Search Results (32)

Deploying distributed fiber-optic sensor (DFOS) technology to gather environmental parameters over expansive areas is an essential monitoring strategy in the context of comprehensive searches for anomalous places. This study utilizes a single temperature measurement channel within a commercial Raman-based distributed temperature sensing (RDTS) interrogator and divides it into two separate, uncorrelated paths to enable spatial duplex temperature measurements. The distinction between temperature events corresponding to each path in the dual separate path (DSP) in RDTS can be achieved when temperature events are concurrently occurring in the DSP. Additionally, the RDTS–DSP solution may integrate free space optics (FSO) into its fiber path, which serves to enhance the user-friendliness, scalability, and cost-effectiveness of DFOS technology. An RDTS measurement channel can effectively function as a DSP, thus doubling the RDTS measurement pathway, and can be combined with FSO to significantly improve RDTS performance. Full article

Optical fiber is increasingly used for both communication and distributed sensing of temperature and strain in environmental studies. In this work, we demonstrate the viability of unreinforced fiber tethers (bare fiber) for Raman-based distributed temperature sensing in deep ocean and deep ice environments. High-pressure testing of single-mode and multimode optical fiber showed little to no changes in light attenuation over pressures from atmospheric to 600 bars. Most importantly, the differential attenuation between Stokes and anti-Stokes frequencies, critical for the evaluation of distributed temperature sensing, was shown to be insignificantly affected by fluid pressures over the range of pressures tested for single-mode fiber, and only very slightly affected in multimode fiber. For multimode fiber deployments to ocean depths as great as 6000 m, the effect of pressure-dependent differential attenuation was shown to impact the estimated temperatures by only 0.15 °K. These new results indicate that bare fiber tethers, in addition to use for communication, can be used for distributed temperature or strain in fibers subjected to large depth (pressure) in varying environments such as deep oceans, glaciers and potentially the icy moons of Saturn and Jupiter. Full article

A novel approach to the development of Distributed Temperature-Sensing (DTS) systems based on Raman Scattering in Multimode optical fibers operating at around 800 nm is presented, focusing on applications requiring temperature profile measurement in the range of a few hundreds of meters. In contrast to the standard Raman DTS systems, which aim to shorten the pulse space width as much as possible to improve the precision of measurement, the novel approach studied in this work is based on the use of pulses with a space width that is approximately equal to the distance covered by the fiber under test. The proposed technique relies on numerical post-processing to obtain the temperature profile measurement with a precision of about $\pm 3°\mathrm{C}$ and a spatial resolution of 8 m, due to the transaction phases of the optical pulses. This solution simplifies the electronic circuit development, also minimizing the required laser peak power needed compared to the typical narrow pulse techniques. Full article

In this paper, a novel distributed optical fiber temperature sensor based on Raman anti-Stokes scattering light is proposed and experimentally demonstrated. The Raman anti-Stokes scattering light is sensitive to temperature parameters that are detected by the fiber under test conditions (FUT), and this allowed the temperature demodulation algorithm to be obtained through the relationship between the temperature and the power of the back-scattered Raman anti-Stokes light. In addition, we propose a new temperature calibration method to ensure accurate temperature measurement, which is greatly affected by the stability of a pulse laser. The experimental system is constructed with an optical fiber length of approximately 3.5 km. The proposed system obtains a 24 dB dynamic range with a pulse width of 20 ns and temperature testing ranges of 30.0 °C to 80.0 °C. The results demonstrate that the maximum temperature deviation range is −1.5 °C to +1.6 °C and the root mean square (RMS) error of the whole temperature range is 0.3 °C, which means it has the potential for practical engineering applications. More importantly, it avoids the walk-off effect that must be corrected in commonly used temperature demodulation schemes adopting both Raman Stokes light and anti-Stokes light. It also saves a signal channel, which is more suitable for the integration of hybrid distributed optical fiber sensing systems for multi-parameter monitoring. Full article

Distributed optical fiber sensors (DOFSs) are a promising technology for their unique advantage of long-distance distributed measurements in industrial applications. In recent years, modern industrial monitoring has called for comprehensive multi-parameter measurements to accurately identify fault events. The hybrid DOFS technology, which combines the Rayleigh, Brillouin, and Raman scattering mechanisms and integrates multiple DOFS systems in a single configuration, has attracted growing attention and has been developed rapidly. Compared to a single DOFS system, the multi-parameter measurements based on hybrid DOFS offer multidimensional valuable information to prevent misjudgments and false alarms. The highly integrated sensing structure enables more efficient and cost-effective monitoring in engineering. This review highlights the latest progress of the hybrid DOFS technology for multi-parameter measurements. The basic principles of the light-scattering-based DOFSs are initially introduced, and then the methods and sensing performances of various techniques are successively described. The challenges and prospects of the hybrid DOFS technology are discussed in the end, aiming to pave the way for a vaster range of applications. Full article

Raman-based distributed temperature sensing (DTS) is a valuable tool for field testing and validating heat transfer models in borehole heat exchanger (BHE) and ground source heat pump (GSHP) applications. However, temperature uncertainty is rarely reported in the literature. In this paper, a new calibration method was proposed for single-ended DTS configurations, along with a method to remove fictitious temperature drifts due to ambient air variations. The methods were implemented for a distributed thermal response test (DTRT) case study in an 800 m deep coaxial BHE. The results show that the calibration method and temperature drift correction are robust and give adequate results, with a temperature uncertainty increasing non-linearly from about 0.4 K near the surface to about 1.7 K at 800 m. The temperature uncertainty is dominated by the uncertainty in the calibrated parameters for depths larger than 200 m. The paper also offers insights into thermal features observed during the DTRT, including a heat flux inversion along the borehole depth and the slow temperature homogenization under circulation. Full article

A submetric spatial resolution Raman optical time-domain reflectometry (ROTDR) temperature sensor assisted by the Wiener deconvolution postprocessing algorithm has been proposed and experimentally demonstrated. Without modifying the typical configuration of the ROTDR sensor and the adopted pump pulse width, the Wiener demodulation algorithm is able to recover temperature perturbations of a smaller spatial scale by deconvoluting the acquired Stokes and anti-Stokes signals. Numerical simulations have been conducted to analyze the spatial resolution achieved by the algorithm. Assisted by the algorithm, a typical ROTDR sensor adopting pump pulses of 20 ns width can realize the distributed temperature sensing with a spatial resolution of 0.5 m and temperature accuracy of 1.99 °C over a 2.1-km sensing fiber. Full article

Observations from Raman backscatter-based Fiber-Optic Distributed Sensing (FODS) require reference sections of the fiber-optic cable sensor of known temperature to translate the primary measured intensities of Stokes and anti-Stokes photons to the secondary desired temperature signal, which also commonly forms the basis for other derived quantities. Here, we present the design and the results from laboratory and field evaluations of a novel Solid-Phase Bath (SoPhaB) using ultrafine copper instead of the traditional mechanically stirred liquid-phase water bath. This novel type is suitable for all FODS applications in geosciences and industry when high accuracy and precision are needed. The SoPhaB fully encloses the fiber-optic cable which is coiled around the inner core and surrounded by tightly interlocking parts with a total weight of 22 kg. The SoPhaB is thermoelectrically heated and/or cooled using Peltier elements to control the copper body temperature within ±0.04 K using commercially available electronic components. It features two built-in reference platinum wire thermometers which can be connected to the distributed temperature sensing instrument and/or external measurement and logging devices. The SoPhaB is enclosed in an insulated carrying case, which limits the heat loss to or gains from the outside environment and allows for mobile applications. For thermally stationary outside conditions the measured spatial temperature differences across SoPhaB parts touching the fiber-optic cable are <0.05 K even for stark contrasting temperatures of $\Delta T>$ 40 K between the SoPhaB’s setpoint and outside conditions. The uniform, stationary known temperature of the SoPhaB allows for substantially shorter sections of the fiber-optic cable sensors of less than <5 bins at spatial measurement resolution to achieve an even much reduced calibration bias and spatiotemporal uncertainty compared to traditional water baths. Field evaluations include deployments in contrasting environments including the Arctic polar night as well as peak summertime conditions to showcase the wide range of the SoPhaB’s applicability. Full article

A simple, one-step and facile method has been introduced to prepare fluorescent and electrochemically active carbon nanoparticles with single-size distribution and good long-term stability by electrochemical exfoliation of polyacrylonitrile-based carbon fibers in an alkaline solution-phase condition. The preparation condition was systematically optimized by studying the effect of temperature and electrolytes. It has been found that an electrochemical exfoliation reaction carried out at an applied potential of 2 V vs. Ag/AgCl in a phosphate-ion-containing alkaline solution at a temperature of 40 °C is an ideal condition for the preparation of 14 ± 4 nm-sized carbon nanoparticles. Unlike the literature protocols, there are no filtration and membrane dialysis-based off-line sample pretreatments adopted in this work. The as-prepared carbon nanoparticles were characterized by fluorescence, Raman spectrum, transmission electron microscope, and X-ray photoelectron spectroscopic characterization methods. It was found that the carbon–oxygen functional group rich in graphene–oxide quantum dots (GOQDs) such as carbon nanoparticles were formed in this work. A preliminary study relating to simultaneous electrochemical oxidation and the sensing of uric acid and ascorbic acid with well-resolved peaks was demonstrated as a model system to extend the new carbon material for electroanalytical applications. Furthermore, in situ synthesis of 2 nm-sized gold nanoparticles stabilized by GOQDs was presented. The carbon nanoparticles prepared by the direct method in this work have shown good stability over 6 months when stored at room temperature. The electrochemical exfoliation reaction has been found to be highly reproducible and suitable for bulk synthesis of luminescence-effective carbon nanoparticles to facilitate fundamental studies and practical applications. Full article

Raman distributed optical fiber temperature sensing (RDTS) has been extensively studied for decades because it enables accurate temperature measurements over long distances. The signal-to-noise ratio (SNR) is the main factor limiting the sensing distance and temperature accuracy of RDTS. We manufacture a low water peak optical fiber (LWPF) with low transmission loss to improve the SNR for long-distance application. Additionally, an optimized denoising neural network algorithm is developed to reduce noise and improve temperature accuracy. Finally, a maximum temperature uncertainty of 1.77 °C is achieved over a 24 km LWPF with a 1 m spatial resolution and a 1 s averaging time. Full article

The negatively charged germanium-vacancy GeV⁻ color centers in diamond nanocrystals are solid-state photon emitters suited for quantum information technologies, bio-sensing, and labeling applications. Due to the small Huang–Rhys factor, the GeV⁻-center zero-phonon line emission is expected to be very intensive and spectrally narrow. However, structural defects and the inhomogeneous distribution of local strains in the nanodiamonds result in the essential broadening of the ZPL. Therefore, clarification and elimination of the reasons for the broadening of the GeV⁻ center ZPL is an important problem. We report on the effect of reactive ion etching in oxygen plasma on the structure and luminescence properties of nanodiamonds grown by hot filament chemical vapor deposition. Emission of GeV⁻ color centers ensembles at about 602 nm in as-grown and etched nanodiamonds is probed using micro-photoluminescence and micro-Raman spectroscopy at room and liquid nitrogen temperature. We show that the etching removes the nanodiamond surface sp²-induced defects resulting in a reduction in the broad luminescence background and a narrowing of the diamond Raman band. The zero-phonon luminescence band of the ensemble of the GeV⁻ centers is a superposition of narrow lines originated most likely from the GeV⁻ center sub-ensembles under different uniaxial local strain conditions. Full article

Gold and silver nanoparticles are widely used as signal amplification elements in various electrochemical and optical sensor applications. Although these NPs can be synthesized in several ways, perhaps one of the simplest methods of their preparation is the thermal annealing of pre-deposited thin metal films on glass. With this method, the parameters of the annealing process (time and temperature) and the pre-deposited thin film thickness influence and define the resulting size and distribution of the NPs on the surface. LSPR is a very sensitive optical phenomenon and can be utilized for a large variety of sensing purposes. SERS is an analytical method that can significantly increase the yield of the Raman scattering of target molecules adsorbed on the surface of metallic nanoparticles. In this work, the performance of Au/Ag nanoislands was investigated for SERS and LSPR applications. The nanoislands were generated by thermally annealing thin layers of silver and gold, which were previously sputtered onto glass surfaces. The sensitivity of LSPR and SERS-based devices were strongly dependent on the used material and the size and geometry of the metallic nanoparticles. By controlling these parameters, the plasmon absorption band can be tuned and the sensitivity can be optimized. This work was supported by the GINOP-2.3.2-15-2016-00041 project. ICs is grateful for the support of the János Bólyai Research Scholarship of the Hungarian Academy of Sciences. Full article

There is an optical interference noise in the conventional Raman-based fiber-optics distributed sensing, which results in a poor temperature resolution performance. In addition, the traditional whole-fiber demodulation principle complicates the operation steps of the system. In this paper, a novel dynamic difference attenuation recognition (DDAR) principle is operated in the DDP scheme (dual demodulation principle) and the SDP scheme (self-demodulation principle) respectively. It not only helps to eliminate the optical interference noise, but also omits the whole-fiber calibration process. In this experiment, a temperature resolution of 0.30 °C (17.0 km) is achieved through using the DDP scheme based on the DDAR principle, and the measurement time can be shortened to 1.5 s. Meanwhile, a temperature resolution of 0.18 °C (17.0 km) is obtained for the SDP scheme under the DDAR principle. The SNR of DDP and DSP schemes can be optimized to 12.82 dB and 13.32 dB by the proposed DDAR technology. Furthermore, the temperature resolution performance under a large temperature measurement range (0–1000 °C) is theoretically analyzed. The results indicate that the temperature responsivity for DDP and SDP schemes are parabolic and linear type respectively, which causes the temperature resolution of the two schemes to show a different trend with the change of temperature. The proposed DDAR method also can improve the temperature resolution in such a large temperature measurement range. Full article

To accurately detect and monitor the internal temperature of an operating power transformer, the distributed optical fiber sensor (DOFS) was creatively applied inside an oil-immersed 35 kV transformer through high integration with the winding wire. On the former basis, the power transformer prototype with a completely global internal temperature sensing capability was successfully developed and it was also qualified for power grid operation through the ex-factory type tests. The internal spatially continuous temperature distribution of the operating transformer was then revealed through a heat-run test and the numerical simulation was also applied for further analysis. Hotspots of windings were continuously located and monitored (emerging at about 89%/90% height of low/high voltage winding), which were furtherly compared with the IEC calculation results. This new nondestructive internal sensing method shows a broad application prospect in the electrical equipment field. Also, the revelation of transformer internal distributed temperature can offer a solid reference for both researchers and field operation staff. Full article