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Keywords = glass preservation/restoration

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11 pages, 2735 KiB  
Case Report
Management of a Complicated Crown Fracture in a 16-Year-Old Patient: A Case Report
by Ralitsa Bogovska-Gigova
Reports 2025, 8(3), 132; https://doi.org/10.3390/reports8030132 - 1 Aug 2025
Viewed by 189
Abstract
Background and Clinical Significance: Traumatic dental injuries, particularly complicated crown fractures of permanent incisors, are common in adolescents, with maxillary central incisors most frequently affected due to their prominent position. These injuries, often resulting from sports or accidents, require prompt management to [...] Read more.
Background and Clinical Significance: Traumatic dental injuries, particularly complicated crown fractures of permanent incisors, are common in adolescents, with maxillary central incisors most frequently affected due to their prominent position. These injuries, often resulting from sports or accidents, require prompt management to prevent complications such as pulp necrosis or infection, which can compromise long-term prognosis. Fragment reattachment offers a conservative, esthetically favorable approach when the fractured segment is intact, with outcomes comparable to composite restorations. This case report underscores the importance of timely intervention and advanced restorative techniques in pediatric dentistry. Case Presentation: A 16-year-old male presented with a complicated crown fracture of the upper left central incisor sustained during a soccer game. The fracture extended subgingivally with pulp exposure. The patient preserved the fragment in saline. Treatment involved fragment reattachment using a dentin bonding agent and flowable composite resin, followed by single-visit root canal therapy due to delayed presentation (48 h). A glass fiber post was placed to reinforce the restoration due to significant coronal loss. Three years of follow-up visits (1, 3, 6, 12, 24, and 36 months) revealed no clinical or radiographic complications, with the tooth remaining asymptomatic and functional. Conclusions: This case underscores the effectiveness of fragment reattachment when combined with meticulous technique and long-term monitoring. Full article
(This article belongs to the Special Issue Oral Disorders in the Pediatric Population)
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30 pages, 1344 KiB  
Review
Bioceramics in Endodontics: Limitations and Future Innovations—A Review
by Peramune Arachchilage Amila Saman Prasad Kumara, Paul Roy Cooper, Peter Cathro, Maree Gould, George Dias and Jithendra Ratnayake
Dent. J. 2025, 13(4), 157; https://doi.org/10.3390/dj13040157 - 1 Apr 2025
Cited by 1 | Viewed by 3341
Abstract
Bioceramic materials for endodontic treatments have gradually transformed over the years into materials with enhanced biocompatibility and chemical and mechanical properties compared to earlier generations. In endodontics procedures, these materials are used as restorative material in applications such as root-end fillings, pulp capping, [...] Read more.
Bioceramic materials for endodontic treatments have gradually transformed over the years into materials with enhanced biocompatibility and chemical and mechanical properties compared to earlier generations. In endodontics procedures, these materials are used as restorative material in applications such as root-end fillings, pulp capping, perforations repair, and apexification repair procedures. However, they have far from ideal mechanical and handling properties, biocompatibility issues, aesthetic concerns due to tooth discolouration, limited antibacterial activity, and affordability, which are amongst several key limitations. Notably, bioceramic materials are popular due to their biocompatibility, sealing ability, and durability, consequently surpassing traditional materials such as gutta-percha and zinc oxide–eugenol sealers. A lack of recent advancements in the field, combined with nanomaterials, has improved the formulations of these materials to overcome these limitations. The existing literature emphasises the benefits of bioceramics while underreporting their poor mechanical properties, handling difficulties, cost, and various other drawbacks. The key gaps identified in the literature are the insufficient coverage of emerging materials, narrow scope, limited insights into future developments, and underreporting of failures and complications of the existing materials. Consequently, this review aims to highlight the key limitations of various endodontic materials, primarily focusing on calcium silicate, calcium phosphate, and bioactive glass-based materials, which are the most abundantly used materials in dentistry. Based on the literature, bioceramic materials in endodontics have significantly improved over recent years, with different combinations of materials and technology compared to earlier generations while preserving many of their original properties, with some having affordable costs. This review also identified key innovations that could shape the future of endodontic materials, highlighting the ongoing evolution and advancements in endodontic treatments. Full article
(This article belongs to the Special Issue Endodontics and Restorative Sciences: 2nd Edition)
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15 pages, 805 KiB  
Review
Clinical Survival Rate and Laboratory Failure of Dental Veneers: A Narrative Literature Review
by Tariq F. Alghazzawi
J. Funct. Biomater. 2024, 15(5), 131; https://doi.org/10.3390/jfb15050131 - 16 May 2024
Cited by 4 | Viewed by 7205
Abstract
There is a vast amount of published literature concerning dental veneers; however, the effects of tooth preparation, aging, veneer type, and resin cement type on the failure of dental veneers in laboratory versus clinical scenarios are not clear. The purpose of the present [...] Read more.
There is a vast amount of published literature concerning dental veneers; however, the effects of tooth preparation, aging, veneer type, and resin cement type on the failure of dental veneers in laboratory versus clinical scenarios are not clear. The purpose of the present narrative review was to determine the principal factors associated with failures of dental veneers in laboratory tests and to understand how these factors translate into clinical successes/failures. Articles were identified and screened by the lead author in January 2024 using the keywords ‘‘dental veneer”, “complication”, “survival rate”, “failure”, and “success rate” using PubMed/Medline, Scopus, Google Scholar, and Science Direct. The inclusion criteria included articles published between January 1999 and January 2024 on the topics of preparation of a tooth, aging processes of the resin cement and veneer, translucency, thickness, fabrication technique of the veneer; shade, and thickness of the resin cement. The exclusion criteria included articles that discussed marginal and internal fit, microhardness, water sorption, solubility, polishability, occlusal veneers, retention, surface treatments, and wear. The results of the present review indicated that dental veneers generally have a high survival rate (>90% for more than 10 years). The amount of preserved enamel layer plays a paramount role in the survival and success rates of veneers, and glass-ceramic veneers with minimal/no preparation showed the highest survival rates. Fracture was the primary failure mechanism associated with decreased survival rate, followed by debonding and color change. Fractures increased in the presence of parafunctional activities. Fewer endodontic complications were associated with veneer restorations. No difference was observed between the maxillary and mandibular teeth. Clinical significance: Fractures can be reduced by evaluation of occlusion immediately after cementation and through the use of high-strength veneer materials, resin cements with low moduli, and thin layers of highly polished veneers. Debonding failures can be reduced with minimal/no preparation, and immediate dentin sealing should be considered when dentin is exposed. Debonding can also be reduced by preventing contamination from blood, saliva, handpiece oil, or fluoride-containing polishing paste; through proper surface treatment (20 s of hydrofluoric acid etching for glass ceramic followed by silane for 60 s); and through use of light-cured polymerization for thin veneers. Long-term color stability may be maintained using resin cements with UDMA-based resin, glass ceramic materials, and light-cure polymerization with thin veneers. Full article
(This article belongs to the Section Dental Biomaterials)
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12 pages, 3938 KiB  
Article
Effects of Er,Cr: YSGG Laser Application in De-Bonding of Different Ceramic Veneer Materials (In Vitro Study)
by Bassam Karem Amin
Coatings 2023, 13(8), 1352; https://doi.org/10.3390/coatings13081352 - 2 Aug 2023
Cited by 2 | Viewed by 2445
Abstract
Background: Ceramic restorations are widely used nowadays as the esthetic demand has increased in the worldwide population, and lithium disilicate and feldspathic porcelain materials are the most widely used veneer materials. The traditional removal procedure for veneers was recently replaced with the use [...] Read more.
Background: Ceramic restorations are widely used nowadays as the esthetic demand has increased in the worldwide population, and lithium disilicate and feldspathic porcelain materials are the most widely used veneer materials. The traditional removal procedure for veneers was recently replaced with the use of laser technology to debond the veneers so that the de-bonded veneers can be preserved and re-used. Aim: Up to now, there have been few studies regarding using lasers to remove ceramic laminate; thus, it is clear why this research topic is important for examining the efficiency of lasers in the use of de-bonding for different ceramic laminates with varying compositions and materials. Materials and Methods: This study employed forty-five normal human maxillary first premolars with comparable proportions. The forty-five teeth were initially split into three groups of fifteen teeth, and the teeth were chosen at random. Each group fused pairs of various ceramic materials. A total of fifteen teeth in the first group underwent feldspathic porcelain restorations. The second group contained fifteen restorations made of lithium disilicate glass-ceramic CAD-CAM. In the third group, fifteen teeth were restored using glass-ceramic that had a lithium disilicate glass-ceramic ingot. The RelyX Veneer A1 shade, available from 3M EPSE in the United States, was used to bond all the samples. The specimens were then submerged for approximately 24 h in distilled water at 37 degrees Celsius in order to simulate the conditions in an oral cavity. An Er,Cr: YSGG laser (Waterlase, iPlus, Biolase, from USA) was used with a turbo headpiece and an MX7 sapphire tip for irradiation. Results: The time needed for the ceramic disc to debond was calculated using a digital stopwatch. The average removal times for the feldspathic porcelain, lithium disilicate glass-ceramic ingot, and lithium disilicate glass-ceramic CAD-CAM were 10.067 ± 1.668 s, 5.200 ± 1.146 s, and 5.133 ± 1.125 s, while the removal times ranged from 8–12 s, 4–7 s, and 4–7 s, respectively. Compared to the other ceramic materials, de-bonding the feldspathic porcelain took longer. Conclusions: According to this study, the Er,Cr: YSGG laser application using the same study parameters made it simpler to de-bond lithium disilicate and feldspathic porcelain. Lithium disilicate, as opposed to feldspathic porcelain, transmits laser light more effectively; hence, the results varied depending on the materials, and the debonding occurred primarily at the veneer–cement interface. Full article
(This article belongs to the Special Issue Laser-Assisted Processes and Thermal Treatments of Materials)
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7 pages, 1264 KiB  
Case Report
Direct Pulp Capping with Advanced Platelet-Rich Fibrin: A Report of Two Cases
by Janet N. Kirilova and Dimitar Kosturkov
Medicina 2023, 59(2), 225; https://doi.org/10.3390/medicina59020225 - 26 Jan 2023
Cited by 3 | Viewed by 4030
Abstract
This article aims to prove dentin bridge formation in two cases after direct pulp capping in reversible pulpitis using the platelet concentrate A-PRF+ and preservation of the vitality of the dental pulp. The hemostasis process for the pulp wound and cavity disinfection with [...] Read more.
This article aims to prove dentin bridge formation in two cases after direct pulp capping in reversible pulpitis using the platelet concentrate A-PRF+ and preservation of the vitality of the dental pulp. The hemostasis process for the pulp wound and cavity disinfection with gaseous ozone was performed under anesthesia. A large A-PRF+ membrane was prepared from blood plasma and applied to the pulp wound. After placing an MTA, the cavity was closed using glass-ionomer cement. Clinical and cone beam computed tomography findings demonstrated the formation of a dentin bridge in both cases. After the definitive restoration was conducted during the sixth month, the teeth from both patients were asymptomatic and had normal electric pulp testing values. Conclusions: Via clinical and CBCT examinations, we observed the dentin bridge formation after placing the platelet concentrate A-PRF+ in both cases. The vitality of the dental pulp was preserved. Further research is needed to refine the clinical protocol, recommended period for control examination, clarification of the precise indications of platelet concentrates, etc. Full article
(This article belongs to the Special Issue Advances in Interdisciplinary Research in Medicine and Dentistry)
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18 pages, 7666 KiB  
Article
Glass Icons in Transylvania (Romania) and the Craft of Painting Them as Cultural Heritage Resources
by Daniela Sorea and Ionuț Mihai Popescu
Heritage 2022, 5(4), 4006-4023; https://doi.org/10.3390/heritage5040206 - 7 Dec 2022
Cited by 4 | Viewed by 4016
Abstract
The craft of painting icons on glass developed in the 17th century in Transylvania (Romania) following the spread of the news about the wooden icon of the weeping Mother of God in the church of Nicula. This news turned Nicula into a pilgrimage [...] Read more.
The craft of painting icons on glass developed in the 17th century in Transylvania (Romania) following the spread of the news about the wooden icon of the weeping Mother of God in the church of Nicula. This news turned Nicula into a pilgrimage centre, and requests for reproductions of the icon led to the locals becoming glass painters. Because of the surplus of icons, some of the Nicula painters set up new icon-painting centres along the road to Brașov (to the south) and the other main trade routes of Transylvania. In order to highlight the potential for sustainable development associated with this craft and to stimulate the painting of icons in the traditional way, we conducted documentary research on the subject of icons on glass. This research revealed the local peculiarities of the icon painters’ workshops and their importance to the identity of the Romanian peasants in Transylvania. We also conducted a participatory observation carried out in Brasov, which revealed that the iconography courses in popular schools of arts and crafts were both a viable way of managing the relationship with the iconographic tradition and a means to capitalize on religious painting on glass as a cultural heritage resource. The research highlighted the way in which, to preserve the traditional dimension of the craft, it is useful to encourage students to use anonymous glass icons as models and to have limited involvement in model restoration. Full article
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15 pages, 1728 KiB  
Article
Polymerisation Kinetics on FT-IR and Colorimetric Changes under UV Irradiation for a Commercial Polycyanoacrylate Adhesive, Addressed to Glass Restoration
by Evangelia C. Vouvoudi, Panagiotis D. Morfis, George D. Verros and Dimitris S. Achilias
Coatings 2022, 12(4), 490; https://doi.org/10.3390/coatings12040490 - 6 Apr 2022
Cited by 4 | Viewed by 3479
Abstract
This study evaluates a commercial polycyanoacrylate adhesive of medium viscosity regarding its suitability for the restoration of glass objects of cultural heritage in a museum environment (exhibition/storage). Loctite® Super Attak was investigated in terms of (a) its polymerisation rate and degree of [...] Read more.
This study evaluates a commercial polycyanoacrylate adhesive of medium viscosity regarding its suitability for the restoration of glass objects of cultural heritage in a museum environment (exhibition/storage). Loctite® Super Attak was investigated in terms of (a) its polymerisation rate and degree of conversion, using Infrared Spectroscopy FT-IR by monitoring the change of the C=C peak vs. C=O peak and (b) the alteration of the colour parameters of its films after its submission to UVC irradiation for several time intervals. It was confirmed that within 6 h, a thin-layered adhesive film acquires 80–85% of its polymerization in ambient conditions, while the reaction continues for up to 12–18 h in the conditions examined. The progress of the reaction is slower when the adhesive is in a protected environment. On the other hand, the effect of UVC rays on the glue is destructive and oxidative, provoking a yellow shade/colour from the first hours of exposure. The intensity of the yellowness becomes higher after 6 h of exposure, showing shifts in the absorption peaks of C–O/C=O groups of the initial IR spectrum and the augmentation of –OH absorptions. It was concluded that the adhesive is suitable for glass restoration, especially for instant, rapid, applications, under mild conditions of maintenance and exposure. Full article
(This article belongs to the Special Issue Science and Technology of Glassy Coatings)
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17 pages, 10513 KiB  
Article
Austrian Stained Glass in the Interplay of Research and Conservation: Reflections on How to Preserve an Endangered Art Genre
by Christina Wais-Wolf, Petra Weiss and Christoph Tinzl
Heritage 2022, 5(1), 509-525; https://doi.org/10.3390/heritage5010029 - 10 Mar 2022
Cited by 1 | Viewed by 4804
Abstract
In 2021, two projects for the protection and preservation of Austrian stained glass were performed in close cooperation between the Federal Monuments Authority Austria and active members of the Corpus Vitrearum Austria. Both projects are dedicated to difficult topics that will increasingly challenge [...] Read more.
In 2021, two projects for the protection and preservation of Austrian stained glass were performed in close cooperation between the Federal Monuments Authority Austria and active members of the Corpus Vitrearum Austria. Both projects are dedicated to difficult topics that will increasingly challenge how we tackle the preservation of monuments in the coming decades. There are questions regarding the correct conservation and restoration treatment of stained glass from the late 19th and early 20th century (stained glass from the so-called art period of Historicism), which, despite all the Guidelines for the Conservation and Restoration of this endangered genre of art, is still far from being treated with the necessary care throughout the country. The protection and preservation of the original substance—the glass, the leading and the painting—are the primary focus of interest here. Using the example of the restoration campaign currently being conducted on the windows of St. Mary’s Cathedral, Linz, a cultural monument of particular importance for Austria, work is being undertaken to elaborate the feasibility of a concept that can be easily implemented in the future at other construction sites and by all the stakeholders involved. The second monitoring project presented concerns the equally important area of “preventive conservation” of medieval and modern stained glass. The focus of the work that took place here was on checking the condition of stained glass from the Middle Ages to the 20th century (with and without exterior protective glazing) and the general identification of damage and determination of the urgency of measures for conservation (using a “traffic light system” developed for this purpose). Full article
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9 pages, 2189 KiB  
Communication
Functional or Nonfunctional Cusps Preservation for Molars Restored with Indirect Composite or Glass-Ceramic Onlays: 3D FEA Study
by Pablo Lenin Benitez Sellan, Larissa Mendes Campaner, João Paulo Mendes Tribst, Amanda Maria de Oliveira Dal Piva, Guilherme Schmitt de Andrade, Alexandre Luiz Souto Borges, Eduardo Bresciani, Antonio Lanzotti and Pietro Ausiello
Polymers 2021, 13(21), 3831; https://doi.org/10.3390/polym13213831 - 5 Nov 2021
Cited by 5 | Viewed by 3701
Abstract
Evidence regarding the effect of the onlay preparation design for different CAD/CAM restorative materials considering the preservation of cusps is lacking. Molars were 3D-modeled in four preparation designs for onlay restoration: traditional design with functional cusp coverage (TFC), non-retentive design with functional cusp [...] Read more.
Evidence regarding the effect of the onlay preparation design for different CAD/CAM restorative materials considering the preservation of cusps is lacking. Molars were 3D-modeled in four preparation designs for onlay restoration: traditional design with functional cusp coverage (TFC), non-retentive design with functional cusp coverage (NFC), traditional design with non-functional cusp coverage (TNFC) and non-retentive design with non-functional cusp coverage (NNFC). The restorations were simulated with two CAD/CAM restorative materials: LD—lithium disilicate (IPS e.max CAD) and RC—resin composite (GrandioBloc). A 100 N axial load was applied to the occlusal surface, simulating the centric contact point. Von Mises (VM) and maximum principal (Pmax) stress were evaluated for restorations, cement layer and dental substrate. The non-retentive preparation design reduced the stress concentration in the tooth structure in comparison to the conventional retentive design. For LD onlays, the stress distribution on the restoration intaglio surface showed that the preparation design, as well as the prepared cusp, influenced the stress magnitude. The non-retentive preparation design provided better load distribution in both restorative materials and more advantageous for molar structure. The resin composite restoration on thenon-functional cusp is recommended when the functional cusp is preserved in order to associate conservative dentistry and low-stress magnitude. Full article
(This article belongs to the Special Issue Bioactive Polymer Composites and Their Clinical Applications)
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11 pages, 6155 KiB  
Communication
Stress Concentration of Endodontically Treated Molars Restored with Transfixed Glass Fiber Post: 3D-Finite Element Analysis
by Alexandre Luiz Souto Borges, Manassés Tercio Vieira Grangeiro, Guilherme Schmitt de Andrade, Renata Marques de Melo, Kusai Baroudi, Laís Regiane Silva-Concilio and João Paulo Mendes Tribst
Materials 2021, 14(15), 4249; https://doi.org/10.3390/ma14154249 - 29 Jul 2021
Cited by 9 | Viewed by 3254
Abstract
The loss of dental structure caused by endodontic treatment is responsible for a decrease in tooth resistance, which increases susceptibility to fracture. Therefore, it is important that minimally invasive treatments be performed to preserve the dental structure and increase the resistance to fracture [...] Read more.
The loss of dental structure caused by endodontic treatment is responsible for a decrease in tooth resistance, which increases susceptibility to fracture. Therefore, it is important that minimally invasive treatments be performed to preserve the dental structure and increase the resistance to fracture of endodontically treated posterior teeth. To evaluate under axial loads, using the finite element method, the stress distribution in endodontically treated molars restored with both transfixed or vertical glass fiber posts (GFP) and resin composite. An endodontically treated molar 3D-model was analyzed using finite element analyses under four different conditions, class II resin composite (G1, control model), vertical glass fiber post (G2), transfixed glass fiber posts (G3) and vertical and transfixed glass fiber posts (G4). Ideal contacts were considered between restoration/resin composite and resin composite/tooth. An axial load (300 N) was applied to the occlusal surface. The resulting tensile stresses were calculated for the enamel and dentin tissue from five different viewports (occlusal, buccal, palatal, mesial and distal views). According to the stress maps, similar stress trends were observed, regardless of the glass fiber post treatment. In addition, for the G1 model (without GFP), a high-stress magnitude can be noticed in the proximal faces of enamel (7.7 to 14 MPa) and dentin (2.1 to 3.3 MPa) tissue. The use of transfixed glass fiber post is not indicated to reduce the stresses, under axial loads, in both enamel and dentin tissue in endodontically treated molar with a class II cavity. Full article
(This article belongs to the Special Issue Contemporary Dental Materials and Their Applications)
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9 pages, 3215 KiB  
Proceeding Paper
Gel-Phase Reduction of Graphene Oxide Coatings by L-Ascorbic Acid
by Mariano Palomba, Angela Longo and Gianfranco Carotenuto
Mater. Proc. 2021, 4(1), 33; https://doi.org/10.3390/IOCN2020-07783 - 10 Nov 2020
Cited by 2 | Viewed by 1915
Abstract
Reduced graphene oxide (r-GO) has physical–chemical properties like graphene and therefore it can be used for most graphene-based technological applications. r-GO is produced by chemical or thermal reduction of graphene oxide (GO). GO is a highly water-soluble organic compound that can be easily [...] Read more.
Reduced graphene oxide (r-GO) has physical–chemical properties like graphene and therefore it can be used for most graphene-based technological applications. r-GO is produced by chemical or thermal reduction of graphene oxide (GO). GO is a highly water-soluble organic compound that can be easily processed in the form of aqueous/alcoholic ink to produce thick self-standing films (i.e., GO paper) or thin coatings supported on a variety of substrates (e.g., polymers, cellulose, glass, silicon, etc.). The best GO reduction technique depends on the substrate chemical/thermal stability, and in the case of thermally unstable substrates (e.g., cellulose), the chemical approach is mandatory. However, traditional reductants, like hydrazine and phenyl-hydrazine, are highly active and therefore detrimental for the substrate. Among the mild reducing agents, L-ascorbic acid (L-aa), a green chemical reductant, has been widely investigated for GO reduction in aqueous solutions. Here, L-aa has been used to convert a GO gel-phase to r-GO by (i) swelling the GO phase with hot water, in order to allow L-aa permeation inside its lamellar structures by diffusion; and (ii) periodically restoring the reductant on the GO layer surface. According to the morphological–structural characterization (SEM, FT-IR, etc.), the proposed approach allowed GO conversion to r-GO, preserving a thin GO interfacial layer essential for a good adhesion. Full article
(This article belongs to the Proceedings of The 2nd International Online-Conference on Nanomaterials)
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36 pages, 5531 KiB  
Review
Recent Advances in Protective Coatings for Cultural Heritage–An Overview
by Alessia Artesani, Francesca Di Turo, Margherita Zucchelli and Arianna Traviglia
Coatings 2020, 10(3), 217; https://doi.org/10.3390/coatings10030217 - 29 Feb 2020
Cited by 112 | Viewed by 15761
Abstract
In the last decades, the interest in the development of protective coatings for movable and immovable Cultural Heritage (CH) assets has decidedly increased. This has been mainly prompted by the raising consciousness on preservation requirements for cultural artefacts and monuments, which has consequently [...] Read more.
In the last decades, the interest in the development of protective coatings for movable and immovable Cultural Heritage (CH) assets has decidedly increased. This has been mainly prompted by the raising consciousness on preservation requirements for cultural artefacts and monuments, which has consequently determined the development of new protective products. From acrylic resins used at the end of the last century to the up-to-date biomaterials and nanoparticles employed nowadays, the research has made a giant step forward. This article reviews the progresses, the technical challenges, and the most recent advances in protective coatings for archaeological metal, glass, and stone artefacts. It aims at offering a comprehensive and critical overview of the progressions in conservation science and displaying how research has optimized polymers in order to solve deterioration problems. Attention is given to recently developed materials, hybrid coatings, and corrosion inhibitors. This work seeks to provide a reference point for future research and to offer a wide-ranging introduction on the newly available material technologies to restorers and conservators. Full article
(This article belongs to the Section Surface Characterization, Deposition and Modification)
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14 pages, 3223 KiB  
Article
Fluorinated Bioactive Glass Nanoparticles: Enamel Demineralization Prevention and Antibacterial Effect of Orthodontic Bonding Resin
by Hyung-Jin Nam, You-Min Kim, Yong Hoon Kwon, Kyung-Hyeon Yoo, Seog-Young Yoon, In-Ryoung Kim, Bong-Soo Park, Woo-Sung Son, Seung-Min Lee and Yong-Il Kim
Materials 2019, 12(11), 1813; https://doi.org/10.3390/ma12111813 - 4 Jun 2019
Cited by 50 | Viewed by 5136
Abstract
Orthodontic treatment involving the bonding of fixed appliances to tooth surfaces can cause white spot lesions (WSLs). WSLs increase the likelihood of cavity formation and hence require preservation and prosthetic restoration. Therefore, the prevention of WSLs is of greater importance than treatment. Application [...] Read more.
Orthodontic treatment involving the bonding of fixed appliances to tooth surfaces can cause white spot lesions (WSLs). WSLs increase the likelihood of cavity formation and hence require preservation and prosthetic restoration. Therefore, the prevention of WSLs is of greater importance than treatment. Application of fluoride or the use of fluoride-containing mouthwash can prevent WSLs, but this requires patient cooperation and additional time and cost. Bioactive glass containing 2.5% fluoride was synthesized and mixed with the orthodontic bonding adhesive Transbond XT Low Flow (LV) at ratios of 1, 3, and 5% to prepare orthodontic adhesive samples. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to characterize the samples. The Vickers hardness test, bracket retention test, and adhesive remnant index (ARI) of the samples were analysed to determine their mechanical properties. To determine the biological cytotoxicity, the cell activity of the samples was evaluated using cell viability tests and the antibacterial activity was analysed using Streptococcus mutans. To evaluate the anti-demineralization effect, the sample was bonded to extracted teeth and a pH cycle test was performed. Micro computed tomography data were obtained from the bonded teeth and sample, and the anti-demineralization effect was evaluated using the ImageJ software program. The Vickers hardness of the sample was higher than that of LV and was dependent on the concentration of fluoride-containing bioactive glass (FBAG). The bracket retention test and ARI of the sample showed no significant differences from those of LV. The cell viability test showed no significant changes at 24 and 48 h after application of the sample. The fluoride ion release test indicated an ion release rate of 9.5–17.4 μg/cm2. The antibacterial activity of the experimental group containing FBAG was significantly higher than that of the LV group. The anti-demineralization test showed a concentration-dependent increase. However, the resin containing 5 mass% FBAG (FBAG5) showed a statistically-significant increase compared with LV. The orthodontic adhesive containing FBAG showed antibacterial and anti-demineralization effects, thus indicating possible WSL prevention activity. Full article
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15 pages, 9447 KiB  
Article
Electrospun Filaments Embedding Bioactive Glass Particles with Ion Release and Enhanced Mineralization
by Francesca Serio, Marta Miola, Enrica Vernè, Dario Pisignano, Aldo R. Boccaccini and Liliana Liverani
Nanomaterials 2019, 9(2), 182; https://doi.org/10.3390/nano9020182 - 1 Feb 2019
Cited by 22 | Viewed by 5611
Abstract
Efforts in tissue engineering aim at creating scaffolds that mimic the physiological environment with its structural, topographical and mechanical properties for restoring the function of damaged tissue. In this study we introduce composite fibres made by a biodegradable poly(lactic acid) (PLLA) matrix embedding [...] Read more.
Efforts in tissue engineering aim at creating scaffolds that mimic the physiological environment with its structural, topographical and mechanical properties for restoring the function of damaged tissue. In this study we introduce composite fibres made by a biodegradable poly(lactic acid) (PLLA) matrix embedding bioactive silica-based glass particles (SBA2). Electrospinning is performed to achieve porous PLLA filaments with uniform dispersion of bioactive glass powder. The obtained composite fibres show in aligned arrays significantly increased elastic modulus compared with that of neat polymer fibres during uniaxial tensile stress. Additionally, the SBA2 bioactivity is preserved upon encapsulation as highlighted by the promoted deposition of hydroxycarbonate apatite (HCA) upon immersion in simulated body fluid solutions. HCA formation is sequential to earlier processes of polymer erosion and ion release leading to acidification of the surrounding solution environment. These findings suggest PLLA-SBA2 fibres as a composite, multifunctional system which might be appealing for both bone and soft tissue engineering applications. Full article
(This article belongs to the Special Issue Electrospun Nanofibers for Biomedical Applications)
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