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14 pages, 2354 KB  
Article
Reduced Bubbles in a PDMS SlipChip: Magnetic Alignment, Oil-Infused Lubrication, and Geometry Optimization
by Rafia Inaam, Imran Md Hussain Mohammad, Hirofumi Yamamoto, Marcela F. Bolontrade, Shunya Okamoto, Takayuki Shibata, Tuhin Subhra Santra and Moeto Nagai
Appl. Sci. 2026, 16(6), 3040; https://doi.org/10.3390/app16063040 (registering DOI) - 21 Mar 2026
Abstract
PDMS SlipChips are vital for precision medicine, but their performance often degrades when solutions leak or air pockets become trapped between layers. These failures stem from the inherent stickiness of PDMS and uneven surface contact, as the sliding nature of the device prevents [...] Read more.
PDMS SlipChips are vital for precision medicine, but their performance often degrades when solutions leak or air pockets become trapped between layers. These failures stem from the inherent stickiness of PDMS and uneven surface contact, as the sliding nature of the device prevents permanent sealing. This work addresses these technical hurdles by integrating magnetic clamping with oil-infused lubrication and refined microwell geometries. A 3D-printed magnetic fixture maintains steady contact pressure during operation, while custom-made microstages provide the precise control needed to align microwells across the xy plane. By allowing the porous PDMS to absorb silicone oil, we created a stable lubricating interface that prevents leakage and reduces friction without sacrificing mobility. We found that a microwell-to-channel width ratio of five substantially suppresses bubble formation compared with narrower designs. These enhancements ensure the generation of consistent, discrete concentration gradients and establish a reliable platform for high-throughput assays using minute sample volumes. Full article
(This article belongs to the Special Issue MEMS Transducers: Fabrication, Performance and Applications)
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20 pages, 2893 KB  
Article
Two-Phase Pockmark Modeling and Gas Saturation Estimation Beneath Hydrate-Bearing Sediments: Insights from the Storegga Slide
by Zheng Su, Yifan Wu, Chao Yang and Nengyou Wu
Geosciences 2026, 16(3), 128; https://doi.org/10.3390/geosciences16030128 - 20 Mar 2026
Abstract
Fluid seepages and seabed pockmarks are widely observed on continental margins worldwide in hydrate- and non-hydrate-bearing sediment. Subsurface gas chimneys connecting seafloor pockmarks to underlying gas reservoirs are commonly revealed by seismic reflection data, indicating pathways of past and present fluid migration. Fluid [...] Read more.
Fluid seepages and seabed pockmarks are widely observed on continental margins worldwide in hydrate- and non-hydrate-bearing sediment. Subsurface gas chimneys connecting seafloor pockmarks to underlying gas reservoirs are commonly revealed by seismic reflection data, indicating pathways of past and present fluid migration. Fluid seepage occurs when the seal of a gas reservoir is breached, allowing fluids to migrate upward and vent at the seafloor, forming pockmarks. In hydrate-bearing settings, gas reservoirs beneath hydrate layers typically consist of coexisting water and gas phases. However, quantitative constraints on gas saturation in free-gas zones beneath hydrates inferred from pockmark morphology remain limited. In this study, a two-phase pockmark model was developed to investigate gas-chimney growth and pockmark formation, and to estimate gas saturation in free-gas zones below hydrates using pockmark depth and gas-zone thickness as key parameters. The model was applied to the Storegga Slide region off Norway, where hydrates, pockmarks, and chimney-like seismic anomalies have been documented. Here, the application is intended to represent localized near-threshold (pre-seepage) conditions leading to pockmark initiation, rather than the present-day post-venting state. Model results for the initiation (near-threshold, pre-venting) stage indicate that the effective gas saturation in the free-gas reservoir beneath the hydrates was approximately 1.36–1.58% for gas-zone thicknesses of 50–100 m, and that the corresponding chimney-propagation timescale during initiation was on the order of ~200 years. These estimates represent threshold conditions required for seal breach and pockmark formation rather than present-day seepage states. During venting, methane gas may form hydrates within the chimney inside the hydrate stability zone, while authigenic carbonates precipitate in pockmarks and shallow sediments. These secondary hydrates and carbonates eventually seal the chimney, leaving behind a residual gas chimney in the subsurface sediment. Full article
(This article belongs to the Section Geophysics)
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21 pages, 18914 KB  
Article
Optimization Design and Experimental Testing of Sound Insulation Performance for Silent Cabins
by Li Tang, Yicheng Lu, Meiping Sheng, Zhiwei Guo and Bin Lu
Appl. Sci. 2026, 16(6), 2996; https://doi.org/10.3390/app16062996 - 20 Mar 2026
Abstract
This study investigates the sound insulation performance of an anechoic chamber, exploring the influence patterns of different multilayer material combinations on wall sound insulation characteristics. Based on sound transmission theory, a predictive model for multilayer material wall sound insulation was established. The finite [...] Read more.
This study investigates the sound insulation performance of an anechoic chamber, exploring the influence patterns of different multilayer material combinations on wall sound insulation characteristics. Based on sound transmission theory, a predictive model for multilayer material wall sound insulation was established. The finite element method was employed to simulate the sound propagation characteristics of walls and glass doors with various material combinations. After validating the simulation results through a double-room method experiment, the material combination scheme for the anechoic chamber walls and glass doors was optimized. Based on this, a 1000 mm × 1000 mm × 2300 mm soundproof room prototype was designed and constructed. Its sound insulation performance under reverberant conditions was tested using the insertion loss method and compared with simulation data. Simultaneously, a hybrid calculation method combining low-frequency finite element analysis with high-frequency statistical energy analysis enabled precise and efficient prediction of the overall sound insulation performance of the soundproof room. Research revealed that single-pane glass with thicknesses between 5 and 20 mm conformed to the mass law, with sound insulation increasing by an average of 0.8 dB per additional millimeter. The 10 mm single-pane glass emerged as the optimal choice for the soundproof room’s glass door due to its ideal thickness and excellent low-to-mid-frequency sound insulation. The optimized wall structure featured compact thickness, outstanding low-frequency sound insulation, and balanced mid-to-high-frequency performance. Simulation and experimental results for the core frequency range of 63–1000 Hz showed high consistency, which validates the reliability of the theoretical model and simulation methodology within this frequency band. The deviation of simulation results from experimental data in the frequency range above 1000 Hz is mainly caused by acoustic leakage due to experimental sealing defects, and the high-frequency simulation results are only used for trend analysis rather than conclusion support. This study identifies the optimal multi-layer material combination for soundproof rooms, providing practical material strategies for acoustic design. It also reveals the sound insulation mechanisms of multi-layer composite structures. The findings offer significant reference for optimizing soundproofing materials and structures in architectural acoustics and transportation noise control. Full article
(This article belongs to the Special Issue Novel Advances in Noise and Vibration Control)
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25 pages, 5741 KB  
Article
An Efficient Geomechanical Modeling and Intelligent Prediction Approach for Fault Slip in Underground Gas Storage During Long-Term Injection-Production Operation
by Haitao Xu, Kang Liu, Zixiu Yao, Guoming Chen, Xiaosong Qiu and Weiming Shao
Sustainability 2026, 18(6), 3039; https://doi.org/10.3390/su18063039 - 19 Mar 2026
Abstract
The steady operation of underground gas storage (UGS) is significant for securing national energy. However, long-term cyclic injection-production operation causes the dynamic changes in formation stress, potentially leading to fault reactivation and slippage. This could affect the seal performance of the fault zone [...] Read more.
The steady operation of underground gas storage (UGS) is significant for securing national energy. However, long-term cyclic injection-production operation causes the dynamic changes in formation stress, potentially leading to fault reactivation and slippage. This could affect the seal performance of the fault zone and cause disastrous consequences. In this paper, a mechanical analysis model for fault slip is constructed to study the dynamic seal performance in response to long-term injection-production cycles. An intelligent approach is proposed to predicate the fault slip value based on machine learning algorithms. It can realize long-term prediction of fault slip value under a new condition of injection-production operation. The study shows that (1) formation pressure tends to accumulate near the fault zone due to the low permeability, and the interface of the reservoir layer, cap layer, and fault zone is the seal weak position of UGS; (2) the response of fault slip is driven by the injection-production rate and the reservoir pressure. There is a significant coupling relationship between the fault slip value and the accumulated injection gas volume; (3) the intelligent prediction approach can capture the nonlinear dynamic characteristics of slip tendency accurately, and it exhibits good prediction performance and generalization ability under the new operating condition. This study effectively assesses the dynamic risk for fault slip of depleted hydrocarbon reservoir UGS during the long-term injection-production procedure. It provides an effective technical approach for fault slip tendency analysis and injection-production process optimization, which is important for the sustainable operation of UGS reducing the risk of seal failure and supporting gas storage security. Full article
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20 pages, 3817 KB  
Article
Improving Corrosion Resistance of Magnesium Alloys via Synergistic Action of TiO2 Superhydrophobic Coating and Micro-Arc Oxidation
by Weirong Quan, Zongfan Duan, Yu Liu, Ruihao Wang, Shuoqing Cui, Shaodong Sun and Dongjie Liu
Coatings 2026, 16(3), 363; https://doi.org/10.3390/coatings16030363 - 13 Mar 2026
Viewed by 159
Abstract
To mitigate the intrinsic high corrosion susceptibility of AZ31B magnesium alloy, a three-step synergistic surface modification strategy was developed in this work: initially, a MgO ceramic coating was in situ fabricated on the AZ31B substrate via micro-arc oxidation (MAO); subsequently, a TiO2 [...] Read more.
To mitigate the intrinsic high corrosion susceptibility of AZ31B magnesium alloy, a three-step synergistic surface modification strategy was developed in this work: initially, a MgO ceramic coating was in situ fabricated on the AZ31B substrate via micro-arc oxidation (MAO); subsequently, a TiO2 sealing barrier layer was deposited on the MAO coating through a deep ultraviolet (DUV)-assisted sol–gel method; finally, a superhydrophobic top layer was constructed via fluoroalkylsilane (FAS) self-assembly. The microstructural characteristics, chemical compositions and corrosion resistance of the coatings at different modification stages were comprehensively characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), water contact angle (WCA) measurements and electrochemical tests. The results showed that the as-deposited TiO2 was predominantly anatase phase, and FAS molecules were firmly anchored on the coating surface via Si-O-Ti covalent bonds, endowing the composite coating with a WCA of up to 160°. Electrochemical tests demonstrated that the FAS-TiO2-MAO composite coating exhibited an ultra-low corrosion current density of 1.31 × 10−9 A/cm2 and a remarkably high charge transfer resistance (Rct) of 3.46 × 108 Ω·cm2. Compared with the bare AZ31B substrate, the corrosion current density was decreased by nearly four orders of magnitude, while the charge transfer resistance was enhanced by approximately six orders of magnitude, indicating a significant improvement in corrosion resistance. Moreover, the composite coating exhibited excellent interfacial adhesion, favorable mechanical durability, and outstanding chemical stability, confirming its reliable long-term corrosion protection and high practical application potential. This work provides a feasible strategy for fabricating high-performance superhydrophobic anticorrosive coatings on magnesium alloys. Full article
(This article belongs to the Special Issue Superhydrophobic Coatings, 2nd Edition)
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23 pages, 2522 KB  
Article
A Synergistic Approach to Sustainable Packaging: Exploring Mater-Bi®/PHBV Multilayer Systems
by Similoluwa Oluwaferanmi Orisaya-Taiwo, Loredana Incarnato, Eugenio Amendola, Stefania Dello Iacono and Luciano Di Maio
Polymers 2026, 18(6), 692; https://doi.org/10.3390/polym18060692 - 12 Mar 2026
Viewed by 291
Abstract
In this study, multilayer films were produced using a co-extrusion process involving two complementary bioplastics: Poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) and Mater-Bi®. PHBV is recognized, among biodegradable polymers, for its excellent oxygen barrier properties, but is also known for being brittle, non-sealable, and difficult [...] Read more.
In this study, multilayer films were produced using a co-extrusion process involving two complementary bioplastics: Poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) and Mater-Bi®. PHBV is recognized, among biodegradable polymers, for its excellent oxygen barrier properties, but is also known for being brittle, non-sealable, and difficult to process. Conversely, Mater-Bi® has good processability, low stiffness, and high ductility, but exhibits poor barrier properties. The research investigated the barrier, mechanical, sealing, and optical properties of the films to evaluate how variations in layer structure and processing parameters influenced their overall performance. The results showed that the addition of the PHBV layer, both as a neat polymer and as a blend with Mater-Bi®, significantly reduced oxygen and water vapor permeability. Additionally, Mater-Bi® was found to be essential for providing the elasticity and sealability required for the multilayer films. The study also demonstrated that layer thickness plays a critical role in property tailoring. Full article
(This article belongs to the Special Issue Polymeric Materials for Food Packaging: Fundamentals and Applications)
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37 pages, 984 KB  
Article
Co-Explainers: A Position on Interactive XAI for Human–AI Collaboration as a Harm-Mitigation Infrastructure
by Francisco Herrera, Salvador García, María José del Jesus, Luciano Sánchez and Marcos López de Prado
Mach. Learn. Knowl. Extr. 2026, 8(3), 69; https://doi.org/10.3390/make8030069 - 10 Mar 2026
Viewed by 385
Abstract
Human–AI collaboration (HAIC) increasingly mediates high-risk decisions in public and private sectors, yet many documented AI harms arise not only from model error but from breakdowns in joint human–AI work: miscalibrated reliance, impaired contestability, misallocated agency, and governance opacity. Conventional explainable AI (XAI) [...] Read more.
Human–AI collaboration (HAIC) increasingly mediates high-risk decisions in public and private sectors, yet many documented AI harms arise not only from model error but from breakdowns in joint human–AI work: miscalibrated reliance, impaired contestability, misallocated agency, and governance opacity. Conventional explainable AI (XAI) approaches, often delivered as static one-shot artifacts, are poorly matched to these sociotechnical dynamics. This paper is a position paper arguing that explainability should be reframed as a harm-mitigation infrastructure for HAIC: an interactive, iterative capability that supports ongoing sensemaking, safe handoffs of control, governance stakeholder roles and institutional accountability. We introduce co-explainers as a conceptual framework for interactive XAI, in which explanations are co-produced through structured dialogue, feedback, and governance-aware escalation (explain → feedback → update → govern). To ground this position, we synthesize prior harm taxonomies into six HAIC-oriented harm clusters and use them as heuristic design lenses to derive cluster-specific explainability requirements, including uncertainty communication, provenance and logging, contrastive “why/why-not” and counterfactual querying, role-sensitive justification, and recourse-oriented interaction protocols. We emphasize that co-explainers do not “mitigate” sociotechnical harms in isolation; rather, they provide an interface layer that makes harms more detectable, decisions more contestable, and accountability handoffs more operational under realistic constraints such as sealed models, dynamic updates, and value pluralism. We conclude with an agenda for evaluating co-explainers and aligning interactive XAI with governance frameworks in real-world HAIC deployments. Full article
(This article belongs to the Section Learning)
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24 pages, 3530 KB  
Article
Investigation of Spiral-Groove Dry Gas Seal Performance Using an Experimental Data-Driven Kriging Surrogate Model
by Jiashu Yu, Xuexing Ding, Jinlin Chen and Jianping Yu
Lubricants 2026, 14(3), 119; https://doi.org/10.3390/lubricants14030119 - 9 Mar 2026
Viewed by 224
Abstract
Spiral-groove dry gas seals are widely used in turbomachinery. However, high-fidelity numerical simulations remain challenging because the gas film is micron-scale and features high shear and pronounced boundary-layer effects, while experimental studies are often expensive due to the large design space and tight [...] Read more.
Spiral-groove dry gas seals are widely used in turbomachinery. However, high-fidelity numerical simulations remain challenging because the gas film is micron-scale and features high shear and pronounced boundary-layer effects, while experimental studies are often expensive due to the large design space and tight machining tolerances. To address these issues, this study integrates a Kriging surrogate model with surrogate-based optimization (SBO) to systematically identify the key structural and operating parameters governing seal performance. The results quantify the individual effects of key geometric parameters, providing practical guidance for spiral-groove seal design and optimization. The Kriging model captures the nonlinear relationships between performance and design variables and shows good generalization, with a maximum residual standard deviation of 2.78 and all others below 1.0. Sobol analysis reveals that structural parameters dominate performance: groove depth and width exhibit total-effect indices of approximately 0.74 and 0.56, respectively, while rotational speed is the most influential operating parameter (≈0.75). Among eight structural variables, groove depth is the most critical, increasing leakage by more than 200% as it rises from 5 to 8 μm, followed by spiral angle and groove number; all remaining parameters each contribute less than 10%. Full article
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17 pages, 5048 KB  
Article
Differential Attachment of Engineered Oral Soft Tissues to Implant Surfaces
by Nour Jalaleddine, Emilia Barker, Kirsty Franklin, Mohamed Jamal, Momen A. Atieh, Zaid H. Baqain and Keyvan Moharamzadeh
Dent. J. 2026, 14(3), 150; https://doi.org/10.3390/dj14030150 - 6 Mar 2026
Viewed by 245
Abstract
Background/Objectives: The formation of a soft tissue seal through mucosal integration around dental implants is critical for potentially achieving long-term peri-implant health and clinical success. Understanding how different implant and abutment surfaces interact with individual layers of the oral mucosa remains limited. [...] Read more.
Background/Objectives: The formation of a soft tissue seal through mucosal integration around dental implants is critical for potentially achieving long-term peri-implant health and clinical success. Understanding how different implant and abutment surfaces interact with individual layers of the oral mucosa remains limited. This study aimed to compare the differential attachment of tissue-engineered oral epithelium, connective tissue, and full-thickness human oral mucosa to various implant and abutment materials and surface topographies. Methods: Sand-blasted, large-grit, acid-etched (TiZr-SLA), machined TiZr (TiZr-M), machined zirconia (ZrO2-M), polished zirconia (ZrO2-P), and machined PEEK rods, along with commercially available titanium and ZrO2 healing abutments, were inserted into 3D oral mucosal models following a 4-mm punch biopsy. Inflammation was induced using Escherichia coli lipopolysaccharide. Analyses included histology, PrestoBlue viability assay, scanning electron microscopy, and ELISA quantification of cytokines IL-1β, IL-6, and IL-8. Results: Epithelial attachment was greater on TiZr-SLA, ZrO2-P, and PEEK-M (p < 0.05 and p < 0.01) surfaces compared with TiZr-M and ZrO2-M. TiZr-SLA exhibited the highest connective tissue attachment (p < 0.05). Commercial titanium and ZrO2 healing abutments demonstrated the highest post-pull PrestoBlue viability and overall soft tissue attachment. SEM confirmed cell retention on all implant surfaces. Elevated IL-1β levels were detected in models exposed to ZrO2-M and PEEK-M, whereas IL-6 and IL-8 levels were not influenced by any material or surface topography. Conclusions: In vitro epithelial and connective tissue responses are influenced by implant material, surface topography, and design. Rough TiZr-SLA surfaces promote superior connective tissue attachment, while smooth commercial abutments support optimal overall soft tissue integration. These findings highlight the importance of surface engineering in preclinical optimization of peri-implant soft tissue attachment. Full article
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18 pages, 6816 KB  
Article
Coalbed Methane Enrichment and Production Potential in Multiple Coal Seams in Yanjiao Composite Syncline, Western Guizhou Province, South China
by Lihua Wang, Guoxiao Zhou, Cunyou Liu and Shida Chen
Processes 2026, 14(5), 842; https://doi.org/10.3390/pr14050842 - 5 Mar 2026
Viewed by 316
Abstract
Coalbed methane (CBM) hosted by multiple (>20) thin (<2 m) seams in South China represents an important unconventional gas supplement. In the Yanjiao composite syncline, high-frequency sea-level fluctuations produced widely distributed thin seams (20–60 layers), with tidal-flat coal groups I (No. 2–No. 9) [...] Read more.
Coalbed methane (CBM) hosted by multiple (>20) thin (<2 m) seams in South China represents an important unconventional gas supplement. In the Yanjiao composite syncline, high-frequency sea-level fluctuations produced widely distributed thin seams (20–60 layers), with tidal-flat coal groups I (No. 2–No. 9) and III (No. 20–No. 35) as primary targets. Variable magma intrusion drives the present coal-rank partitioning (1.8–4.3% Ro) and pronounced reservoir heterogeneity. A basalt floor (>200 m) and the Lower Triassic Feixianguan caprock (~100 m) confine the Longtan strata into an independent hydrodynamic unit. Groundwater migrates from syncline wings to the axial domain and seals CBM in stagnant zones, resulting in higher gas contents toward the axis. Deep CBM is constrained by high in situ stress and low permeability (typically <0.1 mD below 600 m) and a relatively uniform and low-abnormal pressure system. The syncline is divided into four parts: Part I is the most favorable, where staged fracturing of closely spaced (<60 m) coal group III achieved a maximum production rate of 2400 m3/d and a stabilized rate of 2100 m3/d, whereas Part IV (depth > 1000 m) records a peak daily gas rate of 512–654 m3/d and shows no stabilized-production stage. Full article
(This article belongs to the Special Issue Phase Behavior Modeling in Unconventional Resources)
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27 pages, 7094 KB  
Article
Differences in Soil Fauna Communities and Vertical Heterogeneity Between Winter Pre-Sealing and Sealing Periods in Plastic Greenhouse Vineyards
by Xin Li, Mengmeng Qi, Zemeng Zhou and Meixiang Gao
Agriculture 2026, 16(5), 556; https://doi.org/10.3390/agriculture16050556 - 28 Feb 2026
Viewed by 217
Abstract
When cold waves occur in winter, the entire vineyard greenhouse is completely covered with plastic film to improve heat insulation. However, differences in vertical stratification of soil faunal communities between pre-sealing (PSP) and sealing periods (SP) have not been fully quantified. We compared [...] Read more.
When cold waves occur in winter, the entire vineyard greenhouse is completely covered with plastic film to improve heat insulation. However, differences in vertical stratification of soil faunal communities between pre-sealing (PSP) and sealing periods (SP) have not been fully quantified. We compared soil fauna communities and hydrothermal nutrient conditions between PSP and SP in standardized protected vineyards, sampling 0–10, 10–20, and 20–30 cm soil layers. Community traits were analyzed via paired Wilcoxon tests and mixed-effects models, while compositional differentiation was assessed using PCoA/PERMANOVA, NMDS/ANOSIM, and redundancy analysis with hierarchical partitioning. Soil fauna abundance decreased significantly in SP, with sharp declines in 0–10 and 20–30 cm layers, whereas the 10–20 cm layer showed minimal shifts. Taxon richness and alpha-diversity indices exhibited no consistent stage-specific variations. Inter-layer compositional differentiation intensified in SP, indicating enhanced vertical community stratification. Depth-specific analysis revealed the main drivers of community shifts: SOC and C: N in 0–10 cm, pH and C: N in 10–20 cm, and moisture and temperature in 20–30 cm. Overall, we observed layer-dependent shifts in soil microenvironments and faunal communities between PSP and SP, suggesting that soil depth should be considered in protected vineyard management. Full article
(This article belongs to the Section Agricultural Soils)
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21 pages, 4893 KB  
Article
Modeling Wear of KNA-82 Coatings with 0.5% Yttrium for Radial Seals of Gas Turbine Engines
by Vitaliy Kulikov, Vadim Kubich, Yelyzaveta Fasol, Oleg Cherneta, Svetlana Kvon, Aristotel Issagulov, Saniya Arinova and Olga Zharkevich
Coatings 2026, 16(2), 261; https://doi.org/10.3390/coatings16020261 - 20 Feb 2026
Viewed by 261
Abstract
The paper presents the results of a study of linear wear of gas-flame and ion-plasma coatings of KNA-82 seals with an yttrium content of 0.5%, used in gas turbine engine assemblies, during physical modeling of their thermomechanical loading on small-sized samples. Tribotechnical tests [...] Read more.
The paper presents the results of a study of linear wear of gas-flame and ion-plasma coatings of KNA-82 seals with an yttrium content of 0.5%, used in gas turbine engine assemblies, during physical modeling of their thermomechanical loading on small-sized samples. Tribotechnical tests were carried out in four stages, simulating the operating conditions of real gas turbine engines—from the first start-up with running-in of the coating cut-in areas to reaching a steady state with their service properties formed. The surface of the coatings was in contact with the ridges of triangular-shaped plates without heating (20 °C), at average heating (350–470 °C), after holding the samples at 1100 °C and average heating of 410–460 °C, and after grinding off the worn layer that had worn out after holding the samples at 1100 °C at average heating of 320–440 °C. Trends in the change in the linear ear of coatings and the formation of friction tracks caused by the uneven manifestation of the physical and mechanical properties of coatings, which are unevenly distributed throughout their body, were determined. It was found that both coatings tend to stabilize the wear process at certain mechanical pressures in the friction contact zone and only in the temperature range from 20 °C to 400 °C. These pressures range from 4 MPa to 6.7 MPa for gas-flame coatings and from 3 MPa to 4.2 MPa for ion-plasma coatings. It has been determined that within the depth range of 30–100 μm, the wear resistance (as assessed by linear wear) of ion-plasma coatings is higher than that of gas-flame coatings. This predetermines the fact that in the event of a catastrophic collision between the coatings and a blade, the geometry of the damage to the surface of the gas-flame coating will be greater than that of the ion-plasma coating. In the event of damage exceeding 75–100 μm in depth, both coatings become inoperable, since their wear characteristics are no longer maintained. This is indicated by a rapid decrease in their wear resistance under step loading. Moreover, the gas-flame coating is more prone to catastrophic failure than the ion-plasma coating. Full article
(This article belongs to the Section Corrosion, Wear and Erosion)
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17 pages, 3224 KB  
Article
Visualizing Enhanced Microfluidic Electromembrane Desalination Using Nafion-Coated Heterogeneous Ion-Exchange Membranes
by Hyunwoo Choi, Bonseung Ku, Seokhee Han and Bumjoo Kim
Molecules 2026, 31(4), 719; https://doi.org/10.3390/molecules31040719 - 19 Feb 2026
Viewed by 288
Abstract
Heterogeneous ion-exchange membranes (IEMs) are cost-effective but suffer from low electrochemical efficiency due to surface inhomogeneities. While surface coating with homogeneous ionomers is a known modification strategy, its direct impact on electro-hydrodynamic behavior and desalination performance has rarely been visually verified. In this [...] Read more.
Heterogeneous ion-exchange membranes (IEMs) are cost-effective but suffer from low electrochemical efficiency due to surface inhomogeneities. While surface coating with homogeneous ionomers is a known modification strategy, its direct impact on electro-hydrodynamic behavior and desalination performance has rarely been visually verified. In this study, we employed a microfluidic platform to visualize and quantify the performance enhancement of Nafion-coated heterogeneous cation exchange membranes (CEMs). Contrary to conventional theories linking electro-convection (EC) to surface hydrophobicity, our results show that the hydrophilic Nafion coating significantly amplifies EC vortices. Direct visualization revealed that the coating layer acts as an electrical nozzle, inducing intense electric field focusing that triggers macroscopic vortex growth. Furthermore, we visually confirmed that the coating layer physically seals catalytic sites, effectively suppressing parasitic water-splitting reactions. In continuous desalination experiments, this hydrodynamic synergy led to a 32% increase in current efficiency (CE: 1.23) and an 18% increase in salt removal ratio (SRR: 79.4%) compared to bare membranes in the over-limiting regime. These findings demonstrate that inducing controlled hydrodynamic instability via surface modification is a dominant factor for high-efficiency desalination. Full article
(This article belongs to the Special Issue Design, Fabrication, and Applications of Nano-Membrane Materials)
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17 pages, 3585 KB  
Article
Feasibility Study of Manufacturing Hydraulic Fittings Using Additive Manufacturing Technologies: Comparative Analysis of FDM and SLA Methods
by Jakub Backiel, Pawel Dzienis, Karol Golak, Przemysław Zamojski, Maciej Rećko, Rafał Grądzki, José Emiliano Martínez and Rogelio Valdés
Materials 2026, 19(4), 799; https://doi.org/10.3390/ma19040799 - 18 Feb 2026
Viewed by 307
Abstract
This paper investigates the feasibility of manufacturing hydraulic fittings using additive manufacturing (AM) technologies, specifically Fused Deposition Modeling (FDM) and Stereolithography (SLA). The study addresses the environmental challenge of material waste in conventional fitting production by exploring 3D printing as an alternative manufacturing [...] Read more.
This paper investigates the feasibility of manufacturing hydraulic fittings using additive manufacturing (AM) technologies, specifically Fused Deposition Modeling (FDM) and Stereolithography (SLA). The study addresses the environmental challenge of material waste in conventional fitting production by exploring 3D printing as an alternative manufacturing method. Hydraulic fittings were designed using CAD software: SolidWorks 2022 and fabricated using FDM with PETG (Polyethene Terephthalate Glycol) material and SLA with UV-sensitive photopolymer resin. In present studies, on-destructive leak testing was conducted in accordance with PN-EN 1254-4 and PN-EN 1254, at pressures ranging from 0.1 to 1.0 bar. Dimensional accuracy analysis revealed shrinkage of approximately 1% for SLA-printed parts and 2% for FDM-printed parts. Microscopic examination at 50× and 80× magnification showed superior thread quality in SLA samples compared to FDM, which exhibited visible layer separation and material porosity. Leak testing demonstrated that while the brass reference fitting maintained complete seal integrity, both 3D-printed variants failed to achieve leak tightness under operational pressures, with structural failure occurring at 1.0 bar during tightening. The study showed that FDM with PETG material and SLA with UV-sensitive photopolymer resin, despite achieving acceptable dimensional tolerances (±1–2%), do not meet hydraulic leak tightness requirements at pressures exceeding 0.5 bar in their raw state after printing. The results suggest that alternative material formulations (e.g., carbon fiber-reinforced PEEK for FDM or epoxy engineering resins for SLA) warrant further investigation. Potential avenues for improvement include advanced surface treatment, optimization of printing parameters, and modifications to thread geometry to reduce interthread gaps. Full article
(This article belongs to the Topic 3D Printing Materials: An Option for Sustainability)
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14 pages, 1673 KB  
Article
Effects of Provisional Cement Cleaning Methods on Resin–Dentin Bond Strength Following Immediate Dentin Sealing with Different Adhesive Systems
by Zeynep Aydin, Cemile Kedici Alp and Osman F. Aydin
J. Funct. Biomater. 2026, 17(2), 98; https://doi.org/10.3390/jfb17020098 - 16 Feb 2026
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Abstract
This study evaluated the effects of different provisional luting cement removal methods on the shear bond strength (SBS) of resin cement to dentin following immediate dentin sealing (IDS) performed with two adhesive systems. A total of 168 extracted, caries-free human third molars were [...] Read more.
This study evaluated the effects of different provisional luting cement removal methods on the shear bond strength (SBS) of resin cement to dentin following immediate dentin sealing (IDS) performed with two adhesive systems. A total of 168 extracted, caries-free human third molars were used, of which 144 were allocated for SBS testing and 24 for scanning electron microscopy (SEM) analysis. Specimens were assigned according to the IDS protocol (no IDS, IDS with OptiBond FL, or IDS with G2-Bond), followed by provisional cementation using an eugenol-free temporary cement. Contaminated surfaces were subsequently cleaned with a hand scaler, aluminum oxide (Al2O3) air abrasion, or Katana Cleaner prior to final bonding with a dual-cure resin cement. SBS was measured after 24 h of water storage, and surface morphology was evaluated by SEM at 2500× magnification. IDS significantly increased SBS under uncontaminated conditions, with G2-Bond-based IDS exhibiting higher bond strength values than specimens without IDS. However, provisional cement contamination significantly reduced SBS regardless of the cleaning method applied, and none of the tested protocols fully restored the bond strength observed in uncontaminated IDS-treated dentin. SEM analysis revealed residual cement remnants and surface alterations after cleaning, even in specimens that appeared macroscopically clean. Within the limitations of this in vitro study, IDS enhances resin–dentin bonding when contamination is avoided; however, current mechanical and chemical cleaning methods are insufficient to completely recover bond strength compromised by provisional cement contamination, highlighting the importance of preventing contamination and preserving IDS layer integrity during indirect restorative procedures. Full article
(This article belongs to the Section Dental Biomaterials)
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