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Keywords = austenitic welds

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32 pages, 1901 KB  
Review
A Brief Review on Hot Cracking Austenitic Stainless Steel Welds
by Sadok Mehrez, Touileb Kamel and Mohamed M. Z. Ahmed
Crystals 2026, 16(7), 433; https://doi.org/10.3390/cryst16070433 - 2 Jul 2026
Viewed by 222
Abstract
Hot cracking in welding is a very complex phenomenon. It can happen in the weld metal zone during solidification but also in the heat-affected zone (HAZ). Hot cracking defects are material decohesion that occur at high temperatures along grain boundaries when the strain [...] Read more.
Hot cracking in welding is a very complex phenomenon. It can happen in the weld metal zone during solidification but also in the heat-affected zone (HAZ). Hot cracking defects are material decohesion that occur at high temperatures along grain boundaries when the strain and strain rate exceed a certain level. The cracks can be internal or open to the surface in the weld bead. During a welding operation, different types of hot cracks can appear, such as hot cracking due to solidification, hot cracking due to liquation, hot cracking due to loss of ductility. The main factors favoring hot solidification cracking include the presence of residual elements and impurities, leading to the formation of a low-melting eutectic; the solidification mode; and mechanical restraints. This review paper gives an introduction to solidification cracking in stainless-steel welds, the weldability of the austenite grades, and the causes of solidification cracking occurrence. The main methods with which to detect and inspect cracks are investigated. Particular focus is placed on TIG (tungsten inert gas), also known as Gas Tungsten Arc Welding (GTAW). A review of the literature reveals that considerable progress has been made in terms of the improvement in the properties of the weld joint through the application of mitigation means and strategies. The effort made by researchers in understanding solidification cracking phenomena has been key to enhancing cracking resistance and ensuring the integrity of structures. Full article
(This article belongs to the Special Issue Microstructure and Properties of Steel Materials)
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23 pages, 15118 KB  
Article
Effects of Fast-Frequency Pulsed Twin-TIG Welding on Molten Pool Flow, Mechanical Properties and Microstructure in 316L Austenitic Stainless Steel
by Siyu Zhang, Honglei Zhao, Yuze Liu, Bo Zhang and Yunlong Chang
Crystals 2026, 16(7), 406; https://doi.org/10.3390/cryst16070406 - 23 Jun 2026
Viewed by 130
Abstract
To improve the efficiency of TIG (Tungsten Inert Gas) welding, our team developed a novel fast-frequency pulsed twin-TIG welding power source and matched welding procedures to overcome the drawbacks of conventional high-efficiency TIG welding. After parameter optimization, stable, high-efficiency and high-quality welding of [...] Read more.
To improve the efficiency of TIG (Tungsten Inert Gas) welding, our team developed a novel fast-frequency pulsed twin-TIG welding power source and matched welding procedures to overcome the drawbacks of conventional high-efficiency TIG welding. After parameter optimization, stable, high-efficiency and high-quality welding of 316L stainless steel can be realized. Compared with traditional DC TIG welding, the mechanical properties of joints are greatly improved: the weld grain size is refined by 38% under moderate current, while tensile strength, elongation and microhardness rise by 13.6%, 26% and 10% respectively, which achieves simultaneous improvement in strength and ductility. Numerical simulations were carried out to analyze the evolution of molten pool temperature field and velocity vector flow field. The simulation results are highly consistent with experimental data, which verifies the reliability of the model and lays a foundation for the study of molten pool behavior. Combined with molten pool flow characteristics and weld microstructure, the evolution mechanism of microstructure and texture as well as grain refinement in this welding process is revealed. Full article
(This article belongs to the Section Crystalline Metals and Alloys)
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30 pages, 57518 KB  
Article
Microstructure and Abrasive Wear Behavior of Fe–Cr–C Hardfacing on Hammer Tips for Sugarcane Shredders
by Buntoeng Srikarun, Hein Zaw Oo, Anuchit Teherng, Shayfull Zamree Abd Rahim and Prapas Muangjunburee
Metals 2026, 16(6), 675; https://doi.org/10.3390/met16060675 - 18 Jun 2026
Viewed by 396
Abstract
This study investigates the influence of an austenitic buffer layer on the microstructure, hardness, and abrasive wear resistance of Fe–Cr–C hardfacing applied to high-chromium white cast iron (HCWCI) hammer tips used in sugarcane shredders. Hardfacing was performed by shielded metal arc welding with [...] Read more.
This study investigates the influence of an austenitic buffer layer on the microstructure, hardness, and abrasive wear resistance of Fe–Cr–C hardfacing applied to high-chromium white cast iron (HCWCI) hammer tips used in sugarcane shredders. Hardfacing was performed by shielded metal arc welding with two Fe–Cr–C layers deposited directly on the HCWCI substrate and with an austenitic buffer layer followed by an Fe–Cr–C hardfacing layer. Microstructural characterization was carried out using optical microscopy, scanning electron microscopy with energy-dispersive X-ray spectroscopy, while hardness profiles were determined by micro-Vickers testing. Abrasive wear behavior was evaluated using a dry sand–rubber wheel test according to ASTM G65. The non-buffered hardfacing layer exhibited a hypereutectic Fe–Cr–C microstructure consisting of coarse primary chromium carbides, resulting in high hardness values of approximately 840 HV. In contrast, the buffered sample showed an austenite-rich matrix with finer eutectic carbides and reduced hardness of around 600 HV. Abrasive wear tests of the non-buffered sample showed a lower mass loss, whereas the buffered sample exhibited a substantially higher mass loss. These results demonstrate that Fe–Cr–C hardfacing without a buffer layer provides superior wear resistance. Full article
(This article belongs to the Section Welding and Joining)
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17 pages, 17205 KB  
Article
Numerical Modeling and Experimental Characterization of the Mechanical Impact on a Dissimilar Structured Steel by GMAW
by Ramsés Chávez Carrillo, David Jaramillo, César Mendoza and Ricardo Rafael Ambriz
Processes 2026, 14(12), 1938; https://doi.org/10.3390/pr14121938 - 13 Jun 2026
Viewed by 228
Abstract
The Charpy impact resistance of monolithic high-strength and dissimilar structured steel was studied. A gas metal arc welding process was used to fabricate the structured steel by depositing a layer of austenitic stainless steel, followed by a layer of hardfacing material over the [...] Read more.
The Charpy impact resistance of monolithic high-strength and dissimilar structured steel was studied. A gas metal arc welding process was used to fabricate the structured steel by depositing a layer of austenitic stainless steel, followed by a layer of hardfacing material over the high-strength steel plate. ANSYS LS-DYNATM was used to simulate pendulum–striker impacts on steel Charpy samples. A Cowper–Symonds constitutive model was employed to capture the strain rate behavior. The corresponding material constitutive model parameters were obtained from the literature for the monolithic materials; an iterative numerical optimization method was used to couple the parameters of the structured steel simulation and experimental results. Numerical simulation results showed close agreement with experimental ones. Simulation is a valuable tool for explaining the fracture mechanism in the Charpy impact test and can be used to efficiently design parts made of structured steel that will be subjected to impacts or high-speed deformations. Full article
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21 pages, 15073 KB  
Article
Effect of Heat Input on Microstructure and High-Cycle Fatigue Properties of the CGHAZs in Wind Power Steel
by Guodong Zhang, Liyuan Zhu, Jiangli He, Yisen Kong, Qingfeng Wang and Zhongzhu Liu
Metals 2026, 16(6), 635; https://doi.org/10.3390/met16060635 - 9 Jun 2026
Viewed by 277
Abstract
Wind turbine towers rely on welded joints for structural continuity, and the coarse-grained heat-affected zone (CGHAZ) at these joints is the principal site of fatigue damage under service loading. This study characterises the influence of welding heat input on the microstructural constitution, high-cycle [...] Read more.
Wind turbine towers rely on welded joints for structural continuity, and the coarse-grained heat-affected zone (CGHAZ) at these joints is the principal site of fatigue damage under service loading. This study characterises the influence of welding heat input on the microstructural constitution, high-cycle fatigue response, and fracture mechanisms of Gleeble-simulated CGHAZs in a Nb-microalloyed wind power steel. Thermal cycles representative of submerged arc welding at 15, 25, 35, and 45 kJ/cm were applied, and the resulting microstructures were examined by optical microscopy, SEM, EBSD, and TEM. Raising the heat input produced systematic microstructural coarsening: the densities of low-angle grain boundaries (LAGBs) and high-angle grain boundaries (HAGBs) fell by approximately 40% and 26%, respectively, while the mean equivalent diameter (MED) and prior austenite grain (PAG) size grew by roughly 64% and 67%. Life partitioning showed that crack nucleation accounted for more than 84% of total fatigue cycles in every condition, identifying it as the life-governing damage stage. Over the 15-to-45 kJ/cm range, the CGHAZ fatigue strength at 2 × 106 cycles deteriorated from 246.9 MPa to 208.5 MPa (a 15.6% reduction), while the mean fatigue striation spacing widened from 0.142 μm to 0.183 μm (an increase of 28.9%). These results demonstrate that judicious heat-input selection is a practical and effective means of preserving CGHAZ fatigue integrity in wind tower steel fabrication, and they address a previously unresolved gap concerning high-cycle fatigue fracture mechanisms in this critical microstructural zone. Full article
(This article belongs to the Special Issue Recent Advances in High-Performance Steel (2nd Edition))
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24 pages, 8537 KB  
Article
Investigation of Welded Joints of Pipelines from an Existing Gas Transmission Network Exposed to Hydrogen—Part II: Some Aspects of the Microstructural Mechanisms of Hydrogen-Assisted Damage and Fracture
by Boris Yanachkov, Kateryna Valuiska, Yana Mourdjeva, Vanya Dyakova, Krasimir Kolev, Tatiana Simeonova, Rumen Krastev, Stivan Vasilev and Rumyana Lazarova
Metals 2026, 16(6), 573; https://doi.org/10.3390/met16060573 - 24 May 2026
Viewed by 452
Abstract
This study investigates hydrogen embrittlement in welded joints of X52 (L360) pipeline steel obtained from an operating natural gas transmission network after 31 years of service, with particular emphasis on production (longitudinal) and girth (circumferential) welds. The aim is to elucidate the influence [...] Read more.
This study investigates hydrogen embrittlement in welded joints of X52 (L360) pipeline steel obtained from an operating natural gas transmission network after 31 years of service, with particular emphasis on production (longitudinal) and girth (circumferential) welds. The aim is to elucidate the influence of microstructural heterogeneity across the pipe wall and within different welded joint types on hydrogen transport, trapping behavior, and fracture mechanisms. The investigation combines X-ray diffraction, electrochemical hydrogen permeation testing, fractographic analysis, and transmission electron microscopy. X-ray diffraction results show that the base metal and girth weld consist predominantly of body-centered cubic ferrite, whereas the production weld additionally contains retained austenite associated with an elevated manganese content. These phase-related differences are consistent with transmission electron microscopy observations of martensite–austenite constituents within the weld microstructure. Electrochemical hydrogen permeation measurements reveal pronounced microstructure-dependent hydrogen transport behavior. The production weld exhibits a significantly lower apparent diffusion coefficient and a markedly higher hydrogen trap density, approximately five times greater than those of the base metal and girth weld, providing a mechanistic explanation for the observed differences in hydrogen uptake behavior. Fractographic analysis demonstrates a transition from ductile microvoid coalescence in the uncharged condition to predominantly brittle fracture following hydrogen charging. This transition is accompanied by a substantial increase in the fraction of brittle fracture zones, reaching approximately 53% in hydrogen-charged specimens. A pronounced gradient in hydrogen embrittlement susceptibility is observed across the pipe wall thickness, with outer-wall specimens consistently exhibiting greater susceptibility than inner-wall specimens. This behavior reflects the combined influence of long-term soil corrosion and hydrogen-assisted degradation. Transmission electron microscopy reveals that plastic deformation governs dislocation generation, while hydrogen significantly modifies dislocation behavior by promoting dislocation pile-ups near martensite–austenite constituents and non-metallic inclusions. These observations indicate strong interactions between hydrogen, dislocations, and microstructural heterogeneities. A clear size-dependent role of non-metallic inclusions is identified. Sub-micron inclusions act primarily as irreversible hydrogen trapping sites that contribute to hydrogen redistribution within the microstructure, whereas larger inclusions serve as preferential crack initiation sites under hydrogen charging conditions. Overall, the results demonstrate that hydrogen embrittlement behavior is governed by the combined effects of microstructural state, welded joint type, and long-term service-induced degradation, resulting in distinct hydrogen transport characteristics and fracture responses across the pipe wall. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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17 pages, 7855 KB  
Article
Microstructural Evaluation and Tensile Properties for GTAW Weldments of Stainless Steel 304 Seam Pipes
by Eunhye Park and Byounglok Jang
Metals 2026, 16(6), 565; https://doi.org/10.3390/met16060565 - 22 May 2026
Viewed by 316
Abstract
This study examines the microstructural characteristics and tensile properties of autogenous orbital gas tungsten arc (GTA) circumferential butt welds produced on commercially rolled 304 stainless steel seam pipes (outer diameter 38.1 mm, wall thickness 2.0 mm) for high-purity fluid distribution systems. A three-segment [...] Read more.
This study examines the microstructural characteristics and tensile properties of autogenous orbital gas tungsten arc (GTA) circumferential butt welds produced on commercially rolled 304 stainless steel seam pipes (outer diameter 38.1 mm, wall thickness 2.0 mm) for high-purity fluid distribution systems. A three-segment current profile was employed using an AMI 8-4000 orbital system, with peak currents of 70, 67, and 65 A for the penetration, remelting, and downslope (crater-fill) segments, respectively, under high-purity Ar (99.999%) shielding with back purging. Electron backscatter diffraction (EBSD) analysis, including image quality (IQ), inverse pole figure (IPF), and kernel average misorientation (KAM) mapping, showed that the weld metal consists of epitaxially grown columnar austenite grains strongly oriented along the solidification direction, whereas the heat-affected zone (HAZ) exhibits finer equiaxed grains with an increased Σ3 twin boundary fraction and elevated low-angle boundary fraction, indicative of partial recrystallization. Only sparse, discontinuous δ-ferrite stringers were detected in the fusion zone, and no non-metallic inclusions were observed on fracture surfaces, supporting the weld metal’s suitability for semiconductor-grade cleanliness. Vickers microhardness profiles revealed modest hardness differences (typically within 10–20 HV) between the weld metal, HAZ, and base metal, with no pronounced HAZ softening. Cross-weld tensile tests conducted in accordance with ASTM E8/E8M-22 yielded yield strengths above 200 MPa, ultimate tensile strengths of 650–680 MPa, and total elongations approaching 40%, comparable to the as-received pipe. Scanning electron fractography confirmed fully ductile failure via microvoid coalescence without evidence of cleavage, intergranular decohesion, or weld-defect-induced embrittlement. Collectively, these results demonstrate that the three-segment autogenous orbital GTAW procedure produces structurally sound, particle-clean joints suitable for 304 stainless steel seam pipes used in high-purity industrial piping. Full article
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17 pages, 1194 KB  
Article
Material Homogeneity Criterion for Assessing Heterogeneous High-Strength Steel Joints with Austenitic Welds
by Yaroslav Kusyi, Vitalii Ivanov, Andriy Dzyubyk, Nazarii Kusen and Juraj Hajduk
Machines 2026, 14(5), 577; https://doi.org/10.3390/machines14050577 - 21 May 2026
Viewed by 309
Abstract
The modernization of global energy infrastructure within the Industry 5.0 framework requires the use of high-strength steels and reliable joining technologies to ensure safe, sustainable pipeline transport. This study focuses on the analysis of heterogeneous welded joints formed between high-strength alloy steel (34KhN2MA/EN [...] Read more.
The modernization of global energy infrastructure within the Industry 5.0 framework requires the use of high-strength steels and reliable joining technologies to ensure safe, sustainable pipeline transport. This study focuses on the analysis of heterogeneous welded joints formed between high-strength alloy steel (34KhN2MA/EN 34CrNiMo6) and an austenitic welded seam (ER 307). While austenitic welds mitigate the risk of cold cracking, they introduce significant structural and mechanical heterogeneity. To address this, the research proposes and validates a material homogeneity criterion (MHC) derived from the LM-hardness methodology. By analyzing the statistical dispersion of macrohardness (HRC) through indicators such as the Weibull homogeneity coefficient (m) and the coefficient of variation (ν), the study establishes a quantitative approach to assess material degradation and structural uniformity across key weld zones. Results demonstrate that macrohardness profiling effectively distinguishes between structurally heterogeneous regions near the weld axis characterized by low homogeneity coefficients (m = 4.04 < 10, Am = 0.742 < 0.878), elevated variability (ν = 29.68% > 11.6%), and high technological damageability (D = 0.92 > 0.81, jD = 11.87 > 4.38) with pronounced step-like variation in macrohardness (HRC ∈ [12.6; 47]), on the one hand, and stabilized homogeneous zones in the base material, where m = 24.89 > 10, Am = 0.947 > 0.878, ν = 4.39% < 11.6%, D = 0.52 ⟶ 0, jD = 1.09 ⟶ 0, and characteristic range of HRC = 47–55, on the other hand. This methodology provides a robust, quasi-non-destructive tool for enhancing predictive maintenance, digital twins, and the overall integrity management of “smart” pipeline systems. Full article
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18 pages, 3417 KB  
Article
Dual Beam Laser Welding of Superduplex Stainless Steel: Microstructure, Mechanical Properties, and Electrochemical Behavior
by Lucia Kopčanová, Tomáš Dvorák, María Angeles Arenas, Erika Hodúlová, Ana Conde, Miroslav Čavojský, Juan Jose de Damborenea, Martin Nosko and Nad’a Beronská
J. Manuf. Mater. Process. 2026, 10(5), 181; https://doi.org/10.3390/jmmp10050181 - 21 May 2026
Viewed by 708
Abstract
Dual beam laser welding of UNS S32750 superduplex stainless steel was performed to investigate the effect of beam-power distribution on microstructure and mechanical properties. Plates with a thickness of 3 mm were welded at a constant total power and travel speed using leading [...] Read more.
Dual beam laser welding of UNS S32750 superduplex stainless steel was performed to investigate the effect of beam-power distribution on microstructure and mechanical properties. Plates with a thickness of 3 mm were welded at a constant total power and travel speed using leading and lagging power splits of 50:50, 80:20, and 65:35. The heat affected zone width was metallographically estimated at approximately 100 µm for all conditions, consistent with comparable gross thermal exposure under constant nominal linear energy input (Ptotal/v). A slight modification to the power distribution altered the solidification texture and austenite morphology. The 50:50 configuration produced a refined ferritic matrix with a continuous network of grain boundaries, Widmanstätten, and intragranular acicular austenite. The 80:20 condition increased ferrite path continuity, while the 65:35 split produced an intermediate morphology. Vickers hardness reached a maximum for the 80:20 split (HAZ: 345 HV; weld metal: 349 HV). Ultimate tensile strength remained statistically constant between 908 MPa and 914 MPa, whereas elongation decreased from 28% at 50:50 to 24% at 80:20 and 23% at 65:35. All welds exhibited ductile fracture with microvoid coalescence, and electrochemical performance was comparable, with critical pitting temperature values between 78 °C and 91 °C. Beam power distribution primarily affects solidification morphology and enables control of the hardness-to-ductility balance, with a 50:50 split providing the most favorable combination of properties. Full article
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22 pages, 18580 KB  
Article
Effect of Ni Element in Self-Shielded Flux-Cored Wires on the Microstructural and Mechanical Property Evolutions of X80 Pipeline Steel Girth Welds
by Shujun Jia, Chengwu Cui, Chunliang Mao, Gang Liu and Qingyou Liu
Materials 2026, 19(10), 2162; https://doi.org/10.3390/ma19102162 - 21 May 2026
Viewed by 302
Abstract
In the present work, eleven self-shielded flux-cored wires with nickel (Ni) contents ranging from 1.42 wt.% to 4.02 wt.% were designed for the semi-automatic welding of X80 pipeline steel. The effects of Ni on the microstructural evolution and mechanical properties of the weld [...] Read more.
In the present work, eleven self-shielded flux-cored wires with nickel (Ni) contents ranging from 1.42 wt.% to 4.02 wt.% were designed for the semi-automatic welding of X80 pipeline steel. The effects of Ni on the microstructural evolution and mechanical properties of the weld metal were investigated. The results indicate that when the Ni content is below 2.06 wt.%, the microstructures of both the solidification zone and the inter-pass reheating zone are dominated by coarse granular bainite and martensite/austenite (M/A) constituents. As the Ni content increases from 2.06 wt.% to 3.73 wt.%, the microstructure transforms to fine lath bainite with M/A constituents characterized by low content, small size, and uniform distribution. When the Ni content reaches 3.73 wt.%, the microstructure becomes almost fully bainite. Furthermore, with increasing the Ni content, both the yield strength and tensile strength of the weld metal increase from ~600 MPa to ~700 MPa and from ~660 MPa to ~730 MPa, respectively. However, the impact energy at −20 °C of the weld metal initially increases and then decreases, reaching a peak of ~110 J with the lowest degree of dispersion at a Ni content of approximately 3.73 wt.%. When the Ni content exceeds 3.73 wt.%, the ductility decreases slightly. Further analyses indicate that the synergistic effects of Ni in refining the microstructure and reducing the activity coefficient and solubility of nitrogen (N) jointly contribute to the impact toughness of the weld metal. Full article
(This article belongs to the Section Metals and Alloys)
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17 pages, 4357 KB  
Article
Effect of Nb on Solidification Cracking, Mechanical Properties and Corrosion Resistance of 310S Austenitic Stainless-Steel Welded Joints
by Yulu Su, Dan Wang and Xulei Wu
Metals 2026, 16(5), 554; https://doi.org/10.3390/met16050554 - 19 May 2026
Viewed by 257
Abstract
In this study, 310S austenitic stainless-steel was welded using a laser with varying amounts of Nb to systematically investigate the effect of Nb on solidification cracking susceptibility, mechanical properties, and corrosion resistance of the weld. Under the present experimental conditions, the critical restraint [...] Read more.
In this study, 310S austenitic stainless-steel was welded using a laser with varying amounts of Nb to systematically investigate the effect of Nb on solidification cracking susceptibility, mechanical properties, and corrosion resistance of the weld. Under the present experimental conditions, the critical restraint width was higher for the 0.58 wt.% Nb and 1.45 wt.% Nb welds than for the Nb-free and 2.3 wt.% Nb welds, indicating that Nb addition affected the solidification cracking response of the weld. At low-to-moderate Nb contents, Nb can aggravate compositional segregation and increase the presence of low-melting-point liquid films, thereby increasing cracking susceptibility. At higher Nb contents, the reduced cracking susceptibility was accompanied by microstructural refinement and changes in the distribution of Nb-rich constituents during solidification. With increasing Nb content, the number of precipitated phases in the weld increases, mainly distributed at the austenite grain boundaries in granular, elongated, and chain-like forms. The introduction of Nb generally increases the microhardness and tensile strength of the welded joint, attributed to grain refinement strengthening and solid-solution strengthening. The reduction in area first increased and then decreased, suggesting that excessive Nb addition may reduce ductility because of the increased amount of grain-boundary precipitates and local strengthening heterogeneity. With increasing Nb content, the Ir/Ia ratio decreased from 67.6% to 52.2%, suggesting improved intergranular corrosion resistance. This improvement is likely related to the preferential reaction of Nb with carbon, which may suppress the formation of Cr-depleted zones at grain boundaries. Overall, Nb addition improved the corrosion resistance and increased the hardness and tensile strength of the weld; however, its effect on solidification cracking susceptibility was non-monotonic, indicating that careful control of Nb content is required to balance cracking susceptibility, mechanical properties, and corrosion resistance. Full article
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21 pages, 10168 KB  
Article
Assessment of Geometric Scaling Factors and Anisotropic Phase Formation in GMAW-Additively Manufactured Duplex Stainless Steel (ER2209) Components
by Uhamir Patrick, Stefanija Klaric and Sara Havrlisan
Technologies 2026, 14(5), 288; https://doi.org/10.3390/technologies14050288 - 8 May 2026
Viewed by 555
Abstract
Duplex stainless steel (DSS) blends impressive mechanical and chemical characteristics to withstand aggressive environments. Its fabrication by Gas Metal Arc Welding-Additive Manufacturing is an emerging research topic. However, its sensitive grain structure and alloy composition are prone to deterioration by repeated thermal shocks. [...] Read more.
Duplex stainless steel (DSS) blends impressive mechanical and chemical characteristics to withstand aggressive environments. Its fabrication by Gas Metal Arc Welding-Additive Manufacturing is an emerging research topic. However, its sensitive grain structure and alloy composition are prone to deterioration by repeated thermal shocks. Whether optimal weld parameters can resolve these challenges without additional costs from special fillers, gases, or mechanisms is a valid question. In this study, how different wire feed speeds, travel speeds, and weld voltages, chosen from a set of preliminary beads, translate into wall dimensions, phase formation and distribution, morphological transformation, and elemental segregation is investigated. The unique DSS microstructures were characterised using scanning electron microscopy and energy-dispersive spectroscopy to reveal differences in microstructural evolution and ferrite-austenite (α-γ) structure. The deposited walls exhibited satisfactory geometric quality with negligible distortions. However, the height suppression was noticeable at the deposition energy (DE) of 755 J/mm. Metallographic analysis revealed low γ phase formation (<30%) at low DE (230 J/mm) and excessive γ formation (>70%) in the high DE wall (755 J/mm). The parameters WFS:TS = 15, TS = 35 cm/min, WFS = 525 cm/min, and V = 20.804 volts suppressed the elemental segregation while maintaining a suitable phase balance without post-processing. Full article
(This article belongs to the Section Innovations in Materials Science and Materials Processing)
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20 pages, 3430 KB  
Article
Optimization of Resistance Spot Welding Parameters and Shielding Atmosphere Effects on the Mechanical Performance of AISI 201 Stainless Steel
by Eddie Gazo-Hanna, Ahmed Saber, Semaan Amine, Rasha Afify, Essam B. Moustafa and Ahmed O. Mosleh
J. Manuf. Mater. Process. 2026, 10(5), 153; https://doi.org/10.3390/jmmp10050153 - 28 Apr 2026
Viewed by 1157
Abstract
Attaining uniform weld quality in the resistance spot welding (RSW) of AISI 201 stainless steel remains challenging due to the complex interdependence of process parameters and the limited understanding of shielding atmosphere effects on this lean austenitic grade. This study integrates Taguchi optimization, [...] Read more.
Attaining uniform weld quality in the resistance spot welding (RSW) of AISI 201 stainless steel remains challenging due to the complex interdependence of process parameters and the limited understanding of shielding atmosphere effects on this lean austenitic grade. This study integrates Taguchi optimization, analysis of variance (ANOVA), and complementary trend surface visualization to evaluate the effects of welding time, current, electrode pressure, and shielding atmosphere. An L27 orthogonal array was employed, with welding current identified as the dominant parameter for both tensile strength and hardness while nitrogen shielding exhibited a significantly greater influence on hardness than on tensile force, attributable to interstitial solid solution strengthening. The optimal conditions yielded a maximum tensile force of 12.2 kN and a hardness of 353 HV, with prediction errors below 1.5% for tensile force and below 0.5% for hardness. Trend surface visualization further revealed significant current–pressure interactions governing weld quality. These findings provide a validated optimization framework for the industrial RSW of AISI 201, with direct implications for automotive and structural manufacturing. Full article
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17 pages, 32853 KB  
Article
Behavior and Microstructural Evolution of Welded AISI 304 Steel Exposed to Solar Salt Under CSP-Relevant Conditions
by Abdiel Mallco, Mauricio Lague, Fabiola Pineda, Claudia Carrasco, Javier Núñez, Grover Viracochea, Victor Vergara and Carlos Portillo
Processes 2026, 14(9), 1407; https://doi.org/10.3390/pr14091407 - 28 Apr 2026
Viewed by 472
Abstract
While cost-effective austenitic stainless steels like AISI 304 are utilised in intermediate-temperature concentrated solar power (CSP) components, autogenous welding can compromise their structural integrity. This work investigates the corrosion behaviour of autogenous TIG-welded AISI 304 joints exposed to commercial molten solar salt at [...] Read more.
While cost-effective austenitic stainless steels like AISI 304 are utilised in intermediate-temperature concentrated solar power (CSP) components, autogenous welding can compromise their structural integrity. This work investigates the corrosion behaviour of autogenous TIG-welded AISI 304 joints exposed to commercial molten solar salt at 550 °C for up to 1350 h under static conditions. Gravimetric and microstructural analyses revealed a stochastic bimodal breakaway oxidation mechanism. After an initial transient passivation regime (0–650 h) attributed to the formation of a protective Fe3O4/FeCr2O4 bi-layer, a sharp kinetic acceleration occurred. This localized breakdown was synergistically catalysed by trace chloride impurities, which triggered deep pitting along the microsegregated dendritic networks of the weld metal. Furthermore, due to severe X-ray attenuation under massive late-stage oxides, definitive proof of sensitisation was established using the standardised ASTM A262 Practice A topographic evaluation. The appearance of continuous ditch structures only in the heat-affected zone (HAZ) suggests severe intergranular anodic dissolution. This failure is thermodynamically driven by unmitigated residual tensile stresses, highlighting that the long-term reliability of these components is interpreted to be dictated by the localised, asymmetric breakdown of the weldment rather than uniform global oxidation. Full article
(This article belongs to the Special Issue Advances in Solar Energy and Heat Storage Systems)
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14 pages, 17178 KB  
Article
Investigation on the Microstructure and Mechanical Properties of 304 Stainless Steel Joints by Underwater Local Dry Laser Welding
by Xiaodong Zhang, Fangjie Cheng, Yingchao Feng, Jinping Liu, Zhuyuan Li, Yehua Wu, Ke Han and Qianxing Yin
Materials 2026, 19(9), 1723; https://doi.org/10.3390/ma19091723 - 23 Apr 2026
Viewed by 1364
Abstract
In order to verify the feasibility of in situ repair of underwater local dry laser welding (ULDLW) on nuclear power reactor components, this work investigates the microstructure and mechanical properties of 304L austenitic stainless steel repaired by ULDLW using ER308L filler metal. Comprehensive [...] Read more.
In order to verify the feasibility of in situ repair of underwater local dry laser welding (ULDLW) on nuclear power reactor components, this work investigates the microstructure and mechanical properties of 304L austenitic stainless steel repaired by ULDLW using ER308L filler metal. Comprehensive comparison would be made between the ULDLW and conventional in-air laser welding to evaluate their applicability. The results demonstrate that the rapid cooling rate inherent to the underwater environment significantly influences solidification behavior and microstructural evolution. The weld metal (WM) solidifies in the ferritic–austenitic (FA) mode, with an increased proportion of lathy δ-ferrite at the expense of skeletal morphology compared to the in-air welds. Electron backscatter diffraction (EBSD) analysis reveals the substantial grain refinement in underwater welds, with average grain sizes of 39.4 μm versus 47.3 μm for in-air weld bead, accompanied by a higher fraction of low-angle grain boundaries (LAGBs). These microstructural modifications yield superior mechanical properties: underwater weld bead exhibits ultimate tensile strength (UTS) of 685.6 MPa, elongation of 57.5%, and impact toughness of 22.6 J, significantly exceeding the corresponding values for in-air welds (663.9 MPa, 51.8%, and 18.6 J, respectively). Fractographic analysis confirms ductile fracture mechanisms in both conditions. The enhanced performance is attributed to grain refinement strengthening via the Hall–Petch relationship and the increased LAGBs fraction, which impedes dislocation motion and crack propagation. Full article
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