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18 pages, 7553 KiB  
Article
Investigating Experimental and Computational Fluid Dynamics of 3D-Printed TPMS and Lattice Porous Structures
by Guru Varun Penubarthi, Kishore Bhaskar Suresh Babu, Senthilkumar Sundararaj and Shung Wen Kang
Micromachines 2025, 16(8), 883; https://doi.org/10.3390/mi16080883 - 29 Jul 2025
Viewed by 129
Abstract
This study investigates the capillary performance and wetting behavior of SLA (Stereolithography) 3D-printed porous structures, focusing on TPMS (triply periodic minimal surfaces)-Gyroid, Octet, Diamond, and Isotruss lattice designs. High-speed imaging was used to analyze droplet interactions, including penetration, spreading, and contact angles, with [...] Read more.
This study investigates the capillary performance and wetting behavior of SLA (Stereolithography) 3D-printed porous structures, focusing on TPMS (triply periodic minimal surfaces)-Gyroid, Octet, Diamond, and Isotruss lattice designs. High-speed imaging was used to analyze droplet interactions, including penetration, spreading, and contact angles, with 16 μL water droplets dropping from 30 mm at 0.77 m/s. Results showed variable contact angles, with Isotruss and Octet having higher angles, while Diamond faced measurement challenges due to surface roughness. Numerical simulations of TPMS-Gyroid of 2 mm3 unit cells validated the experimental results, and Diamond, Octet, and Isotruss structures were simulated. Capillary performance was assessed through deionized (DI) water weight–time (w-t) measurements, identifying that the TPMS-Gyroid structure performed adequately. Structures with 4 mm3 unit cells had low capillary performance, excluding them from permeability testing, whereas smaller 2 mm3 structures demonstrated capillary effects but had printability and cleaning issues. Permeability results indicated that Octet performed best, followed by Isotruss, Diamond, and TPMS-Gyroid. Findings emphasize unit cell size, beam thickness, and droplet positioning as key factors in optimizing fluid dynamics for cooling, filtration, and fluid management. Full article
(This article belongs to the Special Issue Micro Thermal Devices and Their Applications, 2nd Edition)
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20 pages, 3162 KiB  
Article
Study on Separation of Desulfurization Wastewater in Ship Exhaust Gas Cleaning System with Rotating Dynamic Filtration
by Shiyong Wang, Juan Wu, Yanlin Wu and Wenbo Dong
Membranes 2025, 15(7), 214; https://doi.org/10.3390/membranes15070214 - 18 Jul 2025
Viewed by 362
Abstract
Current treatment methods for desulfurization wastewater in the ship exhaust gas cleaning (EGC) system face several problems, including process complexity, unstable performance, large spatial requirements, and high energy consumption. This study investigates rotating dynamic filtration (RDF) as an efficient treatment approach through experimental [...] Read more.
Current treatment methods for desulfurization wastewater in the ship exhaust gas cleaning (EGC) system face several problems, including process complexity, unstable performance, large spatial requirements, and high energy consumption. This study investigates rotating dynamic filtration (RDF) as an efficient treatment approach through experimental testing, theoretical analysis, and pilot-scale validation. Flux increases with temperature and pressure but decreases with feed concentration, remaining unaffected by circulation flow. For a small membrane (152 mm), flux consistently increases with rotational speed across all pressures. For a large membrane (374 mm), flux increases with rotational speed at 300 kPa but firstly increases and then decreases at 100 kPa. Filtrate turbidity in all experiments complies with regulatory standards. Due to the unique hydrodynamic characteristics of RDF, back pressure reduces the effective transmembrane pressure, whereas shear force mitigates concentration polarization and cake layer formation. Separation performance is governed by the balance between these two forces. The specific energy consumption of RDF is only 10–30% that of cross-flow filtration (CFF). Under optimized pilot-scale conditions, the wastewater was concentrated 30-fold, with filtrate turbidity consistently below 2 NTU, outperforming CFF. Moreover, continuous operation proves more suitable for marine environments. Full article
(This article belongs to the Section Membrane Applications for Water Treatment)
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19 pages, 2239 KiB  
Article
Optimization of Vertical Ultrasonic Attenuator Parameters for Reducing Exhaust Gas Smoke of Compression–Ignition Engines: Efficient Selection of Emitter Power, Number, and Spacing
by Adil Kadyrov, Łukasz Warguła, Aliya Kukesheva, Yermek Dyssenbaev, Piotr Kaczmarzyk, Wojciech Klapsa and Bartosz Wieczorek
Appl. Sci. 2025, 15(14), 7870; https://doi.org/10.3390/app15147870 - 14 Jul 2025
Viewed by 268
Abstract
Compression–ignition engines emit particulate matter (PM) (soot), prompting the widespread use of diesel particulate filters (DPFs) in the automotive sector. An alternative method for PM reduction involves the use of ultrasonic waves to disperse and modify the structure of exhaust particles. This article [...] Read more.
Compression–ignition engines emit particulate matter (PM) (soot), prompting the widespread use of diesel particulate filters (DPFs) in the automotive sector. An alternative method for PM reduction involves the use of ultrasonic waves to disperse and modify the structure of exhaust particles. This article presents experimental results of the effects of ultrasonic emitter parameters, including the number, arrangement, and power, along with the engine speed, on the exhaust smoke density. Tests were conducted on a laboratory prototype equipped with six ultrasonic emitters spaced 0.17 m apart. The exhaust source was a diesel engine from a construction excavator, based on the MTZ-80 tractor design, delivering 80 HP and a displacement of 4750 cm3. A regression model was developed to describe the relationship between the engine speed, emitter power and spacing, and smoke density. The optimal configuration was found to involve an emitter power of 319.35 W and a spacing of 1.361 m for a given engine speed. Under the most effective conditions—an engine speed of 1500 rpm, six active emitters, and a total power of 600 W—smoke emissions were reduced by 18%. These findings support the feasibility of using ultrasonic methods as complementary or alternative exhaust gas filtration techniques for non-road diesel engines. Full article
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22 pages, 8597 KiB  
Article
Mitigation of Membrane Fouling in Lignin Recovery from Black Liquor via Surface-Patterned Ceramic Membrane
by Weikang Wang, Ning Kuang, Wenjie Zhao and Qingdang Li
Polymers 2025, 17(10), 1424; https://doi.org/10.3390/polym17101424 - 21 May 2025
Viewed by 427
Abstract
Among the various methods for recovering lignin from black liquor, membrane separation has gained prominence in the paper industry due to its advantages of uniform molecular weight distribution, high recovery rates, and absence of secondary pollution. However, over time, lignin particles tend to [...] Read more.
Among the various methods for recovering lignin from black liquor, membrane separation has gained prominence in the paper industry due to its advantages of uniform molecular weight distribution, high recovery rates, and absence of secondary pollution. However, over time, lignin particles tend to deposit and form a cake layer on the membrane surface, leading to membrane fouling and a decline in filtration flux. To address this issue, this study investigates the construction of ceramic membranes with radial rib patterns, and examines the effects of different trans-membrane pressure differences and radial rib patterns on membrane surface shear force and particle deposition. The research findings indicate that at a trans-membrane pressure difference of 0.5 bar and a blade rotation speed of 1000 r/min, the membrane surface experiences the highest shear force. Compared with those without patterns, ceramic membranes with radial rib patterns can more effectively delay the deposition of particles. Furthermore, it was observed that ceramic membranes combining coarse and fine rib patterns exhibit a more pronounced increase in membrane surface shear force. Full article
(This article belongs to the Special Issue Lignin Isolation, Characterization and Application)
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14 pages, 4259 KiB  
Article
Preparation and Performance of a Grid-Based PCL/TPU@MWCNTs Nanofiber Membrane for Pressure Sensor
by Ping Zhu and Qian Lan
Sensors 2025, 25(10), 3201; https://doi.org/10.3390/s25103201 - 19 May 2025
Viewed by 652
Abstract
The intrinsic trade-off among sensitivity, response speed, and measurement range continues to hinder the wider adoption of flexible pressure sensors in areas such as medical diagnostics and gesture recognition. In this work, we propose a grid-structured polycaprolactone/thermoplastic-polyurethane nanofiber pressure sensor decorated with multi-walled [...] Read more.
The intrinsic trade-off among sensitivity, response speed, and measurement range continues to hinder the wider adoption of flexible pressure sensors in areas such as medical diagnostics and gesture recognition. In this work, we propose a grid-structured polycaprolactone/thermoplastic-polyurethane nanofiber pressure sensor decorated with multi-walled carbon nanotubes (PCL/TPU@MWCNTs). By introducing a gradient grid membrane, the strain distribution and reconstruction of the conductive network can be modulated, thereby alleviating the conflict between sensitivity, response speed, and operating range. First, static mechanical simulations were performed to compare the mechanical responses of planar and grid membranes, confirming that the grid architecture offers superior sensitivity. Next, PCL/TPU@MWCNT nanofiber membranes were fabricated via coaxial electrospinning followed by vacuum-filtration and assembled into three-layer planar and grid piezoresistive pressure sensors. Their sensing characteristics were evaluated by simple index-finger motions and slide the mouse wheel identified. Within 0–34 kPa, the sensitivities of the planar and grid sensors reached 1.80 kPa−1 and 2.24 kPa−1, respectively; in the 35–75 kPa range, they were 1.03 kPa−1 and 1.27 kPa−1. The rise/decay times of the output signals were 10.53 ms/11.20 ms for the planar sensor and 9.17 ms/9.65 ms for the grid sensor. Both sensors successfully distinguished active index-finger bending at 0–0.5 Hz. The dynamic range of the grid sensor during the extension motion of the index finger is 105 dB and, during the scrolling mouse motion, is 55 dB, affording higher measurement stability and a broader operating window, fully meeting the requirements for high-precision hand-motion recognition. Full article
(This article belongs to the Special Issue Advanced Flexible Electronics and Wearable Biosensing Systems)
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16 pages, 1147 KiB  
Article
Grape Pomace Fibres as a Sustainable Fining Agent to Ensure Red Wine Safety: A First Approach in a Continuous System
by Lucía Osete-Alcaraz, Encarna Gómez-Plaza, José Oliva-Ortiz, Miguel Ángel Cámara, Bodil Jørgensen, Ricardo Jurado-Fuentes and Ana Belén Bautista-Ortín
Foods 2025, 14(9), 1565; https://doi.org/10.3390/foods14091565 - 29 Apr 2025
Viewed by 554
Abstract
Grape pomace is the largest by-product in the oenological industry, and in recent years, there have been multiple attempts to turn it into a high-value product, such as a fining agent. However, most of these attempts have usually been conducted with low volumes [...] Read more.
Grape pomace is the largest by-product in the oenological industry, and in recent years, there have been multiple attempts to turn it into a high-value product, such as a fining agent. However, most of these attempts have usually been conducted with low volumes of wine, and/or in static conditions, using a long contact time between the fibre and wine. To speed up the fining process, this study evaluated the effectiveness of three pomace fibres and a commercial fibre in improving the safety of a young red wine, previously contaminated with ochratoxin A, histamine, and various pesticides, using a continuous filtration system. All the pomace fibres were capable of reducing the OTA concentration by around 50%, and one of the tested fibres exhibited a strong ability to decrease most of the pesticides present in the wine, with the results being even better than when this fibre was used in static conditions. All the tested fibres similarly reduced the tannin concentration of the wines, without having a major impact in the colour index. These results prove that pomace grape fibres are an effective fining agent suitable for use in a continuous filtration system, allowing for a reduction in the fining time from days to hours. Full article
(This article belongs to the Section Food Engineering and Technology)
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19 pages, 5447 KiB  
Article
A Robust Adaptive Strategy for Diesel Particulate Filter Health Monitoring Using Soot Sensor Data
by Bilal Youssef
Vehicles 2025, 7(2), 39; https://doi.org/10.3390/vehicles7020039 - 29 Apr 2025
Viewed by 625
Abstract
The transportation sector mainly relied on fossil fuel and is one of the major causes of climate change and environmental pollution. Advances in smart sensing technology are paving the way for the development of clean and intelligent vehicles that lead to a more [...] Read more.
The transportation sector mainly relied on fossil fuel and is one of the major causes of climate change and environmental pollution. Advances in smart sensing technology are paving the way for the development of clean and intelligent vehicles that lead to a more sustainable transportation system. In response, the automotive industry is actively engaging in new sensor technologies and innovative control and diagnostic algorithms that improve energy sustainability and reduce vehicle emissions. In particular, recent regulations for diesel vehicles require the integration of smart soot sensors to deal with particulate filter on-board diagnostic (OBD) challenges. Meeting the recent, more stringent OBD requirements will be difficult using traditional diagnostic approaches. This study investigates an advanced diagnostic strategy to assess particulate filter health based on resistive soot sensors and available engine variables. The sensor data are projected to generate a 2D signature that reflects the changes in filtration efficiency. A relevant feature (character) is then extracted from the generated signature that can be transformed into an analytical expression used as an indicator of DPF malfunction. The diagnostic strategy uses an adaptive approach that dynamically adjusts the signature’s characters according to the engine’s operating conditions. A correction factor is calculated using an optimization algorithm based on the integral of engine speed measurements and IMEP set points during each sensor loading period. Different cost functions have been tested and evaluated to improve the diagnostic performance. The proposed adaptive approach is model-free and eliminates the need for subsystem models, iterative algorithms, and extensive calibration procedures. Furthermore, the time-consuming and inaccurate estimation of soot emissions upstream of the DPF is avoided. It was evaluated on a validated numerical platform under NEDC driving conditions with simultaneous dispersions on engine-out soot concentration and soot sensor measurements. The promising results highlight the robustness and superior performance of this approach compared to a diagnostic strategy solely reliant on sensor data. Full article
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16 pages, 37103 KiB  
Article
Mechano-Filtering Encapsulation: A Stitching-Based Packaging Strategy Implementing Active Noise Suppression in Piezoresistive Pressure Sensors
by Yi Yu, Yingying Zhao, Tao Xue, Xinyi Wang and Qiang Zou
Micromachines 2025, 16(4), 486; https://doi.org/10.3390/mi16040486 - 20 Apr 2025
Viewed by 422
Abstract
Flexible pressure sensors face the dual challenges of weak signal extraction and environmental noise suppression in wearable electronics and human-machine interfaces. This research proposes an intelligent pressure sensor utilizing chitosan/carbon nanotube/melamine sponge (CS/CNT/MS) composites, achieving high-performance sensing through a dual-stage noise reduction architecture [...] Read more.
Flexible pressure sensors face the dual challenges of weak signal extraction and environmental noise suppression in wearable electronics and human-machine interfaces. This research proposes an intelligent pressure sensor utilizing chitosan/carbon nanotube/melamine sponge (CS/CNT/MS) composites, achieving high-performance sensing through a dual-stage noise reduction architecture that combines mechanical pre-filtration and electrical synergistic regulation. An innovative compressed-stitching encapsulation technique creates pressure sensors with equivalent mechanical low-pass filtering characteristics, actively eliminating interference signals below 3 kPa while maintaining linear response within the 3–20 kPa effective loading range (sensitivity: 0.053 kPa−1). The synergistic effects of CS molecular cross-linking and CNTs’ three-dimensional conductive network endow the device with a 72 ms response time, 24 ms recovery speed, and over 3500-cycle compression stability. Successful applications in smart sport monitoring and tactile interactive interfaces demonstrate a material-structure-circuit co-design paradigm for mechanical perception in complex environments. Full article
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38 pages, 5906 KiB  
Review
Perception and Computation for Speed and Separation Monitoring Architectures
by Odysseus Adamides, Karthik Subramanian, Sarthak Arora and Ferat Sahin
Robotics 2025, 14(4), 41; https://doi.org/10.3390/robotics14040041 - 31 Mar 2025
Cited by 1 | Viewed by 1271
Abstract
Human–Robot Collaboration (HRC) has been a significant research topic within the Industry 4.0 movement over the past decade. The interest in HRC research has continued on with the dawn of Industry 5.0 focusing on worker experience. Within the study of HRC, the collaboration [...] Read more.
Human–Robot Collaboration (HRC) has been a significant research topic within the Industry 4.0 movement over the past decade. The interest in HRC research has continued on with the dawn of Industry 5.0 focusing on worker experience. Within the study of HRC, the collaboration approach of Speed and Separation Monitoring (SSM) has been implemented through various architectures. The different configuration strategies involve different perception-sensing modalities, mounting strategies, data filtration, computational platforms, and calibration methods. This paper explores the evolution of the perception architectures used to perform SSM, and highlights innovations in sensing and processing technologies that can open up the door to significant advancements in this sector of HRC research. Full article
(This article belongs to the Special Issue Embodied Intelligence: Physical Human–Robot Interaction)
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26 pages, 3050 KiB  
Review
Advancements in Circulating Tumor Cell Detection for Early Cancer Diagnosis: An Integration of Machine Learning Algorithms with Microfluidic Technologies
by Ling An, Yi Liu and Yaling Liu
Biosensors 2025, 15(4), 220; https://doi.org/10.3390/bios15040220 - 29 Mar 2025
Cited by 3 | Viewed by 2370
Abstract
Circulating tumor cells (CTCs) are vital indicators of metastasis and provide a non-invasive method for early cancer diagnosis, prognosis, and therapeutic monitoring. However, their low prevalence and heterogeneity in the bloodstream pose significant challenges for detection. Microfluidic systems, or “lab-on-a-chip” devices, have emerged [...] Read more.
Circulating tumor cells (CTCs) are vital indicators of metastasis and provide a non-invasive method for early cancer diagnosis, prognosis, and therapeutic monitoring. However, their low prevalence and heterogeneity in the bloodstream pose significant challenges for detection. Microfluidic systems, or “lab-on-a-chip” devices, have emerged as a revolutionary tool in liquid biopsy, enabling efficient isolation and analysis of CTCs. These systems offer advantages such as reduced sample volume, enhanced sensitivity, and the ability to integrate multiple processes into a single platform. Several microfluidic techniques, including size-based filtration, dielectrophoresis, and immunoaffinity capture, have been developed to enhance CTC detection. The integration of machine learning (ML) with microfluidic systems has further improved the specificity and accuracy of CTC detection, significantly advancing the speed and efficiency of early cancer diagnosis. ML models have enabled more precise analysis of CTCs by automating detection processes and enhancing the ability to identify rare and heterogeneous cell populations. These advancements have already demonstrated their potential in improving diagnostic accuracy and enabling more personalized treatment approaches. In this review, we highlight the latest progress in the integration of microfluidic technologies and ML algorithms, emphasizing how their combination has changed early cancer diagnosis and contributed to significant advancements in this field. Full article
(This article belongs to the Special Issue Microfluidics for Biomedical Applications (3rd Edition))
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15 pages, 11658 KiB  
Article
Polymer Flooding Injectivity Maintaining and Enhancement Strategies: A Field Case Study of Chinese Offshore EOR Project
by Chenxi Wang, Jian Zhang, Bo Huang, Hong Du, Xianghai Meng, Xianjie Li, Xinsheng Xue, Yi Su, Chao Li and Haiping Guo
Processes 2025, 13(3), 903; https://doi.org/10.3390/pr13030903 - 19 Mar 2025
Viewed by 641
Abstract
Polymer flooding has been gradually applied in Chinese offshore oilfields to enhance oil recovery (EOR). Injectivity loss during polymer flooding is a common issue that could cause lower displacement speed and efficiency, and eventually compromise the polymer flooding result. This paper presents a [...] Read more.
Polymer flooding has been gradually applied in Chinese offshore oilfields to enhance oil recovery (EOR). Injectivity loss during polymer flooding is a common issue that could cause lower displacement speed and efficiency, and eventually compromise the polymer flooding result. This paper presents a case study of a Chinese offshore field where injectivity loss issues were encountered in the polymer flooding project. A series of measures are applied to enhance the injectivity. The injectivity enhancement strategies are proposed and conducted from three main aspects, namely, (1) surface polymer fluid preparation; (2) downhole wellbore stimulation; and (3) reservoir–polymer compatibility, respectively. For the surface polymer fluid preparation, a series of sieve flow tests are conducted to obtain the optimal mesh size to improve the polymer fluid preparation quality and reduce the amount of “fish eyes”. The downhole wellbore stimulations involve oxidization-associated acidizing treatment and re-perforation. Polymer–reservoir compatibility tests are conducted to optimize the molecular weight (MW). Regarding the surface measures, the optimal filtration sieve mesh number is 200, which could reduce fish eyes to a desirable level without causing mesh plugging. After mesh refinement, the average injection pressure of the twelve injection wells decreases by 0.5 MPa. For the downhole stimulations, acidizing treatment are applied to six injection wells, which decreases the injection pressures by 6 to 7 MPa. For Well A, where acidizing does not work, the re-perforation measure is used and enhances the injectivity by 300%. Moreover, the laboratory and field polymer–reservoir compatibility tests show that the optimal polymer molecular weight (MW) is sixteen million. Proposed strategies applied from the surface, downhole, and reservoir aspects could be used to resolve different levels of injectivity loss, which could provide guidance for future offshore polymer projects. Full article
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28 pages, 5599 KiB  
Review
From a Spectrum to Diagnosis: The Integration of Raman Spectroscopy and Chemometrics into Hepatitis Diagnostics
by Muhammad Kashif and Hugh J. Byrne
Appl. Sci. 2025, 15(5), 2606; https://doi.org/10.3390/app15052606 - 28 Feb 2025
Cited by 3 | Viewed by 854
Abstract
Hepatitis, most importantly hepatitis B and hepatitis C, is a significant global health concern, requiring an accurate and early diagnosis to prevent severe liver damage and ensure effective treatment. The currently employed diagnostic methods, while effective, are often limited in their sensitivity, specificity, [...] Read more.
Hepatitis, most importantly hepatitis B and hepatitis C, is a significant global health concern, requiring an accurate and early diagnosis to prevent severe liver damage and ensure effective treatment. The currently employed diagnostic methods, while effective, are often limited in their sensitivity, specificity, and rapidity, and the quest for improved diagnostic tools is ongoing. This review explores the innovative application of Raman spectroscopy combined with a chemometric analysis as a powerful diagnostic tool for hepatitis. Raman spectroscopy offers a non-invasive, rapid, and detailed molecular fingerprint of biological samples, while chemometric techniques enhance the interpretation of complex spectral data, enabling precise differentiation between healthy and diseased states and moreover the severity/stage of disease. This review aims to provide a comprehensive overview of the current research, foster greater understanding, and stimulate further innovations in this burgeoning field. The Raman spectrum of blood plasma or serum provides fingerprints of biochemical changes in the blood profile and the occurrence of disease simultaneously, while Raman analyses of polymerase chain reaction/hybridization chain reaction (PCR/HCR)-amplified nucleic acids and extracted DNA/RNA as the test samples provide more accurate differentiation between healthy and diseased states. Chemometric tools enhance the diagnostic efficiency and allow for quantification of the viral loads, indicating the stage of disease. The incorporation of different methodologies like surface enhancement and centrifugal filtration using membranes provides the ability to target biochemical changes directly linked with the disease. Immunoassays and biosensors based on Raman spectroscopy offer accurate quantitative detection of viral antigens or the immune response in the body (antibodies). Microfluidic devices enhance the speed of detection through the continuous testing of flowing samples. Raman diagnostic studies with massive sample sizes of up to 1000 and multiple reports of achieving a greater than 90% differentiation accuracy, sensitivity, and specificity using advanced multivariate data analysis tools indicate that Raman spectroscopy is a promising tool for hepatitis detection. Its reproducibility and the identification of unique reference spectral features for each hepatic disease are still challenges in the translation of Raman spectroscopy as a clinical tool, however. The development of databases for automated comparison and the incorporation of automated chemometric processors into Raman diagnostic tools could pave the way for their clinical translation in the near future. Full article
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14 pages, 6595 KiB  
Article
Effect of GBF Process Conditions on the Microstructural Characteristic, Melt Quality and Mechanical Properties of Al-Si Alloys with Scrap Addition
by Minji Kim, Kyung Il Kim, Jeong-Keun Lee, Soong-Keun Hyun and Kyung-Taek Kim
Materials 2025, 18(5), 943; https://doi.org/10.3390/ma18050943 - 21 Feb 2025
Cited by 1 | Viewed by 508
Abstract
In this study, the applicability of an Al-Si alloy with 30 wt% added scrap for automobile pistons was evaluated by investigating the melt quality, microstructural characteristics, and tensile properties under modified GBF (gas bubbling filtration) process conditions, including increasing rotor rotation speed and [...] Read more.
In this study, the applicability of an Al-Si alloy with 30 wt% added scrap for automobile pistons was evaluated by investigating the melt quality, microstructural characteristics, and tensile properties under modified GBF (gas bubbling filtration) process conditions, including increasing rotor rotation speed and adjusting the air-line supply and the inclination angle of the impeller blade. The melt quality was dramatically improved under modified GBF process conditions, resulting in a very clean melt, with the D.I. value decreasing by 28%, the length of the oxide layer per kilogram decreasing by 65%, and inclusion content decreasing by 97% compared to that of the conventional GBF process conditions. Additionally, the size of primary Si decreased from 40 µm to 27 µm, and the eutectic Si and intermetallic compounds were refined, showing a very fine microstructure. The identified phases included Al4Cu2Mg8Si7, AlxCuyNiz, and MgO. The ultimate tensile strength was 275 MPa, and the elongation was 6.0%, indicating improved tensile properties compared to those of the conventional GBF process conditions. The fracture behavior changed from a brittle microcleavage fracture mode to a ductile dimple fracture mode as the primary Si, eutectic Si particles, and intermetallic compounds were refined under modified GBF process conditions. These results confirmed that Al-Si alloy with added scrap can be used as a material for automobile pistons. Full article
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10 pages, 225 KiB  
Review
History and Development of Water Treatment for Human Consumption
by Philippe Hartemann and Antoine Montiel
Hygiene 2025, 5(1), 6; https://doi.org/10.3390/hygiene5010006 - 4 Feb 2025
Cited by 1 | Viewed by 2499
Abstract
Throughout history, humans have sought to drink water that is good for their health, according to the knowledge of the time. Hippocrates’ definition of water quality, “good water should be clear, light, aerated, without any perceptible odor or taste, warm in winter and [...] Read more.
Throughout history, humans have sought to drink water that is good for their health, according to the knowledge of the time. Hippocrates’ definition of water quality, “good water should be clear, light, aerated, without any perceptible odor or taste, warm in winter and cold in summer”, remained virtually unchanged until 1887, when it was added that water should dissolve soap and foam well, be clear and colorless, have a pleasant taste, leave no large deposits after boiling, and cook vegetables and wash clothes well. This definition guided all treatments to remove the substances responsible for cloudiness, odor and discoloration, as well as the choice of resources: clear water and water with low mineral content. The discoveries by Pasteur and Koch led to the addition of microbiological criteria, like the absence of pathogens, and the definition of microbiological indicators. Throughout the 20th century, advances in scientific knowledge in microbiology, chemistry and toxicology led to major progress in treatment methods. These filtration and disinfection treatments are described here according to their historical implementation. Due to progress in numerous areas, e.g., both chemical and microbiological analytical detection limits, speed of information flow and origins of certain diseases that are discovered to be waterborne, the consumer is now exposed to anxiety-provoking news (microplastics, eternal pollutants (cf. per- and polyfluoroalkyl substances (PFASs)), drugs, pesticides residues, etc.). Thus, the consumer tends to lose confidence in tap or bottled water and turn to buying home purifiers. Drinking water treatment will continue to evolve with more sophisticated processes, as analytical progress enables us to expect further developments. Full article
(This article belongs to the Section Environmental Health)
15 pages, 4516 KiB  
Article
Optimizing the Dealkalization Process of Red Mud: Controlling Calcium Compounds to Improve Solid–Liquid Separation Performance
by Jianfei Zhou, Mengmeng Dai, Qingjun Guan, Hua Zeng, Wei Sun and Li Wang
Minerals 2025, 15(2), 150; https://doi.org/10.3390/min15020150 - 3 Feb 2025
Viewed by 827
Abstract
The acid neutralization process is widely recognized for its effectiveness in the dealkalization of red mud, and it faces challenges in solid–liquid separation due to the formation of numerous colloidal components. This study investigated the impact of calcium-containing compounds (CaO, CaCl2, [...] Read more.
The acid neutralization process is widely recognized for its effectiveness in the dealkalization of red mud, and it faces challenges in solid–liquid separation due to the formation of numerous colloidal components. This study investigated the impact of calcium-containing compounds (CaO, CaCl2, CaCO3, and CaSO4) on the solid–liquid separation and the dealkalization efficiency of red mud during the dealkalization process. The sodium leaching efficiency of the red mud reached 95.6% when the red mud was reacted with 8% of sulfuric acid for 10 min with a stirring speed and liquid to solid ratio of 700 r/min and 5:1, respectively. The replacement of sulfuric acid using simulated waste acid reached similar sodium leaching efficiency. However, the filtration rate of red mud becomes exceedingly sluggish using sulfuric acid or simulated waste acid. Adding calcium-containing compounds significantly augments the efficacy of solid–liquid separation in red mud. With a mass content of 2% for CaO or 8% for CaCl2, the filtration speed experienced a remarkable fivefold and ninefold increase, respectively. Furthermore, a simplification in the composition was observed within the leaching solution derived from red mud, thereby creating favorable conditions for the extraction of sodium. The influence mechanism was investigated with X-ray diffraction, inductively coupled plasma analysis, and scanning electron microscopy. The addition of calcium compounds led to the formation of calcium silicate and iron silicate in the leaching residue, inhibiting the generation of colloidal substances, such as silica gel. Additionally, these compounds increased the size of red mud particles, facilitating the solid–liquid separation process. This study provides valuable technical insights for the dealkalization of red mud. Full article
(This article belongs to the Section Mineral Processing and Extractive Metallurgy)
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