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21 pages, 30112 KB  
Article
Geological Control Factors and Accumulation Patterns of Harmful Gas in Tunnels in Northwest Hunan, China, and the Sustainable Development of Tunnel Engineering
by Bochuan Geng, Peidong Su, Xiao Quan, Xinhua Tao and Xinghao Lu
Appl. Sci. 2026, 16(14), 7155; https://doi.org/10.3390/app16147155 - 16 Jul 2026
Viewed by 127
Abstract
This research addresses the critical safety issue of harmful gas influx during tunnel excavation through unconventional gas-bearing structures. It focuses on six tunnels affected by shale gas influx along the Zhangnan Expressway of northwestern Hunan, China. The research reveals the geochemical characteristics, distribution [...] Read more.
This research addresses the critical safety issue of harmful gas influx during tunnel excavation through unconventional gas-bearing structures. It focuses on six tunnels affected by shale gas influx along the Zhangnan Expressway of northwestern Hunan, China. The research reveals the geochemical characteristics, distribution patterns, and accumulation mechanisms of harmful gas in the shale formations of northwestern Hunan. The research adopts an integrated approach of “geological background analysis—multi-parameter testing—comprehensive evaluation”. It is based on geological and borehole data, field geological surveys, as well as laboratory and field tests. The research systematically analyzes the gas-bearing structural characteristics, geochemical parameters, and reservoir physical properties of the shale gas area in the Zhangnan Expressway. The geological regularities are summarized. The results show that the Longmaxi Formation of the Silurian system and the Qixia Formation of the Permian system serve as source rocks in the tunnel sites. The reservoirs are characterized by ultra-low porosity and permeability, with limited late-stage hydrocarbon generation potential. The gas-related hazard during tunnel construction and operation is primarily associated with the release of existing free and adsorbed gas. According to the calculation standards for absolute gas emission rates during construction, three tunnels are classified as micro-gas tunnels and three as non-gas tunnels. Two accumulation patterns are proposed: the self-sourcing composite accumulation pattern with micro-scale migration, and the accumulation pattern of self-generated and self-storage type of water pressure confinement. Enhanced monitoring, ventilation, and grouting sealing are recommended. This study develops an integrated “geology—testing—evaluation” assessment method for shale-gas-bearing tunnels. It provides important guidance for controlling harmful gas hazards in such tunnels and guaranteeing the sustainable development of tunnel construction. Full article
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20 pages, 2076 KB  
Article
Optimization and Field Validation of an Ultrafine-Cement-Based Grout for Coal Mine Borehole Sealing
by Tianzhu Chen, Jie Zhang, Zexin Chen, Haofei Hu, Changwei Wang, Shaoqiu Wang and Jihua Cai
Appl. Sci. 2026, 16(14), 6912; https://doi.org/10.3390/app16146912 - 10 Jul 2026
Viewed by 216
Abstract
Conventional borehole sealing materials used in coal mines often suffer from slow setting times, insufficient early strength, and poor fluidity, resulting in unsatisfactory sealing performance and reduced gas drainage efficiency. In this study, an ultrafine-cement-based grout was optimized using sodium chloride, LSN, and [...] Read more.
Conventional borehole sealing materials used in coal mines often suffer from slow setting times, insufficient early strength, and poor fluidity, resulting in unsatisfactory sealing performance and reduced gas drainage efficiency. In this study, an ultrafine-cement-based grout was optimized using sodium chloride, LSN, and MZSG as the early-strength agent, accelerator, and water reducer, respectively. Laboratory experiments, including tests of setting time, fluidity, compressive strength, and permeability, were conducted to determine the recommended formulation, followed by field verification in a coal mine in Shanxi Province, China. The optimized grout achieved an initial setting time of 41 min, a fluidity of 348 mm, a compressive strength of 18.1 MPa, and a permeability of 0.0808 mD, indicating a favorable balance between rapid setting, injectability, mechanical integrity, and gas-tightness. The improved performance was attributed to the synergistic effects of the additives: Sodium chloride promoted early hydration, LSN accelerated setting and contributed to early matrix formation, and MZSG improved slurry dispersion and injectability. The field performance further confirmed that the optimized material provided more stable gas drainage behavior under the tested mine conditions. These results demonstrate that the proposed ultrafine-cement-based grout offers a practical sealing material for gas-drainage boreholes in fractured coal seams and provides an effective material-design strategy for coupling early strength development, slurry transportability, and sealing compactness. Full article
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16 pages, 25415 KB  
Article
Numerical Simulation of Grout Diffusion and Overlap Characteristics in Horizontal Curtain Grouting for Underground Mines Within 3D Discrete Fracture Networks
by Xuetong Gao, Guilei Han, Xiaofeng Xue, Dajin Liu, Zhiqi Wang, Chuanyong Wei and Shichong Yuan
Water 2026, 18(14), 1669; https://doi.org/10.3390/w18141669 - 9 Jul 2026
Viewed by 341
Abstract
Deep metal mines face increasing risks of water and sand inrush under complex fracture network conditions, where the unclear mechanism of slurry diffusion limits the reliability of horizontal curtain grouting. Taking the Cuihongshan iron–polymetallic mine as a case study, this paper establishes a [...] Read more.
Deep metal mines face increasing risks of water and sand inrush under complex fracture network conditions, where the unclear mechanism of slurry diffusion limits the reliability of horizontal curtain grouting. Taking the Cuihongshan iron–polymetallic mine as a case study, this paper establishes a stochastic three-dimensional discrete fracture network model and adopts an orthogonal experimental design to systematically investigate the effects of key engineering parameters on grout diffusion behavior. The results reveal that grouting pressure acts as the dominant controlling factor, significantly expanding the diffusion range and promoting the formation of continuous high-fill zones within the fracture network. Conversely, slurry viscosity exhibits a negative correlation with diffusion performance, leading to reduced inter-borehole connectivity as viscosity increases. Compared with conventional macro-indicators, the inter-borehole overlap rate provides a more precise quantitative measure of curtain continuity. The study demonstrates that achieving a sufficiently high overlap rate is critical for transitioning from discontinuous filling to a reliable impermeable curtain. These findings offer a theoretical basis for optimizing grouting parameters and evaluating sealing effectiveness in deep mine construction. Full article
(This article belongs to the Section Hydrogeology)
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20 pages, 12538 KB  
Article
Research and Development of New Slurry Sealing Materials Based on Box–Behnken Design and Multi-Performance Synergistic Regulation
by Baofu Wang, Tuo Qiang, Fucheng Zhang, Huogen Luo, Yayou Xu, Changyuan Xiao and Lintao Hu
Processes 2026, 14(14), 2235; https://doi.org/10.3390/pr14142235 - 8 Jul 2026
Viewed by 261
Abstract
To address gas leakage in coal mine gas extraction boreholes, this study developed a novel slurry-based sealing material using sodium bentonite as the matrix, compounded with sodium dodecylbenzene sulfonate as the dispersant and sodium carboxymethyl cellulose as the thickener. The optimal formulation, determined [...] Read more.
To address gas leakage in coal mine gas extraction boreholes, this study developed a novel slurry-based sealing material using sodium bentonite as the matrix, compounded with sodium dodecylbenzene sulfonate as the dispersant and sodium carboxymethyl cellulose as the thickener. The optimal formulation, determined through single-factor experiments and response surface methodology, consisted of a water-to-bentonite ratio of 4.4:1, a dispersant content of 0.41%, and a thickener content of 0.12%. Under these conditions, the slurry exhibited a flowability of 134.8 mm, a water retention rate of 96.01%, and a permeability of 41.45%, representing improvements of 10.74%, 11.74%, and 14.47%, respectively, compared with the unmodified bentonite material. Fracture seepage tests further demonstrated that the modified slurry exhibited superior permeability to cement-based materials under different fracture porosities and grouting pressures. In addition, results from a self-designed airtightness testing platform showed that the material maintained excellent sealing performance under positive pressures of 0.1–0.3 MPa, with a significantly lower pressure decay rate than those of cement and polyurethane materials. These findings indicate that the proposed bentonite-based slurry provides an effective sealing material for coal mine gas extraction boreholes and may contribute to safer and more efficient coal mine production. Full article
(This article belongs to the Section Energy Systems)
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19 pages, 5960 KB  
Article
Experimental Study on the Enhancement of Waterproof Performance of Shield Tunnel Joints Using Diatomite–MICP Combined Reinforcement Technology
by Yu Liang, Changyu Long, Xingzhong Nong and Quan Yuan
Sustainability 2026, 18(13), 6801; https://doi.org/10.3390/su18136801 - 4 Jul 2026
Viewed by 337
Abstract
With the continuous development of China’s economy and technology, the number of urban transportation shield tunnels has been increasing. As tunnel depth and diameter grow, the geological conditions become increasingly complex, making leakage at segment joints of shield tunnels a more prominent issue, [...] Read more.
With the continuous development of China’s economy and technology, the number of urban transportation shield tunnels has been increasing. As tunnel depth and diameter grow, the geological conditions become increasingly complex, making leakage at segment joints of shield tunnels a more prominent issue, significantly affecting the sustainable development of urban transportation. To address the issue of water leakage, microbially induced calcium carbonate precipitation (MICP) technology offers a green and environmentally friendly solution. However, relying solely on MICP technology is insufficient to enhance the waterproofing performance of large segment joints of shield tunnel. To address this, this study proposes combining diatomite as both a carrier and filler material with MICP technology, using a diatomite–MICP composite grout to improve the waterproofing performance of tunnel segment joints. First, through laboratory macro-scale tests and micro-morphology analysis, the influence of diatomite dosage on the sealing performance of diatomite–MICP composite grout was systematically studied, and the optimal diatomite dosage was determined. Based on this, a self-developed segment joint waterproofing testing platform was adopted to conduct hydraulic tests on double-seal gasket joints, evaluating the enhancement effect of the composite grout on the overall waterproofing performance of tunnel segment joints. The results indicated that the dosage of diatomite significantly affects the sealing performance of the composite grout, with an optimal dosage of 20% by weight of the bacterial solution. At this dosage, the composite grout achieved the highest density, resulting in maximum unconfined compressive strength and shear strength, as well as the lowest permeability coefficient. The joint water pressure test confirmed that after grouting with a diatomite–MICP composite grout at the optimal dosage of 20%, the breakdown water pressures of the inner and outer seal gaskets at the segment joints reached 2011 kPa and 2019 kPa, representing increases of 15.91% and 16.64% compared to the control group without grouting. This study demonstrates the effectiveness and application potential of the green biomineralization technologies in waterproofing of shield tunnel joints. Full article
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30 pages, 6021 KB  
Article
Integrated Evaluation of Grouting Effectiveness and Seepage Control Mechanisms in a Phosphate Mine Shaft Under Complex Hydrogeological Conditions
by Jiangtao Cheng, Fuqing Li, Guotao Xiong, Rui Sun, Fufeng Li, Rongjian Shi, Jianjie Zheng, Yan Shen, Yingtao Li and Ya Shi
Geosciences 2026, 16(7), 252; https://doi.org/10.3390/geosciences16070252 - 25 Jun 2026
Viewed by 202
Abstract
Evaluating grouting effectiveness in deep shafts remains difficult because water-control performance is jointly governed by hydraulic response, seepage-path sealing, grout-body quality, and surrounding rock stability under complex hydrogeological conditions. In this study, an integrated evaluation and seepage analysis framework was developed for the [...] Read more.
Evaluating grouting effectiveness in deep shafts remains difficult because water-control performance is jointly governed by hydraulic response, seepage-path sealing, grout-body quality, and surrounding rock stability under complex hydrogeological conditions. In this study, an integrated evaluation and seepage analysis framework was developed for the Lianhuashan Phosphate Mine shaft project in Zhongxiang City, Hubei Province, China. Multi-source engineering data from hydrogeological observations, geophysical detection, construction records, and laboratory tests were used to evaluate six representative working faces, and a two-dimensional Darcy flow model was established to interpret the seepage-control mechanism. The evaluation results show differences among the treated sections: the auxiliary shaft at the −29.8 m outlet achieved the highest comprehensive score of 74.79, whereas the main shaft at +13 m showed the weakest performance, with a score of 50.16. Overall, three sections were rated as good, two as moderate, and one as poor. The dominant controls on grouting effectiveness are total shaft inflow, surrounding rock integrity/stability, seepage point number, and sealing-related indices. Numerical simulations further show that grouting reduced total shaft inflow from 6.6080 to 2.0198 m3/h, corresponding to a reduction of 69.43%, and shifted the main hydraulic-gradient concentration from the shaft wall to the outer boundary of the grouted ring. Reducing grouting ring permeability from 5.10 × 10−13 to 1.00 × 10−14 m2 further lowered shaft inflow to 0.2929 m3/h and increased water-control efficiency to 95.57%, whereas increasing ring thickness from 8 to 16 m reduced shaft inflow from 2.7063 to 1.7260 m3/h. In addition, moving the water-rich zone away from the shaft reduced total inflow from 2.5503 m3/h at Xf = 10 m to 2.0079 m3/h at Xf = 26 m. These results indicate that effective shaft grouting depends on the coordinated control of inflow suppression, conductive-path sealing, and structural stabilization. The proposed framework provides a practical basis for grouting evaluation and water hazard control in deep shafts under complex hydrogeological conditions. Full article
(This article belongs to the Special Issue Advances in Geohazard Mitigation and Adaptation)
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17 pages, 36049 KB  
Article
Experimental Study on Mechanical Behavior and Crack Evolution of Borehole Coal Samples Before and After Grouting Under Brazilian Splitting Conditions
by Jialiang Zhu, Xiaolong Song and Jiuhui Cheng
Appl. Sci. 2026, 16(12), 5978; https://doi.org/10.3390/app16125978 - 12 Jun 2026
Viewed by 238
Abstract
Grouting and sealing in gas drainage boreholes are two of the critical measures to ensure efficient coal seam gas extraction. However, traditional cement grouting often leads to debonding and cracking of the slurry–coal cemented body under external load, resulting in poor sealing performance. [...] Read more.
Grouting and sealing in gas drainage boreholes are two of the critical measures to ensure efficient coal seam gas extraction. However, traditional cement grouting often leads to debonding and cracking of the slurry–coal cemented body under external load, resulting in poor sealing performance. To suppress crack propagation and achieve borehole reinforcement and efficient sealing, this study compares the mechanical properties and crack evolution characteristics of slurry–coal cemented samples grouted with different modified materials. Five types of cement-based sealing materials, including ordinary Portland cement, were used for grouting coal rock in boreholes. By employing an acoustic emission signal acquisition system and a non-contact full-field strain measurement system, the tensile mechanical properties of coal before and after grouting were compared. The influence of material properties on the reinforcement capacity of borehole coal was analyzed, along with the failure process characteristics and final failure morphology of the slurry–coal cemented body under Brazilian splitting load. Finally, the effects of material toughness and bond strength on the brittleness index and failure mode of the slurry–coal cemented samples under Brazilian splitting conditions were discussed. The results show that the tensile strength improvement rates of the samples were 26.9%, 55.3%, 48.4%, 8.6%, and 45.6%, respectively. Distinct from previous studies focusing on fractured grouting or intact coal rock, this work for the first time systematically reveals the non-monotonic influence of the combination of material toughness and bond strength on the reinforcement effect of borehole coal samples and proposes an evaluation framework based on quantitative acoustic emission crack type analysis and the concept of effectiveness threshold. The varying degrees of tensile strength enhancement indicate differences in the reinforcement capabilities of grouting materials with different properties. The acoustic emission signals during the failure process of the slurry–coal cemented body exhibited typical stage-specific characteristics, though material properties altered the failure modes. By quantifying the intrinsic properties and crack characteristics of the slurry–coal cemented body using the brittleness index and grayscale histograms, this study provides a theoretical basis for guiding efficient sealing of gas drainage boreholes through an in-depth understanding of the mechanical behavior and crack evolution of borehole coal samples before and after grouting under Brazilian splitting conditions. Full article
(This article belongs to the Section Energy Science and Technology)
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18 pages, 7487 KB  
Article
Safety Management and Risk Evaluation for Coal Mine Operations Threatened by Karst Collapse Column Water Inrushes
by Yu Liu, Jiapeng Lu, Qimeng Liu, Jingzhong Zhu and Chongyan Liu
Processes 2026, 14(11), 1718; https://doi.org/10.3390/pr14111718 - 25 May 2026
Viewed by 277
Abstract
Shallow coal resources are being gradually depleted, which has led to an increase in mining depth. However, the safe extraction of deep coal seams is increasingly threatened by limestone water hazards. When vertical hydraulic channels such as karst collapse columns (KCCs) develop in [...] Read more.
Shallow coal resources are being gradually depleted, which has led to an increase in mining depth. However, the safe extraction of deep coal seams is increasingly threatened by limestone water hazards. When vertical hydraulic channels such as karst collapse columns (KCCs) develop in limestone strata, high-pressure water may flow into the mine, potentially causing substantial casualties and property losses. In this study, the 1613A stope of the Zhangji coal mine was investigated through comprehensive detection, grouting treatment, and prevention effect evaluation. A numerical model was established to simulate the dynamic changes in groundwater levels within the limestone aquifers throughout the process. The results reveal that a KCC is developed beneath the C33 stratum, exhibiting an oval shape with a length of 53 m and a width of 35 m in plan view. A combination of surface and underground methods, including exploration, treatment, verification, and reinforcement, has sealed the hydraulic pathway connected to the Ordovician limestone, thereby eliminating the threat of floor water inrush. These findings are of significant value for the application and dissemination of advanced regional control technologies for water hazards in coal mines. Full article
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20 pages, 14199 KB  
Article
Experimental Investigation on the Influence of Inside-Trapped Water Effect and Remedial Grouting on the Vertical Bearing Characteristics of Suction Bucket Foundations for Offshore Wind Turbines in Sand
by Hanbo Zhai, Ming Qin, Tingting Li, Jialin Dai, Zhongping Wang and Jun Xiang
Appl. Sci. 2026, 16(11), 5204; https://doi.org/10.3390/app16115204 - 22 May 2026
Viewed by 193
Abstract
This study investigates the influence of inside-trapped water and remedial grouting on the vertical bearing behaviour of suction bucket foundations in sand through 1 g laboratory model tests. The tests were designed to compare the relative responses of different trapped-water and grouting conditions [...] Read more.
This study investigates the influence of inside-trapped water and remedial grouting on the vertical bearing behaviour of suction bucket foundations in sand through 1 g laboratory model tests. The tests were designed to compare the relative responses of different trapped-water and grouting conditions under the same model scale, sand preparation procedure, and loading protocol. Two target trapped-water conditions were considered: a condition without an observable continuous water layer beneath the bucket lid and a condition with an initial trapped-water thickness of approximately 2 cm. These conditions were controlled and verified before loading using the scale attached to the transparent bucket wall and the underwater camera monitoring system. The results show that inside-trapped water modifies the vertical load-transfer path between the bucket lid and the internal soil plug. When a water layer exists beneath the lid, direct lid–soil plug contact is weakened, and the foundation resistance relies more strongly on skirt-side resistance and the resistance mobilized near the bucket rim. Under cyclic vertical loading, the trapped-water case exhibited larger cumulative displacement and a lower post-cyclic bearing response than the no-trapped-water case. The secant cyclic stiffness showed a continuous increase in the no-trapped-water case, whereas a rise-then-fall trend was observed in the trapped-water case, which may be associated with cyclic densification, soil plug disturbance, changes in lid–soil plug contact, and possible local pore pressure development. Remedial grouting filled the trapped-water space beneath the bucket lid and partially restored the lid–soil plug load-transfer path. Under the present model test conditions, the post-cyclic dimensionless bearing capacity of the grouted cases increased by approximately 13–16% relative to the ungrouted trapped-water case. The grouting cases with different bentonite contents showed similar recovery trends within the limited dataset, suggesting that the improvement was mainly related to filling and sealing the trapped-water space rather than to the intrinsic strength of the grout material. Full article
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20 pages, 24037 KB  
Article
Formation and Performance of a Polymer–Cement Composite Gel in Magnesium Phosphate Cement Grouting Materials Modified by Steel Slag and Latex Powder
by Jingwei Zhang, Aolin Zhang and Jia Li
Gels 2026, 12(6), 455; https://doi.org/10.3390/gels12060455 - 22 May 2026
Viewed by 326
Abstract
Magnesium phosphate cement (MPC) shows great potential for complex underground environments due to its rapid-hardening and early-strength properties. However, its large-scale application is hindered by several drawbacks, including high hydration heat, rapid setting, and insufficient long-term durability. To address these limitations, this study [...] Read more.
Magnesium phosphate cement (MPC) shows great potential for complex underground environments due to its rapid-hardening and early-strength properties. However, its large-scale application is hindered by several drawbacks, including high hydration heat, rapid setting, and insufficient long-term durability. To address these limitations, this study developed a novel MPC grouting material modified with steel slag (SS) and redispersible latex powder (LP). We systematically investigated the workability, mechanical properties, durability, and microstructural evolution of this modified system. Results indicate that incorporating SS and LP decreases both the fluidity and setting time of the grout. An optimal SS dosage accelerates reaction kinetics and raises the peak hydration temperature. Conversely, the LP-induced polymer film suppresses the overall temperature rise, delaying the first exothermic peak and advancing the second. The incorporation of 5% steel slag increased the 28-day compressive strength of the MPC to 54.86 MPa. Building on this, the combined addition of 0.15% latex powder further elevated the strength to 58.82 MPa. Microstructural and pore analyses confirmed that the steel slag enhanced interfacial bonding through physical filling and the formation of calcium phosphate crystals. Meanwhile, the latex powder formed a continuous polymer film, which tightly wrapped and bridged the hydration products and unreacted particles. This synergistic mechanism effectively sealed the capillary pores and reduced the proportion of harmful pores by 15.99% compared to the control group. Consequently, the densified MPC matrix laid a solid microstructural foundation for the material’s excellent durability. It offers reliable, high-performance material for seepage control and strata reinforcement in complex environments. Full article
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20 pages, 18857 KB  
Article
Instability Mechanism and CO2 Phase Transition in Long–Short Borehole Pressure Relief Control of Narrow Coal Pillars in a Gob-Side Roadway Under Water-Immersed Gentle-Dipping Coal Seam Conditions
by Fei Zhao, Dongdong Chen, Kai Liu, Yi Chang, Jiachen Tang, Sining Li and Jingyong Liu
Appl. Sci. 2026, 16(10), 5073; https://doi.org/10.3390/app16105073 - 19 May 2026
Viewed by 266
Abstract
This study addresses asymmetric large surrounding rock deformation induced by narrow coal pillar instability in a gentle-dipping coal seam gob-side coal roadway (GSCR) under water-immersed and high-humidity conditions. The corresponding instability mechanism and control technology are systematically studied via integrated laboratory, theoretical, numerical [...] Read more.
This study addresses asymmetric large surrounding rock deformation induced by narrow coal pillar instability in a gentle-dipping coal seam gob-side coal roadway (GSCR) under water-immersed and high-humidity conditions. The corresponding instability mechanism and control technology are systematically studied via integrated laboratory, theoretical, numerical and field methods. From constant temperature–humidity rock deterioration tests, SEM and XRD analysis, it is revealed that hydration of hydrophilic minerals (kaolinite, chlorite) in immediate roof mudstone intrinsically drives its macro–micro structural disintegration and mechanical degradation, and the catastrophic chain mechanism of water-induced mudstone weakening–force transmission medium failure of coal pillars and overlying strata–sliding instability of key voussoir beam blocks–linked large surrounding rock deformation is clarified. A mechanical model of the overlying voussoir beam structure for the target roadway is established considering both mudstone weakening and excavation-induced load transfer effects. The sliding criterion of key overlying blocks is derived, which quantitatively confirms that higher mudstone weakening and excavation-induced stress concentration elevate the sliding instability risk of the voussoir beam structure. Based on the findings and field conditions, a combined near-field and low-position field support scheme is proposed, including near-field reinforcement (shotcreting sealing, bolt–cable cascade reinforcement, deep grouting modification) and low-position field pressure relief via liquid CO2 phase transition long–short boreholes roof cutting. Field application verifies that the maximum roadway deformation is controlled within 172 mm, with excellent surrounding rock control performance. Full article
(This article belongs to the Topic Advances in Mining and Geotechnical Engineering)
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30 pages, 19759 KB  
Article
Zeolite-Modified Acrylate Grouts: Synergistic Water-Sealing Performance with Cement Slurry Combined Grouting for Water-Rich Sandy Cobble Tunnels
by Qiusheng Wang, Mengchao Cui and Pei Li
Polymers 2026, 18(5), 600; https://doi.org/10.3390/polym18050600 - 28 Feb 2026
Viewed by 561
Abstract
Water seepage in shield tunnels in water-rich sandy cobble strata threatens construction safety and long-term durability. Grouting, a widely used remedial technique, depends on material performance. Among common grouts, conventional acrylate (AC) grouts have inherent limitations in strata. This study develops an enhanced [...] Read more.
Water seepage in shield tunnels in water-rich sandy cobble strata threatens construction safety and long-term durability. Grouting, a widely used remedial technique, depends on material performance. Among common grouts, conventional acrylate (AC) grouts have inherent limitations in strata. This study develops an enhanced zeolite-acrylate composite grouting material by incorporating zeolite powder into the AC matrix. Systematic experiments assessed the impacts of zeolite dosage, slurry ratio, and water use ratio on gel time, water absorption expansion rate, and bond strength, with interfacial characteristics analyzed via SEM. Results indicate zeolite addition shortens gel time by up to 23% (excessive content retards solidification); 24-h expansion rate ranges 63–111%; bond strength shows a non-monotonic trend with zeolite dosage (initial decline then rise), and higher water content weakens adhesion. Scanning electron microscopy (SEM) confirms robust interfacial bonding. Proposed reference field parameters (water use ratio 5:1–6:1, slurry ratio 5:1–6:1, zeolite dosage 0.5–1.0%) require flexible adjustment according to on–site conditions. Notably, gel time is not inherently better when shorter in practice, but tailored to specific construction scenarios. Rigorous tests verify the composite’s superior seepage control capacity with ultrafine cement grout, providing theoretical and practical guidance for grouting design in complex hydrogeological environments. Full article
(This article belongs to the Special Issue Applications of Polymers in Civil Engineering)
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26 pages, 5958 KB  
Article
A Material–Structure Integrated Approach for Soft Rock Roadway Support: From Microscopic Modification to Macroscopic Stability
by Sen Yang, Yang Xu, Feng Guo, Zhe Xiang and Hui Zhao
Processes 2026, 14(3), 414; https://doi.org/10.3390/pr14030414 - 24 Jan 2026
Viewed by 609
Abstract
As a cornerstone of China’s energy infrastructure, the coal mining industry relies heavily on the stability of its underground roadways, where the support of soft rock formations presents a critical and persistent technological challenge. This challenge arises primarily from the high content of [...] Read more.
As a cornerstone of China’s energy infrastructure, the coal mining industry relies heavily on the stability of its underground roadways, where the support of soft rock formations presents a critical and persistent technological challenge. This challenge arises primarily from the high content of expansive clay minerals and well-developed micro-fractures within soft rock, which collectively undermine the effectiveness of conventional support methods. To address the soft rock control problem in China’s Longdong Mining Area, an integrated material–structure control approach is developed and validated in this study. Based on the engineering context of the 3205 material gateway in Xin’an Coal Mine, the research employs a combined methodology of micro-mesoscopic characterization (SEM, XRD), theoretical analysis, and field testing. The results identify the intrinsic instability mechanism, which stems from micron-scale fractures (0.89–20.41 μm) and a high clay mineral content (kaolinite and illite totaling 58.1%) that promote water infiltration, swelling, and strength degradation. In response, a novel synergistic technology was developed, featuring a high-performance grouting material modified with redispersible latex powder and a tiered thick anchoring system. This technology achieves microscale fracture sealing and self-stress cementation while constructing a continuous macroscopic load-bearing structure. Field verification confirms its superior performance: roof subsidence and rib convergence in the test section were reduced to approximately 10 mm and 52 mm, respectively, with grouting effectively sealing fractures to depths of 1.71–3.92 m, as validated by multi-parameter monitoring. By integrating microscale material modification with macroscale structural optimization, this study provides a systematic and replicable solution for enhancing the stability of soft rock roadways under demanding geo-environmental conditions. Soft rock roadways, due to their characteristics of being rich in expansive clay minerals and having well-developed microfractures, make traditional support difficult to ensure roadway stability, so there is an urgent need to develop new active control technologies. This paper takes the 3205 Material Drift in Xin’an Coal Mine as the engineering background and adopts an integrated method combining micro-mesoscopic experiments, theoretical analysis, and field tests. The soft rock instability mechanism is revealed through micro-mesoscopic experiments; a high-performance grouting material added with redispersible latex powder is developed, and a “material–structure” synergistic tiered thick anchoring reinforced load-bearing technology is proposed; the technical effectiveness is verified through roadway surface displacement monitoring, anchor cable axial force monitoring, and borehole televiewer. The study found that micron-scale fractures of 0.89–20.41 μm develop inside the soft rock, and the total content of kaolinite and illite reaches 58.1%, which is the intrinsic root cause of macroscopic instability. In the test area of the new support scheme, the roof subsidence is about 10 mm and the rib convergence is about 52 mm, which are significantly reduced compared with traditional support; grouting effectively seals rock mass fractures in the range of 1.71–3.92 m. This synergistic control technology achieves systematic control from micro-mesoscopic improvement to macroscopic stability by actively modifying the surrounding rock and optimizing the support structure, significantly improving the stability of soft rock roadways. Full article
(This article belongs to the Section Petroleum and Low-Carbon Energy Process Engineering)
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27 pages, 7281 KB  
Article
Precise Grouting in Multi-Bed Separations of Overburden Under Curtain Protection for Isolated Coal Pillar Recovery
by Heng Yang, Mingkui Jia, Dafeng Pi, Shijie Tang, Mingjie Guo, Wenbing Guo, Yu Guo, Guodong Li and Erhu Bai
Energies 2026, 19(2), 501; https://doi.org/10.3390/en19020501 - 19 Jan 2026
Viewed by 685
Abstract
Traditional overburden bed-separation grouting technology often leads to issues of grout leakage and insufficient control of surface subsidence, primarily due to its poor adaptability to specific mining conditions such as isolated coal pillar recovery, the development of stratigraphic faults and fractures, or the [...] Read more.
Traditional overburden bed-separation grouting technology often leads to issues of grout leakage and insufficient control of surface subsidence, primarily due to its poor adaptability to specific mining conditions such as isolated coal pillar recovery, the development of stratigraphic faults and fractures, or the absence of clearly identifiable key strata. To address these limitations, this study proposes an innovative multi-bed-separation precise grouting technology. The formation mechanism of multi-bed separations is analyzed, their development positions are determined, and an engineering solution for controlling surface subsidence after multi-bed-separation grouting is proposed. Key technical parameters, including grouting pressure, stability of grout-isolating layers, grouting space volume, and grout amount, are theoretically analyzed. A “three-step” precise grouting process—consisting of separation detection and verification, fracture curtain sealing, and precise grouting for subsidence reduction—was developed and applied in the 12030 isolated coal pillar panel of Xinyi Coal Mine. A total of 504,500 tons of fly ash (including cement) was grouted, of which 398,600 tons was used for precise grouting in multi-bed separations of overburden. This approach recovered 1,364,400 tons of coal resources beneath village buildings, with a grouting–extraction ratio (volume ratio) of 0.53. The technology demonstrates clear advantages: no grout leakage occurred during the process, the surface subsidence reduction rate reached approximately 75.81%, and building damage was controlled within Grade I. The results demonstrate that this technology has a significant effect on subsidence reduction and damage control, enabling safe and green mining of coal resources beneath villages under special geological and mining conditions. Full article
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22 pages, 4352 KB  
Article
Grading Evaluation of Grouting Seal Quality for Recharge Channels in Water-Hazardous Aquifers of Extremely Complex Mines
by Jianggen He, Hankun Li, Yaolong Huang, Shiyuan Tian, Junchao Yue, Hongwei Meng, Qi Wang and Xinyi Wang
Water 2026, 18(1), 121; https://doi.org/10.3390/w18010121 - 4 Jan 2026
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Abstract
Grouting to seal the recharge channels of water-bearing aquifers is an effective method for reducing mine water inflow. Evaluating effectiveness and establishing a hierarchical classification system are crucial for assessing project quality. Taking the grouting seal project of the Cambrian limestone aquifer recharge [...] Read more.
Grouting to seal the recharge channels of water-bearing aquifers is an effective method for reducing mine water inflow. Evaluating effectiveness and establishing a hierarchical classification system are crucial for assessing project quality. Taking the grouting seal project of the Cambrian limestone aquifer recharge channels at Mine No.7 in the Pingdingshan Coalfield as a case study, this paper first comprehensively evaluates the grouting seal effectiveness based on the difference in dynamic water recharge to goaf before and after grouting, derived from long-term pumping test data. Further, six indicator factors—grout volume, grout volume per unit time, grout volume per unit thickness, final borehole pressure, penetration depth into Cambrian limestone, and variation in rock mechanical strength—were selected. Weights for these factors were determined by integrating the Analytic Hierarchy Process, entropy weight method, and composite weighting method. The TOPSIS model was applied to classify and rank the grouting seal effectiveness in six recharge channels. Results indicate that post-grouting water recharge from goaf decreased by 240.78 m3/h during dry season and 878.57 m3/h during wet season, confirming high-quality grouting seal. The grouting seal quality of the six recharge channels was ranked from highest to lowest as follows: NO.3 > NO.2 > NO.6 > NO.1 > NO.5 > NO.4. The evaluation results corresponded with the actual karst fissure development and distribution of goaf in the exposed recharge channels. Full article
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