Search Results (69)

This research investigated how detergent type and concentration, solution temperature, and flow rate affect ultrasonic cleaning efficiency in jewelry manufacturing. A silver bracelet without gemstones served as the test sample, and the study combined harmonic response analysis to assess acoustic pressure distribution with computational fluid dynamics to examine fluid flow patterns inside an ultrasonic cleaning machine. Cleaning tests were performed under real factory conditions to verify the simulations. Results showed that cleaning efficiency depends on the combined chemical and ultrasonic effects. Adding detergent lowered surface tension, encouraging cavitation bubble formation; higher temperatures (up to 60 °C) softened dirt, making removal easier; and moderate solution flow improved the cleaning, helping to carry dirt away from jewelry surfaces. Too much flow, however, decreased cavitation activity. The highest cleaning efficiency (93.890%) was achieved with 3% U-type detergent at 60 °C and a flow rate of 5 L/min, while pure water at room temperature (30 °C) without flow had the lowest efficiency (0.815%), confirmed by weighing and scanning electron microscope measurements. Interestingly, maximum ultrasonic power concentration did not always match the highest cleaning efficiency. The study supports sustainable practices by limiting detergent use to 3%, in line with Sustainable Development Goal (SDG) 9 (Industry, Innovation, and Infrastructure). Full article

Recent advancements in composite materials design have made glass fiber-reinforced polymer composites (GFRPC) a viable choice for a wide range of engineering and industrial applications. Although GFRPCs boast attractive characteristics such as low specific mass and high specific mechanical strength, identifying and characterizing damage mechanisms in these materials is challenging. Several scientific studies have examined the root causes of GFRPC failure using various methods, including non-destructive techniques and learning algorithms. Despite this, ongoing investigations aim to accurately detect mechanical defects in GFRPCs. This study explores the use of non-destructive testing (NDT) combined with unsupervised learning algorithms to identify and classify damage mechanisms in GFRPCs. The NDT method employed in this study is acoustic emission (AE), which identifies waveforms associated with various failure mechanisms during testing. These waveforms are categorized using unsupervised learning methods such as principal component analysis (PCA) and self-organizing maps. PCA selects the most appropriate AE descriptors for distinguishing between different damage mechanisms, while the self-organizing maps algorithm performs clustering analysis and classifies failure mechanisms. Scanning electron microscope images of the observed failures are provided to sup-port the findings derived from AE data. Full article

Traditional coal quality assessment methods rely exclusively on the laboratory testing of physical samples, which impedes detailed stratigraphic evaluation and limits the integration of intelligent precision mining technologies. To resolve this challenge, this study investigates geophysical logging as an innovative method for coal quality prediction. By integrating scanning electron microscopy (SEM), X-ray analysis, and optical microscopy with interdisciplinary methodologies spanning mathematics, mineralogy, and applied geophysics, this research analyzes the coal quality and mineral composition of the Shanxi Formation coal seams in northern Jiangsu, China. A predictive model linking geophysical logging responses to coal quality parameters was established to delineate relationships between subsurface geophysical data and material properties. The results demonstrate that the Shanxi Formation coals are gas coal (a medium-metamorphic bituminous subclass) characterized by low sulfur content, low ash yield, low fixed carbon, high volatile matter, and high calorific value. Mineralogical analysis identifies calcite, pyrite, and clay minerals as the dominant constituents. Pyrite occurs in diverse microscopic forms, including euhedral and semi-euhedral fine grains, fissure-filling aggregates, irregular blocky structures, framboidal clusters, and disseminated particles. Systematic relationships were observed between logging parameters and coal quality: moisture, ash content, and volatile matter exhibit an initial decrease, followed by an increase with rising apparent resistivity (LLD) and bulk density (DEN). Conversely, fixed carbon and calorific value display an inverse trend, peaking at intermediate LLD/DEN values before declining. Total sulfur increases with density up to a threshold before decreasing, while showing a concave upward relationship with resistivity. Negative correlations exist between moisture, fixed carbon, calorific value lateral resistivity (LLS), natural gamma (GR), short-spaced gamma-gamma (SSGG), and acoustic transit time (AC). In contrast, ash yield, volatile matter, and total sulfur correlate positively with these logging parameters. These trends are governed by coalification processes, lithotype composition, reservoir physical properties, and the types and mass fractions of minerals. Validation through independent two-sample t-tests confirms the feasibility of the neural network model for predicting coal quality parameters from geophysical logging data. The predictive model provides technical and theoretical support for advancing intelligent coal mining practices and optimizing efficiency in coal chemical industries, enabling real-time subsurface characterization to facilitate precision resource extraction. Full article

To investigate the failure mechanisms of roadway-surrounding rock in the wind oxidation zone, where the rock experiences instability under cyclic excavation-induced loading and unloading, this study conducted experiments leveraging acoustic emission analysis, scanning electron microscopy, and a digital image correlation (DIC) system. The research focused on grouting reinforcement under varying gradation indices, examining its mechanical properties, deformation characteristics, and microscopic structure post-failure. Results show that as the gradation index increases, the peak strength of the grouted solid exhibits a non-linear trend, initially decreasing to a minimum of 9.40 MPa (a 40.4% drop) before rising again to a maximum of 15.76 MPa. The hysteresis loop observed follows a pattern of ‘sparse–dense–sparse’. Additionally, the acoustic emission cumulative ringing count demonstrates a three-stage pattern of ‘rising–active–quiet’, with a similar initial decrease followed by an increase correlated with the gradation index. Using digital image correlation (DIC) technology, the study revealed the crack development characteristics of the grouting reinforcement. Higher gradation indices lead to wider localization zones, more extensive crack propagation, and greater damage. Microstructural analysis showed that PVA enhances the formation of hydration products, fostering stronger adhesion between these products and the cement matrix. This leads to a denser and more uniform microstructure, thereby enhancing the macroscopic strength of the samples. It provides a basis for practical mining engineering applications of grouting reinforcement of roadways in wind oxidation zones. Full article

Parallelepipeds specimens were made to further investigate the rockburst occurrence mechanism of ore pillars in underground mining units. The investigation was carried out with uniaxial compression systems and real-time testing systems, such as stress, video, and acoustic emission, combined with digital image correlation (DIC) and SEM electron microscope scanning technology, to systematically analyze the evolution of rockburst of ore pillars, strain field characteristics, acoustic emission characteristics, mesoscopic characteristics of the rockburst fracture, morphology of the bursting crater, and debris characteristics. The findings demonstrate that the pillar’s rockburst process went through four stages, including the calm period, the particle ejection period, the block spalling period, and the full collapse period. According to DIC digital image correlation technology, the development of cracks in the rock is not obvious during the calm period, but during the small particle ejection and block spalling periods, the microcracks started to form and expand more quickly and eventually reached the critical surface of the rock, resulting in the formation of a complete macro-rockburst rupture zone. During stage I of the test, the rate of acoustic emission events and energy was relatively low; from stages II to IV, the rate gradually increased; and in stage V, the rate of acoustic emission events and energy reached its maximum value at the precise moment the rock exploded, releasing all of its stored energy. The specimen pit section primarily exhibits shear damage and the fracture exhibits shear fracture morphology, while the ejecta body primarily exhibits tensile damage and the fracture exhibits tensile fracture morphology. The location of the explosion pit is distributed on the left and right sides of the middle pillar of the specimen, and the shape is a deep “V”. The majority of the rockburst debris is greater than 5 mm, and it mostly takes the shape of thin plates, which is comparable to the field rockburst debris’s shape features. Full article

In this work, we report for the first time the development and complex characterization of new bioceramics based on hydroxyapatite (HAp, Ca₁₀(PO₄)₆(OH)₂). On the other hand, the lyophilization process was used for the first time in this research. The samples were obtained by a modified coprecipitation method and were dried by lyophilization (lyophilized hydroxyapatite (HApLF) and lyophilized zinc-doped hydroxyapatite (5ZnHApLF)). Valuable information about the HApLF and 5ZnHApLF stability was obtained through nondestructive ultrasound measurements. The X-ray diffraction (XRD) studies revealed the phase and the effects of the incorporation of Zn ions into the HAp structure. The chemical composition of the samples was evaluated by energy dispersive X-ray analysis (EDS) and X-ray photoelectron spectroscopy (XPS). Information about the functional groups present in the HApLF and 5ZnHApLF was obtained using Fourier Transform Infrared Spectroscopy (FTIR) studies. The morphology of HApLF and 5ZnHApLF pellets was observed by scanning electron microscopy (SEM). The surface topography of HApLF and 5ZnHApLF pellets was studied with the aid of atomic force microscopy (AFM). Details regarding the roughness of the samples were also obtained using AFM topographies and SEM images. A complementary study was also carried out on a larger analysis surface using a Scanning Acoustic Microscope (SAM). The SAM was used for the first time to analyze the surface of HAp and 5ZnHAp pellets. The biological properties of the HApLF and 5ZnHApLF pellets was investigated with the aid of MG63 and human gingival fibroblasts (HGF-1) cell lines. The results of the cell viability assay highlighted that both the HApLF and 5ZnHApLF pellets exhibited good biological activity. Moreover, SEM and AFM studies were conducted in order to emphasize the development of MG63 and HGF-1 cells on the pellet’s surface. Both SEM and AFM images depicted that the pellets’ surface favored the cell attachment and development of MG63 and HGF-1 cells. Furthermore, the antimicrobial properties of the HApLF and 5ZnHApLF were evaluated against Escherichia coli ATCC 25922, Staphylococcus aureus ATCC 25923, and Candida albicans ATCC 10231. The results of the antimicrobial assays highlighted that the 5ZnHApLF exhibited a strong antimicrobial activity against the tested microbial strains. The results of the biological assays suggested that the samples show great potential for being used in the development of novel materials for biomedical applications. Full article

Modified basalt microfiber-reinforced polyurethane elastomer composites were prepared by a semi-prepolymer method with two different silane coupling agents (KH550 and KH560) in this study. Infrared spectroscopy was used to quantify the degree of microphase separation and analyze the formation of hydrogen bonding in polyurethane. The interfacial surface and the morphology of fibers and composites from tensile fracture were examined by a scanning electron microscope. Further measurements were performed on an electronic universal testing machine for characterizing the mechanical properties of composites. Moreover, the loss factor and transmission loss of composite materials were obtained from dynamic thermomechanical analysis and acoustic impedance tube, respectively. The suitable concentrations in the modification of basalt fibers were established at 1% for KH550 and 1.5% for KH560. The best overall performance was obtained in KH550-BMF/PUE group, as the properties increased by 31% in tensile strength, 37% in elongation at break, and 21% in acoustic insulation. Full article

This study investigates the flexural behavior of three sandwich panels composed of an agglomerated cork core and skins made up of cross-ply [0,90]₂ flax or glass layers with areal densities of 100 and 300 g/m². They are designated by SF100, SF300, and SG300, where S, F, and G stand for sandwich material, flax fiber, and glass fiber, respectively. The three sandwich materials were fabricated in a single step using vacuum infusion with the liquid thermoplastic resin Elium^®. Specimens of these sandwich materials were subjected to three-point bending tests at five span lengths (80, 100, 150, 200, and 250 mm). Each specimen was equipped with two piezoelectric sensors to record acoustic activity during the bending, facilitating the identification of the main damage mechanisms leading to flexural failure. The acoustic signals were analyzed to first track the initiation and propagation of damage and, second, to correlate these signals with the mechanical behavior of the sandwich materials. The obtained results indicate that SF300 exhibits 60% and 49% higher flexural and shear stiffness, respectively, than SG300. Moreover, a comparison of the specific mechanical properties reveals that SF300 offers the best compromise in terms of the flexural properties. Moreover, the acoustic emission (AE) analysis allowed the identification of the main damage mechanisms, including matrix cracking, fiber failure, fiber/matrix, and core/skin debonding, as well as their chronology during the flexural tests. Three-dimensional micro-tomography reconstructions and scanning electron microscope (SEM) observations were performed to confirm the identified damage mechanisms. Finally, a correlation between these observations and the AE signals is proposed to classify the damage mechanisms according to their corresponding amplitude ranges. Full article

Laser cladding has unique technical advantages, such as precise heat input control, excellent coating properties, and local selective cladding for complex shape parts, which is a vital branch of surface engineering. During the laser cladding process, the parts are subjected to extreme thermal gradients, leading to the formation of micro-defects such as cracks, pores, and segregation. These defects compromise the serviceability of the components. Ultrasonic vibration can produce thermal, mechanical, cavitation, and acoustic flow effects in the melt pool, which can comprehensively affect the formation and evolution for the microstructure of the melt pool and reduce the microscopic defects of the cladding layer. In this paper, the coupling model of temperature and flow field for the laser cladding of 45 steel 316L was established. The transient evolution laws of temperature and flow field under ultrasonic vibration were revealed from a macroscopic point of view. Based on the phase field method, a numerical model of dendrite growth during laser cladding solidification under ultrasonic vibration was established. The mechanism of the effect of ultrasonic vibration on the solidification dendrite growth during laser cladding was revealed on a mesoscopic scale. Based on the microstructure evolution model of the paste region in the scanning direction of the cladding pool, the effects of a static flow field and acoustic flow on dendrite growth were investigated. The results show that the melt flow changes the heat and mass transfer behaviors at the solidification interface, concurrently changing the dendrites’ growth morphology. The acoustic streaming effect increases the flow velocity of the melt pool, which increases the tilt angle of the dendrites to the flow-on side and promotes the growth of secondary dendrite arms on the flow-on side. It improves the solute distribution in the melt pool and reduces elemental segregation. Full article

Material development in acoustic engineering plays a significant role in various applications, such as industrial noise control. It is important and relevant to consider alternative materials capable of reducing noise levels in different frequency ranges. One commonly used material in engineering structures is epoxy adhesive compositions. Favoring the use of adhesive compositions are their main characteristics, including weight reduction in structures, corrosion resistance, relatively low manufacturing costs, and high mechanical strength. This paper aims to discuss the relationship between the mechanical properties of modified epoxy adhesives, their structure, and sound absorption efficiency. The subjects of this study were specimens of an epoxy composition in the cured state. Acoustic absorption coefficients were evaluated using a dual-microphone impedance tube, and tensile, compressive, and bending strength properties were determined using a testing machine. The impact strength of the compositions was also investigated. An analysis of the structure of the adhesives in the cured state was carried out using a scanning electron microscope. The test specimens were made from Epidian 5 epoxy resin cured with a polyamide PAC curing agent. Nanobent ZR2 aluminosilicate in an amount of 1%, CaCO₃ calcium carbonate in an amount of 5%, and CWZ-22 activated carbon in an amount of 20% were used as modifiers. The conducted studies revealed that the highest tensile strength was obtained for the adhesive composition with the addition of ZR2 filler. The highest compressive strength was exhibited by the adhesive composition with the addition of CWZ-22 filler. The highest flexural strength was demonstrated by the unmodified composition. For all the tested adhesive compositions, low sound absorption values were achieved, with a maximum of approximately 0.18. From the perspective of the reduction index R, it was observed that these samples performed better in reduction than in absorption. The best values were achieved in the compositions modified with CaCO₃. Full article

The low delamination tendency and high damage tolerance of three-dimensional (3D) braided composites highlight their significant potential in handling defects. To enhance the engineering potential of three-dimensional four-directional (3D4d) braided composites and assess the failure mode of hole defects, this study introduces a series of 3D4d braided composites with prefabricated holes, studying their compressive properties and failure mechanisms through experimental and finite element methods. Digital image correlation (DIC) was used to monitor the compressive strain on the surface of materials. Scanning acoustic microscope (SAM) and scanning electron microscopy (SEM) were used to characterize the longitudinal compression failure mode inside the material. A macroscopic model is established, and the porous materials are predicted by using the general braided composite material prediction theory. While reducing the forecast cost, the error is also controlled within 21%. The analysis of failure mechanisms elucidates the damage extension mode, and the porous damage tolerance ability aligns closely with the bearing mode of braided material structure. Different braiding angles will lead to different bearing modes of materials. Under longitudinal compression, the average strength loss of 15° specimens is 38.21%, and that of 30° specimens is 8.1%. The larger the braided angle, the stronger the porous damage tolerance. Different types of prefabricated holes will also affect their mechanical properties and damage tolerance. Full article

Pre-grouting is an effective method to reinforce fractured coal in front of working faces. The mining of adjacent working faces after grouting can cause early damage to the grouting cemented coal. To explore the mechanical properties of grouting cemented coal with different degrees of early damage, we designed and built a grouting equipment that was used on fractured coal to produce grouting cemented coal. In total, 0%, 20%, 40%, and 60% of the uniaxial compressive strength of complete coal were applied to the grouting cemented coal to produce early damage. The uniaxial compressive test, digital image correlation technology (DIC), acoustic emission (AE), and scan electron microscopy (SEM) were used to explore the changes in the mechanical properties of the grouting cemented coal with different early disturbance, and the surface and internal failure modes of the samples were investigated. The results show that with an increase in the early damage degree from 0% to 60%, the strength of the grouting cemented coal samples first increased and then decreased. Moreover, when the damage degree was 40%, the strength of the grouting cemented coal reached a maximum, which increased by 24.38% compared to that of the grouting cemented coal without damage. Under the low degree of damage, the samples exhibited tensile failure. As the damage degree increases, the samples’ failure mode changes to shear and mixed failure mode, and the breakdown speed increases. Internal crack propagation mostly occurred during the failure stage. As the damage degree increased, the failure stage increased, and the grouting cemented coal exhibited plastic characteristics. However, when the early damage degree increased to 60%, the samples exhibited typical brittle failure characteristics. The microstructure results show that the low degree of early damage for the samples is conducive to the infiltration of the slurry in coal, improving the grouting reinforcement effect. A large degree of early damage can lead to internal structural damage and strength degradation in grouting cemented coal. Full article

Shale is composed of a rock matrix and bedding planes with a layered structure, resulting in significant anisotropy in its mechanical properties. In order to study the anisotropic mechanical properties of shale, the shale samples were prepared in different orientations with respect to the bedding planes, and the composition and microstructure of shale were first analyzed by X-ray diffractometer (XRD) and scanning electron microscope (SEM), and then the uniaxial and triaxial compression experiment on shale samples with five different bedding angles (the angle between the loading direction and the normal direction of the bedding planes, 0°, 30°, 45°, 60°, and 90°) were conducted under five confining pressures (0, 10, 20, 30, and 40 MPa), respectively; meanwhile, the acoustic emission (AE) test was carried out in the uniaxial test. The results indicate that the mechanical properties and parameters of shale have obvious anisotropy, and the AE characteristics of shale samples with different bedding angles are significantly different during uniaxial loading. Furthermore, the compressive strength and elastic modulus of the shale samples first decrease and then increase with the increase in the bedding angle under different confining pressures. Moreover, according to the anisotropic grade of compressive strength, the shale has moderate anisotropy. In addition, the failure mode of the shale samples is also anisotropic, and varies with the bedding angle and confining pressure. Full article

The physical and mechanical properties of rocks change significantly after being subjected to high temperatures, which poses safety hazards to underground projects such as coal underground gasification. In order to investigate the effect of temperature on the macroscopic and microscopic properties of rocks, this paper has taken sandstone as the research object and conducted uniaxial compression tests on sandstone specimens at different temperatures (20–1000 °C) and different heating rates (5–30 °C/min). At the same time, the acoustic emission (AE) test system was used to observe the acoustic emission characteristics of the rock damage process, and the microstructural changes after high temperature were analyzed with the help of a scanning electron microscope (SEM). The test results show that the effect of temperature on sandstone is mainly divided into three stages: Stage I (20–500 °C) is the strengthening zone, the evaporation of water and the contraction of primary fissures, and sandstone densification is enhanced. In particular, the compressive strength and elastic modulus increase, the macroscopic damage mode is dominated by shear damage, and the fracture micromorphology is mainly brittle fracture. Stage II (500–600 °C) is the transition zone, 500 °C is the threshold temperature for the compressive strength and modulus of elasticity, and the damage mode changes from shear to cleavage damage, and the sandstone undergoes brittle–ductile transition in this temperature interval. Stage III is the physicochemical deterioration stage. The changes in the physical and chemical properties make the sandstone compressive strength and modulus of elasticity continue to decline, the macroscopic damage mode is mainly dominated by cleavage damage, and the fracture microscopic morphology is of a more toughness fracture. The effect of different heating rates on the mechanical properties of sandstone was further studied, and it was found that the mechanical properties of the rock further deteriorated under higher heating rates. Full article

The behavior of the EK-181 low-activation ferritic-martensitic reactor steel (Fe–12Cr–2W–V–Ta–B) in the states with different levels of strength and plastic properties after traditional heat treatment (THT) and after high-temperature thermomechanical treatment (HTMT) in the temperature range from −196 to 25 °C, including the range of its cold brittleness (ductile–brittle transition temperature, DBTT) is studied. The investigations are carried out using non-destructive acoustic methods (internal friction, elasticity) and transmission and scanning electron microscopy methods. It is found that the curves of temperature dependence of internal friction (the vibration decrement) of EK-181 steel after THT and HTMT are similar to those of its impact strength. Below the ductile–brittle transition temperature, it is characterized by a low level of dislocation internal friction. The temperature dependence curves of the steel elastic modulus increase monotonically with the decreasing temperature. In this case, the value of Young’s modulus is structure-sensitive. A modification of the microstructure of EK-181 steel as a result of HTMT causes its elastic modulus to increase, compared to that after THT, over the entire temperature range under study. The electron microscopic studies of the steel microstructure evolution near the fracture surface of the impact samples (in the region of dynamic crack propagation) in the temperature range from −196 to 100 °C reveal the traces of plastic deformation (increased dislocation density, fragmentation of the martensitic structure) at all of the temperatures under study, including those below the cold brittleness threshold of EK-181 steel. Full article