 13(5), 513; https://doi.org/10.3390/membranes13050513 - 13 May 2023
Cited by 11 | Viewed by 2834
Abstract
Worldwide water shortage and significant issues related to treatment of wastewater streams, mainly the water obtained during the recovery of oil and gas operations called produced water (PW), has enabled forward osmosis (FO) to progress and become advanced enough to effectively treat as [...] Read more.
Worldwide water shortage and significant issues related to treatment of wastewater streams, mainly the water obtained during the recovery of oil and gas operations called produced water (PW), has enabled forward osmosis (FO) to progress and become advanced enough to effectively treat as well as retrieve water in order to be productively reused. Because of their exceptional permeability qualities, thin-film composite (TFC) membranes have gained increasing interest for use in FO separation processes. This research focused on developing a high water flux and less oil flux TFC membrane by incorporating sustainably developed cellulose nanocrystal (CNC) onto the polyamide (PA) layer of the TFC membrane. CNCs are prepared from date palm leaves and different characterization studies verified the definite formations of CNCs and the effective integration of CNCs in the PA layer. From the FO experiments, it was confirmed that that the membrane with 0.05 wt% of CNCs in the TFC membrane (TFN-5) showed better FO performance in PW treatment. Pristine TFC and TFN-5 membrane exhibited 96.2% and 99.0% of salt rejection and 90.5% and 97.45% of oil rejection. Further, TFC and TFN-5 demonstrated 0.46 and 1.61 LMHB pure water permeability and 0.41 and 1.42 LHM salt permeability, respectively. Thus, the developed membrane can help in overcoming the current challenges associated with TFC FO membranes for PW treatment processes. Full article
(This article belongs to the Special Issue Sustainable Membrane Processes of Water Recycling and Purification)
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20 pages, 3233 KiB  
Article
Exploitation of Sugarcane Bagasse and Environmentally Sustainable Production, Purification, Characterization, and Application of Lovastatin by Aspergillus terreus AUMC 15760 under Solid-State Conditions
by Ahmed M. A. A. Ramadan, Reda M. Shehata, Hussein H. EL-Sheikh, Fuad Ameen, Steven L. Stephenson, Sabry A. H. Zidan and Osama A. M. Al-Bedak
Molecules 2023, 28(10), 4048; https://doi.org/10.3390/molecules28104048 - 12 May 2023
Cited by 9 | Viewed by 4472
Abstract
Using the internal transcribed spacer (ITS) region for identification, three strains of Aspergillus terreus were identified and designated AUMC 15760, AUMC 15762, and AUMC 15763 for the Assiut University Mycological Centre culture collection. The ability of the three strains to manufacture lovastatin in [...] Read more.
Using the internal transcribed spacer (ITS) region for identification, three strains of Aspergillus terreus were identified and designated AUMC 15760, AUMC 15762, and AUMC 15763 for the Assiut University Mycological Centre culture collection. The ability of the three strains to manufacture lovastatin in solid-state fermentation (SSF) using wheat bran was assessed using gas chromatography-mass spectroscopy (GC-MS). The most potent strain was strain AUMC 15760, which was chosen to ferment nine types of lignocellulosic waste (barley bran, bean hay, date palm leaves, flax seeds, orange peels, rice straw, soy bean, sugarcane bagasse, and wheat bran), with sugarcane bagasse turning out to be the best substrate. After 10 days at pH 6.0 at 25 °C using sodium nitrate as the nitrogen source and a moisture content of 70%, the lovastatin output reached its maximum quantity (18.2 mg/g substrate). The medication was produced in lactone form as a white powder in its purest form using column chromatography. In-depth spectroscopy examination, including 1H, 13C-NMR, HR-ESI-MS, optical density, and LC-MS/MS analysis, as well as a comparison of the physical and spectroscopic data with published data, were used to identify the medication. At an IC50 of 69.536 ± 5.73 µM, the purified lovastatin displayed DPPH activity. Staphylococcus aureus and Staphylococcus epidermidis had MICs of 1.25 mg/mL, whereas Candida albicans and Candida glabrata had MICs of 2.5 mg/mL and 5.0 mg/mL, respectively, against pure lovastatin. As a component of sustainable development, this study offers a green (environmentally friendly) method for using sugarcane bagasse waste to produce valuable chemicals and value-added commodities. Full article
(This article belongs to the Special Issue Discovery of Bioactive Ingredients from Natural Products, 4th Edition)
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27 pages, 5655 KiB  
Article
Utilization of Prepared Nanocellulose as a Biopolymer for Adsorption Kinetics of Cobalt Ions from Wastewater
by Khaled Bin Bandar and Saad Aljlil
Polymers 2023, 15(9), 2143; https://doi.org/10.3390/polym15092143 - 30 Apr 2023
Cited by 8 | Viewed by 2242
Abstract
This study evaluated nanocellulose derived from discarded palm leaves for its ability to remove cobalt ions from industrial wastewater. The process involved extracting cellulose nanocrystals (CNCs) from date palm leaves through a series of repeated chemical treatments. The study examined the adsorption rates [...] Read more.
This study evaluated nanocellulose derived from discarded palm leaves for its ability to remove cobalt ions from industrial wastewater. The process involved extracting cellulose nanocrystals (CNCs) from date palm leaves through a series of repeated chemical treatments. The study examined the adsorption rates of cobalt ions under various conditions using different techniques. Two equilibrium models, the Langmuir and Freundlich models, were employed, and the Langmuir model was found to be consistent with the experimental data. The maximum amount of cobalt ions adsorbed at room temperature was 5.98 mg/g. Furthermore, several kinetic models were used to gain insight into the adsorption mechanism, including the pseudo-first-order, pseudo-second-order, Elovich, and intraparticle diffusion models. The pseudo-second-order model provided an accurate description of the adsorption process, while the Elovich equation suggested a chemical reaction between cobalt ions and nanocellulose, involving multiple chemical reactions and mass-transfer processes. Kinetic parameters were critical in interpreting the results, and the study’s findings were in agreement with the pseudo-second-order and intraparticle models, indicating general chemical reactions and diffusion resistance. Full article
(This article belongs to the Section Biobased and Biodegradable Polymers)
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16 pages, 4452 KiB  
Article
TPD1-like Gene as a Suitable Marker for Early Sex Determination in Date Palm (Phoenix dactylifera L.)
by Plosha Khanum, Asif Ali Khan, Iqrar Ahmad Khan, Abdul Ghaffar and Zulqurnain Khan
Genes 2023, 14(4), 907; https://doi.org/10.3390/genes14040907 - 13 Apr 2023
Cited by 3 | Viewed by 4714
Abstract
Date palm (Phoenix dactylifera L.) is a considerably beneficial and economically profitable fruit crop. Female date palm plants produce fruit that is rich in fiber and sugar. Date palm is propagated by two means: suckers and seed. The propagation of date palm [...] Read more.
Date palm (Phoenix dactylifera L.) is a considerably beneficial and economically profitable fruit crop. Female date palm plants produce fruit that is rich in fiber and sugar. Date palm is propagated by two means: suckers and seed. The propagation of date palm through seeds is very necessary for germplasm conservation and breeding. The late reproductive age (4–5 years) and dioecious nature of date palm make genetic improvement and breeding difficult. Early sex determination is the only way to improve breeding by selecting experimental male and female plants at the seedling stage. The primers for Tapetum Determinant 1 (TPD1-like) were designed using Amplify software. The DNA amplification of selected date palm suckers of three genotypes (Ajwa, Amber, and Medjool) was observed through PCR. Expression profiling of selected genotypes was carried out through semi-q PCR and RT-PCR by using the cDNA of suckers and unknown seedlings. Different in silico analyses were performed for the gene and protein characterization and identification of cis-acting elements in the promoter region. The promoter was identified along with the protein’s properties and functionality. The expression of TPD1-like gene was found in the leaves of three selected genotypes of male sucker and in some plants of selected unknown seedlings that are considered male plants, and no expression was observed in female suckers and unknown seedlings that are considered female plants. The findings suggested that the TPD1-like gene has the potential for sex differentiation at the seedling stage, as the TPD1-like gene is essential to the specialization of tapetal cells and plays a critical role in plant reproduction. Full article
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