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Advanced Analytic Techniques in Food Chemistry

A special issue of Applied Sciences (ISSN 2076-3417). This special issue belongs to the section "Chemical and Molecular Sciences".

Deadline for manuscript submissions: closed (20 May 2022) | Viewed by 8673

Special Issue Editors


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Guest Editor
Department of Civil, Environmental, Land, Building and Chemical Engineering, Dicatech, Polytechnic University of Bari, Via Edoardo Orabona 4, 70125 Bari, Italy
Interests: environmental pollutants; food contaminants; metabolomics; human health; bioactive compounds
Special Issues, Collections and Topics in MDPI journals

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Guest Editor
Dipartimento di Ingegneria Civile, Politecnico di Bari, 70126 Bari BA, Italy
Interests: microwave assisted-synthesis; mass spectrometry; nanotechnology; food chemistry; metabolomics

Special Issue Information

Dear Colleagues,

Research in the field of Food Chemistry is gaining significant attention due to the higher consciousness of the final consumer and the stricter international legislature that is in charge of controlling the traceability along the food chain and assessing the authenticity of the final product that will be on the consumer’s table. Moreover, globalization and the free market raise the issue of controlling food quality obtained by the application of different agricultural practices around the world. Despite the introduction on the market of highly sensitive and accurate instruments to perform analytical analysis of the food product, still, great efforts are needed to make this huge amount of data useful to rapidly trace the several steps constituting the food chain and to assess the unique identity of a food product in a way that, ideally, the consumer will have a self-telling product on the table. Such a goal could be reached only if the scientific community involved in this field of research communicates effectively, putting together information derived from different analytical techniques and different approaches. Moreover, the introduction and development of new advanced theoretical algorithms, using the data produced in the laboratories, should give a boost to the quality assessment of the commercialized food products, enhancing the local biodiversity, agricultural practices, and geographical authenticity.

The focus of the Special Issue will be on innovations in the field of analytic techniques used to assess the traceability and authenticity of food products. Considering the multidisciplinarity of this field, a broad range of topics will be explored, including spectroscopic methods, chemometric studies, the Internet of Things, machine learning, and data fusion. Reviews, full papers, and short communications focused on new achievements in this area are expected. Potential topics include but are not limited to:

  • Food metabolomics;
  • Targeted and non-targeted spectroscopic analysis;
  • Chemometric studies;
  • Internet of Things: machine learning and artificial-intelligence-driven applications;
  • Wearable sensors and IoT applied to food chain traceability.

Dr. Biagia Musio
Dr. Antonino Rizzuti
Guest Editors

Manuscript Submission Information

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Keywords

  • food authenticity
  • food chain traceability
  • targeted metabolic analysis
  • non-targeted metabolic analysis
  • fingerprinting
  • metabolic profiling
  • blockchain
  • artificial intelligence
  • internet of things
  • wearable sensors
  • chemometric analysis

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Published Papers (3 papers)

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Research

15 pages, 4052 KiB  
Article
Non-Targeted NMR Method to Assess the Authenticity of Saffron and Trace the Agronomic Practices Applied for Its Production
by Biagia Musio, Stefano Todisco, Marica Antonicelli, Cristiano Garino, Marco Arlorio, Piero Mastrorilli, Mario Latronico and Vito Gallo
Appl. Sci. 2022, 12(5), 2583; https://doi.org/10.3390/app12052583 - 2 Mar 2022
Cited by 10 | Viewed by 2142
Abstract
The development of analytical methods aimed at tracing agri-food products and assessing their authenticity is essential to protect food commercial value and human health. An NMR-based non-targeted method is applied here to establish the authenticity of saffron samples. Specifically, 40 authentic saffron samples [...] Read more.
The development of analytical methods aimed at tracing agri-food products and assessing their authenticity is essential to protect food commercial value and human health. An NMR-based non-targeted method is applied here to establish the authenticity of saffron samples. Specifically, 40 authentic saffron samples were compared with 18 samples intentionally adulterated by using turmeric and safflower at three different concentration levels, i.e., 5, 10, and 20 wt%. Statistical processing of NMR data furnished useful information about the main biomarkers contained in aqueous and dimethyl sulfoxide extracts, which are indicative of the presence of adulterants within the analyzed matrix. Furthermore, a discrimination model was developed capable of revealing the type of agronomic practice adopted during the production of this precious spice, distinguishing between organic and conventional cultivation. The main objective of this work was to provide the scientific community involved in the quality control of agri-food products with an analytical methodology able to extract useful information quickly and reliably for traceability and authenticity purposes. The proposed methodology turned out to be sensitive to minor variations in the metabolic composition of saffron that occur in the presence of the two adulterants studied. Both adulterants can be detected in aqueous extracts at a concentration of 5 wt%. A lower limit of detection was observed for safflower contained in organic extracts in which case the lowest detectable concentration was 20%. Full article
(This article belongs to the Special Issue Advanced Analytic Techniques in Food Chemistry)
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10 pages, 588 KiB  
Article
An Inductively Coupled Plasma Optical Emission Spectrometric Method for the Determination of Toxic and Nutrient Metals in Spices after Pressure-Assisted Digestion
by Natalia Manousi, Eleni Isaakidou and George A. Zachariadis
Appl. Sci. 2022, 12(2), 534; https://doi.org/10.3390/app12020534 - 6 Jan 2022
Cited by 13 | Viewed by 2233
Abstract
The aim of this study was to develop a simple and rapid inductively coupled plasma optical emission spectrometric (ICP-OES) method for the determination of 17 metals (Ag, Al, B, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, Mg, Mn, Ni, Pb, Tl and [...] Read more.
The aim of this study was to develop a simple and rapid inductively coupled plasma optical emission spectrometric (ICP-OES) method for the determination of 17 metals (Ag, Al, B, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, Mg, Mn, Ni, Pb, Tl and Zn) in packaged spices. For this purpose, the spice samples (200 mg) in the form of powder were submitted to pressure-assisted wet-acid digestion with a mixture of 6 mL concentrated HNO3 and 1 mL H2O2. The proposed method was validated in terms of linearity, trueness, precision, limits of detection (LODs) and limits of quantification (LOQs). Good method trueness, precision and linearity were observed for the examined elements. The LODs of the examined analytes ranged between 0.08 and 5.95 mg kg−1. The present method was employed for the analysis of twenty-two packaged commercially available spices including asteroid anise, clove, cardamon, cinnamon, curry, coriander, turmeric, cumin, white pepper, black pepper, nutmeg, allspice, red pepper, paprika, ginger, green pepper and pink pepper from the Greek market that are widely consumed. A wide variety of metal of different concentration ranges were determined in the samples. Full article
(This article belongs to the Special Issue Advanced Analytic Techniques in Food Chemistry)
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10 pages, 488 KiB  
Article
Development and Validation of an ICP-AES Method for the Determination of Toxic and Nutrient Metals in Candies: Application for the Analysis of Different Samples from the Greek Market
by Natalia Manousi and George A. Zachariadis
Appl. Sci. 2021, 11(22), 10599; https://doi.org/10.3390/app112210599 - 11 Nov 2021
Cited by 7 | Viewed by 3761
Abstract
In this study, we present the development and validation of an inductively coupled plasma-atomic emission spectrometric (ICP-AES) method for the determination of Ag, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, Mg, Mn, Ni, Pb and Zn in different candies. Various wet digestion [...] Read more.
In this study, we present the development and validation of an inductively coupled plasma-atomic emission spectrometric (ICP-AES) method for the determination of Ag, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, Mg, Mn, Ni, Pb and Zn in different candies. Various wet digestion protocols were examined in order to ensure minimum consumption of chemicals and sample preparation time. Under optimized conditions, less than 10 min were required for complete sample decomposition. The ICP-AES method was validated in terms of linearity, accuracy, precision, limits of detection (LODs) and limits of quantification (LOQs). The relative recoveries for the proposed method ranged between 80.0% and 119.0%, while the relative standard deviation values were lower than 9.0%, indicating good method accuracy and precision, respectively. The LODs for the examined analytes were 0.04–2.25 mg kg−1. Finally, the proposed method was successfully employed for the analysis of hard candies, jellies and lollipops that are sold in the Greek market, which are highly likely to be consumed by children. Full article
(This article belongs to the Special Issue Advanced Analytic Techniques in Food Chemistry)
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