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22 pages, 3096 KB  
Article
Mechanical Stability Evaluation Method and Application for Subsea Christmas Tree-Wellhead Systems Considering Seismic and Corrosion Effects
by Xuezhan Zhao, Guangjin Chen, Yi Hong, Shuzhan Li, Zhiqiang Hu, Yongqi Ma, Xingpeng Zhang, Qian Xiang, Xingshang Chen and Bingzhen Gao
Processes 2026, 14(3), 431; https://doi.org/10.3390/pr14030431 - 26 Jan 2026
Abstract
To address the failure risks associated with long-term service of subsea Christmas tree-wellhead systems under the complex marine environment of the South China Sea, a multi-factor coupled mechanical analysis method is proposed to evaluate the system’s mechanical characteristics and ensure the safety of [...] Read more.
To address the failure risks associated with long-term service of subsea Christmas tree-wellhead systems under the complex marine environment of the South China Sea, a multi-factor coupled mechanical analysis method is proposed to evaluate the system’s mechanical characteristics and ensure the safety of deepwater oil and gas production. A dynamic model of lateral vibration under seismic loading is established, considering the combined effects of earthquakes, ocean currents, and seabed soil resistance. Based on the actual operating parameters of a well in the Lingshui area of the South China Sea, a three-dimensional finite element model of the subsea Christmas tree-wellhead assembly was developed in ABAQUS 2023. The combined effects of ocean currents, seismic loading, and corrosion over long-term service were simulated to compute and analyze the distributions of stress, bending moment, and associated failure risk. The results indicate that, under a once-in-a-century current combined with seismic waves of intensity V–VI, the system risk remains controllable. However, when the seismic intensity exceeds level VII, the maximum stress and bending moment reach 324.9 MPa and 6.02 MN·m, respectively, surpassing the allowable limits for an X56-grade surface conductor. Considering corrosion effects over a 25-year service life, the extreme stress values increase by 1–5% while the bending moment increases slightly; corrosion significantly amplifies the system’s failure risk. An analysis of the mudline burial height of the subsea wellhead during long-term service shows that, within a range of 1–7 m, variations in system loading are minimal. Based on the mechanical characteristics analysis, it is recommended that the design of subsea Christmas trees and wellheads incorporate regional seismic history, specify X56-grade surface conductors to mitigate corrosion effects, and install leakage-monitoring devices at critical locations to ensure the long-term service safety of the subsea Christmas tree-wellhead system. Full article
(This article belongs to the Special Issue Advanced Research on Marine and Deep Oil & Gas Development)
44 pages, 3456 KB  
Article
Structural Design and Motion Characteristics Analysis of the Inner Wall Grinding Robot for PCCP Pipes
by Yanping Cui, Ruitian Sun, Zhe Wu, Xingwei Ge and Yachao Cao
Sensors 2026, 26(3), 818; https://doi.org/10.3390/s26030818 - 26 Jan 2026
Abstract
Internal wall grinding of pipes constitutes a critical pretreatment procedure in the anti-corrosion repair operations of Prestressed Concrete Cylinder Pipes (PCCP). To address the limitations of low efficiency and poor safety associated with traditional manual internal wall grinding in PCCP anti-corrosion repair, this [...] Read more.
Internal wall grinding of pipes constitutes a critical pretreatment procedure in the anti-corrosion repair operations of Prestressed Concrete Cylinder Pipes (PCCP). To address the limitations of low efficiency and poor safety associated with traditional manual internal wall grinding in PCCP anti-corrosion repair, this study presents the design of a support-wheel-type internal wall grinding robot for pipes. The robot’s structure comprises a walking support module and a grinding module: the walking module employs four sets of circumferentially equally spaced (90° apart) independent-support wheel groups. Through an active–passive collaborative adaptation mechanism regulated by pre-tensioned springs and lead screws, the robot can dynamically conform to the inner wall of the pipe, ensuring stable locomotion. The grinding module is connected to the walking module via a slewing bearing and is equipped with three roller-type steel brushes. During operation, the grinding module revolves around the pipe axis, while the roller brushes rotate simultaneously, generating a composite three-helix grinding trajectory. Mathematical models for the robot’s obstacle negotiation, bend traversal, and grinding motion were established, and multi-body dynamics simulations were conducted using ADAMS for verification. Additionally, a physical prototype was developed to perform basic functional tests. The results demonstrate that the robot’s motion characteristics are highly consistent with theoretical analyses, exhibiting stable and reliable operation, excellent pipe traversability, and robust driving capability, thus meeting the requirements for internal wall grinding of PCCP pipes. Full article
(This article belongs to the Section Sensors and Robotics)
23 pages, 4514 KB  
Article
Fitness-for-Service Analysis of the Interplay Between a Quarter-Circle Corner Crack and a Parallel Semi-Elliptical Surface Crack in a Semi-Infinite Solid Subjected to In-Plane Bending Part II—The Effect on the Semi-Elliptical Surface Crack
by Mordechai Perl, Cesar Levy and Qin Ma
Appl. Sci. 2026, 16(3), 1240; https://doi.org/10.3390/app16031240 - 26 Jan 2026
Abstract
The impact of a quarter-circle corner crack on an adjacent parallel semi-elliptical surface crack (SESC) located in a semi-infinite solid subjected to in-plane bending is studied using a 3-D finite element analysis. The stress intensity factor (SIF) distributions along the front of the [...] Read more.
The impact of a quarter-circle corner crack on an adjacent parallel semi-elliptical surface crack (SESC) located in a semi-infinite solid subjected to in-plane bending is studied using a 3-D finite element analysis. The stress intensity factor (SIF) distributions along the front of the SESC are evaluated to determine said impact. The SESC’s semi-major axis ranged from a1 = 10 mm to 30 mm with ellipticities of b1/a1 varying from 0.1 to 1.0 for a constant quarter-circle corner crack length of a2 = 15 mm. Furthermore, several crack configurations are considered where the normalized vertical and horizontal gaps between the two cracks are taken to be H/a2 = 0.4 and 1.2 and S/a2 = −0.5 and 1.0, respectively. The results show that the effect of the quarter-circle corner crack on the SESC can be considerable both in amplifying and in attenuating the SIFs along the semi-elliptical surface crack front. Moreover, these opposite effects can occur simultaneously, but in different sections of the SESC’s crack front. The magnitude and pattern of these effects depend on the length and ellipticity of the SESC. It is further concluded that when considering the fitness-for-service of a critical real mechanical component, a complete 3-D analysis is needed to provide a reliable solution for such crack configurations. Full article
(This article belongs to the Special Issue Fatigue and Fracture Behavior of Engineering Materials)
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17 pages, 2800 KB  
Article
Characterization of Viscoelastic Performance and VOC Emission of Warm-Mixed SBS Asphalt Binder Under Different Dosages of Warm-Mixed Additive
by Wentao Wang, Yue Yang, Mengxue Xu, Xiangrui Han, Yinghao Miao and Linbing Wang
Materials 2026, 19(3), 485; https://doi.org/10.3390/ma19030485 - 26 Jan 2026
Abstract
Warm-mixed asphalt technology can significantly reduce the heating temperatures required for asphalt pavement construction, which makes it one of the crucial technical approaches in road engineering for achieving energy conservation and emission reduction, and carbon neutrality. Existing research often focuses on designing asphalt [...] Read more.
Warm-mixed asphalt technology can significantly reduce the heating temperatures required for asphalt pavement construction, which makes it one of the crucial technical approaches in road engineering for achieving energy conservation and emission reduction, and carbon neutrality. Existing research often focuses on designing asphalt materials to ensure optimal service performance, but insufficient attention has been paid to the specific extent of reduction in asphalt fume emissions. However, the latter is a critical factor that cannot be neglected when constructing asphalt pavements in environmentally sensitive regions. Considering the environmental factor, this study systematically explores the comprehensive influence of different warm-mixed additive dosages on the viscoelastic properties and VOC emissions of warm-mixed SBS asphalt binder using rotational viscosity, bending beam rheometer (BBR), dynamic shear rheometer (DSR), and gas chromatography–mass spectrometry (GC-MS) test methods. The findings show that the application of warm-mixed additive does not compromise the comprehensive properties of SBS asphalt binder, but partially enhances its service performance instead. Due to the significant reduction in heating temperature, asphalt VOC emissions are indirectly reduced. Although the warm-mixed additive possesses a certain degree of volatility, its application still shows a significant trend toward emission reduction. Despite 0.4% being a relatively economical dosage of warm-mixed additive, a slight increase to 0.5% can achieve more pronounced environmental benefits in VOC emission reduction while maintaining comprehensive service performance that meets specification requirements. The findings can provide new insights for the application and decision-making of warm-mixed asphalt technology in environmentally sensitive regions. Full article
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18 pages, 1312 KB  
Article
Optimization of Sisal Content in Geopolymer Mortars with Recycled Brick and Concrete: Design and Processing Implications
by Oscar Graos-Alva, Aldo Castillo-Chung, Marisol Contreras-Quiñones and Alexander Vega-Anticona
Constr. Mater. 2026, 6(1), 7; https://doi.org/10.3390/constrmater6010007 - 26 Jan 2026
Abstract
Geopolymer mortars were produced from construction and demolition waste using a binary binder of recycled brick powder/recycled concrete powder (RBP/RCP = 70/30 wt%), activated with a hybrid alkaline solution (NaOH/Na2SiO3/KOH) and reinforced with sisal fibres at 0–2 wt%. Mechanical [...] Read more.
Geopolymer mortars were produced from construction and demolition waste using a binary binder of recycled brick powder/recycled concrete powder (RBP/RCP = 70/30 wt%), activated with a hybrid alkaline solution (NaOH/Na2SiO3/KOH) and reinforced with sisal fibres at 0–2 wt%. Mechanical performance (compression and three-point bending) and microstructure–phase evolution (XRD, FTIR, SEM-EDS) were assessed after low-temperature curing. Sisal addition delivered a strength–toughness trade-off with a reproducible optimum at ~1.0–1.5 wt%; at 2.0 wt%, fibre clustering and connected porosity reduced the effective load-bearing section, penalising flexure more than compression. Microstructural evidence indicates coexistence and co-crosslinking of N-A-S-H and C-(A)-S-H gels—enabled by Ca from RCP—leading to matrix densification and improved fibre–matrix anchorage. Fractographic features (tortuous crack paths, bridging, and extensive pull-out at ~1.5 wt%) are consistent with an extended post-peak response and higher fracture work without compromising early-age strength. This study achieves the following: (i) it identifies a practical reinforcement window for sisal in RBP/RCP geopolymers, (ii) it links gel chemistry and interfacial phenomena to macroscopic behaviour, and (iii) it distils processing guidelines (gradual addition, workability control, gentle deaeration, and constant A/S) that support reproducibility. These outcomes provide a replicable, low-embodied-CO2 route to fibre-reinforced geopolymer mortars derived from CDW for non-structural and semi-structural applications where flexural performance and post-peak behaviour are critical. Full article
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17 pages, 2736 KB  
Article
Pt Single-Atom Doping in Ag29 Nanoclusters for Enhanced Band Bending and Z-Scheme Charge Separation in TiO2 Heterojunction Photocatalysts
by Xiao-He Liu, Rui Yuan, Zhi Li, Jing Wang, Nailong Zhao and Zhili Ren
Inorganics 2026, 14(2), 35; https://doi.org/10.3390/inorganics14020035 - 26 Jan 2026
Abstract
In recent years, metal nanoclusters (NCs) with atomic-scale precision have emerged as novel photosensitizers for light energy conversion in metal cluster-sensitized semiconductor (MCSS) systems. However, conventional NCs often suffer from photodegradation after binding with semiconductors, limiting their long-term catalytic stability. Modifying NCs via [...] Read more.
In recent years, metal nanoclusters (NCs) with atomic-scale precision have emerged as novel photosensitizers for light energy conversion in metal cluster-sensitized semiconductor (MCSS) systems. However, conventional NCs often suffer from photodegradation after binding with semiconductors, limiting their long-term catalytic stability. Modifying NCs via single-atom doping provides an effective strategy to tailor their interfacial charge transfer behavior. In this study, PtAg28 NCs were synthesized by doping Pt single atoms into Ag29 NCs and subsequently loaded onto TiO2 via electrostatic adsorption to construct composite photocatalysts. Systematic investigations revealed that Pt doping significantly enhances light absorption and promotes the formation of a direct Z-scheme heterojunction. The optimized PtAg28/TiO2 composite exhibits effective suppression of charge recombination. This enhanced charge separation efficiency, driven by pronounced band bending at the interface, leads to a remarkable hydrogen evolution rate of 14,564 μmol g−1 h−1. This work demonstrates the critical role of single-atom doping in regulating the photophysical properties of metal NCs and offers a feasible approach for designing highly efficient and stable metal-cluster-based photocatalytic systems. Full article
(This article belongs to the Section Inorganic Materials)
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15 pages, 3056 KB  
Article
Research on the Accelerated Fatigue Experiment Method of the Crankshaft Based on a Modified Particle Filtering Algorithm and the Fatigue Crack Growth Property
by Jiahong Fu, Songsong Sun, Xiaolin Gong, Shanshan Shen, Nana Jiang and Jianmin Juan
Materials 2026, 19(3), 481; https://doi.org/10.3390/ma19030481 - 25 Jan 2026
Abstract
Crankshafts are among the most important parts of modern internal combustion engines. Owing to the power transmission demand, sufficiently high strength is usually necessary for the application of the component. In this paper, a new crankshaft bending experimental method was proposed to shorten [...] Read more.
Crankshafts are among the most important parts of modern internal combustion engines. Owing to the power transmission demand, sufficiently high strength is usually necessary for the application of the component. In this paper, a new crankshaft bending experimental method was proposed to shorten the corresponding test. A modified particle filtering algorithm approach was proposed for predicting the remaining fatigue life of a crankshaft during bending fatigue experiments. The predicted fatigue life was used to replace the actual experimental results for further analysis if the accuracy requirements were fulfilled; in this way, the experimental duration was obviously shortened. The main conclusion drawn from the research is that, compared with the traditional particle filtering algorithm approach, the modified particle algorithm approach proposed in this paper can more accurately predict the remaining fatigue life of a crankshaft using less experimental data, which makes it possible to circumvent actual bending fatigue experiments of crankshafts in providing theoretical guidance for the design process. Full article
(This article belongs to the Special Issue Combined Fatigue and Multi-Scale Simulation)
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35 pages, 24985 KB  
Article
From Blade Loads to Rotor Health: An Inverse Modelling Approach for Wind Turbine Monitoring
by Attia Bibi, Chiheng Huang, Wenxian Yang, Oussama Graja, Fang Duan and Liuyang Zhang
Energies 2026, 19(3), 619; https://doi.org/10.3390/en19030619 - 25 Jan 2026
Abstract
Operational expenditure in wind farms is heavily influenced by unplanned maintenance, much of which stems from undetected rotor system faults. Although many fault-detection methods have been proposed, most remain confined to laboratory test. Blade-root bending-moment measurements are among the few techniques applied in [...] Read more.
Operational expenditure in wind farms is heavily influenced by unplanned maintenance, much of which stems from undetected rotor system faults. Although many fault-detection methods have been proposed, most remain confined to laboratory test. Blade-root bending-moment measurements are among the few techniques applied in the field, yet their reliability is limited by strong sensitivity to varying operational and environmental conditions. This study presents a data-driven rotor health-monitoring framework that enhances the diagnostic value of blade bending-moments. Assuming that the wind speed profile remains approximately stationary over short intervals (e.g., 20 s), a machine-learning model is trained on bending-moment data from healthy blades to predict the incident wind-speed profile under a wide range of conditions. During operation, real-time bending-moment signals from each blade are independently processed by the trained model. A healthy rotor yields consistent wind-speed profile predictions across all three blades, whereas deviations for an individual blade indicate rotor asymmetry. In this study, the methodology is verified using high-fidelity OpenFAST simulations with controlled blade pitch misalignment as a representative fault case, providing simulation-based verification of the proposed framework. Results demonstrate that the proposed inverse-modeling and cross-blade consistency framework enables sensitive and robust detection and localization of pitch-related rotor faults. While only pitch misalignment is explicitly investigated here, the approach is inherently applicable to other rotor asymmetry mechanisms such as mass imbalance or aerodynamic degradation, supporting reliable condition monitoring and earlier maintenance interventions. Using OpenFAST simulations, the proposed framework reconstructs height-resolved wind profiles with RMSE below 0.15 m/s (R² > 0.997) under healthy conditions, and achieves up to 100% detection accuracy for moderate-to-severe pitch misalignment faults. Full article
(This article belongs to the Section A3: Wind, Wave and Tidal Energy)
24 pages, 780 KB  
Article
Numerical Investigation of Inlet Velocity Profile Effects on Developing Laminar Flow in a Circular Pipe
by Mesude Avcı and Dimitrios V. Papavassiliou
Appl. Sci. 2026, 16(3), 1215; https://doi.org/10.3390/app16031215 - 24 Jan 2026
Viewed by 30
Abstract
Hydrodynamic development in laminar pipe flow is mostly defined by classical entrance length relations and fully developed friction factor relations. However, in real systems, the inlet velocity profiles are often shaped by upstream components such as bends, contractions, or manifolds, causing them to [...] Read more.
Hydrodynamic development in laminar pipe flow is mostly defined by classical entrance length relations and fully developed friction factor relations. However, in real systems, the inlet velocity profiles are often shaped by upstream components such as bends, contractions, or manifolds, causing them to deviate significantly from the ideal Poiseuille profile. These deviations directly affect both the development length in the entrance region and energy losses. In this study, steady three-dimensional laminar CFD simulations were performed to investigate the effect of three inlet velocity profile shapes, a uniform profile, a parabolic (Poiseuille) profile, and a strongly peaked power-law profile, in a circular pipe over a Reynolds number range of Re = 100–1500. The flow development was quantified using a profile-sensitive deviation metric based on the ratio of the maximum velocity to the local averaged fluid velocity. The results showed that, although, for all modeled cases, the flows reach the same fully developed laminar flow profile, the entrance development length strongly depends on the inlet velocity profile, and this dependence becomes more pronounced as the Reynolds number increases. The parabolic inlet profile evolves toward the Poiseuille profile very rapidly, and the additional entrance loss is minimal. On the other hand, the power-law (n = 7) profile produces the largest entrance distortions, which leads to the longest relaxation distance. Overall, the proposed perspective in this study directly links profile-based flow development with energy loss and provides a basis for shaping entrance conditions in compact laminar flow systems. In addition, an empirical scaling analysis yielded a compact power-law relation linking Ldev/D to the Reynolds number and the inlet profile parameter 𝛽 = 𝑈max/ Ū. Full article
(This article belongs to the Section Fluid Science and Technology)
24 pages, 25014 KB  
Article
DEM-Based Investigation of Sand Mixing Ratio and Recoating Speed Effects on Recoating Performance and Mechanical Properties in 3D Sand Printing
by Guili Gao, Jialin Guo, Jie Liu, Dequan Shi and Huajun Zhang
Materials 2026, 19(3), 473; https://doi.org/10.3390/ma19030473 - 24 Jan 2026
Viewed by 46
Abstract
Based on the discrete element method (DEM), a sand particle contact force model and a motion model for the 3D sand printing (3DSP) process were developed. By accounting for the viscous support force and contact force between sand particles, and gravity acting on [...] Read more.
Based on the discrete element method (DEM), a sand particle contact force model and a motion model for the 3D sand printing (3DSP) process were developed. By accounting for the viscous support force and contact force between sand particles, and gravity acting on each individual sand particle, the displacement of sand particles was calculated, enabling the simulation of the 3DSP process using sand particle ensembles. Furthermore, the effects of the ratio of silica sand to ceramsite sand and the recoating speed on sand-recoating performances and mechanical properties were investigated. Irregularly shaped sand particles (primarily silica sand) were constructed via the multi-sphere filling method. The simulation was performed on a virtual sand-recoating device (180 mm in length, 100 mm in width, 70 mm in height) with reference to the EXONE S-MAX printer. Meanwhile, the EXONE S-MAX was utilized to print the bending samples for experimental validation. Simulation and experimental results indicate that as the ratio increases, the porosity first decreases and then increases, whereas mechanical properties exhibit an initial increase followed by a decrease. At a ratio of 3:7, the porosity reaches a minimum of 21.3%; correspondingly, the shear force of bonding bridges peaks at 908 mN, and the bending strength of specimens attains a maximum of 2.87 MPa. With the increasing recoating speed, the porosity rises consistently, while the shear force of bonding bridges and the bending strength of specimens first increase and then decrease, which is primarily attributed to the penetration behavior of the binder under capillary force. At a recoating speed of 160 mm·s−1, the shear force of bonding bridges reaches its maximum, and the specimens achieve a maximum bending strength of 2.89 MPa. The simulation results are well-validated by the experiments. The DEM-based simulation method proposed in this study offers a practical and convenient tool for parameter optimization in 3DSP process. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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25 pages, 5781 KB  
Article
Optimization and Tradespace Analysis of a Classic Machine—A Street Clock Movement Study
by Pranav Manvi, Yifan Xu, David Moline, Cameron Turner and John Wagner
Machines 2026, 14(2), 136; https://doi.org/10.3390/machines14020136 - 24 Jan 2026
Viewed by 47
Abstract
Computer-based engineering design tools can quicken the cadence for machine design, which enables companies to compete better in the global marketplace. The application of nonlinear optimization and tradespace analysis methods allows the exploration of design variables within dynamic mechanisms. In this paper, the [...] Read more.
Computer-based engineering design tools can quicken the cadence for machine design, which enables companies to compete better in the global marketplace. The application of nonlinear optimization and tradespace analysis methods allows the exploration of design variables within dynamic mechanisms. In this paper, the design of a classical machine, the Seth Thomas pendulum street clock, which offered precision timekeeping and time display at the turn of the 20th century, will be investigated from a modern perspective. A mathematical model serves as the basis for the genetic algorithm optimization method to assess the system design in terms of accuracy, mass, quality factor, and bending stress. To validate the model, experimental data was collected on a 1906 Seth Thomas Model 04 movement. The engineering study findings indicate that the target accuracy, quality factor, and bending stress can be achieved with pendulum mass and gear thickness reductions of 1.4% and 50.3%, respectively. The tradespace exploration offers a visualization of the machine’s performance per design variable adjustments for greater insight into the original solution and subsequent recommended changes. Overall, this mechanical machine review enables an assessment of original design choices made over a century ago and provides an awareness of engineering’s progress during this period. Full article
(This article belongs to the Section Machine Design and Theory)
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13 pages, 3678 KB  
Article
Biomechanical Comparison of Different Fixation Methods for Treating Jones Fracture of the Fifth Metatarsal
by Cheng-Min Shih, Yu-Chun Yen, Chun-Hsiang Wang, Yu-Heng Huang, Shun-Ping Wang and Kuo-Chih Su
Bioengineering 2026, 13(2), 135; https://doi.org/10.3390/bioengineering13020135 - 23 Jan 2026
Viewed by 118
Abstract
Jones fractures are Zone 2 fractures of the fifth metatarsal. Biomechanical comparisons of fixation strategies for Jones fractures remain limited by the lack of standardized, head-to-head evaluations across major fixation methods. The purpose of this study was to perform a standardized biomechanical comparison [...] Read more.
Jones fractures are Zone 2 fractures of the fifth metatarsal. Biomechanical comparisons of fixation strategies for Jones fractures remain limited by the lack of standardized, head-to-head evaluations across major fixation methods. The purpose of this study was to perform a standardized biomechanical comparison of six fixation configurations representing the three primary surgical techniques for Jones fractures and to examine the mechanical factors underlying differences in early construct stability. A synthetic fifth metatarsal model with a simulated Zone 2 fracture was stabilized using lateral plate fixation with different screw configurations, Kirschner wire fixation with or without tension-band wiring, or intramedullary headless screw fixation. All constructs were tested under displacement-controlled cantilever bending, and the force required to reach 1 mm of fracture site displacement was obtained and construct stiffness was calculated. Plate-based fixation demonstrated the highest resistance to bending deformation, followed by intramedullary screw fixation, whereas Kirschner wire-based constructs exhibited the lowest stability. These differences were explained by variations in load-sharing pathways and effective working length among fixation constructs. The addition of tension-band wiring did not result in a measurable improvement in stability compared with Kirschner wire fixation alone, consistent with the dependence of tension-band mechanisms on active muscle loading not represented in the experimental model. These findings provide a unified biomechanical comparison of commonly used fixation constructs for Jones fractures and clarify the mechanical basis for differences in early construct stability. Full article
(This article belongs to the Special Issue Orthopedic and Trauma Biomechanics)
14 pages, 3433 KB  
Article
Defect Reduction in HEMT Epilayers on SiC Meta-Substrates
by Vin-Cent Su, Ting-Yu Wei, Meng-Hsin Chen, Chien-Te Ku and Guan-Shian Liu
Nanomaterials 2026, 16(3), 158; https://doi.org/10.3390/nano16030158 - 23 Jan 2026
Viewed by 66
Abstract
Dislocation reduction in gallium nitride (GaN) epitaxial layers remains a critical challenge for high-performance GaN-based electronic devices. In this study, GaN epitaxial growth on newly-developed 4H-Silicon Carbide (SiC) meta-substrates was systematically investigated to elucidate the role of surface pattern geometry in modulating dislocation [...] Read more.
Dislocation reduction in gallium nitride (GaN) epitaxial layers remains a critical challenge for high-performance GaN-based electronic devices. In this study, GaN epitaxial growth on newly-developed 4H-Silicon Carbide (SiC) meta-substrates was systematically investigated to elucidate the role of surface pattern geometry in modulating dislocation propagation. A series of truncated-hexagonal-pyramid meta-structures with a fixed array period and varying pattern ratios (R) were designed and fabricated to enable controlled tuning of the effective surface morphology. Atomic force microscopy confirmed comparable surface flatness for all samples after epitaxial growth. Cathodoluminescence analysis revealed a non-monotonic dependence of defect density on R, indicating the existence of an optimal pattern geometry. Among all configurations, the outstanding sample exhibited the lowest defect density, achieving a 54.96% reduction in threading dislocations (edge + mixed) compared with a planar reference. Cross-sectional transmission electron microscopy further confirmed a substantially reduced dislocation density and clear evidence of dislocation bending and termination near the meta-structured regions. These results demonstrate that geometry-engineered 4H-SiC meta-substrates provide an effective and scalable strategy for dislocation modulation in GaN epitaxy on SiC meta-substrates, offering a promising pathway toward advanced GaN power and RF devices. Full article
(This article belongs to the Special Issue Nonlinear Optics of Nanostructures and Metasurfaces)
18 pages, 1423 KB  
Article
NaOH-Only Pretreated Wood Densification: A Simplified Sulfite-Free Route Across Wood Species
by Laura Andze, Vadims Nefjodovs, Juris Zoldners, Ulla Milbreta, Marite Skute, Linda Vecbiskena, Inese Filipova and Martins Andzs
Polymers 2026, 18(3), 312; https://doi.org/10.3390/polym18030312 - 23 Jan 2026
Viewed by 96
Abstract
The development of high-performance wood-based materials has attracted increasing interest as a means of enhancing the mechanical properties of wood for structural applications. Mechanical densification combined with chemical pretreatment is an effective approach; however, many reported methods rely on complex multi-component chemical systems [...] Read more.
The development of high-performance wood-based materials has attracted increasing interest as a means of enhancing the mechanical properties of wood for structural applications. Mechanical densification combined with chemical pretreatment is an effective approach; however, many reported methods rely on complex multi-component chemical systems or severe chemical conditions designed to dissolve lignin or hemicelluloses. In this study, a simplified NaOH-only pretreatment followed by hot-press densification was investigated, targeting selective cell-wall plasticization rather than extensive polymer dissolution. Juniper (Juniperus communis), hawthorn (Crataegus monogyna), and birch (Betula pendula) were used as samples of softwood and hardwood species. Wood specimens were pretreated in 1 M NaOH at 145 °C for 10–30 min and subsequently densified by radial compression. Changes in chemical composition were evaluated by HPLC after acid hydrolysis and FTIR spectroscopy, while microstructural changes were examined using SEM. Physical and mechanical properties were assessed through density measurements and three-point bending tests. The results show that NaOH-only pretreatment induces hemicellulose deacetylation and modification of interpolymer linkages without substantial changes in the main wood polymer contents. Densification resulted in effective lumen collapse and a compact microstructure, leading to a significant increase in density and mechanical properties. Overall, the results demonstrate that efficient wood densification and mechanical enhancement can be achieved by promoting polymer mobility through selective cleavage of interpolymer bonds, using a simplified, single-alkali pretreatment that reduces chemical complexity and material loss while avoiding extensive lignin or hemicellulose dissolution. Full article
(This article belongs to the Special Issue Recent Progress on Lignocellulosic-Based Polymeric Materials)
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24 pages, 5617 KB  
Article
Mechanical Properties of Concrete Reinforced with Basalt Fiber and Oil Shale Ash
by Ilgar Jafarli, Olga Kononova, Andrejs Krasnikovs, Laimdota Šnīdere and Ashraf Ali Shaik
Appl. Sci. 2026, 16(3), 1164; https://doi.org/10.3390/app16031164 - 23 Jan 2026
Viewed by 69
Abstract
This study determined the elastic properties of “green” concrete with cement partially replaced by oil shale ash (OSA) and reinforced with short basalt integral fibers (BIFs). Commercially available Deutsche Basalt Faser (DBF) GmbH Turbobuild Integral basalt fibers were used. There is currently a [...] Read more.
This study determined the elastic properties of “green” concrete with cement partially replaced by oil shale ash (OSA) and reinforced with short basalt integral fibers (BIFs). Commercially available Deutsche Basalt Faser (DBF) GmbH Turbobuild Integral basalt fibers were used. There is currently a high demand both for strengthening concrete and applying ecological approaches with respect to circular economy. Oil shale ash is the byproduct of oil shale combustion. Basalt fiber is produced by melting basalt rock. Both BIF and OSA are used as additives in concrete. Cement replacement by OSA non-linearly changes the concrete’s strength properties, and the addition of BIF improves them. An experimental investigation was conducted using four-point bending tests and cube sample compression tests. Theoretical methods such as Voigt and Reuss boundaries, the Halpin–Tsai method, and the Mori–Tanaka method were used to predict the elastic properties of the fabricated samples. The theoretical models can provide useful information, although they may not fully capture the real properties observed experimentally. The results show that BIFs protect against instant brittle destruction. The experiments demonstrated an optimal OSA concentration for a fixed amount of BIF, resulting in the highest load-bearing capacity of the concrete. The addition of either 15% OSA only or 20% OSA and CBF can increase the stiffness of the concrete. This article provides guidance to the construction sector on using OSA and CBF together. Full article
(This article belongs to the Section Materials Science and Engineering)
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