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Search Results (307)

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25 pages, 17296 KB  
Article
A Study on the Long-Term Performance Evaluation of Carbon-Fiber Reinforced Polymer (CFRP) Tendon
by Jongeok Lee, Sung-Jin Lee and Woo-Tai Jung
Fibers 2026, 14(6), 74; https://doi.org/10.3390/fib14060074 - 17 Jun 2026
Viewed by 176
Abstract
Carbon-fiber reinforced polymer (CFRP) tendons have attracted increasing attention as corrosion-resistant prestressing elements for prestressed concrete and cable-supported structures; however, their practical implementation requires reliable verification of long-term mechanical performance and anchorage reliability. In this study, a 9.5 mm pultruded CFRP tendon and [...] Read more.
Carbon-fiber reinforced polymer (CFRP) tendons have attracted increasing attention as corrosion-resistant prestressing elements for prestressed concrete and cable-supported structures; however, their practical implementation requires reliable verification of long-term mechanical performance and anchorage reliability. In this study, a 9.5 mm pultruded CFRP tendon and compression-type anchorage system were developed and experimentally evaluated through relaxation, creep rupture, and fatigue tests. The tendon exhibited a tensile strength of 2501 MPa and an elastic modulus of 132.5 GPa. Relaxation tests were conducted at an initial load corresponding to 70% of the ultimate tensile capacity, and the measured relaxation loss after 1000 h was 1.02%. Based on logarithmic regression of the measured data, the relaxation loss at 1,000,000 h was estimated to be 2.11%; however, this value should be interpreted as an extrapolated long-term estimate rather than a directly verified result. Creep rupture tests performed at load ratios of 82.4–100.0% yielded an estimated 1,000,000 h creep rupture load ratio of approximately 80%, although the prediction is subject to uncertainty because of the limited number of specimens and scatter in rupture times. Fatigue tests indicated that the CFRP tendon–anchorage assembly maintained stable performance up to 2,000,000 cycles without measurable degradation in elastic stiffness under the adopted loading conditions. These results suggest that the developed CFRP tendon–anchorage system has promising potential for prestressing applications, while further long-term tests with a larger number of specimens are required to improve the statistical reliability of the extrapolated relaxation and creep rupture predictions. Full article
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20 pages, 13953 KB  
Article
A Lifetime Consumption Model for Combined Creep and Fatigue Loading of Aluminum Bonding Wires
by Holm Altenbach, Cassandra Moers and Christian Dresbach
Appl. Sci. 2026, 16(12), 6058; https://doi.org/10.3390/app16126058 - 15 Jun 2026
Viewed by 119
Abstract
(1) Aluminum bonding wires are mostly used for electrical contact and transmission of electrical signals in power electronic modules. Combined cyclical mechanical and thermal loads acting on the wires can lead to premature failure of the whole module. For this purpose, based on [...] Read more.
(1) Aluminum bonding wires are mostly used for electrical contact and transmission of electrical signals in power electronic modules. Combined cyclical mechanical and thermal loads acting on the wires can lead to premature failure of the whole module. For this purpose, based on extensive fatigue tests on a 300 µm Al-Pure wire, the authors developed, calibrated and applied a fatigue life model for a cycle range of R=0.1 to R=0.7 to other comparable aluminum wires in two previous publications. (2) Since the model is supposed to be used in an FEM post-processor for predicting the lifetime of wire bridges, the existing model was expanded in the following work. (3) Temperature dependence is included in the fatigue model, and it is made more robust in the whole possible R-range to be able to cope with the highly variable load cases in real components. In addition, a creep rupture model was developed and combined with the fatigue model by linear damage accumulation. (4) The applicability of the lifetime consumption model is demonstrated for several combined load cases. It is shown that it is necessary to consider both fatigue and creep in a combined model for a reliable lifetime prediction. Otherwise, the lifetime could be underestimated by several orders of magnitude, depending on the load case. Full article
(This article belongs to the Special Issue Fatigue and Fracture Behavior of Engineering Materials)
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20 pages, 10213 KB  
Article
GA/KH792 Surface Chemical Co-Modification for Enhancing Performance and Interfacial Properties of PET Fiber-Reinforced Asphalt Mastic
by Yingdong Zhao, Jiefen Kang, Yanan Guo, Yongling Ding, Huiling Yu, Qinxi Dong, Huadong Sun, Wenshu Cheng, Shuhua Song, Hong Yin and Kunpeng Zhao
Coatings 2026, 16(6), 703; https://doi.org/10.3390/coatings16060703 - 11 Jun 2026
Viewed by 190
Abstract
Polyester (PET) fibers are widely used to reinforce asphalt materials; however, their smooth and hydrophobic surfaces limit interfacial bonding and restrict their reinforcing efficiency. This study develops an eco-friendly surface modification method based on the chemical modification of gallic acid (GA) and aminosilane [...] Read more.
Polyester (PET) fibers are widely used to reinforce asphalt materials; however, their smooth and hydrophobic surfaces limit interfacial bonding and restrict their reinforcing efficiency. This study develops an eco-friendly surface modification method based on the chemical modification of gallic acid (GA) and aminosilane (KH792) to enhance the compatibility between PET fibers and asphalt. Modified fibers with various molar ratios of GA/KH792 were prepared and incorporated into asphalt mastic. Their performance was evaluated using softening point, cone penetration, dynamic shear rheometer (DSR), multiple stress creep recovery (MSCR), linear amplitude sweep (LAS), and bending beam rheometer (BBR) tests, combined with interfacial interaction analysis and scanning electron microscopy (SEM). The results show that surface modification significantly improves the reinforcing effect of PET fibers. In particular, the co-modified fiber with a GA/KH792 ratio of 1:1 exhibits the best performance, with increases of 27% in softening point and 105% in shear strength, as well as notable improvements in rutting resistance, fatigue performance, and temperature stability. Interfacial indices and SEM observations confirm enhanced adhesion, dispersion, and load transfer capacity. However, the improvement in low-temperature performance is limited. Overall, GA/KH792 chemical modification effectively enhances fiber asphalt interfacial interaction and provides a simple and sustainable approach for developing high-performance asphalt materials. Full article
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29 pages, 1713 KB  
Article
Preparation and Rheological Properties of Waterborne Epoxy Resin Emulsified Asphalt
by Siyu Wu, Huaxin Chen, Suining Zheng, Yonglu Dong and Wenlan Zhang
Materials 2026, 19(12), 2493; https://doi.org/10.3390/ma19122493 - 10 Jun 2026
Viewed by 198
Abstract
To address the lack of systematic quantitative studies on waterborne epoxy resin (WER)-modified emulsified asphalt regarding its rheological optimization and engineering applicability, this study fills the gap by preparing WER-modified emulsified asphalt via a two-step process. New findings reveal that 20% WER content [...] Read more.
To address the lack of systematic quantitative studies on waterborne epoxy resin (WER)-modified emulsified asphalt regarding its rheological optimization and engineering applicability, this study fills the gap by preparing WER-modified emulsified asphalt via a two-step process. New findings reveal that 20% WER content significantly enhances elastic components, creep–recovery, fatigue life, and fracture energy. The main objective is to establish a theoretical basis for high-performance pavement materials. Modified emulsified asphalt specimens with different waterborne epoxy resin contents were prepared using a two-step method of “emulsification followed by compounding”. The stability of the emulsions was quantitatively evaluated by zeta potential, storage stability, particle size distribution, and demulsification time. Their rheological parameters, multi-stress creep–recovery characteristics, fatigue life, and low-temperature crack resistance were systematically tested across the full temperature range using a dynamic shear rheometer and a bending beam rheometer. In addition, the bonding performance, strength development behavior, and water resistance durability were comprehensively assessed through pull-out tests, Marshall stability and splitting strength tests, as well as freeze–thaw cycle tests. These properties were compared with those of unmodified emulsified asphalt (UEA-0) and SBR-modified emulsified asphalt (SBR-EA). With an increase in waterborne epoxy resin content, the elastic component of the modified asphalt improved significantly, and the phase angle continuously decreased. The specimen with 20% waterborne epoxy resin content (WER-EA-20) exhibited the best performance: its phase angle was lower than those of the other groups under high-, medium-, and low-temperature conditions. After seven creep–recovery cycles, its creep–recovery rate remained at 33%, substantially higher than the 8% observed for the unmodified specimen. The fatigue life reached 15,000 cycles under a shear stress of 2.1 MPa. At −10 °C, the fracture strength was 0.92 MPa, and the fracture energy reached 21.4 J. Furthermore, the pull-out strength of WER-EA-20 was 0.86 MPa, with the failure mode identified as asphalt cohesive failure. After 37 days of curing, the Marshall stability reached 22.5 kN, and the splitting strength was 1.36 MPa. After 40 freeze–thaw cycles, the freeze–thaw splitting strength ratio (TSR) of WER-EA-20 remained above 75%, representing an improvement of more than 110% compared to the unmodified UEA-0 (TSR ≈ 35.5%), which highlights the significant enhancement in water resistance imparted by the waterborne epoxy resin. Compared to SBR-EA, WER-EA-20 has a higher softening point, a lower suitable mixing temperature, and better anti-aging properties. Waterborne epoxy resin can effectively improve the viscoelastic properties and overall road performance of emulsified asphalt, and the modification effect increases with increasing dosage. Full article
(This article belongs to the Special Issue Mechanical Dynamics and Rheological Insights in Advanced Materials)
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16 pages, 1916 KB  
Article
Study on the Modification Mechanism and Rheological Properties of Bio-Oil-Based Composite-Modified Material for TOP-DOWN Crack Treatment in Long-Life Pavement
by Haining Wang, Xiangpeng Yan, Qingming Wang, Wenjuan Wu, Yao Tian and Qinsheng Xu
J. Compos. Sci. 2026, 10(6), 298; https://doi.org/10.3390/jcs10060298 - 29 May 2026
Viewed by 258
Abstract
To address the durability limitations of conventional crack sealants under coupled extreme temperatures and traffic loads in long-life pavements, a bio-oil composite-modified patching material was developed using 90# base asphalt as the matrix, synergistically modified with crumb rubber (CR) and epoxidized soybean oil [...] Read more.
To address the durability limitations of conventional crack sealants under coupled extreme temperatures and traffic loads in long-life pavements, a bio-oil composite-modified patching material was developed using 90# base asphalt as the matrix, synergistically modified with crumb rubber (CR) and epoxidized soybean oil (ESO). To resolve the contradictory requirements for high elasticity and thermal expansion/contraction coordination in sealants, ESO was introduced; its polar epoxy groups optimize phase compatibility and promote low-temperature stress relaxation without restricting thermal deformability. Rheological evaluations revealed that the optimal system (OPT) successfully extended the service temperature window from PG 76–−24 °C (baseline) to PG 82–−24 °C, significantly enhancing its adaptability to extreme climatic fluctuations. At −24 °C, OPT exhibited a reduced creep stiffness (S) of 164 MPa and an increased creep rate (m) of 0.312, with a cracking resistance ratio (k) as low as 525.6; the quantitative significance of these metrics lies in granting the sealant superior stress relaxation capacity, enabling it to accommodate dynamic crack widening without interfacial debonding or brittle fracture. Fatigue testing via time sweeps demonstrated that Nf50 reached 2890 cycles, highlighting robust long-term resistance against high-frequency shear strains induced by tire edges. Micro-mechanistic analyses (FTIR, TG/DTG, and DSC) confirmed that the modification is primarily driven by physical blending. The elevation of the thermal decomposition threshold (T5%) to 302.4 °C and the residue at 600 °C to 44.8% provide a critical safety margin for high-temperature construction heating, preventing thermal degradation. Furthermore, the glass transition temperature (Tg) decreased to approximately −35.2 °C. These findings establish a rigorous quantitative and mechanistic framework for designing sustainable, high-performance patching materials for resilient pavement maintenance. Full article
(This article belongs to the Special Issue Advanced Composite Materials for Civil Construction Applications)
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28 pages, 6587 KB  
Article
Synergistic Effects of Multi-Walled Carbon Nanotubes and SBS on Asphalt Binder Performance
by Amjad H. Albayati, Hasan M. Al-Mosawe, Ahmed M. Mohammed, Mayank Sukhija, Aliaa F. Al-ani, Mazen J. Al-Kheetan and Mustafa M. Moudhafar
Constr. Mater. 2026, 6(3), 34; https://doi.org/10.3390/constrmater6030034 - 29 May 2026
Viewed by 214
Abstract
The performance and durability of asphalt pavements are strongly influenced by the rheological properties of asphalt binders, particularly under severe climatic and traffic conditions. This study investigates the synergistic effects of incorporating multi-walled carbon nanotubes (CNTs) at dosages ranging from 0.25% to 1% [...] Read more.
The performance and durability of asphalt pavements are strongly influenced by the rheological properties of asphalt binders, particularly under severe climatic and traffic conditions. This study investigates the synergistic effects of incorporating multi-walled carbon nanotubes (CNTs) at dosages ranging from 0.25% to 1% into AC 40-50 asphalt binders modified with 4% Styrene–Butadiene–Styrene (SBS). A comprehensive experimental program involving physical, rheological, and chemical characterization tests was conducted, including penetration, softening point, viscosity, storage stability, a Dynamic Shear Rheometer (DSR), Multiple Stress Creep Recovery (MSCR), Linear Amplitude Sweep (LAS), Fourier Transform Infrared Spectroscopy (FTIR), and Glover-Rowe (G-R) analysis. Statistical inference using one-way ANOVA was also conducted to evaluate the significance of differences among the binder formulations investigated. The results showed a continuous increase in binder stiffness with increasing CNT content, as indicated by decreasing penetration values, higher softening points, and increased viscosity. Incorporating 1% CNT reduced the softening-point difference from 3.1 °C to 1.6 °C in SBS-modified binders, indicating improved storage stability. Rheological evaluations showed that 0.75% CNT increased the high-temperature performance grade from 82 °C to 88 °C and provided the best rutting resistance, as indicated by MSCR results. In contrast, the 0.5% CNT formulation exhibited superior fatigue resistance and the lowest Glover-Rowe index, indicating improved cracking resistance and durability. Overall, the findings demonstrate that CNTs can effectively enhance the performance of SBS-modified asphalt binders, with 0.75% CNT being optimal for hot-climate applications, while 0.5% CNT exhibited improved fatigue and cracking resistance under moderate-temperature conditions. Full article
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27 pages, 9397 KB  
Article
Rheological Behavior and Aging Resistance of SBS/Lignin Composite Modified Asphalt
by Wenliang Wu, Longfei Li, Mukai Huang, Junxuan Liang and Zhi Li
Polymers 2026, 18(11), 1319; https://doi.org/10.3390/polym18111319 - 27 May 2026
Viewed by 376
Abstract
The degradation of styrene-butadiene-styrene (SBS) modified asphalt under thermal-oxidative aging can reduce pavement service life. Lignin is a renewable material with active phenolic hydroxyl groups. Incorporating lignin into SBS modified asphalt may provide a potential bio-based auxiliary modification route. To investigate the antioxidative [...] Read more.
The degradation of styrene-butadiene-styrene (SBS) modified asphalt under thermal-oxidative aging can reduce pavement service life. Lignin is a renewable material with active phenolic hydroxyl groups. Incorporating lignin into SBS modified asphalt may provide a potential bio-based auxiliary modification route. To investigate the antioxidative effect and rheological properties of SBS modified asphalt after adding lignin, a molecular dynamics test and experimental tests were employed. The molecular simulation results suggested that lignin preferentially associated with asphaltene and resin molecules and changed the molecular mobility of asphalt components in a component-dependent manner. The SBS/lignin composite modified asphalt was evaluated by temperature sweep (TS), Multiple Stress Creep and Recovery (MSCR), Linear Amplitude Sweep (LAS) and Fourier transform infrared spectroscopy (FTIR). Rheological tests showed that lignin increased the complex shear modulus and rutting factor. LAS results showed that lignin reduced the fatigue life of SBS-modified asphalt in the unaged state due to increased stiffness and embrittlement. However, after long-term aging, the lignin-containing binders retained higher fatigue resistance than the SBS-only control, which may be related to the slower evolution of oxidation-related functional groups and SBS-related spectral indices. FTIR analysis provided semi-quantitative evidence that lignin addition reduced the growth of sulfoxide-related bands and helped maintain the polybutadiene-related index during aging. Overall, lignin may serve as a potential auxiliary antioxidant modifier for SBS modified asphalt, while its exact source-specific molecular mechanism requires further verification. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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57 pages, 37019 KB  
Review
Research Progress on Additively Manufactured Porous Structures of Nickel-Based Superalloys
by Shenghang Xu, Yiye Pan, Nanxuan Mei, Shaoqi Jia, Minghao Huang, Chao Ding, Xin Yang, Jinglong Li, Rong Wang and Huiping Tang
Materials 2026, 19(10), 2144; https://doi.org/10.3390/ma19102144 - 20 May 2026
Viewed by 273
Abstract
Nickel-based superalloys are key materials for aerospace and gas turbine applications. Traditional manufacturing approaches struggle to produce controllable porous structures with complex topologies. This review focuses on additively manufactured porous Ni-based superalloys, and summarizes progress in porous structure design, including disordered, lattice, TPMS, [...] Read more.
Nickel-based superalloys are key materials for aerospace and gas turbine applications. Traditional manufacturing approaches struggle to produce controllable porous structures with complex topologies. This review focuses on additively manufactured porous Ni-based superalloys, and summarizes progress in porous structure design, including disordered, lattice, TPMS, bio-inspired, and AI-assisted structures. Common additive manufacturing technologies are introduced, along with their effects on microstructure evolution and defect formation. The review discusses non-equilibrium microstructures, elemental segregation, and typical defects such as lack-of-fusion, keyhole porosity, and residual stress, as well as their influences on strength, fatigue, and creep behavior. Post-processing strategies for defect mitigation and performance optimization are also summarized. This review highlights the unique mechanical and physical behavior of porous structures compared to bulk materials, with an emphasis on anisotropy, stress localization, and defect sensitivity. Finally, several critical and specific challenges are identified, including multi-scale modeling, microstructure control in complex topologies, fatigue prediction, and physics-constrained AI design. This review aims to provide a clear, focused, and structurally consistent overview of the current state of the field, and to support future research on additively manufactured porous Ni-based superalloys. Full article
(This article belongs to the Special Issue 3D Printing Technology Using Metal Materials and Its Applications)
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23 pages, 3736 KB  
Article
Investigation on the Fatigue and Rutting Behavior of Asphalt Binder Containing Compound Warm Mixing Agent
by Qinghong Fu, Tingting Chang, Qing Yang, Nong Zhang, Ziyang Huang, Keyu Yu and Qi Li
Materials 2026, 19(10), 2136; https://doi.org/10.3390/ma19102136 - 19 May 2026
Viewed by 313
Abstract
A composite warm-mix additive (PNSK) was developed to improve asphalt workability by reducing viscosity while maintaining rheological performance at both high and low temperatures. The warm-mix asphalt binders (PWMA) were analyzed using an integrated approach combining conventional property tests with rheological analysis. Results [...] Read more.
A composite warm-mix additive (PNSK) was developed to improve asphalt workability by reducing viscosity while maintaining rheological performance at both high and low temperatures. The warm-mix asphalt binders (PWMA) were analyzed using an integrated approach combining conventional property tests with rheological analysis. Results showed that penetration, softening point, and ductility improved. The viscosity-reduction effect was enhanced with increasing PNSK dosage, yet the benefit plateaued beyond 11% content. Additionally, the adhesion strength between asphalt and aggregate began to decrease after 11% dosage, with 12% serving as the critical threshold for adhesion deterioration. Consequently, the optimal dosage was determined to be 11% based on comprehensive consideration of all factors. LAS results demonstrated that 11%PWMA exhibited lower strain sensitivity and superior fatigue resistance at low-to-intermediate temperatures, with fatigue life increasing by nearly an order of magnitude under low strain at 20 °C. MSCR results revealed that under low stress, 11%PWMA exhibited significantly lower non-recoverable creep compliance (Jnr) and higher percent recovery (R) than the 70#, especially in the high-temperature range (54–66 °C), demonstrating superior resistance to permanent deformation. However, 11%PWMA exhibited temperature-strain sensitivity characteristics under high-temperature, high-strain conditions, representing an inherent characteristic of WMA technology. Full article
(This article belongs to the Section Construction and Building Materials)
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24 pages, 12607 KB  
Article
Experimental Validation of 2D Skeletal Point Method for Creep-Fatigue-Interaction Life Assessment in Perforated Plate Specimens Under Uniaxial Load
by Shouliang Xiang, Duoqi Shi, Nina Li, Tianxiao Sui, Ya Zhao and Xiaoguang Yang
Aerospace 2026, 13(5), 409; https://doi.org/10.3390/aerospace13050409 - 28 Apr 2026
Viewed by 344
Abstract
Geometric discontinuities in aero-engine turbine blades generate multiple stress concentrations along the airfoil, rendering life prediction exceptionally challenging. While conventional skeletal point method (SPM) offers reasonable accuracy in predicting creep-fatigue-interaction (CFI) life for simple structural specimens, they prove inadequate for geometries with poor [...] Read more.
Geometric discontinuities in aero-engine turbine blades generate multiple stress concentrations along the airfoil, rendering life prediction exceptionally challenging. While conventional skeletal point method (SPM) offers reasonable accuracy in predicting creep-fatigue-interaction (CFI) life for simple structural specimens, they prove inadequate for geometries with poor symmetry. This study introduces a novel two-dimensional skeletal point method (2D SPM) to analyze stress evolution characteristics, identify representative stresses, and predict CFI life in complex structures. Leveraging the film-cooling hole (FCH) features of a representative turbine blade, three perforated plate specimens were designed, manufactured, and subjected to CFI testing. Failure analysis confirmed crack initiation at hole-edge stress concentration zones, followed by inward propagation. Specimen fracture surfaces exhibited predominantly ductile dimpling features, with multi-origin fatigue characteristics observed only near hole-edges, collectively indicating creep-damage-dominated failure mechanisms. Five life prediction methodologies were comparatively evaluated. The results demonstrate that the 2D-SPM achieved the highest accuracy (all predictions within twofold scatter bands), followed by the conventional SPM (also within twofold scatter bands). The nominal stress method showed moderate accuracy (within fivefold scatter bands), while both hot point method and TCD methods proved unsuitable for creep-fatigue scenarios with significant stress evolution. Full article
(This article belongs to the Section Aeronautics)
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18 pages, 903 KB  
Perspective
Gingival Creep Failure: A Viscoelastic Theory of Recession in Thin Periodontal Phenotypes
by Anna Ewa Kuc, Natalia Kuc, Jacek Kotuła, Joanna Lis, Beata Kawala and Michał Sarul
Biology 2026, 15(9), 685; https://doi.org/10.3390/biology15090685 - 27 Apr 2026
Viewed by 478
Abstract
Gingival recession is commonly linked to alveolar bone dehiscence, inflammatory burden, traumatic brushing, or excessive orthodontic forces. However, recession is also observed in some patients despite apparently mild or “biologically acceptable” loading, particularly in thin periodontal phenotypes. Here, we propose the Gingival Creep [...] Read more.
Gingival recession is commonly linked to alveolar bone dehiscence, inflammatory burden, traumatic brushing, or excessive orthodontic forces. However, recession is also observed in some patients despite apparently mild or “biologically acceptable” loading, particularly in thin periodontal phenotypes. Here, we propose the Gingival Creep Failure Theory, a hypothesis-driven conceptual framework in which gingival soft tissues undergo time-dependent viscoelastic deformation (creep) under sustained or repetitive tensile microstrain. Over time, accumulated deformation and microstructural fatigue may reduce recoil capacity and shift the gingival margin apically once tissue-level tolerance is exceeded. Gingival connective tissue is modeled as a fiber-reinforced, fluid-rich viscoelastic composite whose response depends on collagen architecture, cross-linking, proteoglycan-mediated hydration, and vascular support. In thin phenotypes characterized by reduced connective tissue volume and altered extracellular matrix (ECM) organization, creep progression is hypothesized to accelerate, lowering the threshold at which fatigue-related microdamage translates into clinically detectable marginal migration. Evidence from collagenous connective tissue biomechanics supports the plausibility that sub-failure sustained or cyclic loading can produce cumulative deformation and incomplete recovery; however, direct creep–fatigue data for human gingiva remain limited, underscoring the need for targeted validation studies. This hypothesis integrates soft tissue mechanics with periodontal phenotype biology and orthodontic loading patterns and proposes creep and microstructural fatigue as plausible time-dependent contributors to gingival recession in susceptible phenotypes. Because direct in vivo gingival strain and creep–fatigue measurements remain limited, the model should be interpreted as hypothesis-generating and in need of targeted clinical and experimental validation. Full article
(This article belongs to the Section Medical Biology)
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19 pages, 4936 KB  
Article
Viscoelastic Properties of Porcine Pericardium Under Biaxial Tensile Creep and Stress Relaxation: Application for Novel Aortic Valve Bioprosthesis Design
by Edward Matjeka, Alex G. Kuchumov, Harry M. Ngwangwa, Thanyani Pandelani and Fulufhelo Nemavhola
Bioengineering 2026, 13(4), 401; https://doi.org/10.3390/bioengineering13040401 - 30 Mar 2026
Viewed by 829
Abstract
To design novel heart valve bioprostheses, it is extremely important to predict leaflet failure and fatigue for 10–20 years, as the aortic valve opens and closes approximately 40 million times per year. Most studies devoted to aortic valve leaflets mechanical tests employ uniaxial [...] Read more.
To design novel heart valve bioprostheses, it is extremely important to predict leaflet failure and fatigue for 10–20 years, as the aortic valve opens and closes approximately 40 million times per year. Most studies devoted to aortic valve leaflets mechanical tests employ uniaxial or biaxial tests, which do not fully and explicitly describe the time-dependent biomechanical behavior of this tissue. The aim of this study was to evaluate the viscoelastic response of porcine pericardium using biaxial tensile tests. Biaxial creep tests were performed on a biaxial test machine to evaluate the circumferential and axial behavior of the porcine pericardium under creep testing, and biaxial stress relaxation was used to complement creep. The results showed that the creep behavior was the same in both directions after 1 s, 60 s, 300 s, 900 s, and 1800 s. After 30 min of creep, deformation in the circumferential and radial directions was 3303 × 106 and 5192.9 × 106, respectively. Stress relaxation tests showed the same behavior as creep. At stress relaxation test after 30 min, the pericardium deformation in the circumferential and radial directions was 15.28 kPa and 9.6 kPa, respectively. The Prony series with Levenberg–Marquardt as the optimizer was used to obtain material parameters to use for finite element analysis. The data obtained during such tests can be employed in numerical FSI simulations of novel aortic valve bioprosthesis long-term performance in a patient’s body. Full article
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26 pages, 1601 KB  
Article
Performance Control and Mechanism Analysis of DCLR-Based Composite High-Modulus Asphalt Based on Synergistic Modification Effect
by Bin Xu, Xinjie Yu, Aodong Gao, Guanjun Bu and Kaiji Lu
Materials 2026, 19(6), 1268; https://doi.org/10.3390/ma19061268 - 23 Mar 2026
Cited by 1 | Viewed by 453
Abstract
To address the prominent problem of early rutting distress in asphalt pavements under heavy-load traffic in China, this study proposes a composite modifier consisting of direct coal liquefaction residue (DCLR), styrene–butadiene–styrene block copolymer (SBS), and styrene–butadiene rubber (SBR). The preparation process and formula [...] Read more.
To address the prominent problem of early rutting distress in asphalt pavements under heavy-load traffic in China, this study proposes a composite modifier consisting of direct coal liquefaction residue (DCLR), styrene–butadiene–styrene block copolymer (SBS), and styrene–butadiene rubber (SBR). The preparation process and formula were optimized through single-factor experiments and orthogonal tests. Systematic investigations were conducted on its conventional performance, water damage resistance, aging resistance, fatigue performance, rheological properties, and microscopic mechanism, with comparisons made against base asphalt, single DCLR-modified asphalt, SBS-modified asphalt, and SBS/SBR-modified asphalt. The results indicate that the optimal preparation process for the novel composite high-modulus modified asphalt is as follows: DCLR particle size of 0.3 mm, addition in molten state, shear temperature of 170 °C, shear rate of 5000 r·min−1, shear time of 50 min. The optimal formula is 10% DCLR + 3% SBS + 2% SBR + 3% compatibilizer, with the addition sequence of “DCLR → SBS + compatibilizer → SBR”. This asphalt exhibits a softening point of 77.8 ± 2.1 °C, a Brookfield viscosity at 135 °C of 1.928 ± 0.105 Pa·s, and a grading of 5 for adhesion to aggregates; the rutting factor at 64 °C reaches 10.8 ± 0.9 kPa (6.43 times that of the base asphalt), the creep stiffness at −12 °C is 136 ± 12.5 MPa, and the low-temperature limit temperature is −17 °C; the freeze–thaw splitting strength ratio (TSR) is 94.6 ± 1.8%, and both aging resistance and water damage resistance are significantly superior to those of the control group asphalts (p < 0.05). The novel composite high-modulus modified asphalt showed improved overall laboratory performance and may be suitable for heavy-load traffic and complex climatic conditions, however, field validation is needed. Full article
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17 pages, 17938 KB  
Article
Characterization of High-Temperature, Low-Temperature and Fatigue Performance of Phosphogypsum Warm-Mix Asphalt
by Xiaodong Jia, Li Ou and Hongzhou Zhu
Materials 2026, 19(4), 713; https://doi.org/10.3390/ma19040713 - 12 Feb 2026
Viewed by 467
Abstract
To explore the potential of phosphogypsum for resource utilization in asphalt pavements, this study evaluated its feasibility as a warm-mix asphalt (WMA) additive and investigated its influence on the rheological properties of asphalt binder. Phosphogypsum warm-mix asphalt was prepared by incorporating varying dosages [...] Read more.
To explore the potential of phosphogypsum for resource utilization in asphalt pavements, this study evaluated its feasibility as a warm-mix asphalt (WMA) additive and investigated its influence on the rheological properties of asphalt binder. Phosphogypsum warm-mix asphalt was prepared by incorporating varying dosages of phosphogypsum warm-mix additive (PGWA) into both base asphalt and styrene–butadiene–styrene (SBS)-modified asphalt. The high-, medium-, and low-temperature performance of phosphogypsum warm-mix asphalt was evaluated using rheological tests. The results revealed that the complex modulus of PGWA-added base asphalt was higher than that of the base asphalt, with only minor changes in phase angle. The incorporation of the SBS modifier significantly enhanced the stiffness and elasticity of the asphalt binder. Compared with the control asphalt, PGWA-added asphalt exhibited lower creep strain and accumulated strain, higher creep recovery rates, and smaller non-recoverable compliance under the same stress level, indicating an improved resistance to high-temperature permanent deformation. PGWA increased the cumulative damage capacity and extended the fatigue life of the asphalt binder. Although the PGWA slightly reduced the low-temperature performance, the SBS modifier effectively compensated for this drawback. The Burgers model accurately captured the low-temperature rheological behavior of PGWA-added asphalt. Overall, PGWA-added asphalt demonstrated excellent rheological performance and high application potential, offering a promising pathway for the resource utilization of phosphogypsum and the development of sustainable, eco-friendly pavement materials. Full article
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23 pages, 8890 KB  
Article
Anand Model and Finite Element Analysis of Sn-0.3Ag-0.7Cu-3Bi Lead-Free Solder Joints in BGA Packages
by Junchen Liu, Abdullah Aziz Saad, Yuezong Zheng, Hongchao Ji and Zuraihana Bachok
Materials 2026, 19(3), 636; https://doi.org/10.3390/ma19030636 - 6 Feb 2026
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Abstract
Bi-doped low-silver Sn-Ag-Cu solders are increasingly gaining attention in advanced electronic packaging due to their cost-effectiveness and enhanced mechanical properties. However, the thermo-mechanical reliability mechanisms of such modified solders, particularly Sn-0.3Ag-0.7Cu-3Bi (SAC0307-3Bi) within Ball Grid Array (BGA) assemblies, remain insufficiently understood. To address [...] Read more.
Bi-doped low-silver Sn-Ag-Cu solders are increasingly gaining attention in advanced electronic packaging due to their cost-effectiveness and enhanced mechanical properties. However, the thermo-mechanical reliability mechanisms of such modified solders, particularly Sn-0.3Ag-0.7Cu-3Bi (SAC0307-3Bi) within Ball Grid Array (BGA) assemblies, remain insufficiently understood. To address this gap, this research proposes a comprehensive assessment framework integrating constitutive parameter calibration with finite element analysis (FEA) to accurately characterize the mechanical behavior and fatigue durability of SAC0307-3Bi solder joints under cyclic thermal loads. The Anand viscoplastic parameters were first calibrated via the Norton creep law and virtual tensile tests. Subsequently, a 3D quarter-symmetry model was constructed to replicate thermal cycling conditions between 25 °C and 125 °C. Simulation data reveal a strong correlation between stress concentration and the Distance to Neutral Point (DNP), pinpointing the chip-side interface of the corner joint as the critical failure site. Moreover, creep strain was observed to accrue in a “step-wise” pattern, predominantly during the heating and cooling ramps, reflecting distinct temperature sensitivity. Utilizing the Syed model, the fatigue life was estimated at approximately 2239 cycles. These insights serve as a crucial benchmark for designing robust packages using Bi-doped, low-silver lead-free solders. Full article
(This article belongs to the Special Issue Research on Metal Cutting, Casting, Forming, and Heat Treatment)
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