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Journal = Metals
Section = Metal Failure Analysis

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14 pages, 27721 KB  
Article
Experimental Investigation of Microstructural Evolution and Fatigue Damage of Pearlite Wheel Steel During Tread Braking Based on a Full-Size Wheel–Rail Test Rig
by Mingzhe Fan, Guanzhen Zhang, Xiang Li, Guang Li, Shuo Sun, Yi Wu and Pengtao Liu
Metals 2026, 16(6), 662; https://doi.org/10.3390/met16060662 - 15 Jun 2026
Viewed by 173
Abstract
This study investigated the relationship between the surface microstructure of pearlite steel wheels and the formation of fatigue cracks during the braking process by using a full-size wheel braking test rig. After fatigue failure, the surface microstructural evolution and fatigue crack initiation and [...] Read more.
This study investigated the relationship between the surface microstructure of pearlite steel wheels and the formation of fatigue cracks during the braking process by using a full-size wheel braking test rig. After fatigue failure, the surface microstructural evolution and fatigue crack initiation and propagation of the wheel sample were systematically analyzed by optical microscope (OM), scanning electron microscope (SEM), and transmission electron microscope (TEM). The results showed that after braking of 1572 cycles, a large number of fatigue cracks formed at the wheel tread, which caused the wheel to break. After fatigue failure, some dark areas formed at the wheel tread, which were composed of Fe3O4 compounds. This indicates that severe oxidation was produced at the wheel tread during braking due to the high temperature. After fatigue failure, a continuous thermal white etching layer (T-WEL) was formed in some areas of the wheel tread, while crescent-shaped T-WEL was found in other areas. The microstructure of the T-WEL was composed of martensite phase. The rapid increase and decrease in temperature at the wheel tread during the braking process caused martensitic transformation at the wheel tread. The hardness of the sample reached to about 900 HV in WEL and it reduced with the increase in distance from the surface. The cracks were initiated from the surface and gradually propagated into the matrix. However, the crack propagation mode in the continuous T-WEL and crescent-shaped T-WEL was different. In the continuous T-WEL, the continuous T-WEL of the wheel can be peeled off during the braking wear process, and then the crack was gradually propagated into the matrix in the T-WEL peeled area. As for the crescent-shaped T-WEL, due to the large hardness difference between T-WEL and pearlite, the crack initiated at the interface between the T-WEL and pearlite and gradually propagated into the matrix. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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19 pages, 5011 KB  
Article
Study of Fatigue Crack Growth in Superalloy Based on Acoustic Emission K-Entropy
by Ting Jing, Yang Yu and Qiang Liu
Metals 2026, 16(6), 586; https://doi.org/10.3390/met16060586 - 26 May 2026
Viewed by 273
Abstract
Acoustic emission (AE) technology was used to monitor the fatigue crack growth process of superalloy. The analysis results show that both the cumulative values and the K-entropy values of AE parameters have good correspondences with the three stages described by fracture mechanics, which [...] Read more.
Acoustic emission (AE) technology was used to monitor the fatigue crack growth process of superalloy. The analysis results show that both the cumulative values and the K-entropy values of AE parameters have good correspondences with the three stages described by fracture mechanics, which makes it possible to characterize the process of fatigue crack growth. Since K-entropy is more sensitive to changes in fatigue state, the turning points between the second stage and the third stage are earlier than those defined by fracture mechanics, indicating that it has an early warning capability. The K-entropy of AE parameter was first proposed to represent the growth rate of fatigue crack. This method not only effectively decreased the large dispersion of change rate of AE parameters but also ensured the similarity with the fatigue crack growth rate, thereby optimizing the characterization of fatigue crack growth. Full article
(This article belongs to the Section Metal Failure Analysis)
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18 pages, 9586 KB  
Article
Fracture Failure Analysis of U75V Pearlitic Rail on Sharp Radius Curved Track
by Junjie Fei, Hongfang Qi, Bei Yuan, Minbiao Wan and Linlang Zhang
Metals 2026, 16(6), 582; https://doi.org/10.3390/met16060582 - 26 May 2026
Viewed by 280
Abstract
A transverse fracture occurred in U75V pearlitic rail after 5 months of service on a sharp radius curved track of mixed passenger-freight railway. Systematic tests including chemical composition analysis, mechanical properties testing, macroscopic fracture inspection, metallographic observation and microscopic morphology characterization were conducted [...] Read more.
A transverse fracture occurred in U75V pearlitic rail after 5 months of service on a sharp radius curved track of mixed passenger-freight railway. Systematic tests including chemical composition analysis, mechanical properties testing, macroscopic fracture inspection, metallographic observation and microscopic morphology characterization were conducted on the failed rail sample. The results indicate that the rail base metal has qualified metallurgical quality. Its chemical composition, fundamental mechanical properties and microstructure fully meet the requirements of Chinese railway standard TB/T 2344.1-2020. The failure mode is identified as instantaneous brittle fracture. Severe mechanical extrusion and impact cause prominent plastic deformation on the rail foot, leading to surface plastic flow and further triggering micro-crack initiation. Under continuous cyclic stress induced by train loads, the micro-crack tips undergo repeated tearing and closing. Severe stress concentration accelerates the formation of transgranular cracks, which propagate rapidly and unstably toward the rail interior, eventually resulting in catastrophic transverse fracture. Standardized procedures in rail transportation, hoisting and laying are essential to avoid mechanical damage, while regular line inspection and timely replacement of damaged rails should be strictly enforced. Full article
(This article belongs to the Section Metal Failure Analysis)
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24 pages, 8537 KB  
Article
Investigation of Welded Joints of Pipelines from an Existing Gas Transmission Network Exposed to Hydrogen—Part II: Some Aspects of the Microstructural Mechanisms of Hydrogen-Assisted Damage and Fracture
by Boris Yanachkov, Kateryna Valuiska, Yana Mourdjeva, Vanya Dyakova, Krasimir Kolev, Tatiana Simeonova, Rumen Krastev, Stivan Vasilev and Rumyana Lazarova
Metals 2026, 16(6), 573; https://doi.org/10.3390/met16060573 - 24 May 2026
Viewed by 358
Abstract
This study investigates hydrogen embrittlement in welded joints of X52 (L360) pipeline steel obtained from an operating natural gas transmission network after 31 years of service, with particular emphasis on production (longitudinal) and girth (circumferential) welds. The aim is to elucidate the influence [...] Read more.
This study investigates hydrogen embrittlement in welded joints of X52 (L360) pipeline steel obtained from an operating natural gas transmission network after 31 years of service, with particular emphasis on production (longitudinal) and girth (circumferential) welds. The aim is to elucidate the influence of microstructural heterogeneity across the pipe wall and within different welded joint types on hydrogen transport, trapping behavior, and fracture mechanisms. The investigation combines X-ray diffraction, electrochemical hydrogen permeation testing, fractographic analysis, and transmission electron microscopy. X-ray diffraction results show that the base metal and girth weld consist predominantly of body-centered cubic ferrite, whereas the production weld additionally contains retained austenite associated with an elevated manganese content. These phase-related differences are consistent with transmission electron microscopy observations of martensite–austenite constituents within the weld microstructure. Electrochemical hydrogen permeation measurements reveal pronounced microstructure-dependent hydrogen transport behavior. The production weld exhibits a significantly lower apparent diffusion coefficient and a markedly higher hydrogen trap density, approximately five times greater than those of the base metal and girth weld, providing a mechanistic explanation for the observed differences in hydrogen uptake behavior. Fractographic analysis demonstrates a transition from ductile microvoid coalescence in the uncharged condition to predominantly brittle fracture following hydrogen charging. This transition is accompanied by a substantial increase in the fraction of brittle fracture zones, reaching approximately 53% in hydrogen-charged specimens. A pronounced gradient in hydrogen embrittlement susceptibility is observed across the pipe wall thickness, with outer-wall specimens consistently exhibiting greater susceptibility than inner-wall specimens. This behavior reflects the combined influence of long-term soil corrosion and hydrogen-assisted degradation. Transmission electron microscopy reveals that plastic deformation governs dislocation generation, while hydrogen significantly modifies dislocation behavior by promoting dislocation pile-ups near martensite–austenite constituents and non-metallic inclusions. These observations indicate strong interactions between hydrogen, dislocations, and microstructural heterogeneities. A clear size-dependent role of non-metallic inclusions is identified. Sub-micron inclusions act primarily as irreversible hydrogen trapping sites that contribute to hydrogen redistribution within the microstructure, whereas larger inclusions serve as preferential crack initiation sites under hydrogen charging conditions. Overall, the results demonstrate that hydrogen embrittlement behavior is governed by the combined effects of microstructural state, welded joint type, and long-term service-induced degradation, resulting in distinct hydrogen transport characteristics and fracture responses across the pipe wall. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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17 pages, 5401 KB  
Article
Fatigue Crack Propagation in a High-Pressure Turbine Blade Slot Damaged by Fretting
by Hamad Alarfati, Gordana Kastratović, Aleksandar Grbović, Martina Balać and Nenad Vidanović
Metals 2026, 16(6), 564; https://doi.org/10.3390/met16060564 - 22 May 2026
Viewed by 324
Abstract
In this study, fatigue crack propagation due to unexpected damage caused by fretting in an aero engine high-pressure turbine (HPT) blade slot is analyzed. Two different numerical crack models were applied and studied to simulate fatigue crack propagation caused by amplitude service loading. [...] Read more.
In this study, fatigue crack propagation due to unexpected damage caused by fretting in an aero engine high-pressure turbine (HPT) blade slot is analyzed. Two different numerical crack models were applied and studied to simulate fatigue crack propagation caused by amplitude service loading. Also, the goal was to demonstrate the capacities of numerical simulations, including their limitations, especially when the crack propagation behavior should be predicted for critical parts of the real structure. It is shown that the structural integrity of the analyzed component is not jeopardized by the existing damage. Full article
(This article belongs to the Special Issue Fracture Mechanics and Failure Analysis of Metallic Materials)
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18 pages, 7310 KB  
Article
Effect of Surface Layer Removal After Ultrasonic Surface Rolling Processing on the Tension–Tension Fatigue Performance of AZ31B Magnesium Alloy
by Zhonglei Wang, Jie Meng, Qingqiang Chen, Shunlong Li, Fei Wang and Jie Sun
Metals 2026, 16(5), 533; https://doi.org/10.3390/met16050533 - 14 May 2026
Viewed by 249
Abstract
This paper investigates the influence of surface ultrasonic rolling treatment on the fatigue performance of Mg-3Al-1Zn extruded alloy and systematically analyzes the evolution laws of fatigue life and mechanical properties with the thickness of the surface removed layer. The results show that after [...] Read more.
This paper investigates the influence of surface ultrasonic rolling treatment on the fatigue performance of Mg-3Al-1Zn extruded alloy and systematically analyzes the evolution laws of fatigue life and mechanical properties with the thickness of the surface removed layer. The results show that after ultrasonic rolling treatment, the fatigue life of the alloy at a stress amplitude of 240 MPa changes significantly and reaches a peak at a specific removal thickness: when the 80 μm surface layer is removed, the fatigue life reaches 7.79 × 106 cycles, which is much higher than that of the untreated sample (3.87 × 104) and the sample only subjected to ultrasonic surface rolling processing (1.8 × 104). With the increase in the removal thickness, the fatigue life shows a trend of first increasing and then decreasing, and a second increase occurs within the range of 400–500 μm. Microstructure analysis indicates that at a depth of 80 μm from the surface, the strength is enhanced due to grain refinement and the peak hardness, thereby inhibiting the initiation of fatigue cracks, while within the depth range of 400–500 μm, there exist high-density dislocations and deformation layers, which also effectively hinder crack propagation. This study reveals the key role of surface state and subsurface microstructure in the fatigue behavior of magnesium alloys, providing a theoretical basis for improving the fatigue performance of magnesium alloys through surface modification. Full article
(This article belongs to the Section Metal Failure Analysis)
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16 pages, 2834 KB  
Article
A Fatigue Life Prediction Model of Aluminum Alloy Considering Crack Initiation
by Kaiyu Cheng, Shihao Ma, Yuanyuan Fang, Wei Guo, Xia Xu, Guoqiang Chang and Henggao Xiang
Metals 2026, 16(5), 530; https://doi.org/10.3390/met16050530 - 13 May 2026
Viewed by 235
Abstract
In high-cycle fatigue, the majority of fatigue life is spent in the crack initiation stage. However, current models fail to accurately capture the fatigue life consumed in the crack initiation stage, resulting in discrepancies in predictions. Here, we propose a fatigue life prediction [...] Read more.
In high-cycle fatigue, the majority of fatigue life is spent in the crack initiation stage. However, current models fail to accurately capture the fatigue life consumed in the crack initiation stage, resulting in discrepancies in predictions. Here, we propose a fatigue life prediction model based on the crack tip plastic zone, combined with a multi-stage crack growth approach. To quantify the crack initiation life, a modified Tanaka–Mura model is developed by incorporating the effects of localized plastic deformation at the crack tip. The proposed model demonstrates good agreement with experimental observations. Furthermore, a reliability-based fatigue evaluation framework is established by introducing a fatigue safety factor formulation. The results show that the safety factor decreases with increasing applied stress levels, attributed to the reduced standard deviation and lower scatter of fatigue life at higher stresses. The findings provide a practical and physics-informed methodology for fatigue life and safety assessment of aluminum alloy components under complex cyclic loading conditions. Full article
(This article belongs to the Special Issue Fatigue and Fracture of Advanced Metallic Materials)
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15 pages, 6366 KB  
Article
Effect of Trace Titanium on Hydrogen Embrittlement Resistance of 25Mn High-Manganese Steel
by Taoran Shao, Bingbing Wu, Yanxin Wu and Zhenli Mi
Metals 2026, 16(5), 509; https://doi.org/10.3390/met16050509 - 8 May 2026
Viewed by 385
Abstract
High-manganese steel has emerged as a potential alternative material to austenitic stainless steel for liquid hydrogen storage and transportation environments, owing to its superior mechanical characteristics and limited hydrogen diffusivity. However, its hydrogen embrittlement (HE) susceptibility limits its engineering applications. This study investigates [...] Read more.
High-manganese steel has emerged as a potential alternative material to austenitic stainless steel for liquid hydrogen storage and transportation environments, owing to its superior mechanical characteristics and limited hydrogen diffusivity. However, its hydrogen embrittlement (HE) susceptibility limits its engineering applications. This study investigates the effect of microstructural regulation through trace titanium (Ti, 0.021 wt%) addition on HE resistance in high-manganese steel. By means of Electron Backscatter Diffraction (EBSD), TEM, SEM, and Slow Strain Rate Tensile (SSRT) tests, the effects of Ti on the microstructure, mechanical properties, and HE susceptibility of high-manganese steel are systematically investigated. The results show that the addition of Ti did not significantly alter the average austenite grain size or phase composition, but it generated a large number of Ti(C,N) nanoscale precipitates with sizes ranging from 20 to 70 nm within the matrix. The elongation loss of the 25Mn-Ti specimen was significantly lower than that of the 25Mn specimen when hydrogen-charged for 72 h, decreasing from 18.4% to 9.3%. The fracture surfaces consistently exhibited ductile dimple morphology, whereas 25Mn steel demonstrated significant cleavage-induced brittle fracture. EBSD analysis revealed that hydrogen-charged 25Mn-Ti steel exhibited higher Kernel Average Misorientation (KAM) value retention rate and more uniform grain strain distribution, indicating enhanced microstructural deformation compatibility. The main mechanism was that Ti pre-formed nanoscale Ti(C,N) precipitates during the preparation of 25Mn high-manganese steel, which played a key role in inhibiting HE. These precipitates altered hydrogen diffusion behavior and distribution patterns, reduced stress concentration levels, and inhibited hydrogen-induced crack initiation. This work is of great significance for improving the HE resistance of high-manganese steels. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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45 pages, 6216 KB  
Review
Data-Driven and Hybrid Modeling for Metal Fatigue: A Review of Classical Methods, Machine Learning, and Physics-Informed Neural Networks
by Yuzhou Shi, Arko Suryadip Dey and Yazhou Qin
Metals 2026, 16(5), 476; https://doi.org/10.3390/met16050476 - 28 Apr 2026
Viewed by 1175
Abstract
The prediction of metal fatigue life has evolved from classical empirical approaches to advanced, data-driven computational models. However, traditional methods struggle with large data scatter, complex variable-amplitude loading, and the cost of experimental testing. These limitations are particularly pronounced in additively manufactured (AM) [...] Read more.
The prediction of metal fatigue life has evolved from classical empirical approaches to advanced, data-driven computational models. However, traditional methods struggle with large data scatter, complex variable-amplitude loading, and the cost of experimental testing. These limitations are particularly pronounced in additively manufactured (AM) components, which exhibit random porosity and are highly sensitive to process parameters. This review integrates classical fatigue mechanics with modern data-driven methodologies. It evaluates fatigue-life prediction for metallic alloys, welded assemblies, and AM materials. We review classical prediction tools, machine learning (ML) algorithms, deep learning architectures, and physics-informed neural networks (PINNs). ML models capture nonlinear degradation patterns but suffer from limited interpretability (“black-box” behavior) and are unable to extrapolate from small datasets. Embedding governing physical laws into PINNs helps mitigate these limitations. This approach enhances physical consistency, reduces training-data requirements, and strengthens extrapolation capability. In additively manufactured metals, defect location is often a more critical predictor of fatigue failure than defect size or morphology. To address data scarcity, we highlight the use of generative adversarial networks and transfer learning. Integrated models, combined with real-time structural health monitoring data, enable accurate, dynamic digital twins and preemptive fatigue prognosis. Full article
(This article belongs to the Special Issue Fatigue and Fracture Mechanisms of Advanced Metallic Materials)
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17 pages, 58599 KB  
Article
Fatigue Crack Growth Behaviour in Welded Joints of Armour Steel
by Mirza Manjgo, Gorazd Lojen, Jure Bernetič, Mihajlo Aranđelović and Tomaž Vuherer
Metals 2026, 16(5), 468; https://doi.org/10.3390/met16050468 - 25 Apr 2026
Viewed by 648
Abstract
Welded joints are widely recognized as the most critical point in structures made of armour steels due to pronounced thermal effects, microstructural heterogeneity, and the degradation of mechanical and fatigue properties. This study investigates the mechanical properties and fatigue crack growth resistance of [...] Read more.
Welded joints are widely recognized as the most critical point in structures made of armour steels due to pronounced thermal effects, microstructural heterogeneity, and the degradation of mechanical and fatigue properties. This study investigates the mechanical properties and fatigue crack growth resistance of a welded joint produced on SA 500 armour steel, with the aim of preserving the properties of the base material as much as possible. To achieve this, a welding procedure incorporating a high-strength filler wire and optimized welding parameters was applied. Hardness and tensile testing was conducted to evaluate the extent of property degradation caused by welding. The results demonstrate that the applied welding process effectively limited the reduction in hardness and tensile strength, achieving values reasonably close to those of the base material. In addition, fatigue crack growth behaviour was investigated in accordance with ASTM E647, using both the Paris law and the McEvily law. The obtained fatigue crack growth curves and threshold stress intensity factor (ΔKth) values indicate the nearly identical fatigue behaviour of the base material and the heat-affected zone, confirming the successful preservation of base material fatigue behaviour in the thermally affected zone. Moreover, the weld metal exhibited superior resistance to fatigue crack initiation and growth. Overall, the results confirm that the proposed welding approach provides favourable mechanical and fatigue performance for welded joints in armour steel applications. Full article
(This article belongs to the Special Issue Fracture Mechanics and Failure Analysis of Metallic Materials)
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22 pages, 2510 KB  
Article
Corrosion Behavior of AISI 52100 Bearing Steel in Novel Water-Based Lubricants
by Juan Bosch, Elizabeth Kotzalas, K Zin Htut, Rowan King and Christopher DellaCorte
Metals 2026, 16(4), 428; https://doi.org/10.3390/met16040428 - 15 Apr 2026
Viewed by 685
Abstract
Water-based lubricants (WBLs) are increasingly being considered for electrified drivetrain applications; however, their electrochemical stability toward bearing steels remains insufficiently understood. This study evaluated the corrosion behavior of through-hardened AISI 52100 bearing steel in novel WBLs to elucidate the corrosion kinetics and surface [...] Read more.
Water-based lubricants (WBLs) are increasingly being considered for electrified drivetrain applications; however, their electrochemical stability toward bearing steels remains insufficiently understood. This study evaluated the corrosion behavior of through-hardened AISI 52100 bearing steel in novel WBLs to elucidate the corrosion kinetics and surface degradation mechanisms. Round steel disks were cleaned and tested in 50 wt% aqueous dilutions of glycerol, ethylene glycol (MEG), polyethylene glycol (PEG), and polyalkylene glycol (PAG). Electrochemical measurements were conducted using a three-electrode cell in accordance with ASTM G3-14, employing open circuit potential (OCP), linear polarization resistance (LPR), electrochemical impedance spectroscopy (EIS), and potentiodynamic polarization curves. Among the uninhibited fluids, DI water exhibited the highest corrosion current density (19.85 µA/cm2), while glycerol- and PEG-based systems showed the lowest values (0.79 and 0.85 µA/cm2, respectively), attributed to organic adsorption at the steel/electrolyte interface. EIS analysis revealed a single charge-transfer-controlled process across all fluids, consistent with a weak, non-passive interfacial oxide whose protective character is modulated by organic adsorption. The addition of NaNO3 produced divergent effects depending on the base fluid chemistry: the corrosion activity was reduced in DI water and glycerol systems through enhanced passivation, while PEG- and PAG-based formulations showed increased corrosion current densities and reduced charge transfer resistance, attributed to competitive disruption of the polymer boundary layer by nitrate ions. Surface characterization by SEM/EDAX and white-light interferometry corroborated the electrochemical findings, revealing fluid-dependent corrosion morphologies ranging from uniform attack in DI water to localized pitting in polymer-based systems, with NaNO3 shifting the corrosion mode in PEG/PAG systems from localized to combined localized and uniform attack. These findings highlight the critical role of fluid chemistry in controlling corrosion processes in water-based lubricants and provide mechanistic insight for the development of corrosion-stable formulations for high-performance electrified drivetrain applications. Full article
(This article belongs to the Special Issue Corrosion and Fracture of Metallic Materials)
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15 pages, 7517 KB  
Article
Tensile and Low-Cycle Fatigue Properties of GH1059 Superalloy at RT and 550 °C
by Zhaoxiong Chu, Maowen Fu, Yankun Dou, Wen Yang and Bintao Yu
Metals 2026, 16(4), 416; https://doi.org/10.3390/met16040416 - 10 Apr 2026
Viewed by 465
Abstract
The tensile and low-cycle fatigue properties of a Fe-Ni-based GH1059 superalloy were investigated at room temperature (RT, about 25 °C) in air and at 550 °C in high vacuum. The tensile curve at 550 °C indicated that dynamic strain aging in the material [...] Read more.
The tensile and low-cycle fatigue properties of a Fe-Ni-based GH1059 superalloy were investigated at room temperature (RT, about 25 °C) in air and at 550 °C in high vacuum. The tensile curve at 550 °C indicated that dynamic strain aging in the material at high temperature. The fatigue life and stress-strain behavior were analyzed, and fatigue parameters were obtained. The fatigue life decreased with increasing temperature. The cyclic deformation behaviors were composed of three stages at RT: cyclic hardening, gradual cyclic softening, and final rapid rupture. The cyclic deformation behaviors at 550 °C were different: the second stage of specimen at 0.4% strain amplitude was cyclic hardening and the second stage of specimen at 0.9% strain amplitude was stress saturation. The difference is because of dynamic strain aging at high temperature. Based on the fatigue data, the changes of friction stress were analyzed, and the results reflected microstructural evolution associated with fatigue behavior. The microstructural evolution during fatigue process was observed using a scanning electron microscope and a transmission electron microscope. The changes in dislocation densities accounted for the effects of temperature and strain amplitude on the fatigue behavior of GH1059. Full article
(This article belongs to the Section Metal Failure Analysis)
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19 pages, 21367 KB  
Article
Investigation of Welded Joints of Pipelines from an Existing Gas Transmission Network Exposed to Hydrogen—Part I: Structure, Mechanical Properties and Susceptibility to Hydrogen Embrittlement
by Boris Yanachkov, Kateryna Valuiska, Yana Mourdjeva, Rumen Krastev, Vanya Dyakova, Tatiana Simeonova, Roumen H. Petrov, Krasimir Kolev, Margo Cauwels, Tom Depover and Rumyana Lazarova
Metals 2026, 16(4), 388; https://doi.org/10.3390/met16040388 - 31 Mar 2026
Cited by 1 | Viewed by 705
Abstract
The utilization of hydrogen as a clean energy carrier requires an assessment of existing natural gas pipelines with respect to hydrogen embrittlement (HE). In this study, the structural integrity and hydrogen sensitivity of X52 (L360) pipeline steel from the Bulgarian gas transmission network [...] Read more.
The utilization of hydrogen as a clean energy carrier requires an assessment of existing natural gas pipelines with respect to hydrogen embrittlement (HE). In this study, the structural integrity and hydrogen sensitivity of X52 (L360) pipeline steel from the Bulgarian gas transmission network after 31 years of service were investigated, focusing on production (longitudinal) and girth (circumferential) welded joints. Hydrogen content was measured in the base metal, production weld and girth weld before and after electrochemical charging, while in situ hydrogen charging during tensile testing was applied to simulate service conditions. Mechanical behavior was evaluated by tensile tests, and microstructural and fracture characteristics were analyzed by SEM and TEM. The results show significant spatial variations in hydrogen concentration, related to local microstructural heterogeneity and hydrogen trapping. In the as-operated state, fracture was localized mainly in the heat-affected zone. Hydrogen charging led to a pronounced reduction in ductility (approximately twofold), whereas yield and tensile strengths were only slightly affected. Failure analyses indicate a transition toward more brittle fracture mechanisms, dominated by quasi-cleavage and intergranular cracking in the as-charged state, with hydrogen embrittlement susceptibility indices demonstrating higher hydrogen sensitivity of the girth-welded joints. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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11 pages, 990 KB  
Article
Uncertainty Analysis of Plane Strain Fracture Toughness (KIC) Measurements of R350HT Rail Steels According to ASTM E399
by Fazil Husem
Metals 2026, 16(4), 371; https://doi.org/10.3390/met16040371 - 27 Mar 2026
Viewed by 481
Abstract
Fracture toughness is a very important mechanical attribute that affects the strength of rail steel used in high-speed rail systems. This study tests the measurement uncertainty that comes with measuring the plane strain fracture toughness (KIC) of R350HT rail steel. We [...] Read more.
Fracture toughness is a very important mechanical attribute that affects the strength of rail steel used in high-speed rail systems. This study tests the measurement uncertainty that comes with measuring the plane strain fracture toughness (KIC) of R350HT rail steel. We used the Single-Edge Bend (SEB) specimen to do fracture toughness testing. We used the Guide to Expressing Measurement Uncertainty (GUM)-based method to figure out how much uncertainty came from measuring the load, the crack opening displacement (COD), and the specimen’s shape and figuring out the crack length. At a 95% confidence level (k = 2), the combined standard uncertainty was found to be 0.881 MPa·m1/2, which is the same as an expanded uncertainty of 1.761 MPa·m1/2. The measured fracture toughness value of 40.59 ± 1.76 MPa·m1/2 meets the standards for rail steels. The results show how important it is to include measurement uncertainty in conformity assessment methods for safety-critical railway components. They also provide an experimentally proven framework for accurate mechanical property evaluation. Full article
(This article belongs to the Special Issue Fracture Mechanics and Failure Analysis of Metallic Materials)
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15 pages, 7604 KB  
Article
Fatigue Damage in Shot-Peened Al7075-T6 Alloy: Correlation Between Acoustic Emission Spectra and Fractographic Analysis
by Matteo Benedetti, Vigilio Fontanari, Emiliano Rustighi, Pasquale Gallo and Michele Bandini
Metals 2026, 16(3), 346; https://doi.org/10.3390/met16030346 - 19 Mar 2026
Viewed by 430
Abstract
Shot-peening treatments improve the fatigue performance of mechanical components thanks to the surface modifications introduced and mainly due to the residual compressive stresses present in the layer of material near the shot-peened surface. There is no unanimous agreement in scientific literature regarding the [...] Read more.
Shot-peening treatments improve the fatigue performance of mechanical components thanks to the surface modifications introduced and mainly due to the residual compressive stresses present in the layer of material near the shot-peened surface. There is no unanimous agreement in scientific literature regarding the kinetics of the damage process. However, it is generally accepted that, due to morphological and microstructural changes in the shot-peened layer, the material is more prone to early crack initiation, the propagation of which is then significantly slowed down or even stopped by the local stress field. This work focuses on applying the acoustic emission (AE) technique to detect fatigue crack initiation and propagation in shot-peened Al-alloy components. The analysis is conducted on Al-7075-T6 alloy, subjected to different shot-peening conditions and fatigue tested under alternating four-point bending. The results from the AE analyses are then correlated with a fractographic analysis. For all shot-peening conditions investigated, acoustic emission consistently indicated probable crack nucleation at approximately two-thirds of the total fatigue life, followed by a significant damage accumulation phase prior to dominant crack propagation. The final increase in acoustic activity coincided with the measurable loss of stiffness, confirming the onset of accelerated crack growth leading to fracture. The results demonstrate that, despite some experimental challenges, AE monitoring has the potential for the early detection of damage initiation. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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