Search Results (28)

Testing and the estimation methods for predicting the life of crack initiation and crack growth for P92 steel using a circular sharp notched round bar specimen (CNS) under strain-controlled creep and fatigue conditions have been reported previously. A unique estimation method for the cycle-sequential characteristics of tensile and compressive peak stresses is proposed; specifically, the nominal stress range ${∆\sigma }_{net}={{(\sigma }_{max}-{\sigma }_{min})}_{net}$ and the measurement of crack length using the direct current electric potential drop (DCPD) method were adopted. This method was effective in specifying the failure life and crack initiation life by verifying the crack growth length. However, to show the universality of these results, it is important to compare the experimental results obtained under strain-controlled creep and fatigue conditions with those obtained under stress-controlled creep and fatigue conditions and with those for smooth specimens estimated based on the linear and nonlinear damage summation rule. Furthermore, it may also be important to compare these results with those of smooth specimens estimated based on the Manson–Coffin law when the failure life is fatigue-dominant. Considering these aspects, detailed experiments and analyses were systematically conducted for P92 steel in this study, and the above comparisons were conducted. The results aid in achieving a unified understanding of the law of fracture life, including those under stress- and strain-controlled creep and fatigue conditions. Full article

Background/Objectives: A material incompatibility has been established between self-etching adhesives and amine-containing dual-cure resin composite materials used for core buildups. This study aims to compare the dentin bond strength of several amine-containing and amine-free core materials using self-etching adhesives with different pHs. Methods: Extracted human molars were mounted in acrylic and ground flat with 320-grit silicon carbide paper. Next, 520 specimens (n = 10/group) were assigned to a dual-cure core buildup material group (10 amine-containing, 2 amine-free, and 1 reference light-cure only bulk fill flowable composite) and assigned to a self-etching adhesive subgroup (pH levels of approximately 1.0, 3.0, and 4.0). Within 4 h of surface preparation, the adhesive corresponding to the specimen’s subgroup was applied and light-cured. Composite buttons for the assigned dual-cure core material of each group were placed using a bonding clamp apparatus, allowed to self-cure for 2 h at 37 °C, and then unclamped. An additional group with one adhesive (pH = 3.0) was prepared in which the dual-cure core materials were light-cured. The bonded specimens were stored in water at 37 °C for 24 h. The specimens were mounted on a testing clamp and de-bonded in a universal testing machine with a load applied to a circular notched-edge blade at a crosshead speed of 1 mm/min until bond failure. The maximum load divided by the area of the button was recorded as the shear bond strength. The data was analyzed via 2-way ANOVA. Results: The analysis of bond strength via 2-way ANOVA determined statistically significant differences between the adhesives, the core materials, and their interaction (p < 0.01). There was a general trend in shear bond strength for the adhesives, where pH 4.0 > 3.0 > 1.0. The amine-free core materials consistently demonstrated higher shear bond strengths as compared to the other core materials when chemically cured only. Light-curing improved bond strength for some materials with perceived incompatibility. Conclusions: The results of this study suggest that an incompatibility can exist between self-etching adhesives and dual-cure resin composite core materials. A decrease in the pH of the utilized adhesive corresponded to a decrease in the bond strength of dual-cure core materials when self-curing. This incompatibility may be minimized with the use of core materials formulated with amine-free chemistry. Alternatively, the dual-cure core materials may be light-cured. Full article

Using 3D-printed (3DPd) polymers and their composites as shape memory materials in various smart engineering applications has raised the demand for such functionally graded sustainable materials. This study aims to investigate the viscoelastic, shape memory, and fracture toughness properties of the epoxy-based ultraviolet (UV)-curable resin. A UV-based DLP (Digital Light Processing) printer was employed for the 3D printing (3DPg) epoxy-based structures. The effect of the hydrothermal accelerated ageing on the various properties of the 3DPd components was examined. The viscoelastic performance in terms of glass transition temperature (T_g), storage modulus, and loss modulus was evaluated. The shape memory polymer (SMP) performance with respect to shape recovery and shape fixity (programming the shape) were calculated through dynamic mechanical thermal analysis (DMTA). DMTA is used to reveal the molecular mobility performance through three different regions, i.e., glass region, glass transition region, and rubbery region. The shape-changing region (within the glass transition region) between the T_g value from the loss modulus and the T_g value from the tan(δ) was analysed. The temperature memory behaviour was investigated for flat and circular 3DPd structures to achieve sequential deployment. The critical stress intensity factor values of the single-edge notch bending (SENB) specimens have been explored for different crack inclination angles to investigate mode I (opening) and mixed-mode I/III (opening and tearing) fracture toughness. This study can contribute to the development of highly complex shape memory 3DPd structures that can be reshaped several times with large deformation. Full article

Two 3D-printed crown materials (Crown and Ceramic Crown) were examined to determine the best surface treatment and primers for bonding. Discs of the two materials were printed and mounted with their “intaglio” surfaces untouched. Half the specimens from each group were sandblasted with 50 µm alumina. Then, specimens were divided into four groups (n = 10): Gr1—no further treatment; Gr2—one coat of silane; Gr3—one coat of universal adhesive; Gr4—one coat of silane, then one coat of universal adhesive. Bond strength specimens were prepared with an Ultradent shear bond strength apparatus using Filtek Supreme composite. Specimens were stored for 8 weeks in 37 °C water. The specimens were debonded with a circular notched-edge blade applied at 1 mm/min, and the shear bond strength was calculated. The data were compared with a two-way ANOVA (factors: surface treatment and primer) and a Tukey post hoc analysis for both materials independently, with p < 0.01 considered meaningful. The filler content (burned ash) and resin content (FTIR) of the materials were determined. For both materials, factors surface treatment and primer were significant (p < 0.01), but their interaction was not (p = 0.43 for Crown and p = 0.34 for Ceramic Crown). Alumina air particle abrasion improved the bond strength for both materials. The Tukey post hoc analysis grouped primer treatments into the same statistically different groups for both materials: Gr1 and Gr2 < Gr3 and Gr4. The filler percentage of Crown was 32.7% and Ceramic Crown was 48.2%. Resin content was similar for both materials. The most effective method to bond to 3D-printed crowns (regardless of filler percentage) was to sandblast with 50 µm alumina and apply a layer of adhesive (with or without previous application of silane). Full article

Understanding the mechanical properties of coal is crucial for efficient mining and disaster prevention in coal mines. Coal contains numerous cracks and fissures, resulting in low strength and challenges in preparing standard samples for testing coal fracture toughness. In engineering, indicators such as the hardness coefficient (f value) and Hardgrove grindability index (HGI) are straightforward to measure. Various experiments, including drop weight, grinding, uniaxial compressive strength and three-point bending experiments, were conducted using notched semi-circular bend (NSCB) specimens and particle sizes of 1–2 mm/0.425–1 mm. Theoretical and experimental results indicate that the hardness coefficient of coal and rock is proportional to the crushing work ratio and inversely proportional to the mean equivalent diameter. Moreover, the square of the fracture toughness of coal and rock is directly proportional to the crushing work ratio, inversely proportional to the newly added area, directly proportional to the mean equivalent diameter and directly proportional to the hardness coefficient. The Mode-I fracture toughness of coal and rock can be rapidly determined through the density, the equivalent diameter after crushing and the elastic modulus, with experimental verification of its accuracy. Considering that smaller particle sizes exhibit greater resistance to breakage, the distribution mode of new surface areas after particle breakage was established, influenced by the initial particle size and the energy of a single broken particle. This study can assist in quickly and accurately determining the fracture toughness of coal. Full article

This study presents research results concerning the vacuum carburizing of four steel grades, specifically conforming to European standards 1.7243, 1.6587, 1.5920, and 1.3532. The experimental specimens exhibited variations primarily in nickel content, ranging from 0 to approximately 3.8 wt. %. As a comparative reference, gas carburizing was also conducted on the 1.3532 grade, which had the highest nickel content. Comprehensive structural analysis was carried out on the resultant carburized layers using a variety of techniques, such as optical and electron scanning, transmission microscopy, and X-ray diffraction. Additionally, mechanical properties such as hardness and fatigue strength were assessed. Fatigue strength evaluation was performed on un-notched samples having a circular cross-section with a diameter of 12 mm. Testing was executed via a three-point bending setup subjected to sinusoidally varying stresses ranging from 0 to maximum stress levels. The carburized layers produced had effective thicknesses from approximately 0.8 to 1.4 mm, surface hardness levels in the range of 600 to 700 HV, and estimated retained austenite contents from 10 to 20 vol%. The observed fatigue strength values for the layers varied within the range from 1000 to 1350 MPa. It was found that changing the processing method from gas carburizing, which induced internal oxidation phenomena, to vacuum carburizing improved the fatigue properties to a greater extent than increasing the nickel content of the steel. Full article

Despite recent advances in the molecular knowledge of amphistome trematodes, most genera known from fish remain to be genetically characterized. This is the case for Kalitrema, a genus of the speciose family Cladorchiidae and the type of Kalitrematinae. The type and only species of this genus, Kalitrema kalitrema Travassos, 1933, was originally proposed based on two specimens found in an armored suckermouth catfish from Brazil, and its phylogenetic position has not been evaluated. In this study, paramphistomes found in Hypostomus alatus (2/9; 22.2%) and Hypostomus francisci (4/143; 2.8%) from the Paraobepa River (São Francisco River basin), Minas Gerais, Brazil, between December 2019 and November 2021, were subjected to morphological study. The parasites were identified in low intensity of infection [1.2 (1–2)] and redescribed as K. kalitrema. This species exhibits unique features such as a linguiform body with a circular ridge near the anterior end and a deep, median notch present at the posterior extremity of the body, apparently dividing the body into two lobes. A subset of specimens was further subject to phylogenetic analyses based on the most densely sampled markers, the nuclear ribosomal RNA (28S and ITS2) and mitochondrial cox1, which revealed the inclusion of K. kalitrema in a Neotropical clade of fish paramphistomes. The most comprehensive phylogenetic tree, based on the 28S dataset, confirmed K. kalitrema as an independent, early diverging lineage among Neotropical fish cladorchiids. However, the monophyly of Kalitrematinae was not sustained, given that species of the other kalitrematine genera Pseudocladorchis and Iquitostrema included in the phylogenetic analysis fell in a distinct clade with other fish cladorchiids. As a result, we propose here a narrower concept for Kalitrematinae sensu stricto, accommodating only Kalitrema (type genus) until a more natural subfamilial or familial classification is provided. Full article

In order to accurately test the K_IC of the vertical stratification direction of shale, a semi-circular bending specimen with a linear chevron notch ligament (LCNSCB) was designed. The minimum dimensionless stress intensity factor (Y^*_min) of the LCNSCB specimen was calculated by the finite element method and the slice synthesis method, respectively. Two sets of prefabricated samples of the LCNSCB specimen under arrester and divider mode were used to conduct three-point bending loading experiments. The dispersion of the measured K_IC value of the specimens was analyzed by standard deviation and coefficient of variation, and the reason that the K_IC dispersion of specimens in divider mode was larger than in arrester mode was discussed. Compared with the experimental data of the existing literature, the data of this experiment shows that the LCNSCB specimen can avoid the disadvantage of lower measured K_IC values due to a larger fracture processing zone featured in the CSTSCB and CCNBD specimens, combined with the merits of a shorter fracture processing zone of the SR or CR specimens, and the render measured the K_IC value to be closer to the material’s true fracture toughness value. The narrow ligament of the LCNSCB specimen has a favorable crack propagation guiding effect, can generate consistent K_IC values, and could be used to accurately test the fracture toughness of rock material in vertical bedding direction. Full article

In this paper, stress intensity factor (SIF) solutions are numerically obtained for notched bars subjected to tensile loading containing an eccentric circular inner crack located in the cross-section corresponding to the notch root. The finite element method and the J-integral have been used to obtain the SIF and to analyze the effect on it of three elliptical notch geometries (of equal radial depth). The results show how the SIF is greater in the notched bars than in the smooth bar and within the former when the axial semi-axis of the notch rises, its effect being greater as the diameter and eccentricity of the inner crack increase. In addition, the fatigue growth of an eccentric crack induces an increase in such eccentricity, greater as the notch axial semi-axis increases. The cause of these phenomena can be attributed to the constraint loss caused by the notch, which also facilitates bending of the specimen due to the asymmetry generated by the crack eccentricity. Full article

Laminated plates are often modeled with infinite dimensions in terms of the so-called Whitney–Nuismer (WN) stress criteria, which form a theoretical basis for predicting the residual properties of open-hole structures. Based upon the WN stress criteria, this study derived a new formulation involving finite width; the effects of notch shape and size on the applicability of new formulae and the tensile properties of carbon-fiber-reinforced plastic (CFRP) laminates were investigated via experimental and theoretical analyses. The specimens were prepared by using laminates reinforced by plain woven carbon fiber fabrics and machined with or without an open circular hole or a straight notch. Standard tensile tests were performed and measured using the digital image correlation (DIC) technique, aiming to characterize the full-field surface strain. Continuum damage mechanics (CDMs)-based finite element models were developed to predict the stress concentration factors and failure processes of notched specimens. The characteristic distances in the stress criterion models were calibrated using the experimental results of un-notched and notched specimens, such that the failure of carbon fiber laminates with or without straight notches could be analytically predicted. The experimental results demonstrated well the effectiveness of the present formulations. The new formula provides an effective approach to implementing a finite-width stress criterion for evaluating the tensile properties of notched fiber-reinforced laminates. In addition, the notch size has a great effect on strength prediction while the fiber direction has a great influence on the fracture mode. Full article

The conventional fracture in shale hydraulic fracturing belongs to the type-I fracture, and the size of the fracture process zone (FPZ) is an important index to measure the fracability of rock mass. This index is also one of the feasible entry points to study the complexity of the fracture network. In order to visually observe the type-I FPZ at the tip of shale fractures, and to study the relationship between the mechanical properties, the shape and size of the FPZ, and the bedding structure, Notched Semi-Circular Bend (NSCB) tests were conducted with three typical fracture direction-bedding orientations (splitter, arrester, divider). The digital image correlation (DIC) method was used to realize the intuitive observation of the real fracture process and the FPZ near the fracture tip. The test found that the FPZ of shale is narrow and long as a whole and is “flame-like”. The height-to-length ratio of the FPZ at the fracture tip determines whether bending and deflection happen between the new fracture and the prefabricated cracks when the fracture occurs. Most of the specimens often appear in the FPZ with a beaded high shear strain zone before the fracture, which is caused by the oblique communication of micro-cracks in the FPZ before the fracture. The appearance of a beaded zone of high shear strain indicates that macroscopic fracture is imminent. The research results can be used for the design of disaster early warning and prevention programs. Full article

In this paper, to investigate mixed-mode I-II fracture behaviors, three different asymmetric notched semi-circular bending specimens (ANSCB) were designed by adjusting the angle and the distance between supporting rollers to conduct asymmetric three-point bending tests. Several aid technologies, including acoustic emission (AE), digital image correlation (DIC), crack propagation gauge (CPG), and scanning electron microscopy (SEM), was utilized to monitor and assess the fracture characteristic. Meanwhile, the fractal dimension of the fracture surface was assessed based on the reconstructed digital fracture surface. The results show that mixed-mode I-II ANSCB three-point bending fracture is a brittle failure with the characteristics of the main crack being rapidly transfixed and the bearing capacity decreasing sharply. Based on the DIC method, the whole fracture process consists of a nonlinear elastic stage, fracture process zone, crack initiation stage and crack propagation stage. The crack initiation is mainly caused by the tension-shear strain concentration at the pre-existing crack tip. At the microscale, the crack propagation path is always along the grain boundary where the resultant stress is weakest. According to the monitoring of the AE, it can be found that micro-tensile cracks are mainly responsible for the asymmetric three-point bending fracture. The data obtained by CPG suggest that the subcritical crack growth rate is positively correlated to the ultimate load. In addition, asymmetric loading leads to a coarser fracture surface, and thus a higher fractal dimension of the fracture surface. The current study can provide a better understanding of the mixed-mode I-II fracture behaviors of rock. Full article

To determine the Gurson-Tvergaard-Needleman (GTN)damage model parameters of 6061 aluminum alloy after secondary heat treatment, the uniaxial tensile test was carried out on the aluminum alloy circular arc specimen, and the mechanical properties parameters and the load-displacement curve of aluminum alloy tube were obtained. With the help of the finite element reverse method, scanning electron microscope and a orthogonal test method, the GTN damage model parameters (f₀, f_N, f_C, and f_F) were calibrated, and their values were 0.004535, 0.04, 0.1, and 0.2135, respectively. Then the shear specimen and notch specimen were designed to verify the damage model, the results show that the obtained GTN damage model parameters can effectively predict the fracture failure of 6061 aluminum alloy after secondary heat treatment during the tensile process. Full article

The aim of this paper is to assess the size and geometry effects on the mode I notch fracture toughness of polymeric samples containing rounded-tip V-shaped (RV) notches (V-notch with a finite radius at the notch tip). First, using a large number of fracture tests on an RV-notched Brazilian disk and semi-circular bending polymeric samples with four different sizes, the size-dependent values of the notch fracture toughness are obtained. Then, the mean stress criterion is modified for characterizing the size-dependency of notch fracture toughness in polymeric samples. The resulting modified mean stress criterion considers higher order terms of the stress field when calculating the fracture process zone length around the tip of the defect. Additionally, the critical distance r_c is assumed to be associated with the specimen size and a formula containing fitting parameters is utilized for considering this trend of r_c. The comparison between the values of notch fracture toughness obtained from experiments and those predicted by the modified mean stress criterion shows that the suggested approach can provide accurate estimations of size-dependent values of notch fracture toughness in polymeric specimens containing RV notches. Full article

Under strong earthquakes, steel structures are prone to undergoing ultra-low cycle fatigue (ULCF) fracture after sustaining cyclic large-strain loading, leading to severe earthquake-induced damage. Thus, establishing a prediction method for ULCF plays a significant role in the seismic design of steel structures. However, a simple and feasible model for predicting the ULCF life of steel structures has not been recognized yet. Among existing models, the ductile fracture model based on ductility capacity consumption has the advantage of strong adaptability, while the loading history effect in the damage process can also be considered. Nevertheless, such models have too many parameters and are inconvenient for calibration and application. To this end, focusing on the prediction methods for ULCF damage in steel structures, with the fragile parts being in moderate and high stress triaxiality, this paper proposes a simplified uncoupled prediction model that considers the effect of stress triaxiality on damage and introduces a new historical-effect related variable function reducing the calibration work of model parameters. Finally, cyclic loading test results of circular notched specimens verify that the proposed model has the advantages of a small dispersion of parameters for calibration, being handy for application, and possessing reliable results, providing a prediction method for ULCF damage of structural steels. Full article