Search Results (3,096)

Saimaluu-Tash I, located in a high-altitude glacial valley in Kyrgyzstan, preserves one of Central Asia’s largest and most culturally significant concentrations of rock engravings. Despite extensive archaeological research, the physical, mechanical, and chromatic properties of the sandstone substrates relevant for conservation assessment remain poorly characterized. This study integrates petrographic microscopy, scanning electron microscopy, colorimetry, and Vickers hardness testing with the digital documentation of twelve engraved blocks to evaluate weathering processes, engraving practices, and long-term preservation. The engravings are carved into arkosic sandstone with carbonate cement, characterized by a weathered surface enriched in clay minerals and covered by a dark surface coating (patina). Weathered surfaces exhibit significantly lower hardness (0.6 ± 0.2 GPa) than unweathered stone (2.8 ± 0.6 GPa), which facilitated the engraving of the petroglyphs by allowing tools to penetrate more deeply into the stone. Colorimetric analyses reveal a strong chromatic contrast between the surface patina and the lighter sandstone exposed by engraving (ΔE ≈ 22.7). This contrast would have enhanced the original visibility of the petroglyphs and highlights potential conservation issues associated with the progressive reformation of this surface layer. Iconographic analysis identifies recurrent themes related to hunting, herding, mobility, animal management, and symbolic spatial practices within a nomadic high-mountain landscape. Overall, the results demonstrate how an integrated material and interpretative approach contributes to understanding rock art production processes. They support preventive and sustainable conservation strategies for vulnerable engraving landscapes shaped by long-term interactions between geological processes and human activity. Full article

The Late Triassic Bolila Formation in the central Qiangtang Basin is a typical carbonate buildup deposited during a regional transgression in the eastern Tethyan realm. Understanding its sedimentary evolution and reservoir-forming mechanisms is crucial for hydrocarbon exploration. This study integrates petrology, detrital zircon U-Pb geochronology, carbon-oxygen isotopes, and reservoir property analysis of the Quemudongda section. The results show: (1) detrital zircon dating provides a maximum depositional age of 225.7–235.7 Ma (Carnian–Norian), correcting the previous Jurassic misassignment on the 1:250,000 geological map. Carbon-oxygen isotopes (average δ¹³C = +3.2‰, δ¹⁸O = −11.1‰) are consistent with the global Carnian–Norian positive δ¹³C excursion. (2) The section reveals a platform-margin reef (hexactinellid and calcareous sponges) and slump breccia (seven layers) association, representing a steep-rimmed carbonate platform margin. The sedimentary evolution comprises three stages: reef initiation, reef flourishing with frequent slumping, and reef decline with dolomitization. (3) Reservoirs are mainly breccia and reef dolostones, with intergranular, intercrystalline, and fracture-related pores. Porosity averages 2.8% (0.8%–7.2%), permeability averages 0.35 mD (0.001–8.5 mD), defining a low-porosity, ultra-low-permeability fracture-pore reservoir. Breccia dolostone has better properties (porosity 3.71%, permeability 2.412 mD). (4) Reservoir formation is controlled by sedimentation (platform-margin facies), diagenesis (dolomitization generates pores, but high-temperature recrystallization causes densification), and tectonics (microfractures enhance permeability). High-quality reservoirs occur where breccia dolostone and fractures overlap. (5) The Bolila reef-shoal complex and the overlying Bagong Formation source rocks form a “lower reservoir—upper source” assemblage, representing a new exploration target in the Tuonamu area. The breccia dolostone–fracture overlap zone is the core “sweet spot”. Full article

Nanoemulsions are thermodynamically unstable but kinetically stable colloidal dispersion systems with droplet sizes ranging from 20 to 500 nm. With their high specific surface area, excellent optical properties, tunable rheology, and remarkable penetration ability, these systems demonstrate enormous potential in enhanced oil recovery (EOR). This paper systematically reviews the significant advances in nanoemulsion characterization techniques and oil displacement mechanisms. The nanoemulsion characterization techniques are examined, covering a comprehensive multi-scale characterization system from particle size and distribution analysis (e.g., dynamic light scattering, laser diffraction), micro-morphology and structure visualization (e.g., transmission electron microscopy, atomic force microscopy), and interface and surface property characterization (e.g., interfacial tension measurement, zeta potential analysis) to stability and rheology assessment, as well as chemical composition and structure analysis. Furthermore, core mechanisms of nanoemulsions in oil displacement processes are briefly summarized, revealing multiple synergistic enhancement mechanisms including ultra-low interfacial tension and oil film stripping, rock wettability alteration, emulsification and viscosity reduction, improved fluid flow and injection pressure reduction. Finally, prospects for the potential application of nanoemulsion oil displacement technology in the development of low-permeability, tight, and heavy oil reservoirs are described by analyzing the current challenges such as unclear structure–activity relationships, full-chain stability (including storage, transport, injection, and reservoir aging), and environmental safety, and future research directions are pointed out, including clarifying structure–activity relationships, smart responsive system development, artificial intelligence-assisted design, and pilot-scale validation. Clarifying the link between nanoemulsion characterization techniques and oil displacement mechanisms is of significant academic and engineering value for promoting the transition from empirical application to rational design of related technologies. Full article

Conventional rock blasting produces large rock masses that do not fully meet engineering construction requirements. Therefore, mechanical crushing technology is necessary to reduce these masses into crushed stone of a specific particle size. Consequently, enhancing the comprehensive utilisation rate of excavated materials and exploring new application avenues has become critical. Initial crushing experiments were conducted on limestone of varying strengths. Based on the measured parameters, simulation experiments were performed to analyse the accuracy of crushing particles of different strengths. Cube specimens confirmed that the created crushing model accurately reflects the actual crushing behaviour of particles with different strengths. A Structure Sensor 3D scanner was used to scan representative shapes of rock particles. Software processing yielded the true three-dimensional apparent morphology of the rock material. Combined with physical crushing tests and simulation experiments, this confirmed that the developed crushing model accurately reflects the actual crushing behaviour of rock particles when their true morphology is considered. The research findings demonstrate that the digital crushing model can accurately depict the crushing process and particle size distribution of rock materials with different lithological characteristics and true morphology. Full article

To clarify how injection-induced cooling and reservoir properties jointly control rock damage during hydraulic fracturing of deep shale reservoirs, this study develops a coupled thermo–hydro–mechanical phase-field model incorporating fracture pressurization, matrix seepage, heat transfer, thermoelastic stress redistribution, and tensile damage evolution. The hydraulic fracture component is verified against the classical KGD analytical benchmark, and the thermal damage component is benchmarked against a ceramic quenching experiment. The phase-field formulation is constructed using tensile-compressive strain-energy decomposition so that only the tensile part of the elastic energy contributes to damage evolution, while the compressive stiffness is retained. The results show that low-temperature fluid injections produce a steep but spatially limited cooling zone near the fracture wall. The constrained contraction of the cooled rock generates additional thermoelastic tensile stress, strengthens fracture-tip stress localization, and accelerates phase-field damage accumulation. In the baseline case, thermal cooling increases the peak tensile stress near the fracture tip along profile c from 10.2 MPa in the hydraulic-only case to 22.5 MPa at t = 2 h, while the phase-field damage value increases from 0.03 to 0.77. Five-case sensitivity analyses show that, as α_T increases from 0.5 × 10⁻⁵ to 1.5 × 10⁻⁵ 1/°C, the fracture-tip tensile stress at t = 2 h increases from approximately 18.6 MPa to 25.7 MPa, and the damage value increases from approximately 0.80 to 0.96. As permeability increases from 0.0001 mD to 0.01 mD, the pore pressure at 2 m from the fracture wall increases from approximately 50.4 MPa to 71.2 MPa, and the tensile stress along profile c increases from approximately 16.4 MPa to 21.8 MPa. These results demonstrate that coupled thermal and hydraulic effects govern fracture initiation, localization, and propagation tendency during thermally assisted hydraulic fracturing in deep shale reservoirs. Full article

Rainfall-induced delayed instability of fractured rock slopes is strongly affected by fracture preferential flow, hydro-mechanical coupling, and spatial matrix heterogeneity. However, the coupled influence of stress-dependent fracture aperture evolution and heterogeneous matrix properties on delayed slope deformation remains insufficiently quantified. In this study, a two-dimensional discrete fracture network (DFN)–equivalent continuum coupled model was established using spectral random field theory and a representative Monte Carlo-generated fracture geometry. The spectral exponent β = 1.0–2.5 was adopted to characterize different degrees of matrix heterogeneity, and rainfall infiltration–stress coupling simulations were conducted under an extreme rainfall scenario followed by drainage. The results indicate that the wetting front advances irregularly in the heterogeneous matrix, while fracture preferential flow accelerates rainwater infiltration and promotes local pore-pressure accumulation near the phreatic surface. After rainfall cessation, water stored in fractures continues to recharge the deep matrix, leading to delayed pore-pressure increase and post-rainfall deformation. The simulated fracture aperture shows an initial closure followed by gradual dilation, which is controlled by the competition between saturation-induced stress redistribution and pore-pressure-driven effective stress reduction. Under a common strength reduction factor of FOS = 1.4, stronger matrix heterogeneity results in more pronounced plastic strain concentration and larger displacement amplitude along the potential slip zone. These findings suggest that fracture aperture evolution and matrix heterogeneity jointly influence delayed deformation and potential failure-zone development in rainfall-affected fractured rock slopes. The conclusions should be interpreted within the scope of a two-dimensional DFN–equivalent continuum numerical framework with prescribed rainfall conditions and representative fracture/random-field realizations. Full article

Tight gas is a critical unconventional energy resource, yet the geological characteristics and accumulation processes of tight gas in China’s Songliao Basin remain poorly documented. This study aims to investigate the tight gas system in the Songliao Basin as a representative continental basin, with key objectives including evaluating source rock and reservoir properties via mineralogical and geochemical analyses, characterizing lithologies and pore types, determining the gas charging mechanism in tight media, and identifying the main controlling factors for accumulation. Geochemical results indicate that the Shahezi Formation contains medium to good mudstones and excellent coals. Reservoirs consist of tight sandstones and conglomerates deposited in fan delta and braided river delta systems, with pore spaces dominated by dissolution pores and microfractures, resulting in ultra-low porosity and permeability. Conventional buoyancy-driven migration is ineffective; instead, gas charging is driven by hydrocarbon generation expansion force, creating overpressure that expels pore water and forces gas into reservoirs through fault-sand conduits. Accumulation is controlled by continuous gas supply from thick, highly mature source rocks, dissolution-enhanced and fracture-dominated reservoir space, and sufficient source–reservoir pressure difference. This study elucidates tight gas characteristics and accumulation mechanisms in continental basins, providing data applicable to both continental and marine settings. Full article

The synergistic utilization of post-mining spaces and geothermal energy through underground seasonal thermal energy storage (USTES) provides a promising pathway for sustainable heating and the low-carbon redevelopment of mining regions. To advance the thermal management and reveal the thermo-hydraulic evolution patterns within these repurposed environments, this study proposes an integrated approach that utilizes post-mining roadways as heat storage reservoirs, within the scope of a single idealized case study. A comprehensive USTES heating system model was established to systematically evaluate operational characteristics and environmental impacts under diverse conditions assuming homogeneous rock properties and idealized thermal boundaries. Results demonstrate that the surrounding ground temperature and the low thermal conductivity of the rock mass contribute to limiting heat dissipation and maintaining stable seasonal storage performance. For a roadway with a 20,000 m³ water storage capacity and an optimal 3900 m² solar collector area, the system successfully satisfies the thermal demand of 30,000 m² of building area. The configuration achieves 1239 MWh of cumulative heat storage over a 245-day cycle, maintaining a direct heating-to-heat-pump-upgraded heating ratio of 1.02. Furthermore, the implementation of variable-frequency thermal management strategies demonstrates remarkable economic and environmental superiority, yielding a 35.8% cost reduction compared to coal-fired heating, an overall energy saving rate of 77.5% relative to electric heating systems and a 13.5% decrease in CO₂ emissions relative to gas-fired systems. This research provides fundamental design parameters for the synergistic exploitation of mineral and geothermal resources, advancing the development of green heating and the sustainable utilization of post-mining spaces. Full article

This article describes the development of a compact and affordable variable-temperature NMR instrument designed primarily to measure dynamic molecular motion in solids and liquids. The instrument consists of Lab-Tools’ Mk4 palm-top time-domain NMR spectrometer fitted with a Peltier-cooled variable-temperature probe inside a shimmed Halbach magnet. Measurement of NMR relaxation times T₁, T₂, and ${\mathrm{T}}_1\rho$ is possible over the temperature range −20 °C to 70 °C with cooling and heating rates, and data acquisition is controlled from an integrated mini-PC. The overall footprint of the instrument is roughly that of a shoe box, making both in-the-field and bench-top measurements possible. Applications of this instrument include measuring pore-size distribution in porous rocks, the viscosity of oils and tars trapped in porous rock, the properties of polymers, and the viscosity of the liquid components of foods (e.g. fruits, vegetables and seeds). Results of test measurements for calibrated oils and olive oil are presented together with measurements of molecular mobility in a solid polymer. Full article

The blasting-induced environmental impact of tunneling is a major concern in drill and blast excavation practice, particularly in urban areas. The present paper carries out comprehensive numerical modeling to study the vibration attenuation at the soil surface away from the blasting source as well as the resulting interactions between a historical structure and the surrounding soil, with particular attention to the effects of a millisecond delay. Special attention is given to the interpretation of the role of the local site effects in terms of the frequency-dependent changes of the vibration attenuation mechanism and the response of the historical structure. The velocity responses along the ground surface generally exhibit higher-frequency suppression and low-frequency amplification for both instantaneous blasting and millisecond delay blasting cases in the layered soil–rock site. The millisecond delay blasting can effectively avoid excessive vibration velocity and thus reduce the vibration amplitude at the ground surface by 60–70% (compared with instantaneous blasting), with the predominant frequency mainly concentrated in the high frequence band of 400–500 Hz. The empirical formulae for predicting the vibration attenuation along the scale distance in a soil–rock site has been proposed for both instantaneous blasting and millisecond delay blasting. Through the HHT spectral analyses of the velocity response of the historical structure, it is seen that the difference of structure properties between the wood-frame tower and the base masonry structure has a remarkable influence on the structural vibration. The numerical results can provide a reliable reference for the practical blasting scheme and the systematic study of the dynamic responses of historical structures subjected to blasting-induced vibrations. Full article

Grouting and sealing in gas drainage boreholes are two of the critical measures to ensure efficient coal seam gas extraction. However, traditional cement grouting often leads to debonding and cracking of the slurry–coal cemented body under external load, resulting in poor sealing performance. To suppress crack propagation and achieve borehole reinforcement and efficient sealing, this study compares the mechanical properties and crack evolution characteristics of slurry–coal cemented samples grouted with different modified materials. Five types of cement-based sealing materials, including ordinary Portland cement, were used for grouting coal rock in boreholes. By employing an acoustic emission signal acquisition system and a non-contact full-field strain measurement system, the tensile mechanical properties of coal before and after grouting were compared. The influence of material properties on the reinforcement capacity of borehole coal was analyzed, along with the failure process characteristics and final failure morphology of the slurry–coal cemented body under Brazilian splitting load. Finally, the effects of material toughness and bond strength on the brittleness index and failure mode of the slurry–coal cemented samples under Brazilian splitting conditions were discussed. The results show that the tensile strength improvement rates of the samples were 26.9%, 55.3%, 48.4%, 8.6%, and 45.6%, respectively. Distinct from previous studies focusing on fractured grouting or intact coal rock, this work for the first time systematically reveals the non-monotonic influence of the combination of material toughness and bond strength on the reinforcement effect of borehole coal samples and proposes an evaluation framework based on quantitative acoustic emission crack type analysis and the concept of effectiveness threshold. The varying degrees of tensile strength enhancement indicate differences in the reinforcement capabilities of grouting materials with different properties. The acoustic emission signals during the failure process of the slurry–coal cemented body exhibited typical stage-specific characteristics, though material properties altered the failure modes. By quantifying the intrinsic properties and crack characteristics of the slurry–coal cemented body using the brittleness index and grayscale histograms, this study provides a theoretical basis for guiding efficient sealing of gas drainage boreholes through an in-depth understanding of the mechanical behavior and crack evolution of borehole coal samples before and after grouting under Brazilian splitting conditions. Full article

This study investigates the effect of waste cement dust (CD) and rock wool (RW) inorganic fiber on the tribological performance of brake friction composite materials. Five formulations were fabricated by varying CD from 65 to 45 wt.% and RW from 5 to 25 wt.% and evaluated for tribological properties on a Chase friction testing machine in accordance with IS 2742 test procedures. The results show that composites containing higher CD and lower RW exhibited higher coefficients of friction, lower friction variability, and improved fade resistance. In contrast, composites containing higher RW and lower CD showed improved recovery characteristics and substantially enhanced wear resistance. The performance coefficient of friction decreased from about 0.521 to 0.442 as the formulation shifted from CD-rich to RW-rich compositions, while the variability coefficient increased from about 0.364 to 0.516. The highest wear was recorded for the composite containing 65 wt.% CD and 5 wt.% RW inorganic fiber, whereas the lowest friction fluctuations were obtained for the composite containing 55 wt.% CD and 15 wt.% RW inorganic fiber. Finally, a simple ranking process-based decision-making technique was employed to evaluate the overall performance of all the composites, suggesting 55 wt.% CD as the optimal content. These findings confirm the potential of waste CD as a viable functional constituent in brake friction composites when combined with RW inorganic fiber in an optimized manner. Full article

One of the most common problems in drilling operations is lost circulation, which can significantly increase well costs and lead to issues such as pipe sticking, blowouts, and even well closures. Identifying thief zones using analytical models is especially difficult, and there are no robust equations available in the literature due to a wide range of influential parameters, both controllable and uncontrollable. These parameters include operational factors, as well as the physical properties of the rock and drilling fluid. This study presents an artificial intelligence-based model designed to predict lost circulation zones. It investigates the underexplored potential of WV-curves for feature selection. Traditionally used to represent the spectral characteristics of training data, their role in feature selection has not been widely examined in the literature. The presentation of WV-curves is modified, and their effectiveness in identifying the optimal number of input and hidden neurons is evaluated. In this research study, a total of 15,000 data points were used and collected from oil wells in the Middle East. The artificial neural network (ANN) model exhibited a remarkable ability to accurately predict the locations of lost circulation zones based on the collected data, achieving an impressive accuracy of 94.5%. This is a significant achievement when compared to existing ANN models in the literature. The results highlight the strength of the ANN model in predicting lost circulation locations across a wide range of data collected from various wells in the Middle East. In addition, this model takes into account a diverse set of drilling operational parameters, as well as rock characteristics and fluid properties, offering a broader approach compared to other available ANN models. This advancement will also greatly facilitate future studies, enabling the prediction of lost circulation zones, and enabling advanced planning of appropriate prevention and remediation methods during the well planning phase to reduce the risk of lost circulation. Nevertheless, it should be noted that one limitation of the proposed methodology relates to data availability, as comprehensive formation parameters were not fully accessible; the inclusion of additional formation data may offer opportunities for further improvement in future studies. Full article

With deep coal mining in China, high in situ stress frequently causes severe floor deformation, bolt-cable support failure, and excessive floor heave, which critically threaten mine safety. In this study, we use physical experiments, numerical simulation, and theoretical analysis to explore how hydraulic fractures with different azimuth angles affect stress transfer in roadways under floor dynamic pressure. Prefabricated fractures simulate weak planes induced by hydraulic fracturing. Uniaxial compression tests and PFC2D fluid–solid coupling simulations analyze mechanical properties, failure modes, acoustic emission behavior, and stress distribution. Results show that fracture azimuth significantly controls rock damage and failure modes. As the angle increases from 0° to 90°, failure changes from gradual degradation to sudden instability. Peak strength first decreases then increases, reaching the minimum at 22.5°, while roadway damage is minimal at 45°. Small-angle fractures lead to shear failure with clear precursors, and large-angle fractures cause sudden tensile failure. Hydraulic fractures form directional stress-relief zones and enable effective stress transfer and pressure relief. The results support parameter optimization of hydraulic fracturing and stability control for deep roadways under floor dynamic pressure. Full article

As tunnel construction advances toward greater depths and lengths, full-face tunnel boring machines (TBMs) have become the preferred method for large-scale excavation. The operational efficiency of TBMs significantly impacts the progress, cost, and safety of tunnel projects. With the rapid development of machine learning and big data technologies, data-driven models based on cutterhead response signals have emerged as a key approach to improving TBM perception and decision-making. However, conventional rock-breaking indicators predominantly rely on single physical variables, limiting their ability to capture the complex dynamic interactions between the TBM and surrounding rock during excavation, thereby restricting their engineering applicability. To address this limitation, this study proposes a knowledge-driven data processing and indicator construction method to more accurately represent TBM operational states and surrounding rock properties. First, a novel excavation phase division algorithm based on time-domain and penetration-depth features is developed to accurately distinguish different tunneling stages. Subsequently, using data from the YC and YE projects, thrust- and torque-driven rock-breaking indicators are formulated, and the relationship between penetration depth and thrust/torque is optimized via power function fitting. Optimal exponents are determined through algorithmic optimization. Validation with field data confirms that the proposed indicators significantly enhance the accuracy and generalization of surrounding rock classification and control parameter prediction models. Full article