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Article

Wire Electrode Wear in WEDM of Inconel 718: Gravimetric Evaluation Using a 33 Full Factorial Design

1
Faculty of Materials Science and Technology in Trnava, Slovak University of Technology in Bratislava, Ulica Jána Bottu 25, 917 24 Trnava, Slovakia
2
Department of Manufacturing Engineering, Machines and Tools, Sumy State University, Kharkivska Str. 116, 40007 Sumy, Ukraine
*
Author to whom correspondence should be addressed.
Appl. Sci. 2026, 16(11), 5235; https://doi.org/10.3390/app16115235
Submission received: 22 April 2026 / Revised: 13 May 2026 / Accepted: 22 May 2026 / Published: 23 May 2026

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Reliable assessment and control of wire electrode wear are essential for stable WEDM operation, as they reduce wire consumption and machining cost, improve process efficiency, and limit the risk of wire breakage.

Abstract

Wire electrical discharge machining (WEDM) is widely used for the precision cutting of difficult-to-machine materials, including nickel-based superalloys. Wire electrode wear, however, remains a practical limitation, because it affects process stability, wire consumption, and machining cost. This work examines the wear behaviour of a gamma-phase Cu5Zn8-coated copper-core wire electrode (Elecut X, ø 0.25 mm) during the WEDM of Inconel 718 using direct gravimetric measurement. A 33 full factorial experiment was carried out with three electrical parameters: pulse-on time (A), pulse-off time (B), and servo reference voltage (Aj). The discharge process was monitored with an oscilloscope so that measurements only started after the programmed pulse-off time had been reached. Electrode wear was evaluated as the mass loss Δm of 4 m wire segments after 5 min cutting intervals on a Charmilles Robofil 310 machine, and factor significance was assessed by analysis of variance (ANOVA). Pulse-on time was the dominant factor, accounting for 88.45% of the total variation in Δm, followed by servo reference voltage and pulse-off time. SEM/EDS examination showed material transfer from the Inconel 718 workpiece to the worn electrode surface, with local nickel content reaching 16.84 wt.% on the frontal face of the most worn sample. The results provide a quantitative basis for reducing wire consumption during the WEDM of Inconel 718 while recognising the trade-off with cutting productivity.

1. Introduction

Wire electrical discharge machining (WEDM) removes material with controlled electrical discharges between a continuously moving wire electrode and an electrically conductive workpiece immersed in a dielectric fluid. Because there is no direct mechanical contact, the process is well-suited to complex geometries and difficult-to-machine materials that require dimensional accuracy, particularly in aerospace, automotive, and tool-making applications [1]. Ho et al. [1] identified wire breakage and wire electrode wear as persistent limits on WEDM efficiency and accuracy, and these issues remain central in current work on process stability.
Inconel 718 is difficult to machine conventionally because it retains high strength at elevated temperatures, has low thermal conductivity, and work-hardens readily. WEDM is therefore a useful option for this alloy. The discharge environment, however, progressively damages the wire electrode. Wear appears as mass loss, cratering, diameter reduction, and the deposition of workpiece-derived elements on the wire surface. These changes can reduce dimensional accuracy, increase the probability of wire breakage, and raise consumable cost [1,2].
Wire wear has been investigated for several difficult-to-machine materials. Tosun and Cogun [3] studied the WWR (Wire Wear Ratio) during WEDM of AISI 4140 steel and reported discharge voltage as the dominant factor. Goswami and Kumar [4] used a Taguchi L27 array for Nimonic 80A and found pulse-on time, together with its interaction with pulse-off time, to be most influential. Similar trends were reported for Nimonic 75 [5], Al-based metal matrix composites [6], and Nimonic 263 [7], although the relative contributions depended on the workpiece, electrode, and generator system. Taken together, these studies point to pulse-on time as a recurring driver of wire wear, but not as a universal single-factor explanation.
Work focused specifically on Inconel 718 is more limited. Ramakrishnan and Karunamoorthy [8] examined WEDM performance with a brass wire electrode, but their emphasis was on the material removal rate and surface roughness; wire wear was only represented indirectly through wire consumption. Dhale and Deshmukh [9] considered the wire diameter together with dimensional deviation, wire consumption, and surface quality. Abhilash and Chakradhar [10] later compared four wire electrode types for the WEDM of Inconel 718 and linked discharge energy to wire-break failure. In a subsequent study, they proposed a machine-vision system for in-process WWR estimation and showed that adaptive changes in pulse-off time, servo voltage, and the wire feed rate can keep wire wear within safer limits [11]. Buk et al. [12] used surface-topography-based indicators to compare wire wear for Inconel 718, Ti-6Al-4V, and 42CrMo4 steel. These studies show that wire wear in Inconel 718 is recognised as a practical issue, but they do not provide a direct gravimetric factorial decomposition of the principal electrical parameters for the material–electrode combination considered here.
The mechanisms of wire wear have also been studied from the standpoint of discharge behaviour and surface damage. Liao et al. [13] distinguished two wire rupture modes using spark-frequency analysis and SEM observation: sudden thermal overload and gradual deterioration caused by excessive arc discharges. Luo [14] showed that erosion craters reduce the effective load-bearing cross-section of the wire and act as stress concentrators. Lee and Liao [15] further demonstrated that the ratio of normal to arc sparks can serve as an indicator of process stability and wire condition. Morphological studies by Singh et al. [5] and Grigoriev et al. [16] reported wider and deeper craters with increasing pulse-on times and peak currents, along with the transfer of workpiece elements to the wire surface.
The electrode construction is also relevant. Kruth et al. [2] showed that coating composition and thickness affect the discharge process; zinc-rich coatings can improve flushing by promoting explosive vaporisation of the dielectric and reducing arc formation. Elecut X uses a gamma-phase Cu5Zn8 coating on a pure copper core, combining the high conductivity of copper with the discharge behaviour of a zinc-based coating. Altuğ [17] also noted that workpiece thermal and microstructural properties influence WWR, while Kneubühler et al. [18] pointed out that the deposition of workpiece material on the wire surface can bias purely gravimetric wear assessment. This issue is especially relevant for Inconel 718, where transferred elements may remain on the electrode surface after cutting.
The specific combination of Inconel 718, a gamma-phase Cu5Zn8-coated copper-core electrode, and a complete full factorial design with direct gravimetric measurement has not yet been reported. Previous Inconel 718 studies have relied on indirect wire consumption [9], image-based WWR estimation [11], comparisons between other wire materials [10], or surface-topography-based wear indicators [12]. Many gravimetric studies on other materials have used Taguchi-type arrays [4,5,6], which are efficient for screening but do not resolve all two-way interactions. The present work addresses this gap through a complete 33 factorial experiment with the pulse-on time (A), pulse-off time (B), and servo reference voltage (Aj) as factors. Oscilloscope monitoring was used to verify the discharge regime before measurement, and ANOVA was applied to quantify the contribution of each factor.
Novelty and contribution: This study provides (i) a consistent gravimetric dataset for wire electrode wear in the combination Inconel 718 + γ-Cu5Zn8-coated copper-core wire under a complete 33 full factorial design; (ii) an ANOVA decomposition of the main effects and two-way interactions of pulse-on time, pulse-off time, and servo reference voltage; and (iii) SEM/EDS evidence of workpiece-to-electrode material transfer on the Elecut X wire, including a local nickel concentration of 16.84 wt.% on the frontal face of the most worn electrode. These contributions are intended to support both parameter selection and the interpretation of gravimetric wear measurements in this material combination.

2. Materials and Methods

The workpiece material was Inconel 718, a precipitation-hardened nickel-based superalloy used in aerospace, power generation, and high-temperature structural components because of its strength, oxidation resistance, and fatigue performance at elevated temperatures. The chemical composition is listed in Table 1. Values were taken from the mill test certificate supplied with the material and conform to the nominal composition ranges of Inconel 718 according to UNS N07718 (W.Nr. 2.4668). The workpiece was a rectangular block with dimensions of 10 × 30 × 120 mm.
All experiments used an Elecut X wire electrode (ø 0.25 mm, tensile strength 500 N/mm2, and electrical conductivity 65% IACS) supplied by ELERO s.r.o. (Považská Bystrica, Slovakia). The wire consists of a pure copper core with an electrolytically deposited gamma-phase Cu5Zn8 coating. This construction is intended to combine the conductivity of the copper core with the discharge behaviour and thermal response of a zinc-rich coating. The γ-Cu5Zn8 coating thickness was not measured directly on a wire cross-section in the present study; for similar electrolytically coated WEDM electrodes, coating thicknesses of the order of a few micrometres have been reported [2]. Although the γ-Cu5Zn8 phase has lower electrical and thermal conductivity than pure copper [19], the overall wire conductivity (65% IACS) is dominated by the copper core, while the zinc-rich coating mainly contributes through favourable ionisation behaviour and controlled vaporisation during discharge.
The experiments were performed on a Charmilles Robofil 310 CNC wire electrical discharge machine (AgieCharmilles, Losone, Switzerland), with axis travel of 400 × 250 × 400 mm and a maximum workpiece weight of 1000 kg. A Keysight EDUX1002A digital storage oscilloscope (Keysight Technologies, Santa Rosa, CA, USA) was connected to the generator output to monitor the discharge signal. Before each 5 min measurement, cutting continued until the actual pulse-off time B reached the programmed value. Only then was the measurement interval started so that the recorded wear corresponded to the intended parameter settings. The dielectric fluid used in all experiments was deionised water, which is the standard dielectric medium for the Charmilles Robofil 310 transistor-controlled WEDM generator and for the corresponding cutting parameters tested in this study.
The waveform in Figure 1 illustrates the discharge states observed during cutting, including normal discharge pulses, open pulses, the ionisation time, and the pulse-off time (Toff). A normal discharge pulse is preceded by an ionisation period, during which the dielectric breaks down and a plasma channel forms between the wire and the workpiece. If this ionisation period is absent, usually because of debris in the gap, the current peak is lower, and the pulse contributes less energy to material removal. This occurs because conductive debris in the gap establishes a partial current path, triggering breakdown before the voltage reaches its nominal ignition level and preventing the formation of a well-defined plasma channel. Since pulse energy is the time integral of the product of the voltage and current, both the reduced breakdown voltage and the lower current peak diminish the thermal energy delivered to the spark site. Open pulses occur when voltage is applied but breakdown does not take place, either because the gap is too large or because local conditions do not support discharge initiation. Measurements for each experimental run were initiated only after Toff reached its programmed value, confirming stable process conditions.
Figure 1 also shows why the oscilloscope was used as a starting criterion for each measurement. At the beginning of a cut, the machine control system adjusts the discharge gap, and the actual pulse-off time can be longer than the programmed value. After stabilisation, B decreases to the set value. From that point onward, the discharge regime is suitable for comparing the programmed parameter combinations.
After machining, the separated wire segment was cleaned with isopropanol and a paper tissue to remove dielectric residues and loose deposited particles. The segment was then weighed three times on a KERN PCB 350-3 analytical balance (KERN & Sohn GmbH, Balingen, Germany), with 350 g capacity, 0.001 g resolution, and 0.001 g repeatability.
Wire wear was expressed as mass loss Δm (g), calculated from the difference between the initial mass of the new 4 m wire segment (1.672 g) and the mean post-machining mass. The standard uncertainty of the mean was calculated for each run as:
u ( m ¯ )   =   S D n
where SD is the standard deviation of the three repeated weighings, and n = 3 is the number of weighing repetitions. The expanded uncertainty of mass loss at approximately 95% confidence was calculated as
U 95 ( Δ m ) = k   ·   u ( m ¯ )
using a coverage factor k = 2. Across the 27 runs, the mean standard uncertainty of the mean was u( m ¯ ) = 0.91 mg, and the mean expanded uncertainty was U95(Δm) = 1.82 mg. This corresponds to a mean relative uncertainty of 2.7% of the measured mass loss. Because u( m ¯ ) is close to the balance resolution, the balance itself was the dominant uncertainty source.
Surface morphology and elemental composition of selected wire electrode samples were analysed using a JEOL JSM-7600F high-resolution scanning electron microscope (JEOL Ltd., Tokyo, Japan) equipped with an Oxford Instruments X-Max 50 mm2 energy-dispersive X-ray spectrometer (EDS) (Oxford Instruments Plc., High Wycombe, UK) for elemental analysis in a secondary electron imaging (LEI) regime.
Figure 2 shows the experimental setup during a typical WEDM run, with the Inconel 718 workpiece clamped on the working table of the Charmilles Robofil 310 CNC wire EDM machine (AgieCharmilles, Losone, Switzerland). The fully CNC-controlled execution of the programmed parameter combinations, together with the oscilloscope-based stability verification described above, ensured reproducible and well-defined discharge conditions for all 27 experimental runs.
For each run, the wire first cut under the selected parameter combination until stable oscilloscope conditions were reached. The following 5 min interval was used for measurement. After this interval, machining was stopped and the terminal 4 m of wire was separated for gravimetric evaluation. With a constant wire feed speed of 4 m·min−1, this segment corresponds to the wire exposed during the final minute of the stabilised cut.
Wire feed speed (WS) affects how many discharge craters are distributed along a given length of wire, because it controls the supply rate of fresh electrode material into the cutting zone. In this experiment, WS was fixed at a relatively low value of 4 m·min−1. The purpose was to increase the crater density per unit wire length and thereby make the gravimetric wear signal more sensitive to the electrical parameters A, B, and Aj.
A schematic overview of the full experimental procedure, summarising the parameter-setting, machining, stabilisation, gravimetric, and statistical evaluation steps, is shown in Figure 3. The loop back to the parameter-setting block indicates that each of the 27 factorial combinations was processed through the same procedure, and the workflow proceeds to the final ANOVA and SEM/EDS analyses only after all runs have been completed.
The experiment followed a complete 33 factorial design with 27 runs, covering all combinations of three factors at three levels. The variable parameters are listed in Table 2, and the constant parameters are listed in Table 3. The initial mass of the new 4 m Elecut X segment was 1.672 g. Statistical analysis was carried out in Minitab 22 (Minitab LLC, State College, PA, USA) using analysis of variance (ANOVA).
All other process parameters were fixed for the 27 runs and are listed in Table 3. The oscilloscope-based stability criterion described above was applied before each measurement.
The 27 runs were completed sequentially in the systematic factorial order given in Table 4 in one uninterrupted session of approximately 5 h rather than in a randomised order. The three principal sources of potential time-correlated drift—dielectric temperature, dielectric conductivity, and the discharge waveform—were monitored throughout the session: temperature remained constant at 18 °C, conductivity stayed within 12–16 µS/cm (measured every 30 min), and oscilloscope verification before each run showed no systematic change in the waveform. A stabilisation phase preceded each measured cut, and a single wire spool was used for the entire campaign. Despite the absence of strict randomisation, the monitored parameters showed no systematic drift across the session, and therefore, the risk of confounding between run order and the estimated factor effects is low.

3. Results

3.1. Gravimetric Measurement Results

Table 4 gives the complete gravimetric results. Mass loss Δm ranged from 0.021 g in run 9 (A = 0.4 µs, B = 24 µs, and Aj = 50 V) to 0.199 g in run 20 (A = 1.2 µs, B = 16 µs, and Aj = 40 V). The difference is almost tenfold. Across the design, higher pulse-on time consistently produced higher wire mass loss, regardless of the other two factor levels.
As shown in Figure 4, the graphical representation of electrode mass loss reveals a clear increasing trend with increasing pulse energy. Runs performed at the lowest pulse-on time level exhibited the smallest mass loss, whereas intermediate and high pulse-on time levels led to progressively greater electrode wear. This indicates that a higher amount of energy delivered to the discharge gap intensifies thermal loading of the wire electrode, thereby promoting material removal from the electrode surface and increasing Δm.
The ANOVA results are summarised in Table 5. The model was significant (F = 23.40, p < 0.001) and explained 98.14% of the total variation in Δm. Pulse-on time (A) was the dominant factor, contributing 88.45% of the total variance (F = 189.79, p < 0.001). Servo reference voltage (Aj) contributed 5.01% (F = 10.75, p = 0.005), while pulse-off time (B) contributed 3.10% (F = 6.65, p = 0.020). The two-way interactions were not significant (p = 0.822), indicating that, within the tested range, the factors mainly acted through their individual effects.
Because the 33 factorial design was not replicated, the 8 degrees of freedom assigned to the error in Table 5 correspond to the three-factor interaction A × B × Aj. This interaction was pooled into the error term under the standard assumption that a physically meaningful three-way interaction among A, B, and Aj is unlikely [20]. In the present process, this assumption is supported by the fact that the three controlled parameters act through distinct physical mechanisms in the transistor-controlled generator: pulse-on time (A) governs the energy delivered per discharge, pulse-off time (B) controls the dielectric recovery interval between successive discharges, and servo reference voltage (Aj) determines the nominal discharge gap and the associated flushing conditions. Because each parameter influences the discharge process through a separate mechanism within the generator’s control logic, no specific physical interaction mechanism would be expected to act simultaneously through all three. The pooled three-way term therefore captures residual variability rather than a structured higher-order effect. The resulting residual variance was then used to test the main effects and two-way interactions.
Model fit statistics are given in Table 6. R2 = 98.14% shows that the model describes most of the variation in the measured response. The adjusted R2(adj) = 93.94% remains high after accounting for the number of model terms. The predictive R2(pred) = 78.77% is lower, as expected for a single-replicate design, but still indicates a useful predictive capability within the investigated region. The residual standard error was S = 0.0145 g.
The Pareto chart in Figure 5 provides the same ranking visually. The standardised effect of pulse-on time (A) is well above the critical value of 2.31 at α = 0.05. Servo reference voltage (Aj, denoted C in the chart) and pulse-off time (B) also exceed this threshold, whereas all two-way interactions remain below it.
Residual diagnostics were used to check the ANOVA assumptions. In the normal probability plot (Figure 6), the residuals follow the reference line reasonably well. This analysis identifies the systematic effects of A, B, and Aj on wire wear; quantitative characterisation of the run-to-run variability of Δm at fixed parameter settings would require a replicated experiment and is left for future work.
The Ryan–Joiner test gave RJ = 0.959 with p = 0.046, which is slightly below the conventional 0.05 threshold. For this balanced factorial dataset, the small tail deviation was treated as acceptable because ANOVA is generally robust to moderate non-normality [20].
Homogeneity of variance was assessed using the residuals versus fitted values plot shown in Figure 7, which displays a random scatter around zero across the full range of fitted Δm values, with no visible curvature or funnel-shaped pattern. This visual assessment was confirmed quantitatively by Levene’s tests applied separately to each factor, which yielded p = 0.176 (A), p = 0.881 (B), and p = 0.827 (Aj)—all well above the 0.05 threshold—supporting the assumption of constant variance across the factor levels.

3.2. SEM and EDS Analysis of Wire Electrode Wear

SEM combined with EDS was used to examine the wire surface before and after machining. Three samples were selected: the unused wire, the least worn wire from run 9 (A = 0.4 µs, B = 24 µs, Aj = 50 V, and Δm = 0.021 g), and the most worn wire from run 20 (A = 1.2 µs, B = 16 µs, Aj = 40 V, and Δm = 0.199 g).
The unused Elecut X wire is shown in Figure 8. The surface exhibits the regular longitudinal features and fine-scale texture characteristic of an electrolytically deposited γ-Cu5Zn8 coating on a drawn copper-core wire, but no discharge craters, resolidified material, and workpiece-derived deposits are present. This unworn morphology serves as the reference state for the worn electrodes shown in Figure 9 and Figure 10.
EDS analysis (Table 7) confirmed the expected gamma-phase Cu5Zn8 coating composition, with 61.58 wt.% Zn, 37.87 wt.% Cu, and a trace Fe content of 0.55 wt.%.
The least worn electrode (Figure 9) came from run 9, where the lowest pulse-on time was combined with the highest servo reference voltage. Frontal and lateral wear are both visible, but the damage is limited compared with the most worn sample. EDS analysis (Table 8) showed only minor transfer from the workpiece: Ni was 1.90 wt.%, and the surface composition remained close to the original Cu5Zn8 coating. The oxygen content of 10.24 wt.% is attributed to surface oxidation of the zinc-rich coating, originating from the interaction of the heated wire with the deionised water dielectric during discharge and from passive oxidation during post-machining air exposure prior to EDS analysis.
The most worn electrode (Figure 10) came from run 20, which used the highest pulse-on time. The image shows the frontal region of the wire, where direct discharge contact with the workpiece produces the most severe damage. The surface contains pronounced craters and deposited material. EDS analysis was performed at three locations on this frontal face (Table 9). Nickel varied from 1.27 wt.% (Spectrum 2) to 16.84 wt.% (Spectrum 1), showing that transfer from the Inconel 718 workpiece was substantial but highly local. Cu and Zn also varied between spectra, consistent with non-uniform coating degradation and local deposition.
Table 9 summarises the surface composition measured on the most worn electrode.

4. Discussion

The factor ranking is consistent with the wider WEDM literature, where pulse-on time is often reported as a major driver of wire wear [5,6,7]. Its high contribution in the present dataset is partly due to the wide relative range tested, from 0.4 to 1.2 µs, and partly to the low thermal conductivity of Inconel 718, which favours heat concentration in the discharge zone. Differences from studies such as Tosun and Cogun [3], where discharge voltage dominated, can be explained by generator architecture. In RC-type systems, pulse energy depends strongly on open-circuit voltage, whereas in the transistor-controlled Charmilles Robofil 310, it is mainly governed by U·I·ton. In this setting, pulse-on time is the most direct control of thermal loading.
The comparison with Abhilash and Chakradhar [10,11] also shows why factor contributions should be interpreted in context. Their machine-vision WWR method captured local geometric change, whereas the present gravimetric method measures net mass change over a 4 m wire segment. Their wire electrodes also differed from the γ-Cu5Zn8-coated copper-core Elecut X wire used here. The two approaches therefore describe related but not identical aspects of wire wear.
The physical mechanism behind this factor ranking can be interpreted in terms of the thermophysical asymmetry between the γ-Cu5Zn8 coating and the copper core. Zinc, the dominant constituent of the coating, has much lower melting and boiling temperatures than copper: approximately 419.5 °C and 907 °C for Zn, compared with approximately 1084.6 °C and 2562 °C for Cu, respectively. In addition, the γ-Cu5Zn8 phase has lower thermal conductivity than pure copper [19]. The zinc-rich coating can therefore act as a sacrificial thermal layer during discharge: local melting and vaporisation of the coating consume part of the deposited discharge energy, while the lower thermal conductivity of the γ phase delays heat transfer towards the copper core.
The effectiveness of this protective layer depends primarily on the energy delivered during each discharge. At the shortest pulse-on time tested (A = 0.4 µs, run 9), the discharge energy appears to remain largely within the coating-controlled wear regime. This is consistent with the EDS composition of the least worn electrode, which remains close to the original γ-Cu5Zn8 coating composition (Cu = 36.54 wt.%, Zn = 49.19 wt.%; Table 8). At the longest pulse-on time tested (A = 1.2 µs, run 20), the higher discharge energy produces more severe local thermal damage, coating degradation, and local depletion of Zn-rich material. Spectrum 2 in Table 9 (Cu = 73.57 wt.%, Zn = 22.33 wt.%) indicates that the γ-Cu5Zn8 coating has been locally thinned or removed to the extent that the copper core contributes strongly to the analysed surface volume.
This suggests a transition from coating-dominated wear at low pulse-on time to local coating failure and copper-core exposure at high pulse-on time. Once this transition occurs, subsequent discharges no longer only interact with the sacrificial Zn-rich coating but also with the load-bearing copper core, leading to more severe cratering and a higher net mass loss. This mechanism explains why pulse-on time has the dominant ANOVA contribution to Δm (88.45%, Table 5): A directly controls whether the per-discharge thermal load remains within the protective regime of the coating or reaches a regime where the coating is locally breached. Pulse-off time (B) and servo reference voltage (Aj) modulate this primary mechanism indirectly, through dielectric recovery, gap conditions, and flushing efficiency, which is consistent with their smaller statistical contributions.
The secondary roles of servo reference voltage and pulse-off time are consistent with this interpretation. Higher Aj increases the nominal gap between the wire and the workpiece, which can improve debris removal and reduce secondary arc discharges. Longer B extends the dielectric-recovery interval between discharges. Both parameters therefore affect the stability and cooling conditions around the discharge zone, but neither controls the per-discharge thermal load as directly as pulse-on time.
The non-significant two-way interactions suggest that A, B, and Aj can mainly be interpreted through their individual effects within the tested window. This is useful for process tuning, but it should not be extended beyond the investigated range without additional experiments. The gravimetric response also complements surface-topography methods such as that of Buk et al. [12]: gravimetry captures the global net mass response of the wire segment, while profilometry resolves local geometric change.
EDS adds chemical detail to the gravimetric result. The unused wire matched the expected Cu5Zn8 coating, while the worn samples showed increasing workpiece-derived material on the surface. In run 20, Ni reached a local maximum of 16.84 wt.% on the frontal face, although the three EDS spectra varied strongly. This should be read as the local stochastic deposition of resolidified workpiece material, not as an average composition of the whole wire surface. The strong spatial variation in Cu and Zn within run 20 also indicates the extent of coating degradation under high pulse-on time. Spectrum 2 in Table 9, with Cu = 73.57 wt.% and Zn = 22.33 wt.% (compared with the unworn coating composition of 37.87 wt.% Cu and 61.58 wt.% Zn in Table 7), shows that the γ-Cu5Zn8 coating has been locally removed and the underlying copper core is exposed at this location. This provides direct evidence that, at A = 1.2 µs, coating degradation reaches the stage where the copper core is locally engaged in the discharge process; in contrast, the EDS spectrum from the least worn electrode (run 9, Table 8), with Cu = 36.54 wt.% and Zn = 49.19 wt.%, remains close to the original coating composition. Coating wear and core exposure are therefore strongly dependent on pulse-on time within the investigated range.
This distinction matters for Δm, because gravimetry measures a net mass balance rather than pure electrode erosion. Electrode material is removed by melting, vaporisation, and crater formation, while resolidified Inconel 718 material can be locally deposited on the wire surface. The EDS evidence of Ni enrichment therefore indicates that the actual amount of electrode material removed may be partly masked by workpiece material transfer.
The oxygen results should be interpreted cautiously. The least worn electrode contained more oxygen than the most worn electrode, which suggests that oxide formation and retention depend on the balance between zinc-rich coating oxidation, coating erosion, and the deposition of workpiece-derived metals. A more definitive explanation would require time-resolved or more spatially extensive surface analysis.
The model statistics and residual diagnostics in Section 3.1 support the linear ANOVA model used here. The Ryan–Joiner result (p = 0.046) indicates a minor departure from strict normality, but the balanced factorial structure and the absence of variance heterogeneity make the inference acceptable for this exploratory design.
Several limitations should be kept in mind. First, the 33 factorial design was run without experimental replication, and the A × B × Aj interaction was pooled into the error term [20]. Replication would be needed for a direct pure-error estimate. Second, all runs used a fixed, relatively low wire feed speed (WS = 4 m·min−1), chosen to amplify the wear per unit wire length; the absolute Δm values should therefore not be transferred directly to production settings with higher feed speeds. Third, the conclusions apply to one electrode type (γ-Cu5Zn8-coated copper-core Elecut X) and one workpiece material (Inconel 718). Fourth, the reported factor contributions describe the relative effects of A, B, and Aj on the cumulative Δm accumulated within the 5 min stable-cutting condition tested in this study and are not intended to extrapolate directly to extended wire-life intervals; assessing the wear-rate evolution over longer cutting durations would require time-resolved measurements at multiple cutting times. Future work should include replicated designs, a wider WS range, comparisons with other electrode architectures, and time-resolved wear measurements at multiple cutting durations.
The dataset gives a practical basis for tuning electrode wear during the WEDM of Inconel 718. Because the response was measured across the full factorial space, the results support a clear wear-reduction strategy: use shorter pulse-on time as the primary control, and adjust the servo reference voltage and pulse-off time as the secondary controls. The final operating point, however, should also account for productivity and surface integrity.
Pulse-on time should therefore not be reduced in isolation. Lower A decreases electrode wear by supplying less energy per discharge, but it also reduces the energy available for workpiece removal and may lower the cutting speed or MRR. Liao and Yu [21] reported that, under steady WEDM conditions, shorter normal discharge on-time increases the discharge efficiency, whereas increasing the discharge on-time increases material removal but reduces the removed volume per unit input energy. The useful operating region is therefore a compromise between electrode consumption and productivity. A multi-response optimisation approach such as grey relational analysis (GRA) could be used in future work to combine Δm with the cutting speed or MRR and identify a more practical process setting.
These findings have direct implications for the design and optimisation of CNC wire EDM processes, particularly in the precision machining of nickel-based superalloys. The quantitative factor ranking established in this study—pulse-on time as the dominant driver of electrode wear, followed by servo reference voltage and pulse-off time—provides a concrete basis for informed parameter selection in CNC production environments. Because the CNC controller executes each programmed parameter combination deterministically, the present full factorial map of Δm can be translated directly into machining strategies: in applications where electrode consumption and process stability carry significant cost, pulse-on time should be treated as the primary optimisation variable, while the servo reference voltage and pulse-off time serve as secondary levers for fine-tuning. Combined with in-process monitoring approaches—such as the oscilloscope-based stability verification used here or closed-loop vision-based systems recently proposed for CNC WEDM [11]—the present results support the development of more adaptive and cost-efficient CNC machining strategies for Inconel 718 and related difficult-to-cut alloys used in aerospace and power-generation components.

5. Conclusions

This work examined the wear behaviour of the Elecut X wire electrode (ø 0.25 mm, gamma-phase Cu5Zn8 coating on a copper core) during the WEDM of Inconel 718 using a complete 33 factorial design. The main conclusions are:
  • Pulse-on time (A) was the dominant factor controlling wire electrode wear, contributing 88.45% of the total variance in mass loss Δm (F = 189.79, p < 0.001). This confirms the central role of discharge energy in electrode degradation and extends earlier findings for other difficult-to-machine materials to the present Inconel 718/Elecut X combination.
  • Servo reference voltage (Aj) and pulse-off time (B) had smaller but statistically significant effects, contributing 5.01% (p = 0.005) and 3.10% (p = 0.020), respectively, with no significant two-way interactions (p = 0.822); the three process parameters therefore mainly acted independently within the investigated range. The fitted ANOVA model described the data well (R2 = 98.14%, R2(adj) = 93.94%, and S = 0.0145), and residual diagnostics supported the model assumptions.
  • SEM/EDS observations support a transition from coating-dominated wear at low pulse-on time to local coating failure and copper-core exposure at high pulse-on time. The least worn electrode preserved a composition close to the original γ-Cu5Zn8 coating, whereas the most worn electrode showed severe cratering, local Zn depletion, Cu-core exposure, and workpiece material transfer, with Ni reaching 16.84 wt.% locally.
  • From the standpoint of electrode-wear reduction, decreasing the pulse-on time is the most effective control action. A higher servo reference voltage and longer pulse-off time can provide additional, secondary wear reduction and may improve process stability, but the final parameter choice should also consider cutting productivity.

Supplementary Materials

The following supporting information can be downloaded at: https://www.mdpi.com/article/10.3390/app16115235/s1, Supplementary Table S1 is provided as an Excel file and contains the raw gravimetric data for all 27 experimental runs, including the three repeated post-machining mass measurements (m1–m3), the calculated mean mass, and mass loss Δm.

Author Contributions

Conceptualization, V.Š.; methodology, V.Š.; investigation, V.Š., B.L. and V.K.; formal analysis, V.Š. and M.K.; resources, B.L.; data curation, V.Š.; writing—original draft preparation, V.Š.; writing—review and editing, M.K. and A.B.; visualisation, V.Š.; validation, V.Š., V.K., A.B. and O.B.; supervision, M.K.; project administration, M.K.; funding acquisition, V.Š. All authors have read and agreed to the published version of the manuscript.

Funding

This work was supported by the Slovak Research and Development Agency of the Slovak Republic under Contract no. APVV-21-0071, VEGA grant agency of the Ministry of Education, Science, Research and Sport of the Slovak Republic and the Slovak Academy of Sciences, no. 1/0266/23 and KEGA grant agency of the Ministry of Education, Science, Research and Sport of the Slovak Republic and the Slovak Academy of Sciences, no. 004TU Z-4/2024.

Institutional Review Board Statement

Not applicable.

Informed Consent Statement

Not applicable.

Data Availability Statement

The raw gravimetric measurement data supporting this study are provided in Supplementary Table S1. The original contributions presented in this study are included in the article/Supplementary Material. Further inquiries can be directed to the corresponding author.

Acknowledgments

The current paper was prepared during a research stay within the framework of the National Scholarship Program of the Slovak Republic (NSP SAIA). The article was prepared with the assistance and technical support of the non-governmental organisation “INDUSTRY 5.UA”. During the preparation of this manuscript, the authors used OpenAI ChatGPT (GPT-5, accessed April 2026) to support English-language editing, improve readability, and enhance stylistic consistency of the author-prepared text. The tool was not used for study design, data generation, data analysis, interpretation of results, preparation of figures or tables, or reference selection. All AI-assisted suggestions were critically reviewed, edited, and approved by the authors, who take full responsibility for the content of this publication.

Conflicts of Interest

The authors declare no conflicts of interest.

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Figure 1. Representative oscilloscope waveforms recorded during WEDM of Inconel 718 superalloy: CH1 (top, red)—gap voltage; CH2 (bottom, blue)—discharge current.
Figure 1. Representative oscilloscope waveforms recorded during WEDM of Inconel 718 superalloy: CH1 (top, red)—gap voltage; CH2 (bottom, blue)—discharge current.
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Figure 2. Inconel 718 workpiece (10 × 30 × 120 mm) mounted on the Charmilles Robofil 310 WEDM machine during the experiment.
Figure 2. Inconel 718 workpiece (10 × 30 × 120 mm) mounted on the Charmilles Robofil 310 WEDM machine during the experiment.
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Figure 3. Flow diagram of the experimental workflow.
Figure 3. Flow diagram of the experimental workflow.
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Figure 4. Graphical representation of wire electrode mass loss Δm for the 27 experimental runs. Bar colours distinguish the three pulse-on time levels: runs 1–9 (A = 0.4 µs), runs 10–18 (A = 0.8 µs), and runs 19–27 (A = 1.2 µs). Error bars represent the expanded measurement uncertainty U95 (k = 2) of the gravimetric procedure, as defined by Equation (2) in Section 2.
Figure 4. Graphical representation of wire electrode mass loss Δm for the 27 experimental runs. Bar colours distinguish the three pulse-on time levels: runs 1–9 (A = 0.4 µs), runs 10–18 (A = 0.8 µs), and runs 19–27 (A = 1.2 µs). Error bars represent the expanded measurement uncertainty U95 (k = 2) of the gravimetric procedure, as defined by Equation (2) in Section 2.
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Figure 5. Pareto chart of standardised effects for mass loss Δm (α = 0.05). Bars exceeding the reference line at 2.31 are statistically significant.
Figure 5. Pareto chart of standardised effects for mass loss Δm (α = 0.05). Bars exceeding the reference line at 2.31 are statistically significant.
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Figure 6. Normal probability plot of residuals for mass loss Δm. Points lying close to the reference line confirm approximate normality of the residual distribution.
Figure 6. Normal probability plot of residuals for mass loss Δm. Points lying close to the reference line confirm approximate normality of the residual distribution.
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Figure 7. Residuals versus fitted values for mass loss Δm. The random scatter around zero with no discernible pattern confirms homogeneity of variance.
Figure 7. Residuals versus fitted values for mass loss Δm. The random scatter around zero with no discernible pattern confirms homogeneity of variance.
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Figure 8. SEM micrograph of the new, unused Elecut X wire electrode (ø 0.25 mm). SEM magnification 300×.
Figure 8. SEM micrograph of the new, unused Elecut X wire electrode (ø 0.25 mm). SEM magnification 300×.
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Figure 9. SEM micrograph of the least worn Elecut X wire electrode after WEDM of Inconel 718 (run 9: A = 0.4 µs, B = 24 µs, Aj = 50 V, and Δm = 0.021 g). SEM magnification 300×.
Figure 9. SEM micrograph of the least worn Elecut X wire electrode after WEDM of Inconel 718 (run 9: A = 0.4 µs, B = 24 µs, Aj = 50 V, and Δm = 0.021 g). SEM magnification 300×.
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Figure 10. SEM micrograph of the most worn Elecut X wire electrode after WEDM of Inconel 718 (run 20: A = 1.2 µs, B = 16 µs, Aj = 40 V, and Δm = 0.199 g). SEM magnification 300×.
Figure 10. SEM micrograph of the most worn Elecut X wire electrode after WEDM of Inconel 718 (run 20: A = 1.2 µs, B = 16 µs, Aj = 40 V, and Δm = 0.199 g). SEM magnification 300×.
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Table 1. Chemical composition (wt.%) of Inconel 718.
Table 1. Chemical composition (wt.%) of Inconel 718.
NiCrFeMoNbTi
53.4018.3018.772.904.980.95
AlCoMnSiCuC
0.480.100.020.030.020.026
Table 2. Variable process parameters and their levels used in the full factorial experiment.
Table 2. Variable process parameters and their levels used in the full factorial experiment.
ParameterSymbolLevel 1Level 2Level 3Unit
Pulse-on timeA0.40.81.2µs
Pulse-off timeB162024µs
Servo reference voltageAj304050V
Table 3. Constant process parameters used throughout all experiments.
Table 3. Constant process parameters used throughout all experiments.
ParameterSymbolValueUnit
Wire tensionWb1daN
Discharge voltageU−80V
Wire feed speedWS4m·min−1
Dielectric injection pressureINJ3bar
Short pulse timeTAC0.4µs
Ignition currentIAL8A
Dielectric temperatureTd18°C
Dielectric conductivityσd12–16µS/cm
Table 4. Full factorial 33 design matrix (columns A, B, and Aj) and corresponding gravimetric measurement results for the Elecut X wire electrode during WEDM of Inconel 718 superalloy (27 runs). Initial electrode mass: 1.672 g (4 m segment).
Table 4. Full factorial 33 design matrix (columns A, B, and Aj) and corresponding gravimetric measurement results for the Elecut X wire electrode during WEDM of Inconel 718 superalloy (27 runs). Initial electrode mass: 1.672 g (4 m segment).
RunA (µs)B (µs)Aj (V)Mean ± SD (g)Δm ± U95 (g)
10.416301.614 ± 0.0010.058 ± 0.001
20.416401.627 ± 0.0020.045 ± 0.002
30.416501.643 ± 0.0020.029 ± 0.002
40.420301.626 ± 0.0020.046 ± 0.002
50.420401.633 ± 0.0020.039 ± 0.002
60.420501.636 ± 0.0010.036 ± 0.001
70.424301.633 ± 0.0020.039 ± 0.002
80.424401.636 ± 0.0010.036 ± 0.001
90.424501.651 ± 0.0010.021 ± 0.001
100.816301.552 ± 0.0010.120 ± 0.001
110.816401.568 ± 0.0020.104 ± 0.002
120.816501.587 ± 0.0020.085 ± 0.002
130.820301.565 ± 0.0010.107 ± 0.001
140.820401.579 ± 0.0020.093 ± 0.002
150.820501.608 ± 0.0020.064 ± 0.002
160.824301.585 ± 0.0030.087 ± 0.003
170.824401.604 ± 0.0020.068 ± 0.002
180.824501.611 ± 0.0010.061 ± 0.001
191.216301.500 ± 0.0030.172 ± 0.003
201.216401.473 ± 0.0020.199 ± 0.002
211.216501.493 ± 0.0020.179 ± 0.002
221.220301.475 ± 0.0010.197 ± 0.001
231.220401.486 ± 0.0010.186 ± 0.001
241.220501.525 ± 0.0020.147 ± 0.003
251.224301.485 ± 0.0030.187 ± 0.003
261.224401.513 ± 0.0010.159 ± 0.001
271.224501.560 ± 0.0010.112 ± 0.001
Table 5. Analysis of variance (ANOVA) for mass loss Δm of the Elecut X wire electrode during WEDM of Inconel 718.
Table 5. Analysis of variance (ANOVA) for mass loss Δm of the Elecut X wire electrode during WEDM of Inconel 718.
SourceDFSeq SSContributionAdj SSAdj MSFp
Model180.08885798.14%0.0888570.00493623.40<0.001
 Linear60.08743096.56%0.0874300.01457269.06<0.001
  A20.08008788.45%0.0800870.040043189.79<0.001
  B20.0028073.10%0.0028070.0014046.650.020
  Aj20.0045375.01%0.0045370.00226810.750.005
 2-way interactions120.0014261.58%0.0014260.0001190.560.822
  A × B40.0004370.48%0.0004370.0001090.520.726
  A × Aj40.0006210.69%0.0006210.0001550.740.593
  B × Aj40.0003680.41%0.0003680.0000920.440.779
Error80.0016881.86%0.0016880.000211
Total260.090544100.00%
Table 6. Summary statistics of the fitted ANOVA model.
Table 6. Summary statistics of the fitted ANOVA model.
SR2R2 (adj)R2 (pred)
0.014525498.14%93.94%78.77%
Table 7. EDS analysis of the new, unused Elecut X wire electrode (in wt.%).
Table 7. EDS analysis of the new, unused Elecut X wire electrode (in wt.%).
SpectrumFe (wt.%)Cu (wt.%)Zn (wt.%)Total
Spectrum 10.5537.8761.58100.00
Table 8. EDS analysis of the least worn Elecut X wire electrode (run 9) (in wt.%).
Table 8. EDS analysis of the least worn Elecut X wire electrode (run 9) (in wt.%).
SpectrumOCrFeNiCuZnTotal
Spectrum 110.240.911.231.9036.5449.19100.00
Table 9. EDS analysis of the most worn Elecut X wire electrode (run 20) (in wt.%).
Table 9. EDS analysis of the most worn Elecut X wire electrode (run 20) (in wt.%).
SpectrumOCrFeNiCuZnTotal
Spectrum 15.493.240.5516.8455.9217.96100.00
Spectrum 21.960.300.571.2773.5722.33100.00
Spectrum 32.660.520.342.6256.4037.45100.00
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Šimna, V.; Kuruc, M.; Ludrovcová, B.; Belanec, A.; Kolesnyk, V.; Berezniak, O. Wire Electrode Wear in WEDM of Inconel 718: Gravimetric Evaluation Using a 33 Full Factorial Design. Appl. Sci. 2026, 16, 5235. https://doi.org/10.3390/app16115235

AMA Style

Šimna V, Kuruc M, Ludrovcová B, Belanec A, Kolesnyk V, Berezniak O. Wire Electrode Wear in WEDM of Inconel 718: Gravimetric Evaluation Using a 33 Full Factorial Design. Applied Sciences. 2026; 16(11):5235. https://doi.org/10.3390/app16115235

Chicago/Turabian Style

Šimna, Vladimír, Marcel Kuruc, Barbora Ludrovcová, Adam Belanec, Vitalii Kolesnyk, and Oleksandr Berezniak. 2026. "Wire Electrode Wear in WEDM of Inconel 718: Gravimetric Evaluation Using a 33 Full Factorial Design" Applied Sciences 16, no. 11: 5235. https://doi.org/10.3390/app16115235

APA Style

Šimna, V., Kuruc, M., Ludrovcová, B., Belanec, A., Kolesnyk, V., & Berezniak, O. (2026). Wire Electrode Wear in WEDM of Inconel 718: Gravimetric Evaluation Using a 33 Full Factorial Design. Applied Sciences, 16(11), 5235. https://doi.org/10.3390/app16115235

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