Next Article in Journal
Synthesis of Ti4O7 Nanoparticles by Carbothermal Reduction Using Microwave Rapid Heating
Next Article in Special Issue
Metal-Free Organocatalysis
Previous Article in Journal
Monoliths: A Review of the Basics, Preparation Methods and Their Relevance to Oxidation
Previous Article in Special Issue
One-Pot Two-Step Organocatalytic Asymmetric Synthesis of Spirocyclic Piperidones via Wolff Rearrangement–Amidation–Michael–Hemiaminalization Sequence
Open AccessArticle

A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide

School of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, China
Author to whom correspondence should be addressed.
Catalysts 2017, 7(2), 66;
Received: 14 January 2017 / Accepted: 15 February 2017 / Published: 16 February 2017
(This article belongs to the Special Issue Metal-free Organocatalysis)
PDF [5459 KB, uploaded 23 February 2017]


A novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions. This fluorous organocatalyst could be recovered and recycled several times with good purity. View Full-Text
Keywords: organocatalysis; ꞵ‐chloroethers; recycle; fluorous solid‐phase extraction (F‐SPE) organocatalysis; ꞵ‐chloroethers; recycle; fluorous solid‐phase extraction (F‐SPE)

Graphical abstract

This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited (CC BY 4.0).

Supplementary material


Share & Cite This Article

MDPI and ACS Style

Zhu, Y.; Shi, Y.; Yin, Y. A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide. Catalysts 2017, 7, 66.

Show more citation formats Show less citations formats

Note that from the first issue of 2016, MDPI journals use article numbers instead of page numbers. See further details here.

Related Articles

Article Metrics

Article Access Statistics



[Return to top]
Catalysts EISSN 2073-4344 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert
Back to Top