Search Results (34)

Additive manufacturing is currently regarded as one of the enabling technologies for Space Economy since it allows for the reduction of lead time and costs of payloads and platforms. Typically, metal-based additive manufacturing technologies are considered for the development of microwave components for Space applications since they exhibit the best trade-off in radio-frequency performance, benefits, and withstanding adverse environmental conditions. In this view, composite polymers may further increase the benefits arising from the 3D printing of microwave components since lighter parts with the required thermal, mechanical, and RF performances can be placed on board satellites. This paper explores the feasibility of 3D-printed composite polymers, including Ultem and PEEK reinforced with carbon fiber, for the development of microwave waveguide devices intended for Space applications. To this end, three different manufacturing routes were investigated by selecting a specific composite polymer, the corresponding manufacturing system and post-processing, and the necessary metal-plating technique. Hence, relevant radio-frequency test vehicles operating at 10 ÷ 14 GHz were designed, manufactured, and tested. The experimental results prove that waveguide components operating in X and Ku bands can be developed through the material extrusion of PEEK reinforced with carbon fiber, which is subsequently metalized by means of a two-stage electroless/electroplating process. Full article

In this paper, the performance, advantages and challenges of polymer microwave fibers (PMF) for sub-THz links are evaluated first. Then, a simple and elegant transceiver-integrated circuit (IC) and PMF wireless coupling scheme is presented. The proposed solution utilizes an advanced IC packaging technology to implement a Vivaldi antenna-in-package (AiP). The antenna is designed to provide lateral radiation and excellent directivity, so the proposed solution is very simple, compact, robust and cost-efficient: the IC readily connects to the PMF and the coupling is merely achieved by the packaged IC, without the need for any extra interface. The system operates at around 140 GHz, achieving a coupling loss of just 3.5 dB. Full article

Disposing of carbon fiber-reinforced polymers (CFRPs) has become a pressing issue due to their increasing application across various industries. Previous work has focused on removing silane coupling agent residues on recovered carbon fibers via microwave pyrolysis, making them suitable for use in new materials. However, the mechanical performance and structural characteristics of these fibers have not been fully reported. This study investigates the time–temperature curves of CFRPs treated through microwave pyrolysis and analyzes the mechanical and structural properties of silane-controllable recovered carbon fibers. Additionally, emissions—including carbon monoxide, carbon dioxide, and particulate aerosols—were measured using handheld monitors and thermal desorption–gas chromatography/mass spectrometry to determine the composition of fugitive gases around the microwave pyrolysis system. The pyrolysis process at 950 °C, with an additional 1 h holding time, reduced the crystallite size from 0.297 Å to 0.222 Å, significantly enhancing tensile strength (3804 ± 713 MPa) and tensile modulus (200 ± 13 GPa). This study contributes to more sustainable CFRP waste treatment and highlights the potential for reusing high-quality carbon fibers in new applications, enhancing both environmental and worker safety. Full article

Microwave curing can be an alternative curing method for geopolymer production. Although many properties of microwave-cured geopolymer composites have been investigated, the effect of microwave curing on the strength and durability properties of fiber-reinforced geopolymers remains a topic that requires investigation. In this study, the effect of fiber type and length on the properties of microwave-cured metakaolin-based geopolymers was investigated. For this purpose, PVA (6, 12 mm) and polymer (15, 30 mm) fibers were utilized. Compressive and flexural strength, fracture energy, abrasion resistance, high-temperature resistance, water absorption capacity and rate of capillary water absorption tests were conducted and the microstructure was examined using scanning electron microscopy. For curing, a household microwave oven was used at a power level of 300 watts. With the fibers’ inclusion, fracture energies could be increased by up to 1150%, ductility was enhanced, flexural strengths were increased and compressive strengths decreased. Moreover, the rate of capillary water absorption decreased by up to 13%, while water absorption values increased by between 5% and 12%. The results suggested that microwave curing could be an alternative curing method for the production of fiber-reinforced geopolymer composites, offering shorter curing times and lower energy consumption. Full article

This article introduces an eco-friendly method for the reclamation of carbon fiber-reinforced polymers (CFRP). The research project involved numerous experiments using microwave-assisted pyrolysis (MAP) to explore a range of factors, such as the inert gas flow, the power level, the On/Off frequency of rotation, and the reaction duration. To design the experiments, the three-level Box–Behnken optimization tool was employed. To determine the individual and combined effects of the input parameters on the thermal decomposition of the resin, the data were analyzed using least-squares variance adjustment. The results demonstrate that the models developed in this study were successful in predicting the direct parameters of influence in the microwave-assisted decomposition of CFRPs. An optimal set of operating conditions was found to be the maximum nitrogen flow (2.9 L/min) and the maximum operating experimental power (914 W). In addition, it was observed that the reactor vessel’s On/Off rotation frequency and that increasing the reaction time beyond 6 min had no significant influence on the resin elimination percentage when compared to the two other parameters, i.e., power and carrier gas flow rate. Consequently, the above-mentioned conditions resulted in a maximum resin elimination percentage of 79.6%. Following successful MAP, various post-pyrolysis treatments were employed. These included mechanical abrasion using quartz sand, chemical dissolution, thermal oxidative treatment using a microwave (MW) applicator and thermal oxidative treatment in a conventional furnace. Among these post-treatment techniques, thermal oxidation and chemical dissolution were found to be the most efficient methods, eliminating 100% of the carbon black content on the surface of the recovered carbon fibers. Finally, SEM evaluations and XPS analysis were conducted to compare the surface morphology and elementary constitution of the recovered carbon fibers with virgin carbon fibers. Full article

This study presents the utilization of the microwave infrared thermography (MIRT) technique to identify and analyze the defects in the carbon-fiber-reinforced polymer (CFRP) composite reinforcement of concrete specimens. At first, a set of numerical models was created, comprising the broadband pyramidal horn antenna and the analyzed specimen. The utilization of the system operating at a power of 1000 W in a continuous mode, operating at frequency of 2.45 GHz, was analyzed. The specimen under examination comprised a compact concrete slab that was covered with an adhesive layer and, thereafter, topped with a layer of CFRP. An air gap represented a defect at the interface between the concrete and the CFRP within the adhesive layer. In the modeling stage, the study investigated three separate scenarios—a sample with no defects, a sample with a defect located at the center, and a sample with a numerous additional random defects located at the rim of the CFRP matte—to analyze the effect of the natural reinforcement degradation in this area. The next phase of the study involved conducting experiments to confirm the results obtained from numerical modeling. In the experiments, the concrete sample aged for 10 years with the defect in the center and naturally developed defects at the CFRP rim was used. The study employed numerical modeling to explore the phenomenon of microwave heating in complex structures. The aim was to assess the chosen antenna design and identify the most effective experimental setup. These conclusions were subsequently confirmed through experimentation. The observations made during the heating process were particularly remarkable since they deviated from earlier studies that solely conducted measurements of the sample post-heating phase. The findings demonstrate that MIRT has the capacity to be employed as a technique for detecting flaws in concrete structures reinforced with CFRP. Full article

Polyvinylpyrrolidone (PVP) is a synthetic polymer that holds significance in various fields such as biomedical, medical, and electronics, due to its biocompatibility and exceptional dielectric properties. Electrospinning is the most commonly used tool to fabricate fibers because of its convenience and the wide choice of parameter optimization. Various parameters, including solution molarity, flow rate, voltage, needle gauge, and needle-to-collector distance, can be optimized to obtain the desired morphology of the fibers. Although PVP is commercially available in various molecular weights, PVP with a molecular weight of 130,000 g/mol is generally considered to be the easiest PVP to fabricate fibers with minimal challenges. However, the fiber diameter in this case is usually in the micron regime, which limits the utilization of PVP fibers in fields that require fiber diameters in the nano regime. Generally, PVP with a lower molecular weight, such as 10,000 g/mol and 55,000 g/mol, is known to present challenges in fiber preparation. In the current study, parameter optimization for PVP possessing molecular weights of 10,000 g/mol and 55,000 g/mol was carried out to obtain nanofibers. The electrospinning technique was utilized for fiber fabrication by optimizing the above-mentioned parameters. SEM analysis was performed to analyze the fiber morphology, and quantitative analysis was performed to correlate the effect of parameters on the fiber morphology. This research study will lead to various applications, such as drug encapsulation for sustained drug release and nanoparticles/nanotubes encapsulation for microwave absorption applications. Full article

The considerable expenses associated with carbon fiber (CF) production have imposed limitations on its widespread application across diverse industries, primarily due to the costs of precursor materials and energy−intensive post−treatment procedures. This research explores the potential utilization of Alberta oilsands asphaltenes (AOAs), a carbon−rich by−product derived from oilsands extraction, as a more cost−effective precursor for CF production. Polystyrene and poly(styrene–butadiene–styrene) were also used as polymer additives. In addition to conventional thermal post−treatment, microwave plasma was employed for the carbonization process. The CFs generated through this approach were subjected to a comprehensive analysis involving SEM, FTIR, TGA, XRD, and Raman spectroscopy. The best tensile strength and Young’s modulus of the AOA carbon fibers when using conventional thermal post−treatment were 600 MPa and 70 GPa, respectively. The microwave plasma process indicates the higher temperature and promise of eliminating heteroatoms of AOA carbon fibers. The temperature for microwave plasma modelling was set using COMSOL^TM, with the modelling temperature and detection temperature being established at 1600 K and 1568 K, respectively. Full article

A new method for the synthesis and deposition of tungsten oxide nanopowders directly on the surface of a carbon-fiber-reinforced polymer composite (CFRP) is presented. The CFRP was chosen because this material has very good thermal and mechanical properties and chemical resistance. Also, CFRPs have low melting points and are transparent under ionized radiation. The synthesis is based on the direct interaction between high-power-density microwaves and metallic wires to generate a high-temperature plasma in an oxygen-containing atmosphere, which afterward condenses as metallic oxide nanoparticles on the CFRP. During microwave discharge, the value of the electronic temperature of the plasma, estimated from Boltzmann plots, reached up to 4 eV, and tungsten oxide crystals with a size between 5 nm and 100 nm were obtained. Transmission electron microscopy (TEM) analysis of the tungsten oxide nanoparticles showed they were single crystals without any extended defects. Scanning electron microscopy (SEM) analysis showed that the surface of the CFRP sample does not degrade during microwave plasma deposition. The X-ray attenuation of CFRP samples covered with tungsten oxide nanopowder layers of 2 µm and 21 µm thickness was measured. The X-ray attenuation analysis indicated that the thin film with 2 µm thickness attenuated 10% of the photon flux with 20 to 29 KeV of energy, while the sample with 21 µm thickness attenuated 60% of the photon flux. Full article

Polymer matrix wave transparent composites are used in a variety of high-speed communication applications. One of the applications of these involves making protective enclosures for antennas of microwave towers, air vehicles, weather radars, and underwater communication devices. Material performance, structural, thermal, and mechanical degradation are matters of concern as advanced wireless communication needs robust materials for radomes that can withstand mechanical and thermal stresses. These polymer composite radomes are installed externally on antennas and are exposed directly to ambient as well as severe conditions. In this research, epoxy resin was reinforced with a small amount of quartz fibers to yield an improved composite radome material compared to a pure epoxy composite with better thermal and mechanical properties. FTIR spectra, SEM morphology, dielectric constant (Ɛ_r) and dielectric loss (δ), thermal degradation (weight loss), and mechanical properties were determined. Compared to pure epoxy, the lowest values of Ɛ_r and δ were 3.26 and 0.021 with 30 wt.% quartz fibers in the composite, while 40% less weight loss was observed which shows its better thermal stability. The mechanical characteristics encompassing tensile and bending strength were improved by 42.8% and 48.3%. In high-speed communication applications, compared to a pure epoxy composite, adding only a small quantity of quartz fiber can improve the composite material’s dielectric performance, durability, and thermal and mechanical strength. Full article

Glass fiber-reinforced polymer (GFRP) is widely used in engineering fields involving aerospace, energy, transportation, etc. If internal buried defects occur due to hostile environments during fabrication and practical service, the structural integrity and safety of GFRP structures would be severely undermined. Therefore, it is indispensable to carry out effective quantitative nondestructive testing (NDT) of internal defects buried within GFRP structures. Along with the development of composite materials, microwave NDT is promising in non-intrusive inspection of defects in GFRPs. In this paper, quantitative screening of the subsurface impact damage and air void in a unidirectional GFRP via microwave reflectometry was intensively investigated. The influence of the microwave polarization direction with respect to the GFRP fiber direction on the reflection coefficient was investigated by using the equivalent relative permittivity calculated with theoretical analysis. Following this, a microwave NDT system was built up for further investigation regarding the imaging and quantitative evaluation of buried defects in GFRPs. A direct-wave suppression method based on singular-value decomposition was proposed to obtain high-quality defect images. The defect in-plane area was subsequently assessed via a proposed defect-edge identification method. The simulation and experimental results revealed that (1) the testing sensitivity to buried defects was the highest when the electric-field polarization direction is parallel to the GFRP fiber direction; and (2) the averaged evaluation accuracy regarding the in-plane area of the buried defect reached approximately 90% by applying the microwave reflectometry together with the proposed processing methods. Full article

This research paper presents the application of the microwave infrared thermography (MIRT) technique for the purpose of detecting and characterizing defects in the carbon-fiber-reinforced polymer (CFRP) composite reinforcement of concrete specimens. Initially, a numerical model was constructed, which consisted of a broadband pyramidal horn antenna and the specimen. The present study investigated the application of a 360 W power system that operated at a frequency of 2.4 GHz, specifically focusing on two different operational modes: continuous and modulated. The specimen being examined consisted of a solid concrete slab that was coated with an adhesive layer, which was then overlaid with a layer of CFRP. Within the adhesive layer, at the interface between the concrete and CFRP, there was a defect in the form of an air gap. The study examined three distinct scenarios: a sample without any defects, a sample with a defect positioned at the center, and a sample with a defect positioned outside the center. The subsequent stage of the investigation incorporated experimental verification of the numerical modeling results. The experiment involved the utilization of two concrete specimens reinforced using CFRP, one without any defects and the other with a defect. Numerical modeling was used in this study to analyze the phenomenon of microwave heating in complex structures. The objective was to evaluate the selected antenna geometry and determine the optimal experimental configuration. Subsequently, these findings were experimentally validated. The observations conducted during the heating phase were particularly noteworthy, as they differed from previous studies that only performed observation of the sample after the heating phase. The results show that MIRT has the potential to be utilized as a method for identifying defects in concrete structures that are reinforced with CFRP. Full article

Glass Fiber reinforced polymers (GFRPs) are widely used and play an important role in modern society. The multilayer structure of GFRPs can lead to delamination defects during production and service, which can have a significant impact on the integrity and safety of the equipment. Therefore, it is important to monitor these delamination defects during equipment service in order to evaluate their effects on equipment performance and lifespan. Microwave imaging testing, with its high sensitivity and noncontact nature, shows promise as a potential method for detecting delamination defects in GFRPs. However, there is currently limited research on the quantitative characterization of defect images in this field. In order to achieve visual quantitative nondestructive testing (NDT), we propose a 2D-imaging visualization and quantitative characterization method for delamination defects in GFRP, and realize the combination of visual detection and quantitative detection. We built a microwave testing experimental system to verify the effectiveness of the proposed method. The results of the experiment indicate the effectiveness and innovation of the method, which can effectively detect all delamination defects of 0.5 mm thickness inside GFRP with high accuracy, the signal-to-background ratio (SBR) of 2D imaging can reach 4.41 dB, the quantitative error of position is within 0.5 mm, and the relative error of area is within 11%. Full article

This review article covers all types of paper-based humidity sensor, such as capacitive, resistive, impedance, fiber-optic, mass-sensitive, microwave, and RFID (radio-frequency identification) humidity sensors. The parameters of these sensors and the materials involved in their research and development, such as carbon nanotubes, graphene, semiconductors, and polymers, are comprehensively detailed, with a special focus on the advantages/disadvantages from an application perspective. Numerous technological/design approaches to the optimization of the performances of the sensors are considered, along with some non-conventional approaches. The review ends with a detailed analysis of the current problems encountered in the development of paper-based humidity sensors, supported by some solutions. Full article

As a means of introducing environmental responsibility to industrial applications, the usage of biobased composite materials has been encouraged in recent years. Polymer nanocomposites utilize polyolefins increasingly as a matrix, owing to the diversity in their features and prospective applications, even though typical polyester blend materials, such as glass and composite materials, have garnered greater attention from researchers. The mineral hydroxy-apatite, or Ca₁₀(PO₄)₆(OH)₂, is the primary structural component of bone and tooth enamel. Increased bone density and strength result from this procedure. As a result, nanohms are fabricated from eggshells into rods with very tiny particle sizes. Although there have been many papers written on the benefits of HA-loaded polyolefins, the reinforcing effect of HA at low loadings has not yet been taken into account. The purpose of this work was to examine the mechanical and thermal characteristics of polyolefin-HA nanocomposites. These nanocomposites were built out of HDPE and LDPE (LDPE). As an extension of this work, we investigated what would happen when HA is added to LDPE composites at concentrations as high as 40% by weight. Carbonaceous fillers, including graphene, carbon nanotubes, carbon fibers, and exfoliated graphite, all play significant roles in nanotechnology owing to the extraordinary enhancements in their thermal, electrical, mechanical, and chemical properties. The purpose of this study was to examine the effects of adding a layered filler, such as exfoliated graphite (EG), to microwave zones that might have real-world applications for their mechanical, thermal, and electrical characteristics. Mechanical and thermal properties were significantly enhanced by the incorporation of HA, notwithstanding a minor decrease in these attributes at a loading of 40% HA by weight. A higher load-bearing capability of LLDPE matrices suggests their potential usage in biological contexts. Full article