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Keywords = short fiber-reinforced thermoplastics

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34 pages, 11753 KiB  
Review
Fused Deposition Modeling of Polymer Composites: Development, Properties and Applications
by Aldobenedetto Zotti, Teresa Paduano, Francesco Napolitano, Simona Zuppolini, Mauro Zarrelli and Anna Borriello
Polymers 2025, 17(8), 1054; https://doi.org/10.3390/polym17081054 - 14 Apr 2025
Cited by 2 | Viewed by 1299
Abstract
This review summarizes recent research advancements in thermoplastic composites used in Fused Deposition Modeling (FDM) processes. Since its development in 1988, FDM has emerged as one of the primary emerging technologies of Industry 4.0, receiving attention in fields such as industrial manufacturing, automotive, [...] Read more.
This review summarizes recent research advancements in thermoplastic composites used in Fused Deposition Modeling (FDM) processes. Since its development in 1988, FDM has emerged as one of the primary emerging technologies of Industry 4.0, receiving attention in fields such as industrial manufacturing, automotive, aerospace, and others, particularly for rapid prototyping and customization. The intention is to make available a guideline for 3D printing researchers, analyzing the properties and performance characteristics of different polymers and polymeric composites. The review analysis covers various reinforcing agents, including particles/nanoparticles, short fibers, and long fibers, identifying critical parameters of the FDM process which affect printed part quality, integrity and final geometry. Major attention is devoted to the different techniques employed for composite filament fabrication, mostly for structural elements and parts. An extensive overview of various FDM composites and fiber-reinforced composites by polymer matrices such as PLA, ABS, and PEEK is presented, with their mechanical and thermal properties reported for specific applications. Current challenges and prospective future research directions are also outlined, mainly focusing on the enhancement of material performance and sustainability. Full article
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17 pages, 2935 KiB  
Article
Effect of Fiber Content on the Preparation and Mechanical Properties of 3D Printed Short Carbon Fiber Reinforced PA Composites
by Yesong Wang, Feilong Li, Zixuan Sun, Chenyu Gu, Kunkun Fu and Xiangming Zhao
Polymers 2025, 17(5), 671; https://doi.org/10.3390/polym17050671 - 2 Mar 2025
Cited by 2 | Viewed by 1703
Abstract
3D-printed short-carbon-fiber-reinforced thermoplastic composites have attracted significant attention from both the academic and industrial communities due to their remarkable advantages such as lightweight, high strength, and recyclability. However, in most of the current 3D-printing-related nylon composites, the content of short carbon fibers is [...] Read more.
3D-printed short-carbon-fiber-reinforced thermoplastic composites have attracted significant attention from both the academic and industrial communities due to their remarkable advantages such as lightweight, high strength, and recyclability. However, in most of the current 3D-printing-related nylon composites, the content of short carbon fibers is generally low, and the influence laws of short carbon fibers on the mechanical properties of the composites have not been fully explored. This paper focuses on short-carbon-fiber-reinforced nylon (SCF/PA) composites with short-carbon-fiber contents of 15 wt%, 25 wt%, and 35 wt%, respectively. It studies in depth their mechanical properties and related characteristics. The research results show that with the increase in the short-carbon-fiber content, the melt flow rate of the SCF/PA composites shows a downward trend. In terms of mechanical properties, when the short-carbon-fiber content is 25 wt%, the tensile strength and flexural strength of the composite reach their maximum values, which are 101.43 MPa and 173.16 MPa, respectively. Compared with pure nylon, the improvement ranges are 17.01% and 21.4%, respectively. When the short-carbon-fiber content is 35 wt%, the impact resistance of the material reaches its optimal value, which is 6.02 KJ/m2, an increase of 38.1% compared with pure nylon. At the same time, when the short-carbon-fiber content is 35 wt%, the thermal deformation temperature of the material also shows a certain degree of slight increase. In summary, the research results of this paper will provide more abundant and detailed experimental data support for 3D-printed short-carbon-fiber-reinforced nylon composites in various different application scenarios, facilitating further exploration and application in related fields. Full article
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15 pages, 8198 KiB  
Article
Differential Effects of Adding Graphene Nanoplatelets on the Mechanical Properties and Crystalline Behavior of Polypropylene Composites Reinforced with Carbon Fiber or Glass Fiber
by Hiroki Satoh, Ayumu Morita and Yoshihiko Arao
Materials 2025, 18(5), 926; https://doi.org/10.3390/ma18050926 - 20 Feb 2025
Cited by 2 | Viewed by 711
Abstract
Short fiber-reinforced thermoplastic composites (SFRTPs) have excellent recyclability and processability, but their mechanical properties are weak compared to continuous fiber products. Various studies have reported that the addition of GNPs improves the mechanical properties of SFRTPs, but it is unclear what effect different [...] Read more.
Short fiber-reinforced thermoplastic composites (SFRTPs) have excellent recyclability and processability, but their mechanical properties are weak compared to continuous fiber products. Various studies have reported that the addition of GNPs improves the mechanical properties of SFRTPs, but it is unclear what effect different types of reinforcing fibers have on a hybrid composite system. In this study, the effect of adding a small amount (1 wt%) of graphene nanoplatelets (GNPs) to fiber-reinforced polypropylene composites on their mechanical properties was investigated from a crystallinity perspective. GNPs were mixed with polypropylene (PP)/carbon fiber (CF) or PP/glass fiber (GF) using a melt blending process, and composites were molded by injection molding. The results of mechanical property characterization showed no significant effect when GNPs were added to PP/CF, but when GNPs were added to PP/GF, this increased the composite’s tensile strength and Young’s modulus by approximately 20% and 10%, respectively. The interfacial shear strength (IFSS) predicted using the modified Kelly–Tyson equation did not change much before and after the addition of GNPs to PP/CF. On the other hand, the IFSS increased from 10.8 MPa to 19.2 MPa with the addition of GNPs to PP/GF. The increase in IFSS led to an increase in the tensile strength of PP/GF with the incorporation of GNPs. Differential scanning calorimetry (DSC) indicated that GNPs accelerated the crystallization rate, and the X-ray diffraction (XRD) results confirmed that GNPs acted as a crystal nucleating agent. However, CF was also shown to be a nucleating agent, limiting the effect of GNP addition. In other words, it can be said that the addition of GNPs to PP/GF is more effective than their addition to PP/CF due to the differential crystallization effects of each fiber. Full article
(This article belongs to the Special Issue Advanced Resin Composites: From Synthesis to Application)
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16 pages, 7739 KiB  
Article
Development of Short Jute Fiber-Reinforced Thermoplastic Pre-Preg Tapes
by Mengyuan Dun, Haitao Fu, Jianxiu Hao and Weihong Wang
Polymers 2025, 17(3), 388; https://doi.org/10.3390/polym17030388 - 31 Jan 2025
Cited by 2 | Viewed by 1290
Abstract
Jute fibers are renewable, light, and strong, allowing them to be considered as attractive materials in composite manufacturing. In the present work, a simple and effective method for preparing continuous pre-preg tapes from short jute fiber bundles (without twist) is developed and its [...] Read more.
Jute fibers are renewable, light, and strong, allowing them to be considered as attractive materials in composite manufacturing. In the present work, a simple and effective method for preparing continuous pre-preg tapes from short jute fiber bundles (without twist) is developed and its application in winding forming is evaluated. Linear low-density polyethylene film (LLDPE) with good flexibility and weather resistance was used as the thermoplastic matrix; jute fiber bundles were first spread parallel to each other on an LLDPE film and then rolled up to form a pre-roll. The pre-roll enclosing fiber bundles was hot-pressed in a designed mold to form a pre-preg tape, where the fiber bundles were more parallel to the tape than the fibers in twine. Although the untwisted structure exhibited a lower tensile strength for the fiber bundle, it could be processed into a continuous pre-preg with higher tensile strength than the jute twine-impregnated pre-preg. This is based on the good impregnation of the short fiber bundle and its unidirectional, uniform strengthening in the continuous pre-preg. The tensile strength and modulus of the fiber bundle-reinforced pre-preg increased by 16.70% and 257.14%, respectively, compared with jute twine-reinforced pre-preg (within the fiber proportion of 40.wt%). When applied to winding, the fiber bundle-reinforced pre-preg showed advantages of interlayer fusion, surface flatness, and ring stiffness. In contrast, the twisted continuous structure did not retain its advantage in pre-preg. The development of pre-preg tapes by discontinuous fibers might be a good way for utilizing natural fibers in the field of green engineering due to its diverse secondary processing. Full article
(This article belongs to the Special Issue Fiber Reinforced Polymers: Manufacture, Properties and Applications)
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17 pages, 6382 KiB  
Article
Tribological Performance of Short Fibers Reinforced Thermoplastic Polyurethane Composite Materials Under Water-Lubricated Condition
by Yicong Yu, Pan Jiang, Wei Yu and Zhiwei Guo
Polymers 2025, 17(1), 30; https://doi.org/10.3390/polym17010030 - 26 Dec 2024
Viewed by 949
Abstract
The water-lubricated bearing plays a crucial role in the ship propulsion system, significantly impacting vessel safety. However, under the harsh working conditions of low-speed and heavy-load, the lubrication state of water-lubricated bearings is usually poor, leading to serious friction and wear. To improve [...] Read more.
The water-lubricated bearing plays a crucial role in the ship propulsion system, significantly impacting vessel safety. However, under the harsh working conditions of low-speed and heavy-load, the lubrication state of water-lubricated bearings is usually poor, leading to serious friction and wear. To improve the tribological performance of composites and reduce friction, three short fibers (ultra-high-molecular-weight polyethylene fibers, basalt fibers, and bamboo fibers) with the same mass fraction (5%) were added into the melted thermoplastic polyurethane (TPU). The tribological behavior of these three composites under different loads and rotation speeds was investigated using the CBZ-1 friction and wear tester. Through the comprehensive analysis of the friction coefficient, the wear mass loss, and the surface morphology, it was confirmed that the filled fiber positively affected the tribological performance of thermoplastic polyurethane materials. The experimental results indicated that basalt fiber significantly improved the tribological performance of TPU, and the friction coefficient of the sample was only 0.088 under the working conditions of 0.5 MPa and 250 r/min, which was 70.57% lower than that of pure TPU material. And in all the tests, the minimum wear of the basalt fiber-reinforced composite is only 0.4 mg, which is also the smallest of all the materials under all conditions, and a decrease of 98.69% compared to TPU. Under high loads, ultra-high-molecular-weight polyethylene fiber and bamboo fiber-reinforced composites have smoother surfaces and exhibit better tribological properties. This study provides an experimental foundation for tribological performance enhancement for environmentally friendly, water-lubricated bearing composites. Full article
(This article belongs to the Special Issue Advances in Functional Rubber and Elastomer Composites II)
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19 pages, 8782 KiB  
Article
Polyvinyl Butyral Addition Effects on Notched Charpy Impact Strength of Injection-Molded Glass Fiber-Reinforced Polypropylene
by Tetsuo Takayama, Yuuki Yuasa and Quan Jiang
Polymers 2024, 16(24), 3472; https://doi.org/10.3390/polym16243472 - 12 Dec 2024
Cited by 1 | Viewed by 1169 | Correction
Abstract
Glass short fiber-reinforced thermoplastics (GSFRTPs) are a cost-effective alternative to other short fiber-reinforced thermoplastics (SFRTPs). Their excellent mechanical properties make them a suitable material for components that require rigidity and light weight in widely diverse fields, including transportation and office automation equipment. The [...] Read more.
Glass short fiber-reinforced thermoplastics (GSFRTPs) are a cost-effective alternative to other short fiber-reinforced thermoplastics (SFRTPs). Their excellent mechanical properties make them a suitable material for components that require rigidity and light weight in widely diverse fields, including transportation and office automation equipment. The melt-mixing process is used to shorten glass fibers. The notched impact strength of molded products is strongly affected by the fiber length. An important issue is how to conduct melt-molding processing while keeping the fibers long. In this regard, a survey of cases in which additives were used to increase the fiber length revealed no useful reports. However, a growing trend toward the reuse of plastic material wastes has emerged. When reusing GSFRTP wastes, the objective is to recycle the material as GSFRTPs. This promotion of the reuse of GSFRTPs necessitates the production of molded products with the fiber length maintained to the greatest extent feasible. Moreover, GSFRTPs should be recycled in a manner consistent with the original GSFRTPs. In recent years, there has also been a growing movement to reuse polyvinyl butyral (PVB) in accordance with Sustainable Development Goals (SDGs). It has been established that PVB can be extracted from the laminated glass state with high efficiency using mechanical methods. This study evaluated the mechanical properties of GSFRTPs with a PP matrix when PVB was added. The results show that the incorporation of PVB and maleic anhydride-modified PP in quantities of less than 1 wt% into GSFRTPs leads to sizing effects wherein the fibers are dispersed in bundles. Furthermore, this combination enhances the notched impact strength of the resulting molded product by 0.5 kJ/m2 at the maximum. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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13 pages, 3036 KiB  
Article
On the Hydrodynamic and Structural Performance of Thermoplastic Composite Ship Propellers Produced by Additive Manufacturing Method
by Erkin Altunsaray, Serkan Turkmen, Ayberk Sözen, Alperen Doğru, Pengfei Liu, Akile Neşe Halilbeşe and Gökdeniz Neşer
J. Mar. Sci. Eng. 2024, 12(12), 2206; https://doi.org/10.3390/jmse12122206 - 2 Dec 2024
Viewed by 1631
Abstract
In the marine industry, the search for sustainable methods, materials, and processes, from the product’s design to its end-of-life stages, is a necessity for combating the negative consequences of climate change. In this context, the lightening of products is essential in reducing their [...] Read more.
In the marine industry, the search for sustainable methods, materials, and processes, from the product’s design to its end-of-life stages, is a necessity for combating the negative consequences of climate change. In this context, the lightening of products is essential in reducing their environmental impact throughout their life. In addition to lightening through design, lightweight materials, especially plastic-based composites, will need to be used in new and creative ways. The material extrusion technique, one of the additive manufacturing methods, is becoming more widespread day by day, especially in the production of objects with complex forms. This prevalence has not yet been reflected in the marine industry. In this study, the performances of plastic composite propellers produced by the material extrusion technique is investigated and discussed comparatively with the help of both hydrodynamic and structural tests carried out in a cavitation tunnel and mechanical laboratory. The cavitation tunnel test and numerical simulations were conducted at a range of advance coefficients (J) from 0.3 to 0.9. The shaft rate was kept at 16 rps. The thrust and torque data were obtained using the tunnel dynamometer. Digital pictures were taken to obtain structural deformation and cavitation dynamics. The structural performance of the propellers shows that an aluminum propeller is the most rigid, while a short carbon fiber composite propeller is the most flexible. Continuous carbon fiber composite has high strength and stiffness, while continuous glass fiber composite is more cost-effective. In terms of the hydrodynamic performance of the propellers, flexibility reduces the loading on the blade, which can result in thrust and torque reduction. Overall, the efficiency of the composite propellers was similar and less than that of the rigid aluminum propeller. In terms of weight, the composite carbon propeller containing continuous fiber, which is half the weight of the metal propeller, is considered as an alternative to metal in production. These propellers were produced from a unique composite consisting of polyamide, one of the thermoplastics that is a sustainable composite material, and glass and carbon fiber as reinforcements. The findings showed that the manufacturing method and the new composites can be highly successful for producing ship components. Full article
(This article belongs to the Special Issue Marine Technology: Latest Advancements and Prospects)
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21 pages, 8351 KiB  
Review
Application of Poly(lactic Acid) Composites in the Automotive Sector: A Critical Review
by Valentina Giammaria, Monica Capretti, Giulia Del Bianco, Simonetta Boria and Carlo Santulli
Polymers 2024, 16(21), 3059; https://doi.org/10.3390/polym16213059 - 30 Oct 2024
Cited by 15 | Viewed by 3305
Abstract
The introduction of bio-based matrices in automotive applications would, in principle, increase their sustainability and, in case the use of secondary raw materials is also involved, even result in reduced resource depletion. The bio-based polymer composite matrix that has been mainly brought forward [...] Read more.
The introduction of bio-based matrices in automotive applications would, in principle, increase their sustainability and, in case the use of secondary raw materials is also involved, even result in reduced resource depletion. The bio-based polymer composite matrix that has been mainly brought forward towards industrial application is poly(lactic acid) (PLA), which has often been proposed as the replacement for matrices based on polyolefins in fields such as packaging and short-term commodities since, in general, it matches the needs for conventional thermoplastic production processes. The passage to the automotive sector is not obvious, though: problems affecting durability, the relation with water and the environment, together with the requirement for outstanding mechanical and impact performance appear very stringent. On the other hand, PLA has obtained durable success in additive manufacturing as a competitor for acrylonitrile butadiene styrene (ABS). Also, the perspective for 3D and 4D printing does not appear to be confined to bare prototyping. These contrasting pieces of evidence indicate the necessity to provide more insight into the possible development of PLA use in the automotive industry, also considering the pressure for the combined use of more sustainable reinforcement types in automotive composites, such as natural fibers. Full article
(This article belongs to the Section Polymer Applications)
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12 pages, 44605 KiB  
Article
The Investigation of Overflow Water-Powered Projectile-Assisted Injection Molded Short-Glass-Fiber-Reinforced Polypropylene
by Wei Zhang, Mao-Zeng Wang, Tang-Qing Kuang, Qian-Sheng Liao, Shi-Yu Jiang and He-Sheng Liu
Processes 2024, 12(11), 2333; https://doi.org/10.3390/pr12112333 - 24 Oct 2024
Viewed by 959
Abstract
Water-powered projectile-assisted injection molding (W-PAIM) is a novel injection molding technology that has been recently developed based on the ripe water-assisted injection molding (WAIM). Fiber orientation pattern and residual wall thickness (RWT) are two crucial factors determining the quality of W-PAIM parts composed [...] Read more.
Water-powered projectile-assisted injection molding (W-PAIM) is a novel injection molding technology that has been recently developed based on the ripe water-assisted injection molding (WAIM). Fiber orientation pattern and residual wall thickness (RWT) are two crucial factors determining the quality of W-PAIM parts composed of short fiber-reinforced thermoplastics (SFRTCs). However, limited work has been conducted on W-PAIM of SFRTC parts, which restricts its application process. In this work, an intensive investigation of W-PAIM parts composed of short fiber-reinforced polypropylene was conducted via a newly lab-developed W-PAIM platform. The results indicated that fibers were quite well oriented in the region extending from the core zone to the water channel, especially in the water channel zone, but randomly aligned in a small region near the mold wall. Nevertheless, fibers in the water channel zone of W-PAIM part were highly oriented, presenting an opposite alignment trend in fiber orientation compared to that in the water channel zone of the WAIM part as reported earlier. These disparities in fiber orientation between W-PAIM and WAIM parts were primarily attributed to the strong flow fields generated by projectile penetration. Additionally, the influence of three main processing parameters that significantly affected the projectile penetration on these two crucial factors was also investigated using the single-factor method. It was discovered that water injection delay time constituted the primary factor affecting the projectile penetration process, and reducing this time could greatly increase the relative thickness of the ordered area and the uniformity of RWT. More importantly, within the value range of the tested processing parameters, increased water pressure, elevated melt temperatures, and shorter water injection delay time could simultaneously improve fiber orientation and the uniformity of RWT in W-PAIM parts, which may improve the properties of W-PAIM parts and enlarge their application scope. This work provides a comprehensive guide for the fabrication of W-PAIM parts of SFRTCs. Full article
(This article belongs to the Section Materials Processes)
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20 pages, 15194 KiB  
Article
Effect of High Fiber Content on Properties and Performance of CFRTP Composites
by Saeed Ziaee, Eric Kerr-Anderson, Aaron Johnson, David Eastep and Beckry Abdel-Magid
J. Compos. Sci. 2024, 8(9), 364; https://doi.org/10.3390/jcs8090364 - 17 Sep 2024
Cited by 4 | Viewed by 2525
Abstract
Continuously reinforced thermoplastic composites are widely used in structural applications due to their toughness, light weight, and shorter process cycle. Moreover, they provide flexibility in design and material selection. Unlike thermoset composites, continuous fiber content to maximize mechanical properties in thermoplastic composites has [...] Read more.
Continuously reinforced thermoplastic composites are widely used in structural applications due to their toughness, light weight, and shorter process cycle. Moreover, they provide flexibility in design and material selection. Unlike thermoset composites, continuous fiber content to maximize mechanical properties in thermoplastic composites has not been well investigated. In this paper, three thermoplastic systems are investigated to study the optimum content of continuous fiber reinforcement. These systems include carbon fiber/polyphenylene sulfide (PPS), glass fiber/PPS, and glass fiber/high-density polyethylene (HDPE). Tapes were made at several fiber contents, and samples were compression molded and tested using thermo-gravimetric analysis (TGA), differential scanning calorimetry (DSC), dynamic mechanical analysis (DMA), tensile, 3-point flexure, and short-beam shear tests. Results revealed that higher fiber content led to an increase in the glass transition and melt transition temperatures of the polymer. Some mechanical properties increased with fiber content and then began to decrease upon further addition of fibers, while other properties, such as ductility and interfacial bond strength, decreased with more reinforcement. Furthermore, the optimum fiber contents to maximize mechanical properties are different for different properties and different materials. Full article
(This article belongs to the Special Issue Advances in Continuous Fiber Reinforced Thermoplastic Composites)
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18 pages, 6151 KiB  
Article
Enhancing the Fire Resistance of Ablative Materials: Role of the Polymeric Matrix and Silicon Carbide Reinforcement
by Juana Abenojar, Sara López de Armentia and Miguel Angel Martínez
Polymers 2024, 16(17), 2454; https://doi.org/10.3390/polym16172454 - 29 Aug 2024
Cited by 1 | Viewed by 1252
Abstract
The primary characteristic of ablative materials is their fire resistance. This study explored the development of cost-effective ablative materials formed into application-specific shapes by using a polymer matrix reinforced with ceramic powder. A thermoplastic (polypropylene; PP) and a thermoset (polyester; UPE) matrix were [...] Read more.
The primary characteristic of ablative materials is their fire resistance. This study explored the development of cost-effective ablative materials formed into application-specific shapes by using a polymer matrix reinforced with ceramic powder. A thermoplastic (polypropylene; PP) and a thermoset (polyester; UPE) matrix were used to manufacture ablative materials with 50 wt% silicon carbide (SiC) particles. The reference composites (50 wt% SiC) were compared to those with 1 and 3 wt% short glass fibers (0.5 mm length) and to composites using a 1 and 3 wt% glass fiber mesh. Fire resistance was tested using a butane flame (900 °C) and by measuring the transmitted heat with a thermocouple. Results showed that the type of polymer matrix (PP or UPE) did not influence fire resistance. Composites with short glass fibers had a fire-resistance time of 100 s, while those with glass fiber mesh tripled this resistance time. The novelty of this work lies in the exploration of a specific type of material with unique percentages of SiC not previously studied. The aim is to develop a low-cost coating for industrial warehouses that has improved fire-protective properties, maintains lower temperatures, and enhances the wear and impact resistance. Full article
(This article belongs to the Special Issue Flame-Retardant Polymer Composites II)
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26 pages, 11470 KiB  
Article
The Role of Triboloading Conditions in Tribolayer Formation and Wear Resistance of PES-Based Composites Reinforced with Carbon Fibers
by Defang Tian, Changjun He, Dmitry G. Buslovich, Lyudmila A. Kornienko and Sergey V. Panin
Polymers 2024, 16(15), 2180; https://doi.org/10.3390/polym16152180 - 31 Jul 2024
Cited by 1 | Viewed by 1177
Abstract
In this paper, the tribological characteristics of polyethersulfone-based composites reinforced with short carbon fibers (SCFs) at aspect ratios of 14–250 and contents of 10–30 wt.% are reported for linear metal–polymer and ceramic–polymer tribological contacts. The results showed that the wear resistance could be [...] Read more.
In this paper, the tribological characteristics of polyethersulfone-based composites reinforced with short carbon fibers (SCFs) at aspect ratios of 14–250 and contents of 10–30 wt.% are reported for linear metal–polymer and ceramic–polymer tribological contacts. The results showed that the wear resistance could be greatly improved through tribological layer formation. Loading PES with 30 wt.% SCFs (2 mm) provided a minimum WR value of 0.77 × 10−6 mm3/N m. The tribological layer thicknesses were estimated to be equal to 2–7 µm. Several conditions were proposed, which contributed to the formation of a tribological layer from debris, including the three-stage pattern of the changing kinetics of the time dependence of the friction coefficient. The kinetics had to sharply increase up to ~0.4–0.5 in the first (running-in) stage and gradually decrease down to ~0.1–0.2 in the second stage. Then, if these levels did not change, it could be argued that any tribological layer had formed, become fixed and fulfilled its functional role. The PES-based composites loaded with SCFs 2 mm long were characterized by possessing the minimum CoF levels, for which their three-stage changing pattern corresponded to one of the conditions for tribological layer formation. This work provides valuable insight for studying the process parameters of tribological layer formation for SCF-reinforced thermoplastic PES composites and revealing their impact on tribological properties. Full article
(This article belongs to the Special Issue Fiber-Reinforced Polymer Composites: Progress and Prospects)
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15 pages, 5025 KiB  
Article
Estimation of Critical Fatigue Conditions Based on the Accelerated Fatigue Locati Method by Mean of Net Damage
by Isidro A. Carrascal, Soraya Diego, Jose A. Casado, Jose A. Sainz-Aja and Diego Ferreño
Appl. Sci. 2024, 14(11), 4939; https://doi.org/10.3390/app14114939 - 6 Jun 2024
Viewed by 1152
Abstract
The increasing utilization of short fiber-reinforced thermoplastics, due to their advantageous mechanical properties and manufacturing convenience, has led to their application in areas traditionally dominated by metals. This shift underscores the importance of understanding the fatigue behavior of these materials. This study evaluates [...] Read more.
The increasing utilization of short fiber-reinforced thermoplastics, due to their advantageous mechanical properties and manufacturing convenience, has led to their application in areas traditionally dominated by metals. This shift underscores the importance of understanding the fatigue behavior of these materials. This study evaluates the fatigue behavior of short fiber-reinforced thermoplastics through three characterization methods: continuous fatigue, interrupted fatigue, and the Locati method, with the latter serving as a novel approach for estimating critical fatigue conditions from a single specimen. Continuous fatigue testing provides the baseline for comparison. The effect of load interruption is explored through the interrupted fatigue method. The Locati method, characterized by incrementally increasing load steps until failure, offers a significant benefit by enabling the estimation of critical fatigue conditions efficiently. This research aims to provide a comprehensive understanding of the fatigue behavior of short fiber-reinforced thermoplastics, contributing to the optimization of their use in engineering applications. Full article
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21 pages, 5226 KiB  
Article
Characterization and Implementation of Cocoa Pod Husk as a Reinforcing Agent to Obtain Thermoplastic Starches and Bio-Based Composite Materials
by Andrés Mauricio Holguín Posso, Juan Carlos Macías Silva, Juan Pablo Castañeda Niño, Jose Herminsul Mina Hernandez and Lety del Pilar Fajardo Cabrera de Lima
Polymers 2024, 16(11), 1608; https://doi.org/10.3390/polym16111608 - 6 Jun 2024
Cited by 6 | Viewed by 3944
Abstract
When the cocoa pod husk (CPH) is used and processed, two types of flour were obtained and can be differentiated by particle size, fine flour (FFCH), and coarse flour (CFCH) and can be used as a possible reinforcement for the development of bio-based [...] Read more.
When the cocoa pod husk (CPH) is used and processed, two types of flour were obtained and can be differentiated by particle size, fine flour (FFCH), and coarse flour (CFCH) and can be used as a possible reinforcement for the development of bio-based composite materials. Each flour was obtained from chopping, drying by forced convection, milling by blades, and sieving using the 100 mesh/bottom according to the Tyler series. Their physicochemical, thermal, and structural characterization made it possible to identify the lower presence of lignin and higher proportions of cellulose and pectin in FFCH. Based on the properties identified in FFCH, it was included in the processing of thermoplastic starch (TPS) from the plantain pulp (Musa paradisiaca) and its respective bio-based composite material using plantain peel short fiber (PPSF) as a reinforcing agent using the following sequence of processing techniques: extrusion, internal mixing, and compression molding. The influence of FFCH contributed to the increase in ultimate tensile strength (7.59 MPa) and higher matrix–reinforcement interaction when obtaining the freshly processed composite material (day 0) when compared to the bio-based composite material with higher FCP content (30%) in the absence of FFCH. As for the disadvantages of FFCH, reduced thermal stability (323.57 to 300.47 °C) and losses in ultimate tensile strength (0.73 MPa) and modulus of elasticity (142.53 to 26.17 MPa) during storage progress were identified. In the case of TPS, the strengthening action of FFCH was not evident. Finally, the use of CFCH was not considered for the elaboration of the bio-based composite material because it reached a higher lignin content than FFCH, which was expected to decrease its affinity with the TPS matrix, resulting in lower mechanical properties in the material. Full article
(This article belongs to the Special Issue Preparation and Application of Biomass-Based Materials)
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23 pages, 14306 KiB  
Article
Improving the Accuracy of the Evaluation Method for the Interfacial Shear Strength of Fiber-Reinforced Thermoplastic Polymers through the Short Beam Shear Test
by Quan Jiang, Tetsuo Takayama and Akihiro Nishioka
Polymers 2024, 16(7), 883; https://doi.org/10.3390/polym16070883 - 23 Mar 2024
Cited by 3 | Viewed by 2186
Abstract
Short fiber-reinforced thermoplastic polymers (SFRTPs) are commonly used in various molding methods due to their high specific elasticity and strength. To evaluate the interfacial strength, several determination methods have been proposed, including the interfacial shear strength (IFSS). In previous research, an IFSS evaluation [...] Read more.
Short fiber-reinforced thermoplastic polymers (SFRTPs) are commonly used in various molding methods due to their high specific elasticity and strength. To evaluate the interfacial strength, several determination methods have been proposed, including the interfacial shear strength (IFSS). In previous research, an IFSS evaluation method based on the short beam shear method was proposed. However, this method is only applicable to micrometer-sized fibers with high stiffness levels that are not easily bent. When utilizing cellulose fiber, the interfacial shear strength (IFSS) results frequently exhibit significant deviations. To tackle this issue, we suggest an enhanced experimental technique that employs beam-shaped specimens with welding points based on the short beam shear test. Furthermore, we conducted a three-dimensional analysis of the original method to determine the fiber orientation angle and IFSS. The outcomes were compared with previously reported determinations. The IFSS achieved through the novel method proposed in this paper exhibits high precision and reliability, rendering it suitable for use with soft and flexible fibers. Full article
(This article belongs to the Special Issue Polymer Composites: Design, Manufacture and Characterization)
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