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Keywords = crack growth behavior

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17 pages, 1978 KiB  
Article
Analysis of Acoustic Emission Waveforms by Wavelet Packet Transform for the Detection of Crack Initiation Due to Fretting Fatigue in Solid Railway Axles
by Marta Zamorano, María Jesús Gómez, Cristina Castejon and Michele Carboni
Appl. Sci. 2025, 15(15), 8435; https://doi.org/10.3390/app15158435 - 29 Jul 2025
Viewed by 202
Abstract
Railway axles are among the most safety-critical components in rolling stock, as their failure can lead to catastrophic consequences. One of the most subtle damage mechanisms affecting these components is fretting fatigue, which is a particularly challenging damage mechanism in these components, as [...] Read more.
Railway axles are among the most safety-critical components in rolling stock, as their failure can lead to catastrophic consequences. One of the most subtle damage mechanisms affecting these components is fretting fatigue, which is a particularly challenging damage mechanism in these components, as it can initiate cracks under real service conditions and is difficult to detect in its early stages, which is vital to ensure operational safety and to optimize maintenance strategies. This paper focuses on the development of fretting fatigue damage in solid railway axles under realistic service-like conditions. Full-scale axle specimens with artificially induced notches were subjected to loading conditions that promote fretting fatigue crack initiation and growth. Acoustic emission techniques were used to monitor the damage progression, and post-processing of the emitted signals, by using wavelet-based tools, was conducted to identify early indicators of crack formation. The experimental findings demonstrate that the proposed approach allows for reliable identification of fretting-induced crack initiation, contributing valuable insights into the in-service behavior of railway axles under this damage mechanism. Full article
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17 pages, 4992 KiB  
Article
Effect of Heat Treatments and Related Microstructural Modifications on High-Cycle Fatigue Behavior of Powder Bed Fusion–Laser Beam-Fabricated Ti-6Al-2Sn-4Zr-6Mo Alloy
by Gianluca Pirro, Alessandro Morri, Alessandra Martucci, Mariangela Lombardi and Lorella Ceschini
Metals 2025, 15(8), 849; https://doi.org/10.3390/met15080849 (registering DOI) - 29 Jul 2025
Viewed by 133
Abstract
The study investigates the influence of microstructures on fatigue behavior and failure mechanisms of the α-β titanium alloy Ti6246, fabricated via Powder Bed Fusion-Laser Beam (PBF-LB). In particular, the investigation assesses the effect of two post-processing heat treatments, namely α-β annealing at 875 [...] Read more.
The study investigates the influence of microstructures on fatigue behavior and failure mechanisms of the α-β titanium alloy Ti6246, fabricated via Powder Bed Fusion-Laser Beam (PBF-LB). In particular, the investigation assesses the effect of two post-processing heat treatments, namely α-β annealing at 875 °C (AN875) and solution treatment at 825 °C followed by aging at 500 °C (STA825), on the alloy’s rotating and bending fatigue behavior. The results indicate that the STA825 condition provides superior fatigue resistance (+25%) compared to AN875, due to the presence of a finer bilamellar microstructure, characterized by thinner primary α lamellae (αp) and a more homogeneous distribution of secondary α lamellae (αs) within the β matrix. Additionally, an investigation conducted using the Kitagawa–Takahashi (KT) approach and the El-Haddad model, based on the relationship between the fatigue limit and defect sensitivity, revealed improved crack propagation resistance from pre-existing defects (ΔKth) for the STA825 condition compared to AN875. Notably, the presence of fine αs after aging for STA825 is effective in delaying crack nucleation and propagation at early stages, while refined αp contributes to hindering macrocrack growth. The fatigue behavior of the STA825-treated Ti6246 alloy was even superior to that of the PBF-LB-processed Ti64, representing a viable alternative for the production of high-performance components in the automotive and aerospace sectors. Full article
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12 pages, 16238 KiB  
Article
Degradation of HVOF-MCrAlY + APS-Nanostructured YSZ Thermal Barrier Coatings
by Weijie R. Chen, Chao Li, Yuxian Cheng, Hongying Li, Xiao Zhang and Lu Wang
Coatings 2025, 15(8), 871; https://doi.org/10.3390/coatings15080871 - 24 Jul 2025
Viewed by 282
Abstract
The degradation process of HVOF-MCrAlY + APS-nanostructured YSZ (APS-nYSZ) thermal barrier coatings, produced using gas turbine OEM-approved MCrAlY powders, is investigated by studying the TGO growth and crack propagation behaviors in a thermal cycling environment. The TGO growth yields a parabolic mechanism on [...] Read more.
The degradation process of HVOF-MCrAlY + APS-nanostructured YSZ (APS-nYSZ) thermal barrier coatings, produced using gas turbine OEM-approved MCrAlY powders, is investigated by studying the TGO growth and crack propagation behaviors in a thermal cycling environment. The TGO growth yields a parabolic mechanism on the surfaces of all HVOF-MCrAlYs, and the growth rate increases with the aluminum content in the “classical” MCrAlYs. The APS-nYSZ layer comprises micro-structured YSZ (mYSZ) and nanostructured YSZ (nYSZ) zones. Both mYSZ/mYSZ and mYSZ/nYSZ interfaces appear to be crack nucleation sites, resulting in crack propagation and consequent crack coalescence within the APS-nYSZ layer in the APS-nYSZ/HVOF-MCrAlY vicinity. Crack propagation in the TBCs can be characterized as a steady-state crack propagation stage, where crack length has a nearly linear relationship with TGO thickness, and an accelerating crack propagation stage, which is apparently a result of the coalescence of neighboring cracks. All TBCs fail in the same way as APS-/HVOF-MCrAlY + APS-conventional YSZ analogs, but the difference in thermal cycling lives is not substantial, although the HVOF-low Al-NiCrAlY encounters chemical failure in the early stage of thermal cycling. Full article
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11 pages, 2935 KiB  
Proceeding Paper
Crack Growth Modeling in CT Specimens: The Influence of Heat Treatment and Loading
by Raycho Raychev, Ivanka Delova, Tsvetomir Borisov and Yordan Mirchev
Eng. Proc. 2025, 100(1), 61; https://doi.org/10.3390/engproc2025100061 - 21 Jul 2025
Viewed by 80
Abstract
This study provides a combined numerical and analytical investigation of fatigue crack growth in compact tension specimens made of 42CrMo4 steel. Through simulations in ANSYS Workbench (SMART Crack Growth module) and numerical modeling in MATLAB, the model is validated by comparing its results [...] Read more.
This study provides a combined numerical and analytical investigation of fatigue crack growth in compact tension specimens made of 42CrMo4 steel. Through simulations in ANSYS Workbench (SMART Crack Growth module) and numerical modeling in MATLAB, the model is validated by comparing its results with the standard ASTM E399 and Paris’ law relationships. The effect of heat treatments and loading on crack growth rate was investigated. The results confirm the model’s applicability in predicting fatigue behavior in the linear–elastic region. Full article
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29 pages, 8058 KiB  
Article
Hydrogen Embrittlement Behavior and Applicability of X52 Steel in Pure Hydrogen Pipelines
by Tianlei Li, Honglin Zhang, Wentao Hu, Ke Li, Yaxi Wang and Yuanhua Lin
Materials 2025, 18(14), 3417; https://doi.org/10.3390/ma18143417 - 21 Jul 2025
Viewed by 258
Abstract
This study investigates the mechanical behavior of X52 steel pipes and their weld regions under pure hydrogen transport conditions, with a focus on assessing potential hydrogen embrittlement risks. Through experimental analysis, the research evaluates how different pipeline regions—including the base metal, weld metal, [...] Read more.
This study investigates the mechanical behavior of X52 steel pipes and their weld regions under pure hydrogen transport conditions, with a focus on assessing potential hydrogen embrittlement risks. Through experimental analysis, the research evaluates how different pipeline regions—including the base metal, weld metal, and heat-affected zones—respond to varying hydrogen pressures. Key mechanical properties such as elongation, fracture toughness, and crack growth resistance are analyzed to determine their implications for structural integrity and safety. Based on the findings, this study proposes criteria for the safety evaluation of X52 pipelines operating in hydrogen service environments. The results are intended to inform decisions regarding the repurposing of existing pipelines or the design of new infrastructure dedicated to pure hydrogen transport, offering insights into material performance and critical safety considerations for hydrogen pipeline applications. Full article
(This article belongs to the Section Mechanics of Materials)
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28 pages, 17257 KiB  
Article
A Crystal Plasticity Phase-Field Study on the Effects of Grain Boundary Degradation on the Fatigue Behavior of a Nickel-Based Superalloy
by Pengfei Liu, Zhanghua Chen, Xiao Zhao, Jianxin Dong and He Jiang
Materials 2025, 18(14), 3309; https://doi.org/10.3390/ma18143309 - 14 Jul 2025
Viewed by 378
Abstract
Grain boundary weakening in high-temperature environments significantly influences the fatigue crack growth mechanisms of nickel-based superalloys, introducing challenges in accurately predicting fatigue life. In this study, a dislocation-density-based crystal plasticity phase-field (CP–PF) model is developed to simulate the fatigue crack growth behavior of [...] Read more.
Grain boundary weakening in high-temperature environments significantly influences the fatigue crack growth mechanisms of nickel-based superalloys, introducing challenges in accurately predicting fatigue life. In this study, a dislocation-density-based crystal plasticity phase-field (CP–PF) model is developed to simulate the fatigue crack growth behavior of the GH4169 alloy under both room and elevated temperatures. Grain boundaries are explicitly modeled, enabling the competition between transgranular and intergranular cracking to be accurately captured. The grain boundary separation energy and surface energy, calculated via molecular dynamics simulations, are employed as failure criteria for grain boundary and intragranular material points, respectively. The simulation results reveal that under oxygen-free conditions, fatigue crack propagation at both room and high temperatures is governed by sustained shear slip, with crack advancement hindered by grains exhibiting low Schmid factors. When grain boundary oxidation is introduced, increasing oxidation levels progressively degrade grain boundary strength and reduce overall fatigue resistance. Specifically, at room temperature, oxidation shortens the duration of crack arrest near grain boundaries. At elevated service temperatures, intensified grain boundary degradation facilitates a transition in crack growth mode from transgranular to intergranular, thereby accelerating crack propagation and exacerbating fatigue damage. Full article
(This article belongs to the Section Metals and Alloys)
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16 pages, 9519 KiB  
Article
Effect of Post-Weld Heat Treatment on Residual Stress and Fatigue Crack Propagation Behavior in Linear Friction Welded Ti-6Al-4V Alloy
by Sungkyoung Lee, Hyunsung Choi, Yunji Cho, Min Jae Baek, Hyeonil Park, Moo-Young Seok, Yong Nam Kwon, Namhyun Kang and Dong Jun Lee
Materials 2025, 18(14), 3285; https://doi.org/10.3390/ma18143285 - 11 Jul 2025
Viewed by 323
Abstract
In this study, the effects of post-weld heat treatment (PWHT) on residual stress distribution and fatigue crack propagation (FCP) behavior in linear friction welded (LFW) Ti-6Al-4V joints were investigated. Microstructural evolution in the weld center zone (WCZ), thermomechanically affected zone (TMAZ), heat-affected zone [...] Read more.
In this study, the effects of post-weld heat treatment (PWHT) on residual stress distribution and fatigue crack propagation (FCP) behavior in linear friction welded (LFW) Ti-6Al-4V joints were investigated. Microstructural evolution in the weld center zone (WCZ), thermomechanically affected zone (TMAZ), heat-affected zone (HAZ), and base metal (BM) was characterized using scanning electron microscropy (SEM) and electron backscatter diffraction (EBSD). Mechanical properties were evaluated via Vickers hardness testing and digital image correlation (DIC)-based tensile testing. Residual stresses before and after PWHT were measured using the contour method. The LFW process introduced significant residual stresses, with tensile stresses up to 709.2 MPa in the WCZ, resulting in non-uniform fatigue crack growth behavior. PWHT at 650 °C and 750 °C effectively reduced these stresses. After PWHT, fatigue cracks propagated uniformly across the weld region, enabling reliable determination of crack growth rates. The average crack growth rates of the heat-treated specimens were comparable to those of the base metal, confirming that PWHT, particularly at 750 °C, stabilizes the fatigue crack path and relieves internal stress. Full article
(This article belongs to the Section Metals and Alloys)
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17 pages, 5651 KiB  
Article
Experimental Investigation on Fatigue Crack Propagation in Surface-Hardened Layer of High-Speed Train Axles
by Chun Gao, Zhengwei Yu, Yuanyuan Zhang, Tao Fan, Bo Zhang, Huajian Song and Hang Su
Crystals 2025, 15(7), 638; https://doi.org/10.3390/cryst15070638 - 11 Jul 2025
Viewed by 330
Abstract
This study examines fatigue crack growth behavior in induction-hardened S38C axle steel with a gradient microstructure. High-frequency three-point bending fatigue tests were conducted to evaluate crack growth rates (da/dN) across three depth-defined regions: a hardened layer, a heterogeneous transition [...] Read more.
This study examines fatigue crack growth behavior in induction-hardened S38C axle steel with a gradient microstructure. High-frequency three-point bending fatigue tests were conducted to evaluate crack growth rates (da/dN) across three depth-defined regions: a hardened layer, a heterogeneous transition zone, and a normalized core. Depth-resolved da/dN–ΔK relationships were established, and Paris Law parameters were extracted. The surface-hardened layer exhibited the lowest crack growth rates and flattest Paris slope, while the transition zone showed notable scatter due to microstructural heterogeneity and residual stress effects. These findings provide experimental insight into the fatigue performance of gradient-structured axle steels and offer guidance for fatigue life prediction and inspection planning. Full article
(This article belongs to the Special Issue Fatigue and Fracture of Crystalline Metal Structures)
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23 pages, 36557 KiB  
Article
Mixed-Mode Fracture Behavior of Penta-Graphene: A Molecular Dynamics Perspective on Defect Sensitivity and Crack Evolution
by Afia Aziz Kona, Aaron Lutheran and Alireza Tabarraei
Solids 2025, 6(3), 36; https://doi.org/10.3390/solids6030036 - 11 Jul 2025
Viewed by 544
Abstract
This study employs molecular dynamics (MD) simulations to investigate the mechanical response and fracture behavior of penta-graphene, a novel two-dimensional carbon allotrope composed entirely of pentagonal rings with mixed sp2–sp3 hybridization and pronounced mechanical anisotropy. Atomistic simulations are carried out [...] Read more.
This study employs molecular dynamics (MD) simulations to investigate the mechanical response and fracture behavior of penta-graphene, a novel two-dimensional carbon allotrope composed entirely of pentagonal rings with mixed sp2–sp3 hybridization and pronounced mechanical anisotropy. Atomistic simulations are carried out to evaluate the impact of structural defects on mechanical performance and to elucidate crack propagation mechanisms. The results reveal that void defects involving sp3-hybridized carbon atoms cause a more significant degradation in mechanical strength compared to those involving sp2 atoms. During fracture, local atomic rearrangements and bond reconstructions lead to the formation of energetically favorable ring structures—such as hexagons and octagons—at the crack tip, promoting enhanced energy dissipation and fracture resistance. A central focus of this work is the evaluation of the critical stress intensity factor (SIF) under mixed-mode (I/II) loading conditions. The simulations demonstrate that the critical SIF is influenced by the loading phase angle, with pure mode I exhibiting a higher SIF than pure mode II. Notably, penta-graphene shows a critical SIF significantly higher than that of graphene, indicating exceptional fracture toughness that is rare among ultra-thin two-dimensional materials. This enhanced toughness is primarily attributed to penta-graphene’s capacity for substantial out-of-plane deformation prior to failure, which redistributes stress near the crack tip, delays crack initiation, and increases energy absorption. Additionally, the study examines crack growth paths as a function of loading phase angle, revealing that branching and kinking can occur even under pure mode I loading. Full article
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15 pages, 2384 KiB  
Article
ANN-Based Prediction of Corrosion Behavior of Alloy 600: Implications for an Anti-Corrosion Coating Design in PWSCC Environments
by Muhammad Ishtiaq, Xiao-Song Wang, Annabathini Geetha Bhavani, Hyuk Jong Bong and Nagireddy Gari Subba Reddy
Coatings 2025, 15(7), 749; https://doi.org/10.3390/coatings15070749 - 24 Jun 2025
Viewed by 391
Abstract
The modeling of the corrosion rate of Alloy 600 in primary water stress corrosion cracking conditions (PWSCC) is a challenging task for existing as well as new structures due to the wide deviation of its composition across the worldwide PWSCC environment. The major [...] Read more.
The modeling of the corrosion rate of Alloy 600 in primary water stress corrosion cracking conditions (PWSCC) is a challenging task for existing as well as new structures due to the wide deviation of its composition across the worldwide PWSCC environment. The major parameters influencing the rate are temperature, stress intensity factor, pH, conductivity, ECP, Yield strength, B3(OH)3, and LiOH. The individual effects of these parameters on corrosion are known to some extent; however, the combined effect of these parameters together is complex, nonlinear, and unpredictable. Herein, we developed an Artificial Neural Network to predict the corrosion crack growth rate for any combination of the above five parameters and to better understand the effects of these parameters jointly on corrosion behavior. Three-dimensional mappings clearly reveal the complex interrelationship between the temperature and stress intensity factor at different variables, and the effect of the variables rather than a single variable on the corrosion rate of Inconel alloy 600 in PWSCC conditions. Moreover, the index of relative importance for these variables has also been presented providing deep insights for anti-corrosion coating designs in PWSCC environments. Full article
(This article belongs to the Special Issue Anti-corrosion Coatings of Metals and Alloys—New Perspectives)
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17 pages, 5076 KiB  
Article
Enhancing Fatigue Life Prediction Accuracy: A Parametric Study of Stress Ratios and Hole Position Using SMART Crack Growth Technology
by Yahya Ali Fageehi and Abdulnaser M. Alshoaibi
Crystals 2025, 15(7), 596; https://doi.org/10.3390/cryst15070596 - 24 Jun 2025
Viewed by 539
Abstract
This study presents a unique and comprehensive application of ANSYS Mechanical R19.2’s SMART crack growth feature, leveraging its capabilities to conduct an unprecedented parametric investigation into fatigue crack propagation behavior under a wide range of positive and negative stress ratios, and to provide [...] Read more.
This study presents a unique and comprehensive application of ANSYS Mechanical R19.2’s SMART crack growth feature, leveraging its capabilities to conduct an unprecedented parametric investigation into fatigue crack propagation behavior under a wide range of positive and negative stress ratios, and to provide detailed insights into the influence of hole positioning on crack trajectory. By uniquely employing an unstructured mesh method that significantly reduces computational overhead and automates mesh updates, this research overcomes traditional fracture simulation limitations. The investigation breaks new ground by comprehensively examining an unprecedented range of both positive (R = 0.1 to 0.5) and negative (R = −0.1 to −0.5) stress ratios, revealing previously unexplored relationships in fracture mechanics. Through rigorous and extensive numerical simulations on two distinct specimen configurations, i.e., a notched plate with a strategically positioned hole under fatigue loading and a cracked rectangular plate with dual holes under static loading, this work establishes groundbreaking correlations between stress parameters and fatigue behavior. The research reveals a novel inverse relationship between the equivalent stress intensity factor and stress ratio, alongside a previously uncharacterized inverse correlation between stress ratio and von Mises stress. Notably, a direct, accelerating relationship between stress ratio and fatigue life is demonstrated, where higher R-values non-linearly increase fatigue resistance by mitigating stress concentration, challenging conventional linear approximations. This investigation makes a substantial contribution to fracture mechanics by elucidating the fundamental role of hole positioning in controlling crack propagation paths. The research uniquely demonstrates that depending on precise hole location, cracks will either deviate toward the hole or maintain their original trajectory, a phenomenon attributed to the asymmetric stress distribution at the crack tip induced by the hole’s presence. These novel findings, validated against existing literature, represent a significant advancement in predictive modeling for fatigue life assessment, offering critical new insights for engineering design and maintenance strategies in high-stakes industries. Full article
(This article belongs to the Special Issue Fatigue and Fracture of Crystalline Metal Structures)
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16 pages, 5657 KiB  
Article
Crack Propagation Mechanism in Thermal Barrier Coatings Containing Different Residual Grit Particles Under Thermal Cycling
by Xin Shen, Zhiyuan Wei, Zhenghao Jiang, Jianpu Zhang, Dingjun Li, Xiufang Gong, Qiyuan Li, Fei Zhao, Jianping Lai and Jiaxin Yu
Coatings 2025, 15(7), 747; https://doi.org/10.3390/coatings15070747 - 23 Jun 2025
Viewed by 399
Abstract
Residual particles embedded at the bond coat/substrate (BC/SUB) interface after grit blasting can affect the failure behavior of thermal barrier coatings (TBCs) under thermal cycling. This study employed a 2D finite element model combining the cohesive zone method (CZM) and extended finite element [...] Read more.
Residual particles embedded at the bond coat/substrate (BC/SUB) interface after grit blasting can affect the failure behavior of thermal barrier coatings (TBCs) under thermal cycling. This study employed a 2D finite element model combining the cohesive zone method (CZM) and extended finite element method (XFEM) to analyze the effect of interfacial grit particles. Specifically, the CZM was used to simulate crack propagation at the BC/thermally grown oxide (TGO) interface, while XFEM was applied to model the arbitrary crack propagation within the BC layer. Three models were analyzed: no grit inclusion, 20 μm grit particles, and 50 μm grit particles at the BC/SUB interface. This systematic variation allowed isolating the influence of particle size on the location of crack propagation onset, stress distribution, and crack growth behavior. The results showed that grit particles at the SUB/BC interface had negligible influence on the crack propagation location and rate at the BC/TGO interface, due to their spatial separation. However, their presence significantly altered the radial tensile stress distribution within the BC layer. Larger grit particles induced more intense stress concentrations and promoted earlier and more extensive vertical crack propagation within the BC. However, due to plastic deformation and stress redistribution in the BC, the crack propagation was progressively suppressed in the later stages of thermal cycling. Overall, grit particles primarily promoted vertical crack propagation within the BC layer. Optimizing grit blasting to control grit particle size is crucial for improving the durability of TBCs. Full article
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13 pages, 3737 KiB  
Article
The Application of Numerical Ductile Fracture Simulation in the LBB Evaluation of Nuclear Pipes
by Yuxuan Fang, Biao Li, Chang-Sung Seok and Tao Shen
Appl. Sci. 2025, 15(13), 7010; https://doi.org/10.3390/app15137010 - 21 Jun 2025
Viewed by 300
Abstract
The leak-before-break (LBB) concept is widely used in the design and estimation of piping systems of nuclear power plants, which requires considerable test work to obtain the fracture resistance (J-R) curves of nuclear pipes. The application of numerical ductile fracture simulation can effectively [...] Read more.
The leak-before-break (LBB) concept is widely used in the design and estimation of piping systems of nuclear power plants, which requires considerable test work to obtain the fracture resistance (J-R) curves of nuclear pipes. The application of numerical ductile fracture simulation can effectively limit the test work. In this study, an extended stress-modified critical strain (SMCS) model is applied to simulate the crack growth behaviors of full-scale nuclear pipes (SA312 TP304L stainless steel) with a circumferential through-wall crack under a four-point bending load. The LBB evaluation is performed based on the J-R curves of CT specimens and full-scale pipes obtained from fracture resistance tests and numerical simulations. It shows that due to the high crack-tip constraint effect, CT specimens may cause lots of conservatism in the LBB evaluation of nuclear pipes, while the application of numerical ductile fracture simulation can largely reduce the conservatism. Full article
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35 pages, 8248 KiB  
Article
Pre-Failure Deformation Response and Dilatancy Damage Characteristics of Beishan Granite Under Different Stress Paths
by Yang Han, Dengke Zhang, Zheng Zhou, Shikun Pu, Jianli Duan, Lei Gao and Erbing Li
Processes 2025, 13(6), 1892; https://doi.org/10.3390/pr13061892 - 15 Jun 2025
Viewed by 362
Abstract
Different from general underground engineering, the micro-damage prior to failure of the surrounding rock has a significant influence on the geological disposal of high-level radioactive waste. However, the quantitative research on pre-failure dilatancy damage characteristics and stress path influence of hard brittle rocks [...] Read more.
Different from general underground engineering, the micro-damage prior to failure of the surrounding rock has a significant influence on the geological disposal of high-level radioactive waste. However, the quantitative research on pre-failure dilatancy damage characteristics and stress path influence of hard brittle rocks under high stress levels is insufficient currently, and especially, the stress path under simultaneous unloading of axial and confining pressures is rarely discussed. Therefore, three representative mechanical experimental studies were conducted on the Beishan granite in the pre-selected area for high-level radioactive waste (HLW) geological disposal in China, including increasing axial pressure with constant confining pressure (path I), increasing axial pressure with unloading confining pressure (path II), and simultaneous unloading of axial and confining pressures (path III). Using the deviatoric stress ratio as a reference, the evolution laws and characteristics of stress–strain relationships, deformation modulus, generalized Poisson’s ratio, dilatancy index, and dilation angle during the path bifurcation stage were quantitatively analyzed and compared. The results indicate that macro-deformation and the plastic dilatancy process exhibit strong path dependency. The critical value and growth gradient of the dilatancy parameter for path I are both the smallest, and the suppressive effect of the initial confining pressure is the most significant. The dilation gradient of path II is the largest, but the degree of dilatancy before the critical point is the smallest due to its susceptibility to fracture. The critical values of the dilatancy parameters for path III are the highest and are minimally affected by the initial confining pressure, indicating the most significant dilatancy properties. Establish the relationship between the deformation parameters and the crack-induced volumetric strain and define the damage variable accordingly. The critical damage state and the damage accumulation process under various stress paths were examined in detail. The results show that the damage evolution is obviously differentiated with the bifurcation of the stress paths, and three different types of damage curve clusters are formed, indicating that the damage accumulation path is highly dependent on the stress path. The research findings quantitatively reveal the differences in deformation response and damage characteristics of Beishan granite under varying stress paths, providing a foundation for studying the nonlinear mechanical behavior and damage failure mechanisms of hard brittle rock under complex loading conditions. Full article
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18 pages, 1390 KiB  
Article
Durability and Mechanical Analysis of Basalt Fiber Reinforced Metakaolin–Red Mud-Based Geopolymer Composites
by Ouiame Chakkor
Buildings 2025, 15(12), 2010; https://doi.org/10.3390/buildings15122010 - 11 Jun 2025
Cited by 1 | Viewed by 542
Abstract
Cement is widely used as the primary binder in concrete; however, growing environmental concerns and the rapid expansion of the construction industry have highlighted the need for more sustainable alternatives. Geopolymers have emerged as promising eco-friendly binders due to their lower carbon footprint [...] Read more.
Cement is widely used as the primary binder in concrete; however, growing environmental concerns and the rapid expansion of the construction industry have highlighted the need for more sustainable alternatives. Geopolymers have emerged as promising eco-friendly binders due to their lower carbon footprint and potential to utilize industrial byproducts. Geopolymer mortar, like other cementitious substances, exhibits brittleness and tensile weakness. Basalt fibers serve as fracture-bridging reinforcements, enhancing flexural and tensile strength by redistributing loads and postponing crack growth. Basalt fibers enhance the energy absorption capacity of the mortar, rendering it less susceptible to abrupt collapse. Basalt fibers have thermal stability up to about 800–1000 °C, rendering them appropriate for geopolymer mortars designed for fire-resistant or high-temperature applications. They assist in preserving structural integrity during heat exposure. Fibers mitigate early-age microcracks resulting from shrinkage, drying, or heat gradients. This results in a more compact and resilient microstructure. Using basalt fibers improves surface abrasion and impact resistance, which is advantageous for industrial flooring or infrastructure applications. Basalt fibers originate from natural volcanic rock, are non-toxic, and possess a minimal ecological imprint, consistent with the sustainability objectives of geopolymer applications. This study investigates the mechanical and thermal performance of a geopolymer mortar composed of metakaolin and red mud as binders, with basalt powder and limestone powder replacing traditional sand. The primary objective was to evaluate the effect of basalt fiber incorporation at varying contents (0.4%, 0.8%, and 1.2% by weight) on the durability and strength of the mortar. Eight different mortar mixes were activated using sodium hydroxide (NaOH) and sodium silicate (Na2SiO3) solutions. Mechanical properties, including compressive strength, flexural strength, and ultrasonic pulse velocity (UPV), were tested 7 and 28 days before and after exposure to elevated temperatures (200, 400, 600, and 800 °C). The results indicated that basalt fiber significantly enhanced the performance of the geopolymer mortar, particularly at a content of 1.2%. Specimens with 1.2% fiber showed up to 20% improvement in compressive strength and 40% in flexural strength after thermal exposure, attributed to the fiber’s role in microcrack bridging and structural densification. Subsequent research should concentrate on refining fiber type, dose, and dispersion techniques to improve mechanical performance and durability. Examinations of microstructural behavior, long-term durability under environmental settings, and performance following high-temperature exposure are crucial. Furthermore, investigations into hybrid fiber systems, extensive structural applications, and life-cycle evaluations will inform the practical and sustainable implementation in the buildings. Full article
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