Powders, Volume 4, Issue 2 (June 2025) – 3 articles

This collection of studies, conducted within the framework of the DFG-funded Priority Program SPP 2045, explores the role of X-ray tomography in advancing the multidimensional characterization of particulate systems, with a strong focus on enhancing 3D particle-discrete data quality. It critically assesses the limitations of traditional particle characterization methods, particularly those reliant on imaging techniques, and demonstrates how advanced methodologies can overcome these constraints by providing highly detailed and accurate geometric and structural 3D data. The research further introduces innovative sample preparation techniques for particle collectives, aiming to reduce post-processing efforts in image analysis. Additionally, the development of a particle database, aligned with FAIR data principles (Findable, Accessible, Interoperable, and Reusable), supports data sharing and collaborative research. Ultimately, this collection underscores the transformative potential of 3D particle-discrete datasets acquired through X-ray tomography in advancing particle technology and improving particle system analyses across diverse scientific and industrial fields. Full article

To obtain a more comprehensive understanding of the specific properties of complex-shaped technical aerosols—such as partially sintered aggregates formed in combustion processes or structured particles resulting from complex synthesis processes—it is essential to measure more than a single equivalent size. This study examines a novel method for determining a two-dimensional distribution of two distinct particle properties within the size range from $50\mathrm{nm}$ to $1000\mathrm{nm}$: the Centrifugal Differential Mobility Analyzer (CDMA). The CDMA enables the simultaneous measurement of both mobility and Stokes equivalent diameters, providing a detailed two-dimensional particle property distribution. This, in turn, allows for the extraction of shape-related information, which is essential for characterizing particles in terms of their chemical composition, reactivity, and other physicochemical properties. This paper presents a detailed evaluation of a first CDMA prototype. First, CFD simulations of the flow field within the classifier are presented in order to assess and understand non-idealities arising from the exact geometry. Subsequently, the transfer function is evaluated by particle trajectory calculations based on the simulated flow field. It can be demonstrated that the simulated transfer functions agree quite well with transfer functions derived from streamlines of an ideal flow field, indicating that the non-idealities in the classifying region are almost negligible in their effect on the classification result. An experimental determination of the transfer function shows additional effects not covered by the previous simulations, like broadening by diffusion and losses due to diffusion and precipitation within the in- and outlet of the classifier. Finally, the determined transfer functions are used to determine the full two-dimensional distribution with regard to the mobility and Stokes equivalent diameter of real aerosols, like spherical particles and aggregates at different sintering stages, respectively. Full article

This study aims to investigate the suitability of earthen housing for refugees and establish a more efficient system for selecting and adjusting materials by quantitatively analyzing the influence of various factors affecting the mechanical performance of earthen housing. This paper examined the impact of dry unit weight, particle size distribution of soil solidification, clay minerals, and pH on the mechanical performance of soil solidification through compressive strength testing. Additionally, the tensile strength resulting from capillary forces between particles was estimated using a prediction equation, and the effects of capillary forces and cohesive forces due to clay minerals were quantitatively assessed by comparing them with the results of the compressive strength experiments. In an alkaline environment, conflicting results were obtained regarding the effect of the dispersion of particles on compressive strength, depending on the presence or absence of clay minerals in the soil. Based on these results, the implementation of earthen houses constructed in the target refugee camp was evaluated, and strategies for building houses more efficiently under given conditions were discussed. Full article