Search Results (63)

The proliferation of telecommunication devices in recent decades has resulted in a substantial increase in exposure risk to manmade radiofrequency electromagnetic fields (RF-EMFs) for both animals and plants. The physiological effects of these exposures remain to be fully elucidated. In this study, we measured and analyzed the chlorophyll fluorescence rise kinetics of lettuce plants in the presence of RF-EMFs and after a short drought treatment. The analysis of the fluorescence data was conducted using two different strategies: a conventional JIP test and a novel machine learning-assisted anomaly-detection approach. Our results suggest that exposure to RF-EMFs weakens the plant’s hormetic responses induced by drought treatment, both in terms of the response’s magnitude and its extent. These findings provide further evidence supporting the hypothesis that RF-EMFs interfere with plant stress responses. Full article

Two-dimensional (2D) materials have been proposed for use in a multitude of applications, with graphene being one of the most well-known 2D materials. Despite their potential to contribute to innovative solutions, the fabrication of such devices still faces significant challenges. One of the key challenges is the fabrication at a wafer-level scale, a fundamental step for allowing reliable and reproducible fabrication of a large volume of devices with predictable properties. Overcoming this barrier will allow further integration with sensors and actuators, as well as enabling the fabrication of complex circuits based on 2D materials. This work presents the fabrication steps for a process that allows the on-wafer fabrication of active and passive radiofrequency (RF) devices enabled by graphene. Two fabrication processes are presented. In the first one, graphene is transferred to a back gate surface using critical point drying to prevent cracks in the graphene. In the second process, graphene is transferred to a flat surface planarized by ion milling, with the gate being buried beneath the graphene. The fabrication employs a damascene-like process, ensuring a flat surface that preserves the graphene lattice. RF transistors, passive RF components, and antennas designed for backscatter applications are fabricated and measured, illustrating the versatility and potential of the proposed method for 2D material-based RF devices. The integration of graphene on devices is also demonstrated in an antenna. This aimed to demonstrate that graphene can also be used as a passive device. Through this device, it is possible to measure different backscatter responses according to the applied graphene gating voltage, demonstrating the possibility of wireless sensor development. With the proposed fabrication processes, a flat graphene with good quality is achieved, leading to the fabrication of RF active devices (graphene transistors) with intrinsic f_T and f_max of 14 GHz and 80 GHz, respectively. Excellent yield and reproducibility are achieved through these methods. Furthermore, since the graphene membranes are grown by Chemical Vapor Deposition (CVD), it is expected that this process can also be applied to other 2D materials. Full article

Aflatoxins are toxic organic substances that are synthesized on the surfaces of seeds, nuts, and similar products by some fungi under elevated humidity. They decompose at temperatures well above 130 °C, so standard heating or autoclaving is an obsolete technique for the degradation of toxins on surfaces without significant modification of the treated material. Non-equilibrium plasma was used to degrade aflatoxins at low temperatures and determine the efficiency of O atoms. A commercial mixture of aflatoxins was deposited on smooth substrates, and the solvent was evaporated so that about a 3 nm thick film of dry toxins remained on the substrates. The samples were exposed to low-pressure oxygen plasma sustained by an inductively coupled radiofrequency (RF) discharge in either the E or H mode. The gas pressure was 20 Pa, the forward RF power was between 50 and 700 W, and the O-atom flux was between 1.2 × 10²³ and 1.5 × 10²⁴ m⁻² s⁻¹. Plasma treatment caused the rapid degradation of aflatoxins, whose concentration was deduced from the fluorescence signal at 455 nm upon excitation with a monochromatic source at 365 nm. The degradation was faster at higher discharge powers, but the degradation curves fitted well when plotted against the dose of O atoms. The experiments showed that the aflatoxin concentration dropped below the detection limit of the fluorescence probe after receiving the O-atom dose of just above 10²⁵ m⁻². This dose was achieved within 10 s of treatment in plasma in the H mode, and approximately a minute when plasma was in the E mode. The method provides a low-temperature solution for the efficient detoxification of agricultural products. Full article

American ginseng (Panax quinquefolium L.) residue from the extraction industry can be dried and mixed with rice bran as media for black truffle solid-state fermentation to enhance reuse and bioactive functions. Different ratios of rice bran (R) and American ginseng residue (G) mixtures were used as solid-state media for 5 weeks of black truffle fermentation, and then their bio-component contents and whitening effects were analyzed. Finally, four drying methods—hot air drying (HA), microwave drying (MW), hot air-assisted radio frequency (HARF) drying, and radio frequency vacuum (RFV) drying—were assessed to optimize drying efficiency for fermented medium. The results showed that using a 3:1 ratio of rice bran and American ginseng residue as the medium increased the crude polysaccharide and flavonoid contents by approximately threefold and enhanced the ginsenoside Rg3 content about twelvefold. Additionally, the 100 µg/mL ethanol extract of the fermented product inhibited 70% of tyrosinase activity and reduced the melanin area on zebrafish embryos by 42.74%. In the drying study, RFV drying R2G1 required only 13 min without exceeding 70 °C, demonstrating superior drying efficiency, temperature control, and low energy consumption. Overall, this study demonstrates the potential of black truffle fermentation of solid-state media from rice bran and American ginseng residue mixtures for whitening applications and highlights RFV drying as an efficient method for by-products. Full article

Drying is a key method for food preservation; however, conventional techniques often lead to the degradation of bioactive compounds, compromising nutritional quality. This systematic review, following the PRISMA protocol, examines emerging food drying technologies designed to enhance process efficiency while preserving nutritional and functional properties. A bibliometric analysis was conducted to identify research trends from 2014 to 2024. Searches were performed in the Scopus and Web of Science databases accessed on 17 January 2025, including only original research articles published in English focusing on food drying applications. Reviews, editorials, and studies unrelated to the food sector were excluded. Due to the technological nature of the outcomes, a formal risk of bias assessment was not applicable. This review highlights several emerging drying technologies, such as microwave, radiofrequency, infrared, ultrasound, freeze-drying, and cold plasma. The qualitative synthesis indicates these technologies improve the retention of phenolics, flavonoids, and vitamins, thus enhancing nutritional stability. Nevertheless, challenges remain in industrial-scale implementation, particularly regarding the economic feasibility and optimization of operational parameters. This review received no funding and was not registered in any public database. The findings underscore the need for continued research to develop sustainable and functional dried food products that meet current market demands and consumer expectations. Full article

Sputtering onto liquids is rapidly gaining attention for the green and controlled dry synthesis of ultrapure catalysts nanomaterials. In this study, we present a clean and single-step method for the synthesis of gold nanoparticles directly in polyethylene glycol (PEG) liquid using radio frequency (RF) magnetron sputtering and by subsequently transferring them to Nafion ionomer, fabricating a catalyst-coated membrane (CCM), an essential component of the proton exchange membrane water electrolyzer (PEMWE). The samples were systematically characterized at different stages of process development. The innovative transfer process resulted in a monodispersed homogeneous distribution of catalyst particles inside CCM while retaining their nascent nanoscale topography. The chemical analysis confirmed the complete removal of the trapped PEG through the process optimization. The electrochemical catalytic activity of the optimized CCM was verified, and the hydrogen evolution reaction (HER) in acidic media appeared outstanding, a vital step in water electrolysis toward H₂ production. Therefore, this first study highlights the advantages of RF sputtering in liquid for nanoparticle synthesis and its direct application in preparing CCM, paving the way for the development of innovative membrane preparation techniques for water electrolysis. Full article

Inspired by the ventral scale structure of the oriental sand boa, this study successfully fabricated multiscale bioinspired alumina (Al₂O₃) ceramics by combining the excellent mechanical properties, high-temperature resistance, and high hardness of ceramic composites with direct ink writing (DIW) 3D printing technology and femtosecond laser processing. A MoS₂ thin film was then deposited on the ceramic surface via radio frequency magnetron sputtering (PVD) to systematically investigate the impact of bioinspired structures on the tribological properties of ceramic composites under both dry and lubricated conditions. Experimental results demonstrated that bioinspired structures at different scales exhibited significant friction-reducing and wear-resistant characteristics compared to blank structures. Specifically, under room-temperature conditions, the friction coefficients of bioinspired ceramic composites with solid lubricants and oil lubrication were 0.3 and 0.148, respectively, indicating excellent tribological performance. These findings confirm the synergistic lubrication effect between bioinspired structures, two-dimensional solid lubricants, and lubricating oil, which significantly enhanced the friction-reducing and wear-resistant properties of ceramic components. Therefore, the synergistic design of multiscale bioinspired structures and solid lubricants provides an innovative strategy for the advanced application of ceramic components. Full article

Inductively coupled plasma–reactive etching (ICP-RIE) of InGaZnO (IGZO) thin films was studied with variations in gas mixtures of hydrochloride (HCl) and argon (Ar). The dry etching characteristics of the IGZO films were investigated according to radiofrequency bias power, gas mixing ratio, and chamber pressure. The IGZO film showed an excellent etch rate of 83.2 nm/min from an optimized etching condition such as a plasma power of 100 W, process pressure of 3 mTorr, and HCl ratio of 75% (HCl:Ar at 30 sccm:10 sccm). In addition, this ICP-RIE etching condition with a high HCl composition ratio at a moderate RIE power of 100 W showed a low etched pattern skew and low photoresist damage on the IGZO patterns. It also provided excellent surface morphology of the SiO₂ film underneath after the entire dry etching of the IGZO layer. The IGZO thin film as an active layer was successfully patterned under the ICP-RIE dry etching under the HCl-Ar gas mixture, affording an excellent electrical characteristic in the resultant top-gate IGZO thin-film transistor. Full article

To enhance the physicochemical quality, drying efficiency, and nutrient retention of dried Licorice products, this study investigated the effects of ultrasonic pretreatment on the radio frequency vacuum (RFV) drying characteristics, microstructure, and retention of natural active substances in Licorice slices. The ultrasonic time, power, and frequency were considered as experimental factors. The results showed that, compared with conventional RFV drying, ultrasonic pretreatment reduced the drying time of Licorice slices by 20–60 min. The Weibull model accurately described the moisture ratio changes under different pretreatment conditions (R² > 0.9984, χ² < 2.381 × 10⁻⁵). The optimal retention of polysaccharides, total phenols, total flavonoids, and antioxidants was achieved under pretreatment conditions of 30 min of ultrasonic time, 180 W of ultrasonic power, and 40 kHz of ultrasonic frequency. Furthermore, ultrasonic pretreatment preserved the internal cellular structure of Licorice slices, maintaining intact tissue cells and well-defined microchannels. However, a slight reduction in sample color was observed following ultrasound application. In conclusion, ultrasonic pretreatment significantly improved the RFV drying process for Licorice slices by enhancing drying efficiency, preserving active ingredients, and optimizing the physicochemical quality of the dried product. This study provides novel insights and methods for optimizing the drying process of Licorice, offering a foundation for further research and industrial applications. Full article

Rice is a water-intensive crop, conventionally grown under submerged conditions, with standing water for about 80% of its growth period. There is an urgent need for water-saving technologies to address challenges associated with conventional irrigation techniques for rice. The alternate wetting and drying (AWD) technique is one of these water-saving techniques; however, it requires continuous monitoring of water levels in the field. The implementation of real-time, electronic sensor-based precision irrigation technology may address the problems associated with conventional irrigation systems and AWD leading to high water use efficiency. Therefore, a study was undertaken to develop a suitable sensor-based automated irrigation system to maintain optimal water levels in rice fields. This study conceptualized an electronic sensor-based automated irrigation system for rice cultivated under the AWD technique. In this method, the rice field is initially flooded to a maximum depth of 5 cm. Irrigation is reapplied once the water level reduces to 10 cm below the soil surface. This developed system helps address water scarcity by regulating water levels, preventing excess ponding. It uses magnetic float-based sensors and electronic circuits to detect water levels, converting them into electronic signals transmitted wirelessly via radio frequency (RF) to a controller. The controller has been programmed for different growth stages that need to be set manually during the cropping period. The system is designed primarily for the AWD method but includes an option for continuous ponding (CP), needed during the flowering stage. The maximum water level at full maturity is set at 5 cm above the soil surface, while irrigation with the AWD method begins when the water level falls 10 cm below the soil surface. The developed system was tested during the Kharif season of 2018–19; the irrigation water productivity was 6.15 kg ha⁻¹mm⁻¹ with the automated system, compared to 3.06 kg ha⁻¹mm⁻¹ in the control (continuous ponding). Total water productivity was 4.80 kg ha⁻¹mm⁻¹ for the automated system and 2.63 kg ha⁻¹mm⁻¹ for the control. The automated system achieved 36% more water savings over the control, which used continuous ponding as farmers practice. The developed system supports AWD, a proven water-saving technique in rice cultivation. Full article

This study aimed to formulate a black bean soy sauce using black beans and black rice as media for the solid-state fermentation of white truffle. Various proportions of these media (4:0, 3:1, 2:2, 1:3, and 0:4) were prepared, with methionine concentrations (0, 0.3, 0.6, 0.9, 1.2, and 1.5%) serving as precursors for a 4-week solid-state fermentation to analyze the aroma profiles. GC-MS analysis showed that samples with 1.5% methionine exhibited significantly higher levels of sulfur-containing volatile compounds compared to those without methionine. GC-IMS analysis revealed that a 2:2 ratio of black beans to black rice produced the most enriched aroma. Lower methionine levels improved mycelial growth, with 0.3% methionine yielding the richest aroma components. After fermentation, the white truffle products were sterilized using autoclaving, hot air assisted radio frequency (HARF), and high pressure processing (HPP), followed by freeze drying. GC-IMS analysis showed that HPP samples had an aroma closest to fresh samples, whereas HARF and autoclave resulted in similar aromas. However, 24 h freeze drying significantly diminished the aroma, resulting in no significant difference in aroma among the freeze-dried products treated with different sterilization methods. Full article

In this study, the radio frequency vacuum drying (RFVD) technique was used to dry Codonopsis pilosula slices. The effects of the drying temperature, slice thickness, plate spacing, and vacuum degree on the drying characteristics and physicochemical properties of the slices were investigated. The results showed that as the drying temperature and vacuum degree increased and the slice thickness and plate distance decreased, the drying rate and effective moisture diffusion coefficient of the Codonopsis pilosula slices improved, and the required drying time was shortened by 11.11% to 29.41% compared to that after hot air drying (HAD). Through comparison, it was found that the Midilli and Weibull models could better describe the moisture variation trend during the RFVD of Codonopsis pilosula. After RFVD, the retention of lobetyolin and syringin in Codonopsis pilosula significantly increased, with maximum contents of 135.74 mg/100 g and 19.16 mg/100 g respectively, which were 75.2% and 124.28% higher than those obtained by HAD. The contents of polysaccharides, total phenolics, and total flavonoids and antioxidant performance were also enhanced. The color, shrinkage rate, and internal tissue structure were significantly improved. In conclusion, RFVD not only increases the drying speed of Codonopsis pilosula slices but also ensures the good quality of the dried products. Full article

To fully leverage the advantages of both hot air drying and radio frequency vacuum drying, a segmented combination drying technique was applied to post-harvest Cistanche. This new drying method involves using hot air drying in the initial stage to remove the majority of free water, followed by radio frequency vacuum drying in the later stage to remove the remaining small amount of free water and bound water. During the radio frequency vacuum drying (RFV) phase, the effects of temperature (45, 55, and 65 °C), vacuum pressure (0.020, 0.030, and 0.040 MPa), plate spacing (65, 75, and 85 mm), and slice thickness (4, 5, and 6 mm) on the drying characteristics, quality, and microstructure of Cistanche slices were investigated. Additionally, infrared thermal imaging technology was used to examine the surface temperature distribution of the material during the drying process. The results showed that compared to radio frequency vacuum drying alone, the hot air–radio frequency combined drying significantly shortened the drying time. Under conditions of lower vacuum pressure (0.020 MPa), plate spacing (65 mm), and higher temperature (65 °C), the drying time was reduced and the drying rate increased. Infrared thermal imaging revealed that in the early stages of hot air–radio frequency vacuum combined drying, the center temperature of Cistanche was higher than the edge temperature. As drying progressed, the internal moisture of the material diffused from the inside out, resulting in higher edge temperatures compared to the center and the formation of overheating zones. Compared to natural air drying, the hot air–radio frequency vacuum combined drying effectively preserved the content of active components such as polysaccharides (275.56 mg/g), total phenols (38.62 mg/g), total flavonoids (70.35 mg/g), phenylethanoid glycosides, and iridoids. Scanning electron microscopy observed that this combined drying method reduced surface collapse and cracking of the material. This study provides theoretical references for future drying processes of Cistanche. Full article

This study aims to maximize the post-harvest quality of Moutan Cortex and reduce energy consumption. Radio frequency vacuum (RFV) technology was used to dehydrate Moutan Cortex in this study to investigate the effects of different drying temperatures, plate spacing, and vacuum degree on the drying kinetics, physicochemical quality, and microstructure of Moutan Cortex. The results showed that RFV drying shortened the dehydration time of the Moutan Cortex by 10.71–28.57% and increased the drying rate by 15.79–54.39% compared to hot-air drying. The best color (∆E = 6.08 ± 0.28, BI = 26.97 ± 0.98) and relatively high retention of polysaccharides, total phenolics, total flavonoids, antioxidant properties, paeonol, gallic acid, paeoniflorin, and benzoylpaeoniflorin contents were observed in the dried products of Moutan Cortex at a drying temperature of 50 °C, spacing of 90 mm, and vacuum of 0.025 MPa. Analyzing the microstructure, it was found that RFV drying could effectively inhibit the shrinkage and collapse of the cellular structure, and a regular and loose honeycomb pore structure appeared inside the samples, which contributed to the rapid migration of the internal moisture. This study can provide a theoretical reference basis for the selection and application of industrialized processing methods of high-quality Moutan Cortex. Full article

In this paper, an Improved Pelican Optimization Algorithm (IPOA) was proposed to optimize a BP neural network model to predict the dielectric loss factor of wood in the RF heating and drying process. The neural network model was trained and optimized using MATLAB 2022b software, and the prediction results of the BP neural network with POA-BP and IPOA-BP models were compared. The results show that the IPOA-optimized BP neural network model is more accurate than the traditional BP neural network model. After the BP neural network model with IPOA optimization was used to predict the dielectric loss factor of wood, the value increased by 4.3%, the MAE decreased by 68%, and the RMSE decreased by 67%. The results provided by the study using the IPOA-BP model show that the prediction of the dielectric loss factor of wood under different macroscopic conditions in radio frequency heating and drying of wood can be realized without the need for highly costly and prolonged experimental studies. Full article