Search Results (548)

Grout propagation is a critical aspect of fracture grouting. This study investigated grout propagation at fracture intersections under flowing conditions using a simplified two-dimensional (2D) fracture network. Transparent soil technology was employed to simulate the porous filling material within the fractures. The results showed that the penetration velocity of grout decreased significantly after passing through an intersection, and the velocity in the main fracture was consistently higher than that in the branch fractures. In the unfilled fracture network, the diffusion ratio between branch and main fractures ranged from 0.35 to 0.88, whereas after filling, it ranged from 0.71 to 0.86. For each intersection, the ratio of grout length in the downstream branch to that in the main fracture (RDM) was positively correlated with branch width. This trend was especially evident in unfilled fractures, whereas in filled fractures, the increase in RDM was much less pronounced. Regarding the upstream ratio (RUM), it was consistently lower than RDM. RUM increased with branch width in unfilled fractures but decreased in filled fractures. Additionally, higher fluid velocity amplified these anisotropic propagation behaviors. Based on the simplified filled fracture model, it was concluded that porous filling materials reduce permeability differences between fractures with different aperture widths. Furthermore, increased flow rate intensified the anisotropic diffusion of grout. This study provides valuable insight into the mechanism of anisotropic grout propagation and offers guidance for engineering grouting applications. Full article

Drilling fluid losses into formation voids are among the major issues that lead to increases in the costs and nonproductive time of operations. Lost circulation materials have been widely used to stop or mitigate losses. In most cases, the size of the loss zone is not known, making conventional lost circulation materials unsuitable for plugging the loss zone. In this study, novel temperature-sensitive LCM (TS-LCM) particles composed of diglycidyl ether of bisphenol A (DGEBA) and 4,4′-diaminodiphenyl methane were prepared. It is a thermal-response shape-memory polymer. The molecular structure was analyzed by Fourier transform infrared spectroscopy. The glass transition temperature (T_g) was tested by Different scanning calorimetry (DSC). The shape-memory properties were evaluated by a bend-recovery test instrument. The expansion and mechanical properties of particles were investigated under high temperature and high pressure. Fracture sealing testing apparatus was used to evaluate sealing performance. The mechanism of sealing fracture was discussed. Research results indicated that the T_g of the TS-LCM was 70.24 °C. The shape fixation ratio was more than 99% at room temperature, and the shape recovery ratio was 100% above the T_g. The particle was flaky before activation. It expanded to a cube shape, and the thickness increased when activated. The rate of particle size increase for D90 was more than 60% under 120 °C and 20 MPa. The activated TS-LCM particles had high crush strength. The expansion of the TS-LCM particles could self-adaptively bridge and seal the fracture without knowing the width. The addition of TS-LCM particles could seal the tapered slot with entrance widths of 2 mm, 3 mm and 4 mm without changing the lost circulation material formulation. The developed TS-LCM has good compatibility with local saltwater-based drilling fluid. In field tests in the Yan’an area of the Ordos Basin, 15 shale oil horizontal wells were plugged with excellent results. The equivalent circulating density of drilling fluid leakage increased by an average of 0.35 g/cm³, and the success rate of plugging malignant leakage increased from 32% to 82.5%. The drilling cycle was shortened by an average of 14.3%, and the effect of enhancing the pressure-bearing capacity of the well wall was significant. The prepared TS-LCM could cure fluid loss in a fractured formation efficiently. It has good prospects for promotion. Full article

This study investigates the fracture behavior of recycled aggregate concrete by integrating fractal theory and empirical modeling to quantify how recycled coarse aggregates (RCAs) and recycled fine aggregates (RFAs) influence crack complexity and maximum crack width under varying content and loads. The results reveal distinct scale-dependent behaviors between RCA and RFA. For RCA, moderate dosages enhance fractal complexity (a measure of surface roughness) by promoting micro-crack proliferation, while excessive RCA reduces complexity due to matrix homogenization. In contrast, RFA significantly increases both fractal complexity and crack width under equivalent loads, reflecting its susceptibility to micro-scale interfacial transition zone (ITZ) degradation. Non-linear thresholds are identified: RCA’s fractal complexity plateaus at high loads as cracks coalesce into fewer dominant paths, while RFA’s crack width growth decelerates at extreme dosages due to balancing effects like particle packing. Empirical models link aggregate dosage and load to fractal dimension and crack width with high predictive accuracy (R² > 0.85), capturing interaction effects such as RCA’s load-induced complexity reduction and RFA’s load-driven crack width amplification. Secondary analyses further demonstrate that fractal dimension correlates with crack width through non-linear relationships, emphasizing the coupled nature of micro- and macro-scale damage. These findings challenge conventional design assumptions by differentiating the impacts of RCA (macro-crack coalescence) and RFA (micro-crack proliferation), providing actionable thresholds for optimizing mix designs. The study also advances sustainable material design by offering a scientific basis for updating standards to accommodate higher recycled aggregate percentages, supporting circular economy goals through reduced carbon emissions and waste diversion, and laying the groundwork for resilient, low-carbon infrastructure. Full article

Hydrate-based CO₂ sequestration is considered one of the most promising methods in the field of carbon capture, utilization, and storage. The abundant fractured environments in marine sediments provide an ideal setting for the sequestration of CO₂ hydrate. Investigating the kinetics and morphological characteristics of CO₂ hydrate formation within fractures is a critical prerequisite for achieving efficient and safe CO₂ sequestration using hydrate technology in subsea environments. Based on the aforementioned considerations, the kinetic experiments on the formation, dissociation, and reformation of CO₂ hydrates were conducted using a high-pressure visualization experimental system in this study. The kinetic behaviors and morphological characteristics of CO₂ hydrates within sandstone fractures were comprehensively investigated. Particular emphasis was placed on analyzing the effects of fracture width, type, and surface roughness on the processes of hydrate formation, dissociation, and reformation. The experimental results indicate the following: (1) At a formation pressure of 2.9 MPa, the 10 mm width fracture exhibited the shortest induction time, the longest formation duration, and the highest hydrate yield (approximately 0.52 mol) compared to the other two fracture widths. The formed CO₂ hydrates exhibited a smooth, thin-walled morphology. (2) In X-type fractures, the formation of CO₂ hydrates was characterized by concurrent induction and dissolution processes. Compared to I-type fractures, the hydrate formation process in X-type fractures exhibited shorter formation durations and generally lower hydrate yields. (3) An increase in fracture roughness enhances the number of nucleation sites for the formation of hydrates. In both fracture types (I-type and X-type), the induction time for CO₂ hydrate formation was nearly negligible. However, a significant difference in the trend of formation duration was observed under varying roughness conditions. (4) Hydrate dissociation follows a diffusion-controlled mechanism, progressing from the fracture walls towards the interior. The maximum gas production was achieved in the 10 mm-width fracture, reaching 0.24 mol, indicating optimal heat and mass transfer conditions under this configuration. (5) During the reformation process, the induction time was significantly shortened due to the “memory effect.” However, the hydrate yield after the reformation process remained consistently lower than that of the first formation, which is primarily attributed to the high solubility of CO₂ in the aqueous phase. Full article

In this study, under varying PDSP (plunging depths of stirring pin) and process parameters, refill friction stir spot welding tests were performed on 6061-T6 aluminum alloy, relying on a stirring tool with a 12 mm sleeve diameter and an 8 mm stirring pin diameter. The results manifested the internal defects in the weld zone when PDSP was 0, notwithstanding the alterations in process parameters. However, these flaws disappeared when PDSP was 0.5 mm and 1 mm. In the weld zone, PDSP exerted a dramatic effect on the internal metal flow state, particularly the curvature of the “Hook” shape and the width of the bonding ligament. It changed the downward bending of the ‘Hook’ into an upward one, influencing the fracture behavior of the weld zone and elevating the ULSF (ultimate lap shear force) by up to 20% (PDSP = 0.5 mm, welding speed = 30 mm/min, rotation speed is 1200 rpm). Besides, the PDSP intensified the PAZ (pin affected zone) pressure, induced more metal flowing into the SAZ (sleeve affected zone), thus reinforced the SAZ-TMAZ(thermomechanically affected zone) bonding strength, and upgraded the region’s microhardness. In summary, the PDSP is commendable for bolstering the weld zone’s performance, but excessively large PDSP values incur drastic indentations in the PAZ, which diminish the ULSF. Full article

This study investigates the mechanisms of gas-containing tectonic coal outbursts by modeling tectonic coal and gas as analogous to soil and pore water. Analytical methods from soil mechanics, specifically those related to quicksand and seismic liquefaction, are employed to classify these outbursts into two types: “quicksand type” and “fluidization type.” Their formation mechanisms are elucidated based on a fracture network model and a one-dimensional seepage failure criterion developed for tectonic coal. The findings indicate that “quicksand type” outbursts result from the continuous detachment of tectonic coal slices within the pressure relief zone under gas seepage pressure. The thickness-to-radius ratio of these coal slices increases with rising gas pressure but decreases with increasing coal strength and normal geostress. A larger thickness-to-radius ratio signifies a more pronounced granular characteristic and accelerates the development of coal and gas outbursts. “Fluidization type” outbursts occur when the effective stress drops to zero, resulting in a complete loss of coal strength. These outbursts represent a specific case of “quicksand type” outbursts and can be triggered by vibrations. The susceptibility of tectonic coal to outbursts is attributed to its low mechanical strength and the presence of dense fractures, which increase the acting area of seepage pressure and, consequently, raise the overall seepage force. According to this analysis, the depth of outburst cavities is generally less than the width of the pressure relief zone, which can result in delayed outbursts. This study enhances the understanding of quicksand and seismic liquefaction theories in soil mechanics and provides valuable guidance for predicting and mitigating coal and gas outbursts. Full article

To reveal the fracture mechanism of overburden aquifers during mining under anticlinal structural zones in western mining areas, this study takes Panel 1309 of the Guojiahe Coal Mine as the engineering background and employs field investigations, physical similarity simulation, and numerical simulation methods to systematically investigate the overburden fracture and crack evolution laws during extra-thick coal seam mining in anticlinal zones. The research results demonstrate the following: (1) The large slope angle of the anticlinal zone and significant elevation difference between slope initiation points and the axis constitute the primary causes of water inrush-induced support failures in working face 1309. The conglomerate of the Yijun Formation serves as the critical aquifer responsible for water inrush, while the coarse sandstone in the Anding Formation acts as the key aquiclude. (2) Influenced by the slope angle, both overburden fractures and maximum bed separation zones during rise mining predominantly develop toward the goaf side. The water-conducting fracture zone initially extends in the advance direction, when its width is greater than its height, and changes to a height greater than its width when the key aquifer fractures and connects to the main aquifer. (3) The height of the collapse zone of the working face is 65 m, and the distribution of broken rock blocks in the collapse zone is disordered; after the fracture of the water-insulating key layer, the upper rock layer is synchronously fractured and activated, and the water-conducting fissure leads to the water-conducting layer of the Yijun Formation. (4) Compared to the periodic ruptures of the main roof, the number of fractures and their propagation speed are greater during the initial ruptures of each stratum. Notably, the key aquiclude’s fracture triggers synchronous collapse of overlying strata, generating the most extensive and rapidly developing fracture networks. (5) The fracture surface on the mining face side and the overlying strata separation zone jointly form a “saddle-shaped” high-porosity area, whose distribution range shows a positive correlation with the working face advance distance. During the mining process, the porosity variation in the key aquiclude undergoes three distinct phases with advancing distance: first remaining stable, then increasing, and finally decreasing, with porosity reaching its peak when the key stratum fractures upon attaining its ultimate caving interval. Full article

This study addresses the critical challenge of optimizing coal pillar width in burst-prone mines with thick, hard roof strata, balancing resource recovery, roadway stability, and coal burst mitigation. Through integrated analytical modeling and rigorously calibrated numerical simulations, the research reveals the complex interplay between pillar width, roof mechanics, and stress redistribution. Key findings demonstrate that pillar width dictates roof failure mechanics and energy accumulation. The case study indicates that increasing the coal pillar width from 6 m to 20 m shifts the tensile fracture location from solid coal toward the pillar center, migrates shear failure zones closer to roadways, and relocates elastic strain energy accumulation to the pillar area. This concentrates static and dynamic loads directly onto wider pillars upon roof fracture, escalating instability risks. A risky coal pillar width is identified as 10–20 m, where pillars develop severe lateral abutment pressures perilously close to roadways, combining high elastic energy storage with exposure to roof fracture dynamics. Conversely, narrow pillars exhibit low stress concentrations and limited energy storage due to plastic deformation, reducing burst potential despite requiring robust asymmetric support. Strategic selection of narrow or wide pillars provides a safer pathway. The validated analytical–numerical framework offers a scientifically grounded methodology for pillar design under hard roof conditions, enhancing resource recovery while mitigating coal burst risks. Full article

In deep shale gas fracturing, the narrow width of micro fractures presents a challenge for conventional proppants (40/70 mesh, 70/140 mesh), which often fail to enter branch fractures, resulting in inadequate effective support volume. To address this, a high-efficiency propping strategy is proposed based on the hybrid use of micro-proppants and conventional proppants. Utilizing a proppant transport experiment device, the effects of proppant size ratios and injection timing on proppant distribution were investigated to determine the optimal design parameters. The results indicate that the 200/400 mesh micro-proppant can effectively enter the distal micro fractures, thereby mitigating the problem of the non-uniform distribution of the proppant within the fracture network. To ensure effective propping of secondary fractures, the optimal pumping sequence is to inject quartz sand first, followed by ceramic proppants. The recommended ratio of 70/140 mesh quartz sand to 40/70 mesh ceramic proppants is 7:3. Additionally, for blended injection, the optimal mixing ratio of 70/140 mesh quartz sand to micro-proppant is 8:2. Field trials at the L-X1 well in the LZ block demonstrate that this strategy significantly boosts post-fracturing production, with test yields increasing 2.4 to 4 times. Full article

Direct copper-plated ceramic (DPC) substrates have emerged as a favored solution for power device packaging due to their unique technical advantages. AuSn, characterized by its high hermeticity and environmental adaptability, represents the optimal sealing technology for DPC substrates. Through the application of vacuum sintering techniques and adjustment of peak temperatures (325 °C, 340 °C, and 355 °C), the morphology and composition of interfacial compounds were systematically investigated, along with an analysis of their formation mechanisms. A gradient aging experiment was designed (125 °C/150 °C/175 °C × oxygen/argon dual atmosphere × 600 h) to elucidate the synergistic effects of environmental temperature and atmosphere on the growth of intermetallic compounds (IMCs). The results indicate that the primary reaction in the sealing weld seam involves Ni interacting with Au-Sn to form (Ni, Au)₃Sn₂ and Au₅Sn. However, upon completion of the sealing process, this reaction remains incomplete, leading to a coexistence state of (Ni, Au)₃Sn₂, Au₅Sn, and AuSn. Additionally, Ni diffuses into the weld seam center via dendritic fracture and locally forms secondary phases such as δ(Ni) and ζ’(Ni). These findings suggest that the weld seam interface exhibits a complex, irregular, and asymmetric microstructure comprising multiple coexisting compounds. It was determined that Tpeak = 325 °C to 340 °C represents the ideal welding temperature range, where the weld seam morphology, width, and Ni diffusion degree achieve optimal states, ensuring excellent device hermeticity. Aging studies further demonstrate that IMC growth remains within controllable limits. These findings address critical gaps in the understanding of the microstructural evolution and interface characteristics of asymmetric welded joints formed by multi-material systems. Full article

Deep coalbed methane (CBM) reservoirs are characterized by high hydrocarbon content and are considered an important strategic resource. Due to their inherently low permeability and porosity, horizontal well drilling is commonly employed to enhance production, with the length of the horizontal section playing a critical role in determining CBM output. However, during extended horizontal drilling, wellbore instability frequently occurs as a result of drilling fluid invasion into the coal formation, posing significant safety challenges. This instability is primarily caused by the physical intrusion of drilling fluids and their interactions with the coal seam, which alter the mechanical integrity of the formation. To address these challenges, interpenetrating and semi-interpenetrating network (IPN/s-IPN) hydrogels have gained attention due to their superior physicochemical properties. This material offers enhanced sealing and support performance across fracture widths ranging from micrometers to millimeters, making it especially suited for plugging applications in deep CBM reservoirs. A self-degradable interpenetrating double-network hydrogel particle plugging agent (SSG) was developed in this study, using polyacrylamide (PAM) as the primary network and an ionic polymer as the secondary network. The SSG demonstrated excellent thermal stability, remaining intact for at least 40 h in simulated formation water at 120 °C with a degradation rate as high as 90.8%, thereby minimizing potential damage to the reservoir. After thermal aging at 120 °C, the SSG maintained strong plugging performance and favorable viscoelastic properties. A drilling fluid containing 2% SSG achieved an invasion depth of only 2.85 cm in an 80–100 mesh sand bed. The linear viscoelastic region (LVR) ranged from 0.1% to 0.98%, and the elastic modulus reached 2100 Pa, indicating robust mechanical support and deformation resistance. Full article

Background/Objectives: Platelets play a role in bone metabolism and fracture healing. This study aimed to investigate the association between platelet indices and the derived systemic immune inflammation index (SII) with fracture risk in postmenopausal women. Methods: Platelet count, mean platelet volume, platelet distribution width (PDW), platelet crit, percentage of large platelets (P-LCR), platelet–lymphocyte ratio, and the SII, calculated as (NxP)/L, where N, P, and L represented neutrophils, platelets and lymphocytes counts, respectively, were evaluated. Bone mineral density (BMD) was measured using dual-energy X-ray absorptiometry. Results: A total of 124 women (mean age 68.4 ± 9 years) were stratified into two groups based on the median platelet count; the “lower platelet count group” (n = 58) had a count of 200,000 (174,000 to 226,000), while the “higher platelet count group” (n = 66) had a count of 281,500 (256,500 to 308,500). The higher platelet count group showed a higher hip fracture risk (7.4 vs. 4.5%, p = 0.08) and lower lumbar spine BMD (0.773 vs. 0.83 gr/cm², p = 0.03). By dividing the participants into two groups with higher SSI (950,848.6 ± 746,097.99) (n = 61) and lower SII (355,751.2 ± 88,662.6) (n = 63), the group with the higher SII showed the higher hip fracture risk (7.4 vs. 3.6%, p = 0.01). Univariate regression analysis revealed correlations between chronological age and PDW (r = 0.188, p = 0.047), and P-LCR (r = 0.208, p = 0.03), as well as associations between vitamin D status and P-LCR (r = −0.301, p = 0.034), and between SII and hip fracture risk (r = 0.12, p = 0.007). Conclusions: Platelet count and SII were associated with fracture risk in postmenopausal women undergoing osteoporosis assessment. Given their reproducibility and cost-effectiveness, these markers warrant further investigation in future prospective studies focused on bone fragility. Full article

Horizontal well fracturing is vital for low-permeability tight oil reservoirs, but multi-fracture effectiveness is hampered by stress shadowing and fluid-rock interactions, particuarly in optimizing fracture geometry and conductivity under different sequencing strategies. While previous studies have addressed aspects of pore pressure and stress effects, a comprehensive comparison of sequencing strategies using fully coupled models capturing the intricate seepage–stress–damage interactions remains limited. This study employs a novel 2D fully coupled XFEM model to quantitatively evaluate three fracturing approaches: simultaneous, sequential, and alternating. Numerical results demonstrate that sequential and alternating strategies alleviate stress interference, increasing cumulative fracture length by 20.6% and 26.1%, respectively, versus conventional simultaneous fracturing. Based on the research findings, fracture width reductions are 30.44% (simultaneous), 18.78% (sequential), and 7.21% (alternating). As fracture width directly governs conductivity—the critical parameter determining hydrocarbon flow efficiency—the alternating strategy’s superior width preservation (92.79% retention) enables optimal conductivity design. These findings provide critical insights for designing fracture networks with targeted dimensions and conductivity in tight reservoirs and offer a practical basis to optimize fracture sequencing design. Full article

The anode assembly, as a key component in the electrolytic aluminum process, is composed of steel claws and aluminum guide rods. The connection quality between the steel claws and guide rods directly affects the current conduction efficiency, energy consumption, and operational stability of equipment. Achieving high-quality joining between the aluminum alloy and steel has become a key process in the preparation of the anode assembly. To join the guide rods and steel claws, this work uses Cold Metal Transfer (CMT) technology to clad aluminum on the steel surface and employs machine vision to detect surface forming defects in the cladding layer. The influence of different currents on the interfacial microstructure and mechanical properties of aluminum alloy cladding on the steel surface was investigated. The results show that increasing the cladding current leads to an increase in the width of the fusion line and grain size and the formation of layered Fe₂Al₅ intermetallic compounds (IMCs) at the interface. As the current increases from 90 A to 110 A, the thickness of the Al-Fe IMC layer increases from 1.46 μm to 2.06 μm. When the current reaches 110 A, the thickness of the interfacial brittle phase is the largest, at 2 ± 0.5 μm. The interfacial region where aluminum and steel are fused has the highest hardness, and the tensile strength first increases and then decreases with the current. The highest tensile strength is 120.45 MPa at 100 A. All the fracture surfaces exhibit a brittle fracture. Full article

A Cu-11.85Al-3.2Mn-0.1Ti shape memory alloy (SMA) with excellent superelasticity and shape memory effect was successfully fabricated via selective laser melting (SLM). Increasing the energy density enhanced grain refinement, achieving a 90% refinement rate compared to cast alloy, with an average width of ~0.15 µm. Refined martensite lowered transformation temperatures and increased thermal hysteresis. Nanoscale Cu₂TiAl phases precipitated densely within the matrix, forming a dual strengthening network combining precipitation hardening and dislocation hardening. This mechanism yielded a room-temperature tensile strength of 829.07 MPa, with 6.38% fracture strain. At 200 °C, strength increased to 883.68 MPa, with 12.26% strain. The maximum tensile strength represents a nearly 30% improvement on existing laser-melted quaternary Cu-based SMAs. Full article