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Polymers
Volume 14
Issue 23
10.3390/polym14235323
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Article
Peer-Review Record

Enhancement of Mechanical Properties and Bonding Properties of Flake-Zinc-Powder-Modified Epoxy Resin Composites

Polymers 2022, 14(23), 5323; https://doi.org/10.3390/polym14235323
by Xu Luo, Yu Li, Shuaijie Li * and Xin Liu *
Reviewer 1: Anonymous
Reviewer 2:
Md Najib Alam
Polymers 2022, 14(23), 5323; https://doi.org/10.3390/polym14235323
Submission received: 9 November 2022 / Revised: 30 November 2022 / Accepted: 30 November 2022 / Published: 5 December 2022
(This article belongs to the Section Polymer Composites and Nanocomposites)

Round 1

Reviewer 1 Report

In this manuscript, flake zinc powder was incorporated to modify the epoxy resin composites and the authors observed enhancement of mechanical and bonding properties. Overall, the experiments were well-designed and the manuscript was well-written. I support its publication after the following points are properly addressed.

1. At what temperature did the curing reaction take place and for how long?

2. How does the incorporation of zinc powder (either flake or sphere) affect the curing kinetics?

3. In the abstract and conclusion part, it was mentioned the dielectric properties were also studied. However, no dielectric experiments or results were discussed.

Author Response

Please see the attachment.

Author Response File: Author Response.docx

Reviewer 2 Report

Dear Authors,

In this paper authors modified the Zn filler by a silane coupling reagent and utilized as reinforcing filler for epoxy resin. The research methodology is fine and the results are informative. Paper is well written and I recommend some major revisions before final acceptance as suggested bellow.  

1.     Please modify these sentences “The two components were mixed and fully mixed. Vacuum defoaming and sample preparation after full mixing. The Mf-Zn modified CTPBA / EP epoxy resin composite was named Mf-Zn/CTPBA/EP, and the Ms-Zn modified CTPBA/EP epoxy resin composite was named Ms-Zn/CTPBA/EP.”

2.     The FT-IR of Silane coupling agent (KH-550) should be presented and have to see the peak shifts for a successful Zn-modification. I guess there should be a Zn-O-Si peak in the successful modification or at least peak shift. Si-O-Si peak can be obtained from remaining coupling reagent even after washing. Authors have to confirm.

3.     Generally, for reinforcing filler tan δ height becomes lower. Could you please provide loss modulus and storage modulus?

4.     Please include some suitable references in the mechanical properties discussion section. 

Author Response

Please see the attachment

Author Response File: Author Response.docx

Round 2

Reviewer 2 Report

Thanks for your well revision.

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