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26 pages, 6942 KB  
Article
Application of the Akaike Information Criterion to Ultrasonic Measurement of Liquid Volume in a Cylindrical Tank
by Krzysztof J. Opieliński and Tomasz Świetlik
Sensors 2025, 25(23), 7191; https://doi.org/10.3390/s25237191 - 25 Nov 2025
Viewed by 508
Abstract
The ultrasonic sensor method is the most significant and widely accepted technique for measuring liquid levels in tanks. Ultrasonic waves are particularly advantageous in the case of explosive, flammable, or aggressive liquids because of the possibility of introducing ultrasonic pulses through the tank [...] Read more.
The ultrasonic sensor method is the most significant and widely accepted technique for measuring liquid levels in tanks. Ultrasonic waves are particularly advantageous in the case of explosive, flammable, or aggressive liquids because of the possibility of introducing ultrasonic pulses through the tank wall safely. Often, the measurement of these liquids should be performed automatically using electronic devices to ensure that the tank remains sealed. In the case of ultrasound, measurements are made using the echo method, with a transmitting-receiving (transceiver) ultrasonic transducer that sends vibration pulses into the tank. The measured delay between the transmitted pulse and the pulse reflected from the liquid surface is proportional to the liquid level in the tank. The volume of liquid can be calculated on the basis of the dimensions of the tank. In this method, it is very important to accurately determine the delay by detecting the beginning of the reflected pulse, which determines the accuracy of the measurement of the level of the liquid and its quantity in the tank. To improve this accuracy, this paper proposes the use of the Akaike Information Criterion (AIC) used in statistics for model selection. As part of the research, ultrasonic test measurements were performed for a tank filled with water and extraction gasoline. This allowed a favorable comparison of the AIC method with the most commonly used threshold method and for determining the accuracy of liquid volume measurements in the tank using both methods in relation to the parameters of several selected ultrasonic sensors. The accuracy obtained using the AIC method was found to be better than that of the fixed-fractional amplitude threshold method. Furthermore, the AIC method is more versatile because it is less sensitive to interference and is capable of detecting the onset of a pulse regardless of its shape and frequency, even in noise. It is suitable for real-time embedded systems for liquid level measurement as well. Full article
(This article belongs to the Special Issue Nondestructive Sensing and Imaging in Ultrasound—Second Edition)
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1687 KB  
Proceeding Paper
Architecture of a Piezoelectric Acoustic Detector for Applications in Tissue and Soft Material
by Raúl Alberto Reyes-Villagrana
Eng. Proc. 2025, 118(1), 63; https://doi.org/10.3390/ECSA-12-26606 - 7 Nov 2025
Viewed by 70
Abstract
There are various non-destructive techniques for determining the internal properties of materials in fluids, semi-solids, solids, and biological tissue. One of these techniques is low-intensity ultrasonic testing. In this proceeding paper, a study on the architecture of a piezoelectric acoustic detector (PAD) is [...] Read more.
There are various non-destructive techniques for determining the internal properties of materials in fluids, semi-solids, solids, and biological tissue. One of these techniques is low-intensity ultrasonic testing. In this proceeding paper, a study on the architecture of a piezoelectric acoustic detector (PAD) is presented, from which an analysis for the design, development, and construction of an acoustic wave detector in the ultrasonic spectrum has emerged. Its purpose is to be applied to soft matter and tissue. The 110 μm thick polyvinylidene fluoride (PVDF) piezoelectric element was used as the active element in the thickness mode configuration. Piezoelectric constitutive equations were applied to a one-dimensional model for the analysis. A cylindrical iron–nickel backing was used, and the parts were bonded with conductive silver epoxy glue. The results are presented. The equation for the output voltage of the piezoelectric acoustic detector is described. Functional testing of the PAD is demonstrated using the pulse-echo technique, in which an acoustic wave generator excites an ultrasonic immersion sensor in emission configuration and the DAP is connected to a digital oscilloscope to observe the received signal. Finally, pulsed photoacoustic spectroscopy was applied to a biological tissue emulator and yielded significant results in the detection of a ruby sphere embedded in the emulator. It is proposed to further investigation the DAP models in multilayer structural configurations to increase their sensitivity. Full article
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26 pages, 12809 KB  
Article
Coating Thickness Estimation Using a CNN-Enhanced Ultrasound Echo-Based Deconvolution
by Marina Perez-Diego, Upeksha Chathurani Thibbotuwa, Ainhoa Cortés and Andoni Irizar
Sensors 2025, 25(19), 6234; https://doi.org/10.3390/s25196234 - 8 Oct 2025
Viewed by 912
Abstract
Coating degradation monitoring is increasingly important in offshore industries, where protective layers ensure corrosion prevention and structural integrity. In this context, coating thickness estimation provides critical information. The ultrasound pulse-echo technique is widely used for non-destructive testing (NDT), but closely spaced acoustic interfaces [...] Read more.
Coating degradation monitoring is increasingly important in offshore industries, where protective layers ensure corrosion prevention and structural integrity. In this context, coating thickness estimation provides critical information. The ultrasound pulse-echo technique is widely used for non-destructive testing (NDT), but closely spaced acoustic interfaces often produce overlapping echoes, which complicates detection and accurate isolation of each layer’s thickness. In this study, analysis of the pulse-echo signal from a coated sample has shown that the front-coating reflection affects each main backwall echo differently; by comparing two consecutive backwall echoes, we can cancel the acquisition system’s impulse response and isolate the propagation path-related information between the echoes. This work introduces an ultrasound echo-based methodology for estimating coating thickness by first obtaining the impulse response of the test medium (reflectivity sequence) through a deconvolution model, developed using two consecutive backwall echoes. This is followed by an enhanced detection of coating layer thickness in the reflectivity function using a 1D convolutional neural network (1D-CNN) trained with synthetic signals obtained from finite-difference time-domain (FDTD) simulations with k-Wave MATLAB toolbox (v1.4.0). The proposed approach estimates the front-side coating thickness in steel samples coated on both sides, with coating layers ranging from 60μm to 740μm applied over 5 mm substrates and under varying coating and steel properties. The minimum detectable thickness corresponds to approximately λ/5 for an 8 MHz ultrasonic transducer. On synthetic signals, where the true coating thickness and speed of sound are known, the model achieves an accuracy of approximately 8μm. These findings highlight the strong potential of the model for reliably monitoring relative thickness changes across a wide range of coatings in real samples. Full article
(This article belongs to the Special Issue Nondestructive Sensing and Imaging in Ultrasound—Second Edition)
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22 pages, 3629 KB  
Article
Pulse-Echo Ultrasonic Verification of Silicate Surface Treatments Using an External-Excitation/Single-Receiver Configuration: ROC-Based Differentiation of Concrete Specimens
by Libor Topolář, Lukáš Kalina, David Markusík, Vladislav Cába, Martin Sedlačík, Felix Černý, Szymon Skibicki and Vlastimil Bílek
Materials 2025, 18(16), 3765; https://doi.org/10.3390/ma18163765 - 11 Aug 2025
Viewed by 561
Abstract
This study investigates a non-destructive, compact pulse-echo ultrasonic method that combines an external transmitter with a single receiving sensor to identify different surface treatments applied to cementitious materials. The primary objective was to evaluate whether treatment-induced acoustic changes could be reliably quantified using [...] Read more.
This study investigates a non-destructive, compact pulse-echo ultrasonic method that combines an external transmitter with a single receiving sensor to identify different surface treatments applied to cementitious materials. The primary objective was to evaluate whether treatment-induced acoustic changes could be reliably quantified using time-domain signal parameters. Three types of surface conditions were examined: untreated reference specimens (R), specimens treated with a standard lithium silicate solution (A), and those treated with an enriched formulation containing hexylene glycol (B) intended to enhance pore sealing via gelation. A broadband piezoelectric receiver collected the backscattered echoes, from which the maximum amplitude, root mean square (RMS) voltage, signal energy, and effective duration were extracted. Receiver operating characteristic (ROC) analysis was conducted to quantify the discriminative power of each parameter. The results showed excellent classification performance between groups involving the B-treatment (AUC ≥ 0.96), whereas the R vs. A comparison yielded moderate separation (AUC ≈ 0.61). Optimal cut-off values were established using the Youden index, with sensitivity and specificity exceeding 96% in the best-performing scenarios. The results demonstrate that a single-receiver, one-sided pulse-echo arrangement coupled with straightforward amplitude metrics provides a rapid, cost-effective, and field-adaptable tool for the quality control of silicate-surface treatments. By translating laboratory ultrasonics into a practical on-site protocol, this study helps close the gap between the experimental characterisation and real-world implementation of surface-treatment verification. Full article
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13 pages, 7320 KB  
Article
Determination of Main Bearing Dynamic Clearance in a Shield Tunneling Machine Through a Broadband PMUT Array with a Decreased Blind Area and High Accuracy
by Guoxi Luo, Haoyu Zhang, Delai Liu, Wenyan Li, Min Li, Zhikang Li, Lin Sun, Ping Yang, Ryutaro Maeda and Libo Zhao
Sensors 2025, 25(13), 4182; https://doi.org/10.3390/s25134182 - 4 Jul 2025
Cited by 1 | Viewed by 768
Abstract
Traditional PMUT ultrasonic ranging systems usually possess a large measurement blind area under the integrated transmit–receive mode, dramatically limiting its distance measurement in confined spaces, such as when determining the clearance of large bearing components. Here, a broadband PMUT rangefinder was designed by [...] Read more.
Traditional PMUT ultrasonic ranging systems usually possess a large measurement blind area under the integrated transmit–receive mode, dramatically limiting its distance measurement in confined spaces, such as when determining the clearance of large bearing components. Here, a broadband PMUT rangefinder was designed by integrating six types of different cells with adjacent resonant frequencies into an array. Through overlapping and coupling of the bandwidths from the different cells, the proposed PMUTs showed a wide –6 dB fractional bandwidth of 108% in silicon oil. Due to the broadening of bandwidth, the device could obtain the maximum steady state with less excitation (5 cycles versus 14 cycles) and reduce its residual ring-down (ca. 6 μs versus 15 μs) compared with the traditional PMUT array with the same cells, resulting in a small blind area. The pulse–echo ranging experiments demonstrated that the blind area was effectively reduced to 4.4 mm in air or 12.8 mm in silicon oil, and the error was controlled within ±0.3 mm for distance measurements up to 250 mm. In addition, a specific ultrasound signal processing circuit with functions of transmitting, receiving, and processing ultrasonic waves was developed. Combining the processing circuit and PMUT device, the system was applied to determine the axial clearance of the main bearing in a tunneling machine. This work develops broadband PMUTs with a small blind area and high resolution for distance measurement in narrow and confined spaces, opening up a new path for ultrasonic ranging technology. Full article
(This article belongs to the Section Industrial Sensors)
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20 pages, 3047 KB  
Article
Comparison of Pulse-Echo Tomography and Through-Transmission Ultrasonic Test for UPV Characterization of Building Materials
by Emilia Vasanelli, Davide Di Gennaro, Matteo Sticchi, Gianni Blasi and Luigi Capozzoli
Infrastructures 2025, 10(7), 162; https://doi.org/10.3390/infrastructures10070162 - 27 Jun 2025
Cited by 1 | Viewed by 1383
Abstract
Ultrasonic pulse velocity (UPV) is a widely used technique for diagnosis and structural safety assessment of existing buildings. The main difficulties in UPV tests on-site are due to one-sided accessibility of materials and degraded/irregular surfaces. Pulse-echo ultrasonic tomography (PE-UT) can overcome the problem. [...] Read more.
Ultrasonic pulse velocity (UPV) is a widely used technique for diagnosis and structural safety assessment of existing buildings. The main difficulties in UPV tests on-site are due to one-sided accessibility of materials and degraded/irregular surfaces. Pulse-echo ultrasonic tomography (PE-UT) can overcome the problem. Though it has been widely applied for detecting inhomogeneities within concrete, few works use the instrument to assess UPV. The present paper aims to fill the gap by comparing PE-UT results with those of through-transmission ultrasonic tests (TT-UT) commonly used for UPV characterization. TT-UT measurements were performed with cylindrical and exponential transducers. The latter are used on irregular surfaces or when coupling gel is forbidden. Few data are in the literature comparing exponential and cylindrical transducers’ results. This is a further element of novelty of the paper. PE-UT and TT-UT results were compared considering the effect of material compositeness, water, transmission mode, and transducer type. It was found that PE-UT allows for reliable and rapid one-sided measurements on concrete and stone in different conditions. The differences between PE-UT and TT-UT results were between 1 and 3%. Exponential transducers gave reliable results on fine-grained stone in direct transmission, with differences lower than 4% with cylindrical transducer results. Full article
(This article belongs to the Section Infrastructures Materials and Constructions)
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11 pages, 1586 KB  
Article
Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
by Songwei Wang and Haiying Huang
Sensors 2025, 25(13), 3983; https://doi.org/10.3390/s25133983 - 26 Jun 2025
Viewed by 734
Abstract
Aluminum–Magnesium (Al–Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al2Mg3) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al–Mg alloys to intergranular corrosion, exfoliation, and stress corrosion cracking. This study [...] Read more.
Aluminum–Magnesium (Al–Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al2Mg3) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al–Mg alloys to intergranular corrosion, exfoliation, and stress corrosion cracking. This study introduces a time-frequency analysis (TFA) technique to determine the frequency-dependent ultrasonic attenuation parameter and correlate the frequency-attenuation slope to the Degree of Sensitization (DoS) developed in heat-treated Al–Mg alloy samples. Broadband pitch-catch signal was generated using a laser ultrasonic testing (LUT) system, from which the narrowband pitch-catch signal at different frequencies can be digitally generated. The attenuation parameters of sensitized Al–Mg samples were determined from these narrowband pitch-catch signals using the primary pulse-first echo (PP-FE) method. By identifying the frequency range within which the attenuation parameter is linearly proportional to the frequency, the slopes of the frequency-attenuation relationship were determined and correlated with the DoS values of the sample plates. The experimental results validate that the frequency-attenuation slope has a higher sensitivity and lower scattering as compared to other conventional ultrasonic attenuation measurement techniques. Full article
(This article belongs to the Special Issue Feature Papers in Optical Sensors 2025)
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20 pages, 9176 KB  
Article
Research on Drive and Detection Technology of CMUT Multi-Array Transducers Based on MEMS Technology
by Chenyuan Li, Jiagen Chen, Chengwei Liu, Yao Xie, Yangyang Cui, Shiwang Zhang, Zhikang Li, Libo Zhao, Guoxing Chen, Shaochong Wei, Yu Gao and Linxi Dong
Micromachines 2025, 16(6), 604; https://doi.org/10.3390/mi16060604 - 22 May 2025
Viewed by 3236
Abstract
This paper presents an ultrasonic driving and detection system based on a CMUT array using MEMS technology. Among them, the core component CMUT array is composed of 8 × 8 CMUT array elements, and each CMUT array element contains 6 × 6 CMUT [...] Read more.
This paper presents an ultrasonic driving and detection system based on a CMUT array using MEMS technology. Among them, the core component CMUT array is composed of 8 × 8 CMUT array elements, and each CMUT array element contains 6 × 6 CMUT units. The collapse voltage of a single CMUT unit obtained through finite element analysis is 95.91 V, and the resonant frequency is 3.16 MHz. The driving section achieves 64-channel synchronous driving, with key parameters including an adjustable excitation signal frequency ranging from 10 kHz to 5.71 MHz, a delay precision of up to 1 ns, and an excitation duration of eight pulse cycles. For the echo reception, a two-stage amplification circuit for high-frequency weak echoes with 32 channels was designed, achieving a gain of 113.72 dB and −3 dB bandwidth of 3.89 MHz. Simultaneously, a 32-channel analog-to-digital conversion based on a self-calibration algorithm was implemented, with a sampling rate of 50 Mbps and a data width of 10 bits. Finally, the experimental results confirm the successful implementation of the driving system’s designed functions, yielding a center frequency of 1.4995 MHz and a relative bandwidth of 127.9%@−6 dB for the CMUT operating in silicone oil. This paper successfully conducted the transmit–receive integrated experiment of the CMUT and applied Butterworth filtering to the echo data, resulting in high-quality ultrasonic echo signals that validate the applicability of the designed CMUT-based system for ultrasonic imaging. Full article
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17 pages, 7653 KB  
Article
Research on Wireless Passive Ultrasonic Thickness Measurement Technology Based on Pulse Compression Method
by Long Pan, Kunsan Shi, Lei Han, Dingrong Qu, Yanling Zhang and Wenwu Chen
Sensors 2024, 24(24), 8023; https://doi.org/10.3390/s24248023 - 16 Dec 2024
Viewed by 1198
Abstract
Fixed-point thickness measurement is commonly used in corrosion detection within petrochemical enterprises, but it suffers from low detection efficiency for localized thinning, limitations regarding measurement locations, and high equipment costs due to insulation and cooling layers. To address these challenges, this paper introduces [...] Read more.
Fixed-point thickness measurement is commonly used in corrosion detection within petrochemical enterprises, but it suffers from low detection efficiency for localized thinning, limitations regarding measurement locations, and high equipment costs due to insulation and cooling layers. To address these challenges, this paper introduces a wireless passive ultrasonic thickness measurement technique based on a pulse compression algorithm. The research methodology encompassed the development of mathematical and circuit models for single coil and wireless energy transmission, the proposal of a three-terminal wireless energy mutual coupling system, and the establishment of a finite element model simulating the ultrasonic body wave thickness measurement and wireless energy transmission system. An experimental setup was constructed to conduct thickness measurements on metal samples varying in thickness, shape, and material composition. The experimental findings revealed that the wireless ultrasonic echo signal, when processed using the pulse compression algorithm, achieved a thickness measurement accuracy approximately ten times superior to that of the untreated echo signal. This significant improvement in accuracy facilitates the high-density deployment of thickness measurement points in petrochemical applications. Full article
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17 pages, 8620 KB  
Article
Unique Characteristics of Pulse-Echo Sensing Systems for Ultrasonic Immersion Testing in Harsh Environments
by Gaofeng Sha, Andrew R. Bozek, Bernhard R. Tittmann and Cliff J. Lissenden
Sensors 2024, 24(23), 7748; https://doi.org/10.3390/s24237748 - 4 Dec 2024
Viewed by 1591
Abstract
Ultrasound is an excellent way to acquire data that reveal useful information about systems operating in harsh environments, which may include elevated temperature, ionizing radiation, and aggressive chemicals. The effects of harsh environments on piezoelectric materials have been studied in much more depth [...] Read more.
Ultrasound is an excellent way to acquire data that reveal useful information about systems operating in harsh environments, which may include elevated temperature, ionizing radiation, and aggressive chemicals. The effects of harsh environments on piezoelectric materials have been studied in much more depth than the other aspects of ultrasonic transducers used in pulse-echo mode. Therefore, finite element simulations and laboratory experiments are used to demonstrate the unique characteristics of pulse-echo immersion testing. Using an aluminum nitride piezoelectric element mounted on a vessel wall, characteristics associated with electrode thickness, couplant, backing material, and an acoustic matching layer are investigated. Considering a wave path through a vessel wall and into a fluid containing a target, when the travel distance in the fluid is relatively short, it can be difficult to discern the target echo from the reverberations in the vessel wall. When an acoustic matching layer between the vessel wall and the fluid does not suffice, a simple subtractive signal-processing method can minimize the reverberations, leaving just the target echoes of interest. Simulations and experiments demonstrate that sufficient target echoes are detected to determine the time of flight. Furthermore, a simple disc-like surface anomaly on the target is detectable. Full article
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14 pages, 5226 KB  
Article
Porous Metal Backing for High-Temperature Ultrasonic Transducers
by Guy Feuillard, Dang Chi Nguyen, Marc Lethiecq, Mathieu Jean and Frédéric Navacchia
Acoustics 2024, 6(4), 1074-1087; https://doi.org/10.3390/acoustics6040058 - 25 Nov 2024
Cited by 1 | Viewed by 2245
Abstract
Improving the performance of high-temperature ultrasonic transducers is a goal of major importance in many industrial applications. To this aim, we propose to use porous metals that support high temperatures as backings. Thus, the acoustic properties of stainless steel and porous stainless steel [...] Read more.
Improving the performance of high-temperature ultrasonic transducers is a goal of major importance in many industrial applications. To this aim, we propose to use porous metals that support high temperatures as backings. Thus, the acoustic properties of stainless steel and porous stainless steel with porosity of 25% and 35% are determined at ambient temperature and up to 400 °C. Over the temperature range, the longitudinal wave velocity variation is comprised between 5% and 6% in the porous metals. We find that temperature does not significantly affect the attenuation in the material. The pulse-echo response and frequency response of a LiNbO3-based transducer with a porous backing are simulated using a one dimensional electroacoustic model. These simulations, compared to those of a reference transducer, show that the axial resolution with such a design allows these transducers to be used for imaging and/or Non-Destructive Testing and evaluation at high temperature. Full article
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13 pages, 4201 KB  
Article
Convolutional Neural Network for Interface Defect Detection in Adhesively Bonded Dissimilar Structures
by Damira Smagulova, Vykintas Samaitis and Elena Jasiuniene
Appl. Sci. 2024, 14(22), 10351; https://doi.org/10.3390/app142210351 - 11 Nov 2024
Cited by 3 | Viewed by 2119
Abstract
This study presents an ultrasonic non-destructive method with convolutional neural networks (CNN) used for the detection of interface defects in adhesively bonded dissimilar structures. Adhesive bonding, as the weakest part of such structures, is prone to defects, making their detection challenging due to [...] Read more.
This study presents an ultrasonic non-destructive method with convolutional neural networks (CNN) used for the detection of interface defects in adhesively bonded dissimilar structures. Adhesive bonding, as the weakest part of such structures, is prone to defects, making their detection challenging due to various factors, including surface curvature, which causes amplitude variations. Conventional non-destructive methods and processing algorithms may be insufficient to enhance detectability, as some influential factors cannot be fully eliminated. Even after aligning signals reflected from the sample surface and interface, in some cases, due to non-parallel interfaces, persistent amplitude variations remain, significantly affecting defect detectability. To address this problem, a proposed method that integrates ultrasonic NDT and CNN, and which is able to recognize complex patterns and non-linear relationships, is developed in this work. Traditional ultrasonic pulse-echo testing was performed on adhesive structures to collect experimental data and generate C-scan images, covering the time gate from the first interface reflection to the time point where the reflections were attenuated. Two classes of datasets, representing defective and defect-free areas, were fed into the neural network. One subset of the dataset was used for model training, while another subset was used for model validation. Additionally, data collected from a different sample during an independent experiment were used to evaluate the generalization and performance of the neural network. The results demonstrated that the integration of a CNN enabled high prediction accuracy and automation of the analysis process, enhancing efficiency and reliability in detecting interface defects. Full article
(This article belongs to the Special Issue New Technology Trends in Smart Sensing)
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25 pages, 10965 KB  
Article
Bottom Crack Detection with Real-Time Signal Amplitude Correction Using EMAT-PEC Composite Sensor
by Yizhou Guo, Yu Hu, Kai Wang, Yini Song, Bo Feng, Yihua Kang and Zhaoqi Duan
Sensors 2024, 24(16), 5196; https://doi.org/10.3390/s24165196 - 11 Aug 2024
Cited by 5 | Viewed by 2520
Abstract
During electromagnetic ultrasonic testing, it is difficult to recognize small-size bottom cracks by time of flight (ToF), and the lift-off fluctuation of the probe affects the accuracy and consistency of the inspection results. In order to overcome the difficulty, a novel composite sensor [...] Read more.
During electromagnetic ultrasonic testing, it is difficult to recognize small-size bottom cracks by time of flight (ToF), and the lift-off fluctuation of the probe affects the accuracy and consistency of the inspection results. In order to overcome the difficulty, a novel composite sensor of an electromagnetic acoustic transducer (EMAT) and pulse eddy current (PEC) is designed. We use the amplitude of a bottom echo recorded by EMAT to identify the tiny bottom crack as well as the amplitude of PEC signals picked up by the integrated symmetric coils to measure the average lift-off of the probe in real time. Firstly, the effects of lift-off and bottom cracks on the amplitude of bottom echo are distinguished by combining the theoretical analysis and finite element method (FEM). And then an amplitude correction method based on the fusion of EMAT and PEC signals is proposed to reduce the impact of lift-off on the defect signal. The experimental results demonstrate that the designed composite sensor can effectively detect a bottom crack as small as 0.1 mm × 0.3 mm. The signal fusion method can accurately correct the amplitude of defect signals and the relative error is less than ±8%. Full article
(This article belongs to the Special Issue Novel Sensors for Structural Health Monitoring: 2nd Edition)
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16 pages, 71175 KB  
Article
Acoustic Assessment of Microstructural Deformation Mechanisms on a Cold Rolled Cu30Zn Brass
by María Sosa, Linton Carvajal, Vicente Salinas Barrera, Fernando Lund, Claudio Aguilar and Felipe Castro Cerda
Materials 2024, 17(13), 3321; https://doi.org/10.3390/ma17133321 - 4 Jul 2024
Cited by 2 | Viewed by 1889
Abstract
The relationship between acoustic parameters and the microstructure of a Cu30Zn brass plate subjected to plastic deformation was evaluated. The plate, previously annealed at 550 °C for 30 min, was cold rolled to reductions ranging from 10% to 70%. Linear ultrasonic measurements were [...] Read more.
The relationship between acoustic parameters and the microstructure of a Cu30Zn brass plate subjected to plastic deformation was evaluated. The plate, previously annealed at 550 °C for 30 min, was cold rolled to reductions ranging from 10% to 70%. Linear ultrasonic measurements were performed on each of the nine specimens, corresponding to the nine different reductions, using the pulse-echo method to record the times of flight of longitudinal waves along the thickness axis. Subsequently, acoustic measurements were conducted to determine the nonlinear parameter β through second harmonic generation. Microstructural analysis, carried out by X-ray diffraction, Vickers hardness testing, and optical microscopy, revealed an increase in deformation twins, reaching a maximum at 40% thickness reduction. At higher deformations, the microstructure showed the generation and proliferation of shear bands, coinciding with a decrease in the twinning structure and an increase in dislocation density. The longitudinal wave velocity exhibited a 0.9% decrease at 20% deformation, attributed to dislocations and initial twin formation, followed by a continuous increase up to 2% beyond this point, resulting from the combined effects of twinning and shear banding. The nonlinear parameter β displayed a notable maximum, approximately one order of magnitude greater than its original value, at 40% deformation. This peak correlates with a roughly tenfold increase in twinning fault probability at the same deformation level. Full article
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14 pages, 3818 KB  
Article
Use of Non-Destructive Ultrasonic Techniques as Characterization Tools for Different Varieties of Wine
by José Ángel Corbacho, David Morcuende, Montaña Rufo, Jesús M. Paniagua, María Ángeles Ontalba and Antonio Jiménez
Sensors 2024, 24(13), 4294; https://doi.org/10.3390/s24134294 - 2 Jul 2024
Cited by 1 | Viewed by 2369
Abstract
In this work, we have verified how non-destructive ultrasonic evaluation allows for acoustically characterizing different varieties of wine. For this, a 3.5 MHz transducer has been used by means of an immersion technique in pulse-echo mode. The tests were performed at various temperatures [...] Read more.
In this work, we have verified how non-destructive ultrasonic evaluation allows for acoustically characterizing different varieties of wine. For this, a 3.5 MHz transducer has been used by means of an immersion technique in pulse-echo mode. The tests were performed at various temperatures in the range 14–18 °C. The evaluation has been carried out studying, on the one hand, conventional analysis parameters (velocity and attenuation) and, on the other, less conventional parameters (frequency components). The experimental study comprised two stages. In the first, the feasibility of the study was checked by inspecting twelve samples belonging to six varieties of red and white wine. The results showed clearly higher ultrasonic propagation velocity values in the red wine samples. In the second, nine samples of different monovarietal wine varieties (Grenache, Tempranillo and Cabernet Sauvignon) were analyzed. The results show how ultrasonic velocity makes it possible to unequivocally classify the grape variety used in winemaking with the Cabernet Sauvignon variety having the highest values and the Grenache the lowest. In addition, the wines of the Tempranillo variety are those that present higher values of the attenuation coefficient, and those from the Grenache variety transmit higher frequency waves. Full article
(This article belongs to the Section Intelligent Sensors)
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