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Keywords = vibrational property

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12 pages, 2376 KiB  
Article
Investigating Helium-Induced Thermal Conductivity Degradation in Fusion-Relevant Copper: A Molecular Dynamics Approach
by Xu Yu, Hanlong Wang and Hai Huang
Materials 2025, 18(15), 3702; https://doi.org/10.3390/ma18153702 - 6 Aug 2025
Abstract
Copper alloys are critical heat sink materials for fusion reactor divertors due to their high thermal conductivity (TC) and strength, yet their performance under extreme particle bombardment and heat fluxes in future tokamaks requires enhancement. While neutron-induced transmutation helium affects the properties of [...] Read more.
Copper alloys are critical heat sink materials for fusion reactor divertors due to their high thermal conductivity (TC) and strength, yet their performance under extreme particle bombardment and heat fluxes in future tokamaks requires enhancement. While neutron-induced transmutation helium affects the properties of copper, the atomistic mechanisms linking helium bubble size to thermal transport remain unclear. This study employs non-equilibrium molecular dynamics (NEMD) simulations to isolate the effect of bubble diameter (10, 20, 30, 40 Å) on TC in copper, maintaining a constant He-to-vacancy ratio of 2.5. Results demonstrate that larger bubbles significantly impair TC. This reduction correlates with increased Kapitza thermal resistance and pronounced lattice distortion from outward helium diffusion, intensifying phonon scattering. Phonon density of states (PDOS) analysis reveals diminished low-frequency peaks and an elevated high-frequency peak for bubbles >30 Å, confirming phonon confinement and localized vibrational modes. The PDOS overlap factor decreases with bubble size, directly linking microstructural evolution to thermal resistance. These findings elucidate the size-dependent mechanisms of helium bubble impacts on thermal transport in copper divertor materials. Full article
(This article belongs to the Special Issue Advances in Computation and Modeling of Materials Mechanics)
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29 pages, 3167 KiB  
Article
A Comparative Evaluation of Polymer-Modified Rapid-Set Calcium Sulfoaluminate Concrete: Bridging the Gap Between Laboratory Shrinkage and the Field Strain Performance
by Daniel D. Akerele and Federico Aguayo
Buildings 2025, 15(15), 2759; https://doi.org/10.3390/buildings15152759 - 5 Aug 2025
Abstract
Rapid pavement repair demands materials that combine accelerated strength gains, dimensional stability, long-term durability, and sustainability. However, finding materials or formulations that offer these balances remains a critical challenge. This study systematically evaluates two polymer-modified belitic calcium sulfoaluminate (CSA) concretes—CSAP (powdered polymer) and [...] Read more.
Rapid pavement repair demands materials that combine accelerated strength gains, dimensional stability, long-term durability, and sustainability. However, finding materials or formulations that offer these balances remains a critical challenge. This study systematically evaluates two polymer-modified belitic calcium sulfoaluminate (CSA) concretes—CSAP (powdered polymer) and CSA-LLP (liquid polymer admixture)—against a traditional Type III Portland cement (OPC) control under both laboratory and realistic outdoor conditions. Laboratory specimens were tested for fresh properties, early-age and later-age compressive, flexural, and splitting tensile strengths, as well as drying shrinkage according to ASTM standards. Outdoor 5 × 4 × 12-inch slabs mimicking typical jointed plain concrete panels (JPCPs), instrumented with vibrating wire strain gauges and thermocouples, recorded the strain and temperature at 5 min intervals over 16 weeks, with 24 h wet-burlap curing to replicate field practices. Laboratory findings show that CSA mixes exceeded 3200 psi of compressive strength at 4 h, but cold outdoor casting (~48 °F) delayed the early-age strength development. The CSA-LLP exhibited the lowest drying shrinkage (0.036% at 16 weeks), and outdoor CSA slabs captured the initial ettringite-driven expansion, resulting in a net expansion (+200 µε) rather than contraction. Approximately 80% of the total strain evolved within the first 48 h, driven by autogenous and plastic effects. CSA mixes generated lower peak internal temperatures and reduced thermal strain amplitudes compared to the OPC, improving dimensional stability and mitigating restraint-induced cracking. These results underscore the necessity of field validation for shrinkage compensation mechanisms and highlight the critical roles of the polymer type and curing protocol in optimizing CSA-based repairs for durable, low-carbon pavement rehabilitation. Full article
(This article belongs to the Special Issue Study on Concrete Structures—2nd Edition)
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29 pages, 2636 KiB  
Review
Review on Tribological and Vibration Aspects in Mechanical Bearings of Electric Vehicles: Effect of Bearing Current, Shaft Voltage, and Electric Discharge Material Spalling Current
by Rohan Lokhande, Sitesh Kumar Mishra, Deepak Ronanki, Piyush Shakya, Vimal Edachery and Lijesh Koottaparambil
Lubricants 2025, 13(8), 349; https://doi.org/10.3390/lubricants13080349 - 5 Aug 2025
Viewed by 69
Abstract
Electric motors play a decisive role in electric vehicles by converting electrical energy into mechanical motion across various drivetrain components. However, failures in these motors can interrupt the motor function, with approximately 40% of these failures stemming from bearing issues. Key contributors to [...] Read more.
Electric motors play a decisive role in electric vehicles by converting electrical energy into mechanical motion across various drivetrain components. However, failures in these motors can interrupt the motor function, with approximately 40% of these failures stemming from bearing issues. Key contributors to bearing degradation include shaft voltage, bearing current, and electric discharge material spalling current, especially in motors powered by inverters or variable frequency drives. This review explores the tribological and vibrational aspects of bearing currents, analyzing their mechanisms and influence on electric motor performance. It addresses the challenges faced by electric vehicles, such as high-speed operation, elevated temperatures, electrical conductivity, and energy efficiency. This study investigates the origins of bearing currents, damage linked to shaft voltage and electric discharge material spalling current, and the effects of lubricant properties on bearing functionality. Moreover, it covers various methods for measuring shaft voltage and bearing current, as well as strategies to alleviate the adverse impacts of bearing currents. This comprehensive analysis aims to shed light on the detrimental effects of bearing currents on the performance and lifespan of electric motors in electric vehicles, emphasizing the importance of tribological considerations for reliable operation and durability. The aim of this study is to address the engineering problem of bearing failure in inverter-fed EV motors by integrating electrical, tribological, and lubrication perspectives. The novelty lies in proposing a conceptual link between lubricant breakdown and damage morphology to guide mitigation strategies. The study tasks include literature review, analysis of bearing current mechanisms and diagnostics, and identification of technological trends. The findings provide insights into lubricant properties and diagnostic approaches that can support industrial solutions. Full article
(This article belongs to the Special Issue Tribology of Electric Vehicles)
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20 pages, 3145 KiB  
Article
Determination of Dynamic Elastic Properties of 3D-Printed Nylon 12CF Using Impulse Excitation of Vibration
by Pedro F. Garcia, Armando Ramalho, Joel C. Vasco, Rui B. Ruben and Carlos Capela
Polymers 2025, 17(15), 2135; https://doi.org/10.3390/polym17152135 - 4 Aug 2025
Viewed by 210
Abstract
Material Extrusion (MEX) process is increasingly used to fabricate components for structural applications, driven by the availability of advanced materials and greater industrial adoption. In these contexts, understanding the mechanical performance of printed parts is crucial. However, conventional methods for assessing anisotropic elastic [...] Read more.
Material Extrusion (MEX) process is increasingly used to fabricate components for structural applications, driven by the availability of advanced materials and greater industrial adoption. In these contexts, understanding the mechanical performance of printed parts is crucial. However, conventional methods for assessing anisotropic elastic behavior often rely on expensive equipment and time-consuming procedures. The aim of this study is to evaluate the applicability of the impulse excitation of vibration (IEV) in characterizing the dynamic mechanical properties of a 3D-printed composite material. Tensile tests were also performed to compare quasi-static properties with the dynamic ones obtained through IEV. The tested material, Nylon 12CF, contains 35% short carbon fibers by weight and is commercially available from Stratasys. It is used in the fused deposition modeling (FDM) process, a Material Extrusion technology, and exhibits anisotropic mechanical properties. This is further reinforced by the filament deposition process, which affects the mechanical response of printed parts. Young’s modulus obtained in the direction perpendicular to the deposition plane (E33), obtained via IEV, was 14.77% higher than the value in the technical datasheet. Comparing methods, the Young’s modulus obtained in the deposition plane, in an inclined direction of 45 degrees in relation to the deposition direction (E45), showed a 22.95% difference between IEV and tensile tests, while Poisson’s ratio in the deposition plane (v12) differed by 6.78%. This data is critical for designing parts subject to demanding service conditions, and the results obtained (orthotropic elastic properties) can be used in finite element simulation software. Ultimately, this work reinforces the potential of the IEV method as an accessible and consistent alternative for characterizing the anisotropic properties of components produced through additive manufacturing (AM). Full article
(This article belongs to the Special Issue Mechanical Characterization of Polymer Composites)
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19 pages, 9135 KiB  
Article
A Study on the Characterization of Asphalt Plant Reclaimed Powder Using Fourier Transform Infrared Spectroscopy
by Hao Wu, Daoan Yu, Wentao Wang, Chuanqi Yan, Rui Xiao, Rong Chen, Peng Zhang and Hengji Zhang
Materials 2025, 18(15), 3660; https://doi.org/10.3390/ma18153660 - 4 Aug 2025
Viewed by 176
Abstract
Asphalt plant reclaimed powder is a common solid waste in road engineering. Reusing reclaimed powder as filler holds significant importance for environmental protection and resource conservation. The key factors affecting the feasibility of reclaimed powder reuse are its acidity/alkalinity and cleanliness. Traditional evaluation [...] Read more.
Asphalt plant reclaimed powder is a common solid waste in road engineering. Reusing reclaimed powder as filler holds significant importance for environmental protection and resource conservation. The key factors affecting the feasibility of reclaimed powder reuse are its acidity/alkalinity and cleanliness. Traditional evaluation methods, such as the methylene blue test and plasticity index, can assess reclaimed powder properties to guide its recycling. However, these methods suffer from inefficiency, strong empirical dependence, and high variability. To address these limitations, this study proposes a rapid and precise evaluation method for reclaimed powder properties based on Fourier transform infrared spectroscopy (FTIR). To do so, five field-collected reclaimed powder samples and four artificial samples were evaluated. Scanning electron microscopy (SEM), X-ray fluorescence spectroscopy (XRF), and X-ray diffraction (XRD) were employed to characterize their microphase morphology, chemical composition, and crystal structure, respectively. Subsequently, FTIR was used to establish correlations between key acidity/alkalinity, cleanliness, and multiple characteristic peak intensities. Representative infrared characteristic peaks were selected, and a quantitative functional group index (Is) was proposed to simultaneously evaluate acidity/alkalinity and cleanliness. The results indicate that reclaimed powder primarily consists of tiny, crushed stone particles and dust, with significant variations in crystal structure and chemical composition, including calcium carbonate, silicon oxide, iron oxide, and aluminum oxide. Some samples also contained clay, which critically influenced the reclaimed powder properties. Since both filler acidity/alkalinity and cleanliness are affected by clay (silicon/carbon ratio determining acidity/alkalinity and aluminosilicate content affecting cleanliness), this study calculated four functional group indices based on FTIR absorption peaks, namely the Si-O-Si stretching vibration (1000 cm−1) and the CO32− asymmetric stretching vibration (1400 cm−1). These indices were correlated with conventional testing results (XRF for acidity/alkalinity, methylene blue value, and pull-off strength for cleanliness). The results show that the Is index exhibited strong correlations (R2 = 0.89 with XRF, R2 = 0.80 with methylene blue value, and R2 = 0.96 with pull-off strength), demonstrating its effectiveness in predicting both acidity/alkalinity and cleanliness. The developed method enhances reclaimed powder detection efficiency and facilitates high-value recycling in road engineering applications. Full article
(This article belongs to the Special Issue Innovative Approaches in Asphalt Binder Modification and Performance)
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21 pages, 14595 KiB  
Article
Synchronous Improvement of Mechanical and Room-Temperature Damping Performance in Light-Weight Polyurethane Composites by a Simple Carbon-Coating Strategy
by Qitan Zheng, Zhongzheng Zhu, Junyi Yao, Qinyu Sun, Qunfu Fan, Hezhou Liu, Qiuxia Dong and Hua Li
Polymers 2025, 17(15), 2115; https://doi.org/10.3390/polym17152115 - 31 Jul 2025
Viewed by 279
Abstract
In order to address vibration and noise challenges in modern industry while satisfying the lightweighting requirements for aerospace and transportation applications, the development of polymer elastomers integrating both lightweight and high-damping properties holds substantial significance. This study developed polyurethane (PU) with optimized damping [...] Read more.
In order to address vibration and noise challenges in modern industry while satisfying the lightweighting requirements for aerospace and transportation applications, the development of polymer elastomers integrating both lightweight and high-damping properties holds substantial significance. This study developed polyurethane (PU) with optimized damping and mechanical properties at room temperature through monomer composition optimization. Hollow glass microspheres (HGMs) were introduced into the PU matrix to increase stiffness and reduce density, though this resulted in decreased tensile strength (Rm) and loss factor (tanδ). To further improve mechanical and damping properties, we applied a carbon coating to the surface of the HGMs to optimize the interface between the HGMs and the PU matrix, and systematically investigated the energy dissipation and load-bearing behavior of PU composites. The effect of enhanced interface damping of HGM@C/PU resulted in broadening of the effective damping temperature range (tanδ ≥ 0.3) and higher maximum loss factor (tanδmax) compared to HGM/PU at equivalent filler loading. The tensile and dynamic properties significantly improved due to optimized interfacial adhesion. In PU composites reinforced with 10 wt% HGM and HGM@C, a 46.8% improvement in Rm and 11.0% improvement in tanδmax occurred after carbon coating. According to acoustic testing, average transmission loss of HGM/PU and HGM@C/PU with the same filler content showed a difference of 0.3–0.5 dB in 500–6300 Hz, confirming that the hollow structure of the HGMs was preserved during carbon coating. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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17 pages, 3995 KiB  
Article
Nonlinear Vibration and Post-Buckling Behaviors of Metal and FGM Pipes Transporting Heavy Crude Oil
by Kamran Foroutan, Farshid Torabi and Arth Pradeep Patel
Appl. Sci. 2025, 15(15), 8515; https://doi.org/10.3390/app15158515 - 31 Jul 2025
Viewed by 102
Abstract
Functionally graded materials (FGMs) have the potential to revolutionize the oil and gas transportation sector, due to their increased strengths and efficiencies as pipelines. Conventional pipelines frequently face serious problems such as extreme weather, pressure changes, corrosion, and stress-induced pipe bursts. By analyzing [...] Read more.
Functionally graded materials (FGMs) have the potential to revolutionize the oil and gas transportation sector, due to their increased strengths and efficiencies as pipelines. Conventional pipelines frequently face serious problems such as extreme weather, pressure changes, corrosion, and stress-induced pipe bursts. By analyzing the mechanical and thermal performance of FGM-based pipes under various operating conditions, this study investigates the possibility of using them as a more reliable substitute. In the current study, the post-buckling and nonlinear vibration behaviors of pipes composed of FGMs transporting heavy crude oil were examined using a Timoshenko beam framework. The material properties of the FGM pipe were observed to change gradually across the thickness, following a power-law distribution, and were influenced by temperature variations. In this regard, two types of FGM pipes are considered: one with a metal-rich inner surface and ceramic-rich outer surface, and the other with a reverse configuration featuring metal on the outside and ceramic on the inside. The nonlinear governing equations (NGEs) describing the system’s nonlinear dynamic response were formulated by considering nonlinear strain terms through the von Kármán assumptions and employing Hamilton’s principle. These equations were then discretized using Galerkin’s method to facilitate the analytical investigation. The Runge–Kutta method was employed to address the nonlinear vibration problem. It is concluded that, compared with pipelines made from conventional materials, those constructed with FGMs exhibit enhanced thermal resistance and improved mechanical strength. Full article
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31 pages, 5334 KiB  
Article
Tailoring a Three-Layer Track Model to Delay Instability and Minimize Critical Velocity Effects at Very High Velocities
by Zuzana Dimitrovová
Infrastructures 2025, 10(8), 200; https://doi.org/10.3390/infrastructures10080200 - 31 Jul 2025
Viewed by 102
Abstract
The aim of this paper is to tailor the geometry and material parameters of a three-layer railway track model to achieve favorable properties for the circulation of high-speed trains at very high velocities. The three layers imply that the model should have three [...] Read more.
The aim of this paper is to tailor the geometry and material parameters of a three-layer railway track model to achieve favorable properties for the circulation of high-speed trains at very high velocities. The three layers imply that the model should have three critical velocities for resonance. However, in many cases, some of these values are missing and must be replaced by pseudo-critical values. Since no resonance occurs at pseudo-critical velocities, even in the absence of damping, deflections never reach infinity. By using optimization techniques, it is possible to adjust the model’s parameters, so that the increase in vibrations remains minimal and does not pose a real danger. In this way, circulation velocities could be extended beyond the critical value, thereby increasing the network capacity and, consequently, improving the competitiveness of rail transport compared to other modes of transportation, thus contributing to decarbonization. The presented results are preliminary and require further analysis and validation. Several optimization techniques are implemented, leading to the establishment of designs that already have rather high pseudo-critical velocities. Further research will show how these theoretical findings can be utilized in practice. Full article
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21 pages, 1569 KiB  
Article
A Multibody-Based Benchmarking Framework for the Control of the Furuta Pendulum
by Gerardo Peláez, Pablo Izquierdo, Gustavo Peláez and Higinio Rubio
Actuators 2025, 14(8), 377; https://doi.org/10.3390/act14080377 - 31 Jul 2025
Viewed by 161
Abstract
The Furuta pendulum is a well-known benchmark in the field of underactuated mechanical systems due to its reduced number of control inputs compared to its degrees of freedom, and richly nonlinear behavior. This work addresses the challenge of accurately modeling and controlling such [...] Read more.
The Furuta pendulum is a well-known benchmark in the field of underactuated mechanical systems due to its reduced number of control inputs compared to its degrees of freedom, and richly nonlinear behavior. This work addresses the challenge of accurately modeling and controlling such a system without relying on traditional linearization techniques. In contrast to the common approach based on Lagrangian analytical modeling and state–space linearization, we propose a methodology that integrates a high-fidelity multibody model developed in Simscape Multibody (MATLAB), capturing the complete nonlinear dynamics of the system. The multibody model includes all geometric, inertial, and joint parameters of the physical hardware and interfaces directly with Simulink, enabling realistic simulation and control integration. To validate the physical fidelity of the multibody model, we perform a frequency-domain analysis of the pendulum’s natural free response. The dominant vibration frequency extracted from the simulation is compared with the theoretical prediction, demonstrating accurate capture of the system’s inertial and dynamic properties. This validation strategy strengthens the reliability of the model as a digital twin. The classical analytical formulation is provided to validate the simulation model and serve as a comparative framework. This dual modeling strategy allows for benchmarking control strategies against a trustworthy nonlinear digital twin of the Furuta pendulum. Preliminary experimental results using a physical prototype validate the feasibility of the proposed approach and set the foundation for future work in advanced nonlinear control design using the multibody representation as a digital validation tool. Full article
(This article belongs to the Special Issue Dynamics and Control of Underactuated Systems)
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16 pages, 1867 KiB  
Review
Histological Processing of Scaffolds: Challenges and Solutions
by Tomas Ragauskas, Ilona Uzieliene and Eiva Bernotiene
J. Funct. Biomater. 2025, 16(8), 279; https://doi.org/10.3390/jfb16080279 - 31 Jul 2025
Viewed by 344
Abstract
Scaffolds are widely used in bioengineering, both as 3D native tissue-mimicking models for investigating mechanisms under physiological and pathological conditions and also as implantable agents in regenerative medicine. Histological approaches, mainly formalin-fixed paraffin-embedded (FFPE) and frozen sample sectioning, are commonly applied to evaluate [...] Read more.
Scaffolds are widely used in bioengineering, both as 3D native tissue-mimicking models for investigating mechanisms under physiological and pathological conditions and also as implantable agents in regenerative medicine. Histological approaches, mainly formalin-fixed paraffin-embedded (FFPE) and frozen sample sectioning, are commonly applied to evaluate cell distribution and tissue-like properties of scaffolds. However, standard histological processing is not always compatible with the materials that scaffolds are made of. Thus, some adaptations to protocols are required to obtain intact sections. In this review we discuss challenges related to the histological processing of scaffolds and solutions to overcome them. We sequentially cover processing steps of the three main histological techniques for sample preparation—cryomicrotomy, FFPE samples microtomy and vibrating microtomy. Furthermore, we highlight the critical considerations in choosing the most appropriate method based on scaffold composition, mechanical properties and the specific research question. The goal of this review is to provide practical guidance on choosing reliable histological evaluation of complex scaffold-based systems in tissue engineering research. Full article
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10 pages, 1596 KiB  
Article
Investigating the Effect of Hydrogen Bonding on the Viscosity of an Aqueous Methanol Solution Using Raman Spectroscopy
by Nan-Nan Wu, Fang Liu, Zonghang Li, Ziyun Qiu, Xiaofan Li, Junhui Huang, Bohan Li, Junxi Qiu and Shun-Li Ouyang
Molecules 2025, 30(15), 3204; https://doi.org/10.3390/molecules30153204 - 30 Jul 2025
Viewed by 184
Abstract
Water science has always been a central part of modern scientific research. In this study, the viscosity and hydrogen bond structures of methanol aqueous solutions with different molar ratios were investigated via confocal microscopic Raman spectroscopy. The Raman spectra of methanol in the [...] Read more.
Water science has always been a central part of modern scientific research. In this study, the viscosity and hydrogen bond structures of methanol aqueous solutions with different molar ratios were investigated via confocal microscopic Raman spectroscopy. The Raman spectra of methanol in the CH and CO stretching regions were measured in order to investigate the structure of water/methanol molecules. The points of transition were identified by observing changes in viscosity following changes in concentration, and the bands were assigned to the C-H bond vibration shifts where the molar ratios of methanol and water were 1:3 and 3:1. Furthermore, the large band shift of 19 cm−1 between the methanol solutions with the lowest and highest concentrations contained three hydrogen bond network modes, affecting the viscosity of the solution. This study provides an explanation for the relationship between the microstructures and macroscopic properties of aqueous solutions. Full article
(This article belongs to the Section Molecular Liquids)
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19 pages, 4569 KiB  
Article
Tailored Magnetic Fe3O4-Based Core–Shell Nanoparticles Coated with TiO2 and SiO2 via Co-Precipitation: Structure–Property Correlation for Medical Imaging Applications
by Elena Emanuela Herbei, Daniela Laura Buruiana, Alina Crina Muresan, Viorica Ghisman, Nicoleta Lucica Bogatu, Vasile Basliu, Claudiu-Ionut Vasile and Lucian Barbu-Tudoran
Diagnostics 2025, 15(15), 1912; https://doi.org/10.3390/diagnostics15151912 - 30 Jul 2025
Viewed by 183
Abstract
Background/Objectives: Magnetic nanoparticles, particularly iron oxide-based materials, such as magnetite (Fe3O4), have gained significant attention as contrast agents in medical imaging This study aimsto syntheze and characterize Fe3O4-based core–shell nanostructures, including Fe3O4 [...] Read more.
Background/Objectives: Magnetic nanoparticles, particularly iron oxide-based materials, such as magnetite (Fe3O4), have gained significant attention as contrast agents in medical imaging This study aimsto syntheze and characterize Fe3O4-based core–shell nanostructures, including Fe3O4@TiO2 and Fe3O4@SiO2, and to evaluate their potential as tunable contrast agents for diagnostic imaging. Methods: Fe3O4, Fe3O4@TiO2, and Fe3O4@SiO2 nanoparticles were synthesized via co-precipitation at varying temperatures from iron salt precursors. Fourier transform infrared spectroscopy (FTIR) was used to confirm the presence of Fe–O bonds, while X-ray diffraction (XRD) was employed to determine the crystalline phases and estimate average crystallite sizes. Morphological analysis and particle size distribution were assessed by scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDX) and transmission electron microscopy (TEM). Magnetic properties were investigated using vibrating sample magnetometry (VSM). Results: FTIR spectra exhibited characteristic Fe–O vibrations at 543 cm−1 and 555 cm−1, indicating the formation of magnetite. XRD patterns confirmed a dominant cubic magnetite phase, with the presence of rutile TiO2 and stishovite SiO2 in the coated samples. The average crystallite sizes ranged from 24 to 95 nm. SEM and TEM analyses revealed particle sizes between 5 and 150 nm with well-defined core–shell morphologies. VSM measurements showed saturation magnetization (Ms) values ranging from 40 to 70 emu/g, depending on the synthesis temperature and shell composition. The highest Ms value was obtained for uncoated Fe3O4 synthesized at 94 °C. Conclusions: The synthesized Fe3O4-based core–shell nanomaterials exhibit desirable structural, morphological, and magnetic properties for use as contrast agents. Their tunable magnetic response and nanoscale dimensions make them promising candidates for advanced diagnostic imaging applications. Full article
(This article belongs to the Section Medical Imaging and Theranostics)
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17 pages, 2616 KiB  
Article
Investigation of the Dynamic Characterization of Traditional and Modern Building Materials Using an Impact Excitation Test
by Anil Ozdemir
Buildings 2025, 15(15), 2682; https://doi.org/10.3390/buildings15152682 - 30 Jul 2025
Viewed by 246
Abstract
This study presents a comprehensive non-destructive evaluation of a broad range of construction materials using the impulse excitation of vibration (IEV) technique. Tested specimens included low- and normal-strength concrete, fiber-reinforced concrete (with basalt, polypropylene, and glass fibers), lime mortars (NHL-2 and -3.5), plaster, [...] Read more.
This study presents a comprehensive non-destructive evaluation of a broad range of construction materials using the impulse excitation of vibration (IEV) technique. Tested specimens included low- and normal-strength concrete, fiber-reinforced concrete (with basalt, polypropylene, and glass fibers), lime mortars (NHL-2 and -3.5), plaster, and clay bricks (light and dark). Compressive and flexural strength tests complemented dynamic resonance testing on the same samples to ensure full mechanical characterization. Flexural and torsional resonance frequencies were used to calculate dynamic elastic modulus, shear modulus, and Poisson’s ratio. Strong correlations were observed between dynamic elastic modulus and shear modulus, supporting the compatibility of dynamic results with the classical elasticity theory. Flexural frequencies were more sensitive to material differences than torsional ones. Fiber additives, particularly basalt and polypropylene, significantly improved dynamic stiffness, increasing the dynamic elastic modulus/compressive strength ratio by up to 23%. In contrast, normal-strength concrete exhibited limited stiffness improvement despite higher strength. These findings highlight the reliability of IEV in mechanical properties across diverse material types and provide comparative reference data for concrete and masonry applications. Full article
(This article belongs to the Special Issue Advanced Studies in Structure Materials—2nd Edition)
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30 pages, 5612 KiB  
Review
In-Situ Monitoring and Process Control in Material Extrusion Additive Manufacturing: A Comprehensive Review
by Alexander Isiani, Kelly Crittenden, Leland Weiss, Okeke Odirachukwu, Ramanshu Jha, Okoye Johnson and Osinachi Abika
J. Exp. Theor. Anal. 2025, 3(3), 21; https://doi.org/10.3390/jeta3030021 - 29 Jul 2025
Viewed by 237
Abstract
Material extrusion additive manufacturing (MEAM) has emerged as a versatile and widely adopted 3D printing technology due to its cost-effectiveness and ability to process a diverse range of materials. However, achieving consistent part quality and repeatability remains a challenge, mainly due to variations [...] Read more.
Material extrusion additive manufacturing (MEAM) has emerged as a versatile and widely adopted 3D printing technology due to its cost-effectiveness and ability to process a diverse range of materials. However, achieving consistent part quality and repeatability remains a challenge, mainly due to variations in process parameters and material behavior during fabrication. In-situ monitoring and advanced process control systems have been increasingly integrated into MEAM to address these issues, enabling real-time detection of defects, optimization of printing conditions, reliability of fabricated parts, and enhanced control over mechanical properties. This review examines the state-of-the-art in-situ monitoring techniques, including thermal imaging, vibrational sensing, rheological monitoring, printhead positioning, acoustic sensing, image recognition, and optical scanning, and their integration with process control strategies, such as closed-loop feedback systems and machine learning algorithms. Key challenges, including sensor accuracy, data processing complexity, and scalability, are discussed alongside recent advancements and their implications for industrial applications. By synthesizing current research, this work highlights the critical role of in-situ monitoring and process control in advancing the reliability and precision of MEAM, paving the way for its broader adoption in high-performance manufacturing. Full article
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21 pages, 2195 KiB  
Article
Physicochemical and Sensory Analysis of Apple Cream Fillings for Use in the Pastry Industry
by Marios Liampotis, Zacharias Ioannou, Kosmas Ellinas and Konstantinos Gkatzionis
Appl. Sci. 2025, 15(15), 8386; https://doi.org/10.3390/app15158386 - 29 Jul 2025
Viewed by 261
Abstract
The sensory and physicochemical properties of three different recipes for apple cream filling were investigated, focusing on their potential to enhance consumer appeal in pastry applications. Two of the recipes incorporate dried apple cubes (AP1, 48% and AP2, 38% w/w, respectively), while [...] Read more.
The sensory and physicochemical properties of three different recipes for apple cream filling were investigated, focusing on their potential to enhance consumer appeal in pastry applications. Two of the recipes incorporate dried apple cubes (AP1, 48% and AP2, 38% w/w, respectively), while the third recipe (PD) features a cube-free formulation with higher quantities of sugar, potato starch, xanthan gum, dextrose, cinnamon and malic acid. The study evaluated the impact of ingredient composition and processing techniques on sensory attributes. The results indicate that AP1 and AP2 resulted in higher moisture, ash and fiber content but lower viscosity, pH values and emulsion stability compared to PD. All samples exhibited pseudoplastic behavior. The AP2 sample exhibited the most hydrophilic behavior. FT-IR spectra have shown three main peaks, i.e., O-H (3300–3320 cm−1), C=O (1640–1730 cm−1) and C-O (1025–1030 cm−1) stretching vibrations. AP1 and AP2 significantly enhanced hardness and cohesion, providing a more engaging sensory experience. PD offers a smoother, creamier texture with lower inhomogeneity compared to AP1 and AP2 samples, making it ideal for consumers who prefer a uniform mouthfeel. This research demonstrates the critical role of formulation choices in tailoring sensory and physicochemical properties of apple cream fillings to meet diverse consumer preferences. Full article
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