Search Results (702)

With the increasing demand for tunnel construction under extreme geological conditions such as high geo-stress, rock bursts, and fault zones, the performance requirements for shotcrete in initial support systems have become more stringent. This study develops a cross-scale structured hybrid fiber-reinforced shotcrete by incorporating alkali-resistant glass fibers including HP and HD types with different lengths and carbon nanotubes (CNTs) into a conventional shotcrete matrix. An orthogonal experimental design at four factors and four levels was adopted to investigate the effects of fiber and CNT contents on the mechanical properties and microstructure of shotcrete. Uniaxial compressive strength, splitting tensile strength, slumping, rebound rate, and microscopic characteristics such as SEM were evaluated at 3, 7, and 28 days. Results show that the optimal mix proportion is 4% HP fiber (24 mm), 2% HD fiber (18 mm), 2% HD fiber (6 mm), and 0.2% CNT. Under this formulation, the 28-day compressive and splitting tensile strengths reached 43.53 MPa and 4.85 MPa, respectively, with a rebound rate as low as 3.85%. The enhanced performance is attributed to the multi-scale reinforcement mechanism. Long fibers suppress macroscopic cracks, short fibers bridge micro-cracks, and CNTs densify the interfacial transition zone. This study provides a parametric reference for the development of high-performance shotcrete and its engineering application in complex underground excavations. Full article

Evaluation of dentin-replacement materials (DRMs) is essential for optimizing material selection and restorative outcomes. Four restorative groups, each comprising a DRM (SDR^® Plus, group A; EverX Posterior^™, group B-control; Filtek^™ Z250, group C; Fuji II LC^®, group D) overlayed with a microhybrid composite (Filtek Z250) to replace enamel layer, were evaluated for mechanical, optical, and handling characteristics. Standardized specimens were prepared for color change (ΔEab/E00) and fracture toughness (K_IC) testing (n = 8/group/test), with application time and handling evaluated by two independent assessors. Data were collected and analyzed statistically. The greatest color difference was observed in group B, which was significantly higher than that in groups A and C (p < 0.05), while group D did not differ significantly from any other group. Groups A and B exhibited significantly higher (p < 0.001) fracture toughness than groups C and D with no significant differences within either pair of groups. Group A required the least application time (p < 0.001), followed sequentially by groups B, C, and D. Handling ratings varied by material, with moderate inter-rater reliability (κ = 0.53). Within the study’s limitations, restorations with SDR Plus composites offered clinical application efficiency with improved fracture toughness and favorable optical integration. Full article

Natural fiber-reinforced polymer composites are attractive for lightweight and sustainable engineering applications; however, property scatter remains a major barrier to reliable design. Mean tensile properties alone are insufficient when material selection depends on repeatability and lower-tail performance. This study presents a statistical variability and lower-tail reliability assessment of flax, jute, and carbon fiber composite laminates using 590 open-access tensile test records from a published natural-fiber composite dataset. Flax and jute were selected as representative bast-fiber systems covering a range of woven, unidirectional, and short-fiber architectures; carbon fiber was included as a synthetic-fiber reference system. Three mechanically important properties were analyzed: the recalculated tensile modulus, tensile strength, and axial failure strain. Normal, lognormal, and two-parameter Weibull distributions were screened for each material–property combination using the Akaike information criterion (AIC); empirical fifth percentiles (P5) and bootstrap 95% confidence intervals (CI) were computed as lower-tail descriptors. The results show that Carbon-0 has the highest lower-tail modulus and strength, with empirical fifth percentiles of 104.95 GPa and 989.64 MPa, respectively. Among the natural fiber systems, Flax-0 and Flax-VE-0 provided the highest lower-tail strengths, whereas Flax-Twill and Flax-CP showed the highest lower-tail failure strains. The lowest tensile strength coefficient of variation was observed for Flax-90 (2.41%), followed by Flax-Twill (3.43%), Flax-0 (4.50%), Jute-Satin (4.83%), and Jute-Plain (4.92%). A balanced reliability ranking that combined lower-tail property ranks and coefficient of variation ranks identified Flax-0, Flax-VE-0, Flax-Twill, Flax-CP, and Jute-Satin as the most favorable natural-fiber systems. The lower coefficient of variation values observed in aligned and satin-weave architectures relative to short-fiber and plain-weave systems reflect the role of fiber orientation uniformity in moderating property scatter at the laminate scale. This study provides a reproducible statistical framework based on lower-tail performance descriptors for comparative screening purposes, not on formal design allowables for distinguishing high mean performance from reliable minimum-level performance in natural fiber composite laminates. Full article

Lunar regolith simulant (LRS) geopolymers are promising construction materials for lunar in situ resource utilization, but their brittle behavior and limited crack resistance restrict their structural applications. This study investigated the effect of basalt fiber length on the mechanical properties, failure modes, stress–strain behavior, constitutive relationship, and microstructure of CQU-1 LRS geopolymers. Basalt fiber-reinforced LRS geopolymers were prepared under weak alkali activation and high-temperature curing at 80 °C. The basalt fiber content was fixed at 0.1%, and six fiber lengths of 0, 6, 9, 12, 15, and 18 mm were considered. Compressive and flexural tests were conducted after curing for 1 d and 7 d, and the normalized stress–strain curves were fitted using the Saenz L.P., Carreira D.J., and Zhenhai Guo models. The results showed that basalt fiber length significantly affected the mechanical performance of LRS geopolymers. An appropriate fiber length improved strength, stiffness, ductility, and post-peak load-bearing capacity, whereas excessively short or long fibers weakened the reinforcing effect. The 15 mm fiber group exhibited the best overall performance. After curing for 1 d, its compressive strength reached 2.23 MPa, 49.7% higher than that of the control group, and its elastic modulus increased approximately 2.5-fold. After curing for 7 d, its compressive strength reached 13.44 MPa, 32.0% higher than that of the control group. The Zhenhai Guo model provided the best fit for the stress–strain curves. SEM-EDS analysis showed that basalt fibers improved interfacial bonding and promoted gel enrichment near the fiber–matrix interface. Overall, 15 mm was recommended as the optimal basalt fiber length for CQU-1 LRS geopolymers under the conditions used in this study. Full article

This study comprehensively investigates the thermal and mechanical degradation behavior of molded glass-fiber-reinforced plastic (GFRP) grating composites subjected to temperatures ranging from 80 °C to 320 °C. Three types of industrially produced GFRP gratings—open-type (OG), thin closed-skin (CG), and thick closed-skin (TCG)—were evaluated using mechanical, microstructural, chemical, and crystallographic analyses. Three-point bending tests revealed that TCG-type specimens exhibited superior thermal resistance, experiencing only a 43.9% loss in strength at 320 °C, whereas OG-type specimens showed significant resin degradation, fiber–matrix decomposition, and microcrack formation at temperatures above 200 °C. Scanning Electron Microscopy (SEM) and Fourier Transform Infrared Spectroscopy (FTIR) analyses revealed significant resin degradation, fiber–matrix decomposition, and microcrack formation. Thermogravimetric analysis (TGA) and Differential Scanning Calorimetry (DSC) confirmed substantial mass loss and structural disintegration at temperatures above 200 °C. Dynamic Mechanical Analysis (DMA) results revealed that the glass transition temperature (Tg) occurred at approximately 115–120 °C. The second-order regression model developed to estimate flexural strength under increasing temperature provided high accuracy (R² > 0.99) for all grating types. It should be noted that this investigation focuses on the short-term thermo-mechanical response under fundamental flexural loading to provide an accurate baseline for preliminary engineering design. The findings emphasize that the effect of temperature should be considered a critical parameter in the structural design of GFRP systems, especially in industrial environments with temperatures above 120 °C. Accordingly, tables for material selection and load-carrying capacity should be recalibrated to account for short-term temperature effects. Full article

Timber is a natural and renewable construction material, so it is environmentally friendly. However, timber has natural defects and also deteriorates over time. These problems require structural reinforcement. The present study aims to systematically explore the compression performance of natural Larch circular columns reinforced with Carbon Fiber-Reinforced Polymer (CFRP) and Basalt Fiber-Reinforced Polymer (BFRP). Thirty specimens were tested in pure axial compression to investigate the influence of the number of wrapping layers (0–3 layers), the specimen height (150, 200 and 300 mm) and the type of FRP material. The strengthening mechanism primarily relies on the passive hoop confinement provided by the FRP, which restricts the transverse expansion of the timber under axial load. Because CFRP possesses a higher tensile strength and elastic modulus than BFRP, it activates confining stresses more rapidly and provides a stronger restraint, leading to distinct improvements in load-bearing performance. The experimental results show that the failure mode of the short columns changes from inherent brittle splitting to a more ductile failure pattern, characterized by FRP ruptures and crushing of the timber as a result of external FRP wrapping. The axial compressive performance of the timber columns has been improved with both FRP materials. Given the same conditions, the CFRP caused increases in load-bearing capacity and stiffness, as a result of its higher tensile strength and elastic modulus, which gave rise to peak loads that were 4.9% to 7.8% greater than the BFRP-strengthened groups. There was a tendency for the reinforcement efficiency to increase with the number of layers of CFRP wrapping, and 2–3 layers of CFRP was found to be the optimal number of layers based on the aspect of material efficiency. In addition, FRP confinement was able to prevent premature failure and improve the ultimate transverse strain by as much as 2.1 times, significantly increasing ductility and energy dissipation. Finally, a theoretical ultimate strength prediction model was developed based on the passive confinement theory with the introduction of a height correction factor to consider the slenderness effects. The proposed model showed an overall coefficient of determination R² of 0.8027, which was good for reference for designing the reinforcement and evaluation of the performance of sustainable timber structure. Full article

Gravel soil used as backfill behind rockfall barriers in mountainous roads can extend structural service life and support sustainable resource utilization. However, rainfall-induced erosion may cause soil loss and reduce its buffering capacity. The fibers are short discrete fibers with a length of approximately 12 mm and an average diameter of 32.7 μm, corresponding to an aspect ratio of approximately 367. Reinforcement is achieved through fiber–soil interaction mechanisms, including particle bridging, interfacial friction, and pull-out resistance. The effects of polyurethane and fiber contents on compressive strength, shear strength, and impact resistance were evaluated using response surface methodology. Scanning electron microscopy was used to examine the microstructural features associated with the reinforcement mechanisms, and engineering-scale model tests were conducted to assess erosion and impact resistance under representative service conditions. The results show that polyurethane and fibers produce significant nonlinear enhancement effects on the mechanical properties of gravel soil, mainly through their individual contributions, whereas their interaction is limited. Multi-objective optimization indicates that the optimal mixture contains 6.8% polyurethane and 0.19% fiber, with prediction errors below 5%. The unconfined compressive strength of the gravelly soil increased from 107.6 kPa to 931.5 kPa, representing a 765.7% increase. Cohesion increased from 23.4 kPa to 83.44 kPa, representing a 256.4% increase. The internal friction angle increased from 43.4° to 61.23°, corresponding to a 41.08% increase. Under 1 h of intense rainfall erosion, the stabilized soil exhibited only slight surface particle detachment and maintained overall integrity. In impact tests, the velocity attenuation rate reached 65.6–71.4%. The proposed material provides a sustainable solution for improving buffer layers in rockfall barriers. Full article

Optimizing the injection molding of short-fiber-reinforced thermoplastics (SFRTs) is a persistent challenge due to the complex interplay between processing parameters and final mechanical performance. To address this, we developed and validated a machine learning (ML) pipeline to maximize both the tensile strength and Charpy impact resistance in polyamide 6 with 30% glass fiber (PA6-GF30). Through a designed experimental campaign, we systematically varied four key process parameters—melt temperature (260–300 °C), injection pressure (600–1000 bar), packing pressure (400–800 bar), and cooling time (15–35 s). The resulting dataset was used to train and compare three different regression models: Random Forest (RF), Gradient Boosting (GB), and Support Vector Regression (SVR). Our findings indicate that the Gradient Boosting (GB) algorithm yielded the most reliable predictions, significantly outperforming the other evaluated models. Further analysis using SHAP (Shapley Additive exPlanations) identified packing pressure as the dominant factor influencing tensile strength (contributing approximately 40% to the prediction), while melt temperature emerged as the key driver for impact resistance (around 35% contribution). By integrating our best-performing GB model with a multi-objective genetic algorithm, we identified an optimal set of parameters that simultaneously enhances both mechanical properties. Among the evaluated models (Random Forest, Support Vector Regression, and Gradient Boosting), the Gradient Boosting algorithm achieved the highest predictive accuracy. Compared to the baseline condition (280 °C melt temperature, 800 bar injection pressure, 600 bar packing pressure, 25 s cooling time), experimental validation of these optimized settings demonstrated substantial improvement: tensile strength increased from 145 MPa to 171 MPa (an 18% enhancement), and impact resistance rose from 45 kJ/m² to 55 kJ/m² (a 22% gain). This work establishes that an integrated ML and optimization framework can serve as a transformative approach for high-precision manufacturing of advanced engineering polymers. The primary novelty of this work lies in the development of a fully integrated, bias-free methodological framework that explicitly couples physical interpretability with multi-objective optimization, bridging the critical gap between black-box predictions and actionable industrial insights. Full article

Fused deposition modeling (FDM) provides a flexible manufacturing route for continuous fiber-reinforced thermoplastic composites, but weak interlaminar bonding and the trade-off between load-bearing capacity and deformation capability still limit their structural applications. In this study, multi-scale carbon/Kevlar fiber hybridization was introduced into acrylonitrile butadiene styrene (ABS)-based composites by combining continuous carbon fiber (CCF) or continuous Kevlar fiber (CKF) with short carbon fiber-filled ABS (ABS/SCF) or short Kevlar fiber-filled ABS (ABS/SKF). Four hybrid configurations and two continuous-fiber baseline composites were fabricated by FDM and evaluated through three-point bending tests, floating roller peel tests, peeled-surface SEM observations, and Rule-of-Mixtures-based hybrid effect analysis. The flexural results showed that short-fiber-filled matrices improved the flexural properties of both CCF- and CKF-based composites, but the degree of improvement depended on the fiber combination. Among the investigated configurations, CCF + ABS/SCF exhibited the highest flexural modulus and strength, which were 34.31% and 27.26% higher than those of CCF + ABS, respectively. For the CKF-based composites, CKF + ABS/SCF increased the flexural modulus and strength by 31.51% and 26.78%, compared with CKF + ABS, while maintaining the progressive deformation behavior associated with Kevlar reinforcement. The peel results showed that all hybrid composites had higher interlaminar peel resistance than their corresponding baselines, with increases ranging from 18.66% to 54.42%. The peeled-surface SEM observations indicated that the short-fiber-filled matrices changed the crack-propagation features, with more matrix tearing, fiber pull-out, and irregular peeling areas. The RoM-based comparison showed that the measured flexural properties of all hybrid configurations were higher than the corresponding RoM reference values. Overall, CCF + ABS/SCF was more suitable for improving stiffness and load-bearing capacity, whereas CKF + ABS/SCF showed a more balanced response in terms of flexural performance, interlaminar peel resistance, and progressive deformation behavior. Full article

Carbon nanotube (CNT)-reinforced composites are promising advanced materials due to their exceptional mechanical properties. This paper presents a comprehensive investigation of the mechanical behavior of CNT/epoxy composites through theoretical modeling and experimental validation. An equivalent cylindrical fiber model was developed to transform CNTs into effective reinforcement phases, enabling the application of classical composite mechanics. Three reinforcement configurations were analyzed: two unidirectional short fiber models (aligned and staggered) and a three-dimensional four-directional braided long-fiber model. The effects of geometric parameters, including the diameter-to-thickness ratio (D/t) and fiber aspect ratio, on the effective elastic moduli were systematically evaluated. Static and dynamic compression experiments were conducted using an MTS 810 testing system and a Split Hopkinson Pressure Bar (SHPB) to examine the influence of loading rate, vacuum treatment, and reinforcement type (CNT, SiC, and hybrid SiC/CNT) on composite strength. The results indicated that 3 wt% CNT reinforcement increases the Young’s modulus by 30% under static loading and enhanced the dynamic compressive strength under impact loading. The vacuum degassing process significantly affected composite quality, with insufficient vacuum leading to strength degradation due to void formation. Theoretical predictions using Mori–Tanaka and dilute methods showed good agreement with experimental results at low reinforcement volume fractions. Scanning electron microscopy revealed uniform CNT dispersion and provided insights into failure mechanisms, including CNT pull-out and breakage. This work contributes to the understanding of structure–property relationships in CNT-reinforced polymer composites and provides guidelines for achieving their optimal design. Full article

Short-fiber-reinforced composites (SFRCs) are widely used for their high strength-to-weight ratio. In the Additive Manufacturing (AM) field, Material Extrusion (MEX) processes inherently induce anisotropy, primarily due to fiber alignment along the deposition path, making printing direction and layer orientation critical for mechanical performance. In this study, specimens made of Onyx^®, a carbon short-fiber-reinforced polyamide, were fabricated by varying their orientation on the build platform, thereby producing different infill deposition directions. Each replica contained 25 layers. Two deposition strategies were investigated: a conventional alternating ±45° raster pattern and a 0°/90° configuration. Owing to the odd number of deposited layers, the latter resulted in two distinct stacking configurations, namely 0°/90° and 90°/0°, depending on the orientation of the first deposited layer. With such a strategy, it was possible to obtain configurations with a predominance of fibers either aligned with or transverse to the loading direction, depending on the orientation of the first-deposited layer. Mechanical test results were systematically compared to evaluate the influence of deposition strategy and fiber orientation on tensile performances. The effect of extrusion on fiber alignment was evaluated using Scanning Electron Microscopy (SEM). Mechanical behavior was evaluated using replicated tensile testing (five specimens per condition) and SEM-based fiber-orientation analysis. The investigation confirms the anisotropic nature of MEX-produced SFRCs. In particular, the 0°/90° configuration showed reductions of approximately 24% in tensile strength and 58% in elongation at break compared with the ±45° configuration. These results demonstrate that both extrusion-induced fiber orientation and layer-wise deposition strategy play a crucial role in defining the mechanical response of the material. Full article

Existing research on the axial compressive performance and size effect of carbon fiber-reinforced polymer (CFRP)-confined recycled aggregate concrete (RAC) short columns mainly relies on macroscopic experimental analysis, lacking research methods capable of reflecting the heterogeneous characteristics of materials and mesoscopic damage evolution mechanisms. Accordingly, a three-dimensional mesoscale finite element method was adopted in this study to establish a five-phase RAC mesoscopic model, including natural aggregates, old mortar, old interfacial transition zones (ITZs), new mortar, and new interfacial transition zones. Different from existing studies, predominantly based on macroscopic experiments or empirical models, this paper focuses on revealing the coupled effects of the recycled aggregate replacement ratio, the number of CFRP confinement layers, and specimen size. A total of 48 specimens were designed, covering four specimen sizes, four recycled coarse aggregate replacement ratios, and three CFRP confinement layers. The effects of these parameters on failure modes, stress–strain relationships, and size effect were systematically analyzed. The results indicate that the peak stress decreases significantly with the increase in the recycled coarse aggregate replacement ratio; the increase in CFRP layers markedly improves both the bearing capacity and post-peak bearing capacity retention rate; the ultimate stress generally declines as the specimen size increases, which highlights the pronounced size effect of CFRP-confined RAC short columns. Based on peak parameters and normalization analysis, a simplified stress–strain model was established: the goodness of fit R² of the ascending branch is 0.98565, and the goodness of fit for the descending branch parameters are ${\mathrm{R}}_{\mathsf{\beta }}^2$= 0.9655 and ${\mathrm{R}}_{\mathsf{\gamma }}^2$= 0.9350. Compared with existing models, the proposed model achieves a low prediction error of only 1.5–6.9%, demonstrating superior prediction accuracy. It can accurately describe the complete compressive process of CFRP-confined RAC short columns and provide a mesoscopic mechanistic basis for engineering design. Full article

This study investigated the effects of 7-day water storage as an accelerated aging condition on the mechanical properties of short fiber-reinforced resin composites (SFRCs) and a bulk-fill resin composite (RC). Two SFRCs (everX Flow Bulk, EXB; everX Flow Dentin, EXD) and one bulk-fill RC (SDR) serving as a control were evaluated. Specimens were stored in distilled water at 37 °C for either 1 or 7 days. Flexural strength, flexural modulus, and Vickers hardness were evaluated. Fractured surfaces were observed using scanning electron microscopy (SEM). For statistical analysis, a two-way ANOVA and Tukey’s test were used (α = 0.05). After 7-day water storage, the flexural strength of SDR significantly decreased (p < 0.05), while SFRCs maintained their initial strength (p > 0.05). In contrast, the flexural modulus significantly decreased in all materials (p < 0.05). Vickers hardness remained unaffected by water storage for all groups (p > 0.05). SEM observation revealed fiber pull-out in SFRCs. Although water immersion induced matrix degradation reflected in a reduced flexural modulus, SFRCs demonstrated promising resistance to initial water aging by maintaining flexural strength after water storage. These findings suggest that SFRCs may be a promising option for biomimetic dentin replacement under short-term hydrolytic aging conditions. Full article

Pultrusion is an efficient continuous manufacturing process for fiber-reinforced polymer (FRP) composites, but conventional open-bath impregnation has limitations such as resin exposure, quality variation, and resin loss. To overcome these limitations, closed-injection pultrusion (CIP) and short-pot-life resin systems have recently been introduced. However, the effects of processing variables on the quality and properties of composites manufactured using such resin systems have not been fully clarified. In this study, the effects of resin viscosity and pulling speed on the quality and mechanical properties of carbon FRP (CFRP) and glass FRP (GFRP) composites manufactured by CIP were investigated. CFRP and GFRP composites were fabricated at resin temperatures of 30 and 40 °C and pulling speeds of 300, 400, and 500 mm/min. The manufactured composites were evaluated in terms of void content, microstructure, hardness, and tensile properties. The results showed that increasing pulling speed increased void content and promoted macrovoids and locally poor impregnation, whereas the influence of resin temperature was relatively limited. Hardness, tensile strength, and elastic modulus decreased as pulling speed increased. These results demonstrate that CFRP and GFRP composites can be successfully manufactured by CIP using short-pot-life resin systems, and that precise control of resin viscosity and pulling speed is essential for achieving high quality and mechanical performance. Full article

This study investigates the thermo-mechanical performance of fused filament fabrication (FFF)-printed polyphthalamide reinforced with 15 wt.% short carbon fibers (PPA CF15) for engineering applications under elevated temperature and cyclic loading conditions. The material was characterized by quasi-static tensile testing, fatigue testing, dynamic mechanical analysis (DMA), scanning electron microscopy (SEM), and finite element analysis (FEA). Tensile tests performed from 20 to 180 °C revealed a strong temperature-dependent reduction in mechanical properties: the elastic modulus decreased from 2.437 to 0.401 GPa, while the ultimate tensile strength decreased from 64.537 to 9.190 MPa. In contrast, elongation at break generally increased with temperature, indicating a transition toward more ductile deformation governed by thermal softening of the polymer matrix. Fatigue tests showed reduced fatigue resistance at higher temperatures and stress levels; however, stable cyclic performance was achieved when the applied stress remained below approximately 60–70% of the ultimate tensile strength, with several specimens reaching 10⁶ cycles. DMA confirmed the viscoelastic nature of PPA CF15 and enabled the construction of frequency–temperature superposition master curves for numerical modelling. SEM observations revealed increased matrix deformation and fiber pull-out at elevated temperatures. FEA of an automotive intake manifold (IM) case study demonstrated that experimentally derived material data can be used to predict deformation, stress redistribution, and viscoelastic stabilization under combined thermal and mechanical loading. The results indicate that FFF-printed PPA CF15 is a promising lightweight composite for thermally and mechanically demanding automotive applications. Full article