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Search Results (981)

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Keywords = abrasive wear resistance

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19 pages, 6005 KB  
Article
Stress Analysis and Wear-Resistant Optimization of Shield Cutterhead in Sandy Cobble Strata Using Discrete Element Method
by Zhe Liu, Zhiyong Yang, Dingtao Kou, Qingquan Lu, Yingtao Sun and Yusheng Jiang
Appl. Sci. 2026, 16(3), 1180; https://doi.org/10.3390/app16031180 - 23 Jan 2026
Viewed by 50
Abstract
To address the challenges of wear resistance for shield cutterheads and cutters in high-abrasion sandy cobble strata, this study uses the Beijing Metro Line 19 tunnel Niujie–Jinrongjie section as an engineering case study. It employs the DEM to develop a crushable sandy cobble [...] Read more.
To address the challenges of wear resistance for shield cutterheads and cutters in high-abrasion sandy cobble strata, this study uses the Beijing Metro Line 19 tunnel Niujie–Jinrongjie section as an engineering case study. It employs the DEM to develop a crushable sandy cobble model, evaluate the stress characteristics of fishtail cutters, rippers, and scrapers, and analyze load distribution in the cutterhead and cutters—including underlying causes. Based on simulations, the study proposes and implements targeted wear-resistant designs for field application. The results indicate that the stress variation patterns of fishtail cutters, rippers, and scrapers with respect to time and installation radius are similar. The cutterhead’s opening distribution significantly influences the intensity of normal and lateral stresses. Caused by cutting resistance, high-stress loads in cutters accumulate at the cutting edge, while those in the cutterhead localize to the soil-facing side of its spokes. Meanwhile, hindered muck flow and cutting failure of gauge cutters also cause stress concentration in the cutterhead’s transition zones and outer side of the large ring. Adopting a DEM-based method that characterizes the stress of the cutterhead and cutters to develop targeted wear-resistant designs can effectively control the wear of cutters and cutterheads in in situ engineering. The rate of abnormal cutter damage was limited to merely 5.84%, while the observed wear of the ripper cutters remained consistently below the values predicted by the IHI empirical model. This study provides a scientific basis for wear-resistant design of cutterheads in similar high-abrasion strata. Full article
(This article belongs to the Section Civil Engineering)
22 pages, 51561 KB  
Article
Effect of V Content on Microstructure and Properties of TiNbZrVx Medium-Entropy Alloy Coatings on TC4 Substrate by Laser Cladding
by Wen Zhang, Ying Wu, Chuan Yang, Yongsheng Zhao, Zhenhong Wang, Jia Yang, Wei Feng, Yang Deng, Junjie Zhang, Qingfeng Xian, Xingcheng Long, Zhirong Liang and Hui Chen
Coatings 2026, 16(1), 141; https://doi.org/10.3390/coatings16010141 - 22 Jan 2026
Viewed by 44
Abstract
In order to improve the wear resistance of titanium alloy and apply it to the high-speed train brake disc, TiNbZrVx (x = 0, 0.2, 0.4, 0.6, 0.8) refractory medium-entropy alloy coatings were prepared on Ti-6Al-4V (TC4) substrate. The effect of V content [...] Read more.
In order to improve the wear resistance of titanium alloy and apply it to the high-speed train brake disc, TiNbZrVx (x = 0, 0.2, 0.4, 0.6, 0.8) refractory medium-entropy alloy coatings were prepared on Ti-6Al-4V (TC4) substrate. The effect of V content on the microstructure, mechanical properties, and friction and wear properties of the coatings was studied. TiNbZrVx coatings achieved good metallurgical bonding with the substrate, forming BCC and B2 phases and AlZr3 intermetallic compound (IMC). From TiNbZr coating to TiNbZrV0.8 coating, V promotes element segregation and new phase formation, which decreased the average grain size from 85.055 μm to 56.515 μm, increased the average hardness from 265.5 HV to 343.4 HV, and reduced the room temperature (RT) wear rate by 97.8%. However, the ductility of the coatings decreased from 15.7% to 5.8% because the grain boundary precipitates changed the dislocation arrangement, and the tensile fracture mode changed from ductile fracture to brittle fracture. Abrasive wear was the main wear mode at RT, and adhesive wear and oxidation wear were the main wear modes at elevated temperature. The COF at elevated temperature was lower than that at RT, because a large number of friction pair components were transferred to the coating surface at high temperature and were repeatedly rolled to form a dense film, which played a certain lubricating role. Full article
(This article belongs to the Section Laser Coatings)
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20 pages, 2130 KB  
Article
Microstructural, Hardness, and Abrasive Wear Properties of Functionally Graded Al/ZrB2 Composites Produced by In Situ Centrifugal Casting
by İbrahim Güney, Ömer Faruk Demirok, Yunus Emre Benkli, Çağlar Yüksel and Ömer Savaş
Metals 2026, 16(1), 125; https://doi.org/10.3390/met16010125 - 21 Jan 2026
Viewed by 172
Abstract
Functionally graded aluminum matrix composites are of interest for applications requiring region-dependent mechanical and tribological performance. In this study, the micro-structure, hardness, and abrasive wear properties of functionally graded Al/ZrB2 compo-site materials produced by an in situ centrifugal casting method were investigated. [...] Read more.
Functionally graded aluminum matrix composites are of interest for applications requiring region-dependent mechanical and tribological performance. In this study, the micro-structure, hardness, and abrasive wear properties of functionally graded Al/ZrB2 compo-site materials produced by an in situ centrifugal casting method were investigated. The ZrB2 reinforcement phase was synthesized in situ within the molten aluminum matrix, and functional grading was achieved through the action of centrifugal force during solidification. Samples taken from cylindrical castings were characterized using optical microscopy, scanning electron microscopy (SEM), X-Ray diffraction (XRD), density measurements, Brinell hardness testing, and abrasive wear experiments. Phase analyses con-firmed the successful in situ formation of ZrB2 and verified that the phase distribution in-creased toward the direction of centrifugal force. Hardness increased with reinforcement content, rising from approximately 28 HB in the matrix-rich region to 68 HB and 72 HB in regions reinforced with 12% and 15% ZrB2, respectively. Abrasive wear behavior was evaluated using the pin-on-disk method, and a Taguchi L (35) orthogonal array was employed for experimental design. Statistical analyses showed that the composite region was the most influential parameter affecting wear performance, followed by abrasive particle size and applied load, while sliding distance and sliding speed were not statistically significant. These findings demonstrate that in situ centrifugal casting is an effective approach for producing functionally graded Al/ZrB2 composites with improved hardness and wear resistance. Full article
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19 pages, 4052 KB  
Article
Microstructure and Wear Resistance of (Mg2Si + SiCp)/Al Composites
by Dekun Zhou, Xiaobo Liu and Miao Yang
Metals 2026, 16(1), 111; https://doi.org/10.3390/met16010111 - 18 Jan 2026
Viewed by 172
Abstract
The microstructure and wear behaviors of Mg2Si/Al composites with 0 wt.%, 5 wt.%, and 10 wt.% SiC particles were studied using XRD, OM observation, SEM observation, EDS analysis, an extraction experiment, a hardness test, and the dry sliding wear test. It [...] Read more.
The microstructure and wear behaviors of Mg2Si/Al composites with 0 wt.%, 5 wt.%, and 10 wt.% SiC particles were studied using XRD, OM observation, SEM observation, EDS analysis, an extraction experiment, a hardness test, and the dry sliding wear test. It is shown by the results that after the addition of 10 wt.% SiC particles, the population of primary Mg2Si particles increased, while the mean size of these particles reduced from 40 ± 10 μm (in the SiC-free composite) to 25 ± 8 μm. Both the matrix and the eutectic structure were refined. The tetrakaidecahedral morphologies of Mg2Si crystals were confirmed by the results of extraction tests. The wear test results with GCr15 steel as the friction pair show that the Mg2Si/Al composite with 10 wt.% SiC particles displayed more favorable wear resistance than the specimens with 0 wt.% and 5 wt.% SiC particle additions under both constant load and constant sliding velocity conditions. Under applied loads of 10 N, 20 N, and 30 N at a fixed sliding speed of 300 r/min, the wear rate of the Mg2Si-Al composites reinforced with 10 wt.% SiC particles was 36.01%, 48.29%, and 23.32% lower than that of the SiC-free composites, respectively. When the sliding speed was set to 300 r/min, 550 r/min, 750 r/min, and 1000 r/min under a constant applied load of 20 N, the wear rate of the 10 wt.% SiC-reinforced Mg2Si-Al composites was reduced by 40.37%, 40.87%, 26.20%, and 25.78%, respectively, compared with the SiC-free counterparts. The wear failure mechanisms of (Mg2Si + SiCP)/Al composites were mainly adhesive wear and abrasive wear, but the proportion of oxidation wear increased after the addition of the SiC particles. Full article
(This article belongs to the Special Issue Recent Advances in Forming Processes of Lightweight Metals)
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15 pages, 5573 KB  
Article
The Microstructure and Properties of Hard Anodic Oxide Coatings on 5754 Aluminium Alloy Modified with Al2O3, PTFE and CaCO3 Nanoparticles
by Anna Kozik, Marek Nowak, Kamila Limanówka and Anna Góral
Materials 2026, 19(2), 378; https://doi.org/10.3390/ma19020378 - 17 Jan 2026
Viewed by 125
Abstract
Hard anodic oxide coatings on aluminium have long been used to enhance surface functionality. However, increasing industrial demands are driving the need for coatings with superior hardness, wear resistance, corrosion resistance and self-lubricating properties. Due to their porous structure, anodic oxide coatings can [...] Read more.
Hard anodic oxide coatings on aluminium have long been used to enhance surface functionality. However, increasing industrial demands are driving the need for coatings with superior hardness, wear resistance, corrosion resistance and self-lubricating properties. Due to their porous structure, anodic oxide coatings can be modified by incorporating various nanoparticles. The properties of the modified coatings depend on both the type of nanoparticles used and the method employed to incorporate them. In this study, anodic oxide coatings were produced using direct and duplex methods on a semi-industrial scale to enable process control and potential industrial implementation. The coatings were modified with hard (Al2O3) and soft (CaCO3, PTFE) nanoparticles in order to customise their functional properties. Their microstructure and chemical composition were characterised by SEM and TEM. Their microhardness, abrasion resistance and electrochemical behaviour were also evaluated. Among the tested production methods and methods for modifying nanoparticles, the duplex process incorporating Al2O3 particles proved to be the most promising. Its optimisation resulted in coatings with a microhardness of 430 HV0.05 and a mass loss of 9.4 mg after the Taber abrasion test, demonstrating the potential of this approach for industrial applications. Full article
(This article belongs to the Special Issue Advances in Electrodeposition of Thin Films and Alloys)
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23 pages, 5255 KB  
Article
Analysis of Wear Behavior Between Tire Rubber and Silicone Rubber
by Juana Abenojar, Miguel Angel Martínez and Daniel García-Pozuelo
Appl. Sci. 2026, 16(2), 878; https://doi.org/10.3390/app16020878 - 14 Jan 2026
Viewed by 194
Abstract
Vulcanized NR-SBR is widely used in vehicle components; however, its irreversible crosslinking limits recyclability and contributes to the large number of tires discarded annually worldwide, and in this context, this work presents an experimental comparative assessment of the tribological behavior of conventional tire [...] Read more.
Vulcanized NR-SBR is widely used in vehicle components; however, its irreversible crosslinking limits recyclability and contributes to the large number of tires discarded annually worldwide, and in this context, this work presents an experimental comparative assessment of the tribological behavior of conventional tire rubber and silicone VMQ, motivated by a wheel concept based on a detachable tread aimed at improving durability and sustainability rather than proposing an immediate material substitution. Wear and friction behavior were investigated under abrasive and self-friction conditions using pin-on-disk testing with an abrasive counterpart representative of asphalt, supported by optical and scanning electron microscopy. The results show that NR-SBR undergoes severe abrasive and erosive wear, characterized by deep and irregular wear tracks, pronounced fluctuations in the dynamic friction coefficient, and strong sensitivity to load and sliding speed, particularly during the initial stages of track formation. In contrast, VMQ exhibits mild abrasive wear dominated by viscoelastic deformation, leading to shallow and stable wear tracks, lower friction coefficients, and significantly reduced material loss once the contact track is fully developed. These differences are attributed to the distinct mechanical responses of the elastomers, as the higher hardness and limited strain capacity of rubber promote micro-tearing and unstable material removal, while the high elasticity of silicone enables stress redistribution and stable contact conditions under abrasive loading. UV aging increases stiffness of rubber, resulting in reduced wear and friction, while silicone remains largely unaffected after 750 h due to the stability of its Si–O–Si backbone. Self-friction tests further indicate that smooth silicone sliding against rubber yields the lowest friction values, highlighting a favorable material pairing for detachable tread concepts. Factorial design analysis confirms material type as the dominant factor influencing both wear and friction. Overall, for the specific materials and operating conditions investigated, VMQ demonstrates higher durability, greater tribological stability, and improved aging resistance compared to NR-SBR, providing experimental evidence that supports its potential for long-life, more sustainable detachable tread applications. Full article
(This article belongs to the Section Materials Science and Engineering)
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63 pages, 16077 KB  
Review
Problems with Intake Air Filtration in Piston and Turbine Combustion Engines Used in Conditions of High Air Dust Content
by Tadeusz Dziubak
Energies 2026, 19(2), 388; https://doi.org/10.3390/en19020388 - 13 Jan 2026
Viewed by 156
Abstract
The operating conditions of engines in motor vehicles used in conditions of high air dustiness resulting from sandy ground and helicopters using temporary landing sites were analyzed. The impact of mineral dust on accelerated abrasive and erosive wear of components and assemblies of [...] Read more.
The operating conditions of engines in motor vehicles used in conditions of high air dustiness resulting from sandy ground and helicopters using temporary landing sites were analyzed. The impact of mineral dust on accelerated abrasive and erosive wear of components and assemblies of piston and turbine engines was presented. Attention was drawn to the formation of dust deposits on turbine engine components. Possibilities for minimizing abrasive wear through the use of two-stage intake air filtration systems in motor vehicle engines were presented. Three forms of protection for helicopter engines against the intake of dust-laden air and for extending their service life are presented: intake barrier filters (IBF), tube separators (VTS), and particulate separators (IPS) called Engine Air Particle Separation (EAPS). It has been shown that pleating the filter bed significantly increases the filtration area. It has been shown that increasing the suction flow from inertial filters increases separation efficiency and flow resistance. IPS are characterized by a compact design, low external resistance, and no need for periodic maintenance, but it has a lower separation efficiency (86–91%) than VTS and IBF systems (up to 99.3–99.9%). The tested “cyclone-partition filter” filtration system achieves a filtration efficiency of 99.9%, reaching the acceptable pressure drop value four times slower than if it were operating without a cyclone. Two-stage filtration systems ensure high friction durability at the lowest possible energy costs. Full article
(This article belongs to the Section I2: Energy and Combustion Science)
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16 pages, 6941 KB  
Article
Microstructural, Corrosion and Mechanical Properties of Ni–Al–Cr/SiC Coatings on Inconel 600 Deposited by Arc Welding
by Tayfun Çetin
Crystals 2026, 16(1), 49; https://doi.org/10.3390/cryst16010049 - 11 Jan 2026
Viewed by 236
Abstract
In this study, the microstructural, mechanical, wear, and corrosion behavior of Ni-Al-Cr and Ni–Al–Cr/SiC composite coatings with different composition ratios, produced by electric arc melting on Inconel 600 substrates, was systematically investigated. Microhardness measurements revealed a significant and consistent increase in the hardness [...] Read more.
In this study, the microstructural, mechanical, wear, and corrosion behavior of Ni-Al-Cr and Ni–Al–Cr/SiC composite coatings with different composition ratios, produced by electric arc melting on Inconel 600 substrates, was systematically investigated. Microhardness measurements revealed a significant and consistent increase in the hardness values of the coatings depending on the increase in SiC reinforcement ratio (1%, 3%, and 5%). Wear tests showed that the coated samples exhibited significantly higher wear resistance compared to the pure Inconel 600 substrate. A significant improvement in wear resistance was achieved with the addition of SiC at 1% and 3% weight percentages; the width and depth of wear tracks were significantly reduced with SiC reinforcement. In contrast, increasing the SiC ratio to 5% weight percentage led to a decrease in wear resistance. This was attributed to particle aggregation at high SiC content, weakening of bonds at the matrix-reinforcement interface, and the behavior of SiC particles separated from the matrix as third-body abrasives. Electrochemical corrosion tests have shown that SiC-reinforced coatings form a more stable and permanent passive film, and corrosion resistance increases as the SiC content increases (1%, 3%, and 5%). The results indicate that the SiC reinforcement ratio affects the mechanical and electrochemical properties of Ni-Al-Cr/SiC composite coatings produced by electric arc melting. Full article
(This article belongs to the Special Issue Microstructure Analysis, Phase Composition and Properties of Metal)
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11 pages, 4386 KB  
Article
Tribological Performance Under Silica Debris in PAO–Fe Interfaces: An Atomistic Study
by Xiang Jiao, Guochen Huang, Yuyan Zhang, Juan Li, Chenchen Peng and Guoqing Wang
Coatings 2026, 16(1), 91; https://doi.org/10.3390/coatings16010091 - 11 Jan 2026
Viewed by 326
Abstract
Silica-rich dust intrusion is a persistent challenge for lubrication systems in agricultural machinery, where abrasive third-body particles can accelerate wear and shorten component service life. Here, molecular dynamics simulations are employed to elucidate how SiO2 nanoparticle contamination degrades polyalphaolefin (PAO) boundary lubrication [...] Read more.
Silica-rich dust intrusion is a persistent challenge for lubrication systems in agricultural machinery, where abrasive third-body particles can accelerate wear and shorten component service life. Here, molecular dynamics simulations are employed to elucidate how SiO2 nanoparticle contamination degrades polyalphaolefin (PAO) boundary lubrication at the atomic scale. Two confined sliding models are compared: a pure PAO film and a contaminated PAO film containing 7 wt% SiO2 nanoparticles between crystalline Fe substrates under a constant normal load and sliding velocity. The contaminated system exhibits a higher steady-state friction force, faster lubricant film disruption and migration, and consistently higher interfacial temperatures, indicating intensified energy dissipation. Substrate analyses reveal deeper and stronger von Mises stress penetration, increased severe plastic shear strain, elevated Fe potential energy associated with defect accumulation, and reduced structural order. Meanwhile, PAO molecules store more intramolecular deformation energy (bond, angle, and dihedral terms), reflecting stress concentration and disturbed shear alignment induced by nanoparticles. These results clarify the multi-pathway mechanisms by which abrasive SiO2 contaminants transform PAO from a protective boundary film into an agent promoting abrasive wear, providing insights for designing wear-resistant lubricants and improved filtration strategies for particle-laden applications. Full article
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24 pages, 12322 KB  
Article
Research on the Properties of Clad Layers Applied to Biomass Shredding Tools
by Ján Viňáš, Milan Fiľo, Janette Brezinová, Miroslav Džupon, Viktor Puchý, Jakub Brezina, Samuel Mikita, Gyula Bagyinszki and Péter Pinke
Metals 2026, 16(1), 74; https://doi.org/10.3390/met16010074 - 8 Jan 2026
Viewed by 181
Abstract
This paper investigates the applicability of plasma transferred arc (PTA) cladding for extending the service life of biomass shredder tools. The study evaluates the possibility of replacing Hardox 500 steel with a lower-cost structural steel S355J2 whose functional surfaces are modified by PTA [...] Read more.
This paper investigates the applicability of plasma transferred arc (PTA) cladding for extending the service life of biomass shredder tools. The study evaluates the possibility of replacing Hardox 500 steel with a lower-cost structural steel S355J2 whose functional surfaces are modified by PTA cladding. Three commercially available powder fillers were examined: CoCrWNi (PL1), FeCoCrSi (PL2), and NiCrMoFeCuBSi (PL3). The quality and performance of the cladded layers were assessed through hardness measurements, microstructural analysis using SEM and EDX, and tribological testing focused on abrasive and adhesive wear at room temperature. The results showed that the PL1 cladding achieved the highest surface hardness, reaching up to 602 HV0.1, due to the presence of hard carbide phases. In contrast, the PL2 cladding exhibited the best resistance to abrasive wear, demonstrating the lowest mass loss for both as-deposited and machined surfaces. The PL3 cladding showed intermediate performance in terms of wear resistance. Overall, the findings indicate that PTA cladding using an FeCoCrSi-based filler on an S355J2 substrate represents a promising and cost-effective alternative to Hardox 500 for biomass shredder applications. Full article
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14 pages, 2815 KB  
Article
Preparation and Research of a Metal Anti-Corrosion Coating Based on PDMS Reinforcement
by Chenyan Xie, Peng Dou, Gaojie Fu, Jiaqi Wang, Zeyi Wei, Xinglin Lu, Suji Sheng, Lixin Yuan and Bin Shen
Coatings 2026, 16(1), 74; https://doi.org/10.3390/coatings16010074 - 8 Jan 2026
Viewed by 275
Abstract
Metal materials are widely used in power grid infrastructure, but they are prone to metal corrosion due to long-term exposure to various environmental conditions, resulting in significant losses. The existing superhydrophobic coatings have good anti-corrosion performance, but poor wear resistance. Therefore, it is [...] Read more.
Metal materials are widely used in power grid infrastructure, but they are prone to metal corrosion due to long-term exposure to various environmental conditions, resulting in significant losses. The existing superhydrophobic coatings have good anti-corrosion performance, but poor wear resistance. Therefore, it is extremely important to improve the wear resistance of superhydrophobic coatings. In this study, a kind of fluorine-modified SiO2 particle was prepared with pentafluorooctyltrimethoxysilane (FAS-13) as the low surface energy modifier, following the fabrication of a superhydrophobic coating on metal substrate via a PDMS-doped spray deposition method to reinforcement wear resistance property. XPS, FT-IR and Raman spectra confirmed the successful introduction of FAS-13 on SiO2 particles, as evidenced by the characteristic fluorine-related peaks. TGA revealed that the fluorine modified SiO2 (F-SiO2) particles exhibited excellent thermal stability, with an initial decomposition temperature of 354 °C. From the perspective of surface morphology, the relevant data indicated a peak-to-valley height difference of only 88.7 nm, with Rq of 11.9 nm and Ra of 8.86 nm. And it also exhibited outstanding superhydrophobic property with contact angle (CA) of 164.44°/159.48°, demonstrating remarkable self-cleaning performance. And it still maintained CA of over 150° even after cyclic abrasion of 3000 cm with 800 grit sandpaper under a 100 g load, showing exceptional wear resistance. In addition, it was revealed that the coated electrode retained a high impedance value of 8.53 × 108 Ω·cm2 at 0.1 Hz after 480 h of immersion in 5 wt% NaCl solution, with the CPE exponent remaining close to unity (from 1.00 to 0.97), highlighting its superior anti-corrosion performance and broad application prospects for metal corrosion prevention. Full article
(This article belongs to the Collection Feature Paper Collection in Corrosion, Wear and Erosion)
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20 pages, 16874 KB  
Article
A Pilot Study for “In Vitro” Testing the Surface Conditioning Effects on CAD/CAM Hybrid Nanoceramic Adhesion
by Georgi Veselinov Iliev, Lucian Toma Ciocan, Vlad Gabriel Vasilescu, Gaudențiu Vărzaru, Florin Miculescu, Ana Maria Cristina Țâncu, Marina Imre and Silviu Mirel Pițuru
Dent. J. 2026, 14(1), 36; https://doi.org/10.3390/dj14010036 - 6 Jan 2026
Viewed by 179
Abstract
Background/Objectives: The clinical application of CAD/CAM restorative materials continues to evolve due to increasing demand for aesthetic, durable, and minimally invasive indirect restorations. Hybrid nanoceramics, such as Grandio disc (VOCO GmbH, Cuxhaven, Germany), are increasingly used in indirect restorative dentistry due to [...] Read more.
Background/Objectives: The clinical application of CAD/CAM restorative materials continues to evolve due to increasing demand for aesthetic, durable, and minimally invasive indirect restorations. Hybrid nanoceramics, such as Grandio disc (VOCO GmbH, Cuxhaven, Germany), are increasingly used in indirect restorative dentistry due to their favourable combination of mechanical strength, polishability, wear resistance, and bonding potential. One challenge associated with adhesive protocols for CAD/CAM materials lies in achieving durable bonds with resin cements. Extensive post-polymerization during fabrication reduces the number of unreacted monomers available for chemical interaction, thereby limiting the effectiveness of traditional adhesive strategies and necessitating specific surface conditioning approaches. This study aimed to evaluate, in a preliminary, non-inferential manner, the influence of several combined conditioning protocols on surface micromorphology, elemental composition, and descriptive SBS trends of a CAD/CAM hybrid nanoceramic. This work was designed as a preliminary pilot feasibility study. Due to the limited number of specimens (two discs per protocol, each providing two independent enamel bonding measurements), all bond strength outcomes were interpreted descriptively, without inferential statistical testing. This in vitro study investigated the effects of various surface conditioning protocols on the adhesive performance of CAD/CAM hybrid nanoceramics (Grandio disc, VOCO GmbH, Cuxhaven, Germany) to dental enamel. Hydrofluoric acid (HF) etching was performed to improve adhesion to indirect resin-based materials using two commercially available gels: 9.5% Porcelain Etchant (Bisco, Inc., Schaumburg, IL, USA) and 4.5% IPS Ceramic Etching Gel (Ivoclar Vivadent, Schaan, Liechtenstein), in combination with airborne-particle abrasion (APA), silanization, and universal adhesive application. HF may selectively dissolve the inorganic phase, while APA increases surface texture and micromechanical retention. However, existing literature reports inconsistent results regarding the optimal conditioning method for hybrid composites and nanoceramics, and the relationship between micromorphology, elemental surface changes, and adhesion remains insufficiently clarified. Methods: A total of ten composite specimens were subjected to five conditioning protocols combining airborne-particle abrasion with varying hydrofluoric acid (HF) concentrations and etching times. Bonding was performed using a dual-cure resin cement (BiFix QM) and evaluated by shear bond strength (SBS) testing. Surface morphology was examined through environmental scanning electron microscopy (ESEM), and elemental composition was analyzed via energy-dispersive X-ray spectroscopy (EDS). Results: indicated that dual treatment with HF and sandblasting showed descriptively higher SBS, with values ranging from 5.01 to 6.14 MPa, compared to 1.85 MPa in the sandblasting-only group. ESEM revealed that higher HF concentrations (10%) created more porous and irregular surfaces, while EDS indicated an increased fluorine presence trend and silicon reduction, indicating deeper chemical activation. However, extending HF exposure beyond 20 s did not further improve bonding, suggesting the importance of protocol optimization. Conclusions: The preliminary observations suggest a synergistic effect of mechanical and chemical conditioning on hybrid ceramic adhesion, but values should be interpreted qualitatively due to the pilot nature of the study. Manufacturer-recommended air abrasion alone may provide limited adhesion under high-stress conditions, although this requires confirmation in studies with larger sample sizes and ageing simulations. Future studies should address long-term durability and extend the comparison to other hybrid CAD/CAM materials and to other etching protocols. Full article
(This article belongs to the Special Issue Dental Materials Design and Application)
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27 pages, 8982 KB  
Article
Tribological Performance of Micro and Nano-Titanium Carbide-Reinforced Copper Composites Manufactured by Powder Metallurgy: Experimental Studies and Modelling
by Anwar Ulla Khan, Sajjad Arif, Muhammed Muaz, Mohammad Shan, Ateyah Alzahrani and Ahmad Alghamdi
Metals 2026, 16(1), 66; https://doi.org/10.3390/met16010066 - 5 Jan 2026
Viewed by 306
Abstract
This study reports the fabrication of copper-based metal matrix composites reinforced with a combination of micro- and nano-sized titanium carbide (TiC) particles using the powder metallurgy route. The micro-TiC content was maintained at 5 wt.%, while the nano-TiC addition was systematically varied between [...] Read more.
This study reports the fabrication of copper-based metal matrix composites reinforced with a combination of micro- and nano-sized titanium carbide (TiC) particles using the powder metallurgy route. The micro-TiC content was maintained at 5 wt.%, while the nano-TiC addition was systematically varied between 1 and 3 wt.% in increments of 1 wt.%. The consolidation of the blends was achieved by uniaxial compaction at 500 MPa, followed by sintering in a nitrogen atmosphere at 750–900 °C for 2 h. Tribological assessment under dry sliding conditions was performed using a pin-on-disk apparatus. Structural and microstructural examinations using X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-dispersive spectroscopy (EDS) confirmed a uniform incorporation of the reinforcements within the Cu matrix. The incorporation of nano-TiC up to 2 wt.% significantly enhanced density, hardness, and wear resistance, after which a marginal decline was observed. SEM analysis of worn surfaces revealed that adhesive wear, abrasion, and delamination were the primary wear mechanisms. To better understand the relationship between processing conditions and material responses, response surface methodology (RSM) was employed. The developed models for density, hardness, and wear loss showed good agreement with the experimental results, with confirmatory tests yielding errors of 1.59%, 2.06%, and 2%, respectively, thereby validating the approach’s reliability. Full article
(This article belongs to the Special Issue Powder Metallurgy of Metals and Composites)
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18 pages, 2918 KB  
Article
Study on Tire–Road Wear Interface Behavior of Porous Elastic Road Surface Based on Image Processing
by Hongjin Liu, Ke Zhong, Jing Gu, Ting Gan and Yuchun Li
Appl. Sci. 2026, 16(1), 534; https://doi.org/10.3390/app16010534 - 5 Jan 2026
Viewed by 149
Abstract
The use of waste rubbers and polyurethane has a significant impact on the abrasion resistance of the porous elastic road surface (PERS) mixture. The purpose of this work is to study the anti-abrasion performance of the PERS mixture under different contents of waste [...] Read more.
The use of waste rubbers and polyurethane has a significant impact on the abrasion resistance of the porous elastic road surface (PERS) mixture. The purpose of this work is to study the anti-abrasion performance of the PERS mixture under different contents of waste rubbers. First, features of the surface of the PERS mixture were collected by image processing technology. Then, the abrasion performance of the mixture was studied by image processing and wear tests. The correlation between the surface texture parameters and the anti-abrasion performance of the mixture was analyzed by the gray entropy correlation method. It is found that the change of convex particle area in the equivalent diameter range of 2–5 mm had the greatest correlation with the abrasion resistance of the PERS mixture. The effect of the waste rubber content of the mixture on the anti-abrasion performance was investigated, and a waste rubber content of 10% showed the best anti-abrasion performance. It is expected that this work can provide a new method for analyzing the anti-abrasion performance of functional pavement. Full article
(This article belongs to the Special Issue Advanced Materials and Technologies in Pavement Engineering)
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18 pages, 10634 KB  
Article
Effect of Nano-TiO2 Addition on Some Properties of Pre-Alloyed CoCrMo Fabricated via Powder Technology
by Jawdat Ali Yagoob, Mahmood Shihab Wahhab, Sherwan Mohammed Najm, Mihaela Oleksik, Tomasz Trzepieciński and Salwa O. Mohammed
Materials 2026, 19(1), 186; https://doi.org/10.3390/ma19010186 - 4 Jan 2026
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Abstract
The CoCrMo alloys are progressively utilized as biomaterials. This research is dedicated to studying the consequence of (1, 3, and 5) wt% nano-TiO2 addition on the porosity, microstructure, microhardness, and wear behavior of pre-alloyed CoCrMo powder produced by powder metallurgy (PM). Microstructural [...] Read more.
The CoCrMo alloys are progressively utilized as biomaterials. This research is dedicated to studying the consequence of (1, 3, and 5) wt% nano-TiO2 addition on the porosity, microstructure, microhardness, and wear behavior of pre-alloyed CoCrMo powder produced by powder metallurgy (PM). Microstructural features were examined using SEM, SEM mapping, and XRD. Wear behavior was assessed through pin-on-disk tests performed under dry sliding conditions at varying loads and durations. Porosity increased with the addition of nano-TiO2, from 15.26 at 0 wt% reaching 25.12% at 5 wt%, while density decreased from 7.16 to 6.33 g/cm3. Microhardness exhibited a slight improvement, attaining 348 HV at 5 wt%. SEM and XRD analyses confirmed partial particle separation after sintering and identified the TiO2 reinforcement as rutile. Wear tests revealed that adding 1 wt% nano-TiO2 enhanced wear resistance, whereas extended sliding durations resulted in increased wear rates. Adhesive wear was the predominant mechanism, accompanied by limited abrasive wear, oxidation, and plastic deformation. Full article
(This article belongs to the Section Biomaterials)
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