Search Results (12)

Liquid-nitrogen biobanks need temporary, spatially distributed temperature records, but conventional batteries and radios become unreliable far below their rated operating temperatures. We developed a finite-duration wireless logging system that separates sensing and communication in both space and time. A remote PT1000 probe follows the cryogenic environment, whereas a polytetrafluoroethylene (PTFE)/aerogel enclosure delays cooling of the battery and electronics; data are stored locally during exposure and retrieved by Bluetooth Low Energy only after warm-up. This differentiated thermal-path and staged-communication architecture is the principal novelty of this work. A transient node model reproduced the internal cooling trend, with a mean absolute error (MAE) of 3.74 °C, a root mean square error (RMSE) of 3.92 °C, and r = 0.9986, with a 123.5 s difference in the time to reach −50 °C. Nine nodes logged for 38.4–47.2 min (mean 44.2 min), and all reconnected after 35 min of warm-up at approximately 25 °C. In a one-node indoor engineering test, historical records were recovered without packet loss over 2–10 m, and 18 locations in an operating biobank yielded retrievable temperature histories. The system therefore supports short, non-real-time mapping and workflow assessment; it is not a substitute for fixed real-time alarm or metrological monitoring systems. Full article

This paper discusses the issue of the self-heating effect of resistance sensors during temperature measurement. The self-heating effect causes temperature measurement errors. The aim of this work was to develop a method for in situ assessment of the thermal resistance between a self-heating thermometer and its surrounding environment, the temperature of which is measured. The proposed method is used to assess the uncertainty resulting from the heat transfer from the thermometer to the surrounding environment, which allows increased measurement accuracy. The proposed method consists of experimental determination of the sensor’s temperature characteristics in relation to the heating power for different values of the measuring current. Sample measurements were carried out on a representative group of resistance temperature sensors. The relationship of the internal thermal resistance to the type of sensor design and the relationship of the external resistance to the ambient conditions were demonstrated. The developed method allows the appropriate measuring current of the resistance temperature sensor to be selected according to its design, the mounting method, and the environmental conditions, which ensures that measurement errors are maintained at an appropriately low level. Full article

This paper describes the development and validation of an apparatus for the realization of the triple point of argon (83.8058 K), with a novel automatic pressure control system for the liquid nitrogen cryostat. The automatic pressure controller, together with custom-made software, was developed and tested in the Laboratory for Process Measurement at the Faculty of Mechanical Engineering and Naval Architecture, University of Zagreb (FSB-LPM). Performance testing and characterization of the automatic pressure controller confirmed its suitability for precise and reliable control of gauge pressure in the cryostat. The characteristics and uncertainty of the measurement setup for the realization of the triple point of argon were validated through a bilateral hybrid comparison with the Laboratory of Metrology and Quality at the Faculty of Electrical Engineering, University of Ljubljana (MIRS/UL-FE/LMK). A long-stem quartz-sheathed standard platinum resistance thermometer was used as a transfer standard. The realizations of the International Temperature Scale (ITS-90) were compared in the subrange from the triple point of argon to the triple point of water. The comparison results show that resistance ratio (W) values determined by FSB-LPM at the fixed points of argon and mercury deviate from the MIRS/UL-FE/LMK values, within the determined combined uncertainty of the comparison. Full article

A compact thermometer for air temperature based on the measurement of the speed of sound was developed at INRIM. This paper focuses on the comparison of this instrument with platinum resistance thermometers in a climatic chamber over a temperature range (−30 ÷ +55) °C, relative humidity (10 ÷ 90)%rh, and irradiation (>1 kW/m²) values similar to those of surface atmospheric conditions. Overall uncertainty values of 0.2 °C over the range from −30 °C to +30 °C, and from 0.6 °C to +55 °C, were found. Moreover, the instrument proved to be immune to irradiation errors and free from the need for temperature calibration. Full article

Accurate measurements of long distances (in the order of tens of meters or more) are necessary in manufacturing processes of large structures, as, for example, in the aerospace industry. In the most demanding applications, the goal is to achieve a relative accuracy of 10⁻⁷ in the measurement of distances (e.g., 1 µm over 10 m). This goal can be obtained with laser interferometers whose accuracy is based on knowledge of the speed of light, which, in turn, depends on the temperature of air. A thermometer based on the measurement of the speed of sound in air has been realized at INRIM. Its purpose is the measurement of the air temperature along the measurement path of the interferometer with an accuracy of 0.1 °C at distances up to 11 m. The paper describes the principle and the experimental setup of the acoustic thermometer and demonstrates its performance by comparison with calibrated reference platinum resistance thermometers. Furthermore, we demonstrate the potentiality of the method to measure the vertical temperature gradient, which is the main error source in triangulation measurements when using laser trackers. Full article

Temperature is one of the most relevant physical quantities that affects almost all processes in nature. However, the realization of accurate temperature standards using current temperature references, like the triple point of water, is difficult due to the requirements on material purity and stability of the environment. In addition, in harsh environments, current temperature sensors with electrical readout, like platinum resistors, are difficult to implement, urging the development of optical temperature sensors. In 2018, the European consortium Photoquant, consisting of metrological institutes and academic partners, started investigating new temperature standards for self-calibrated, embedded optomechanical sensor applications, as well as optimised high resolution and high reliability photonic sensors, to measure temperature at the nano and meso-scales and as a possible replacement for the standard platinum resistant thermometers. This article presents an overview of the results obtained with sensor prototypes that exploit photonic and optomechanical techniques for sensing temperatures over a large temperature range (5 K to 300 K). Different concepts are demonstrated, including ring resonators, ladder-like resonators and suspended membrane optomechanical thermometers, highlighting initial performance and challenges, like self-heating that need to be overcome to realize photonic and optomechanical thermometry applications. Full article

In this work, the authors exploited the whispering gallery mode (WGM) resonator properties as a thermometer. The sensor is made of a cylindrical sapphire microwave resonator in the center of a gold-plated copper cavity. Two coaxial cables act as antennas and excite the WGM standing waves in the cylindrical sapphire at selected resonance frequencies in the microwave range. The system affords a high quality factor that enables temperature measurements with a resolution better than 15 µK and a measurement standard uncertainty of 1.2 mK, a value approximately three times better than that achieved in previous works. The developed sensor could be a promising alternative to platinum resistance thermometers, both as a transfer standard in industrial applications and as an interpolating instrument for the dissemination of the kelvin. Full article

Satellite instruments operating in the thermal infrared wavelength range >3 µm provide information for applications such as land surface temperature (LST), sea surface temperatures (SST), land surface emissivity, land classification, soil composition, volcanology, fire radiative power, cloud masking, aerosols, and trace gases. All these instruments are dependent on blackbody (BB) calibration sources to provide the traceability of the radiometric calibration to SI (Système International d’Unités). A key issue for flight BB sources is to maintain the traceability of the radiometric calibration from ground to orbit. For example, the temperature of the BB is measured by a number of precision thermometers that are calibrated against a reference Standard Platinum Resistance Thermometer (SPRT) to provide the traceability to the International Temperature Scale of 1990 (ITS-90). However, once calibrated the thermometer system is subject to drifts caused by on-ground testing, the launch and space environments. At best the uncertainties due to thermometer ageing can only be estimated as there is no direct method for recalibrating. Comparisons with other satellite sensors are useful for placing an upper limit on calibration drifts but do not themselves provide a traceable link to the SI. In this paper, we describe we describe some of the technology developments, including phase change cells for use as reference standards, thermometer readout electronics and implementation of novel coatings, that are in progress to enhance the traceability of flight calibration systems in the thermal infrared. Full article

Temperature measurement is essential in industries. The advantages of resistance temperature detectors (RTDs) are high sensitivity, repeatability, and long-term stability. The measurement performance of this thermometer is of concern. The connection between RTDs and a novel microprocessor system provides a new method to improve the performance of RTDs. In this study, the adequate piecewise sections and the order of polynomial calibration equations were evaluated. Systematic errors were found when the relationship between temperature and resistance for PT-1000 data was expressed using the inverse Callendar-Van Dusen equation. The accuracy of these calibration equations can be improved significantly with two piecewise equations in different temperature ranges. Two datasets of the resistance of PT-1000 sensors in the range from 0 °C to 50 °C were measured. The first dataset was used to establish adequate calibration equations with regression analysis. In the second dataset, the prediction temperatures were calculated by these previously established calibration equations. The difference between prediction temperatures and the standard temperature was used as a criterion to evaluate the prediction performance. The accuracy and precision of PT-1000 sensors could be improved significantly with adequate calibration equations. The accuracy and precision were 0.027 °C and 0.126 °C, respectively. The technique developed in this study could be used for other RTD sensors and/or different temperature ranges. Full article

The design, fabrication, and use of a hotspot-producing and temperature-sensing resistance thermometer for evaluating the thermal properties of low-dimensional materials are described in this paper. The materials that are characterized include one-dimensional (1D) carbon nanotubes, and two-dimensional (2D) graphene and boron nitride films. The excellent thermal performance of these materials shows great potential for cooling electronic devices and systems such as in three-dimensional (3D) integrated chip-stacks, power amplifiers, and light-emitting diodes. The thermometers are designed to be serpentine-shaped platinum resistors serving both as hotspots and temperature sensors. By using these thermometers, the thermal performance of the abovementioned emerging low-dimensional materials was evaluated with high accuracy. Full article

This paper presents a state-of-the-art whispering gallery mode (WGM) thermometer system, which could replace platinum resistance thermometers currently used in many industrial applications, thus overcoming some of their well-known limitations and their potential for providing lower measurement uncertainty. The temperature-sensing element is a sapphire-crystal-based whispering gallery mode resonator with the main resonant modes between 10 GHz and 20 GHz. In particular, it was found that the WGM around 13.6 GHz maximizes measurement performance, affording sub-millikelvin resolution and temperature stability of better than 1 mK at 0 °C. The thermometer system was made portable and low-cost by developing an ad hoc interrogation system (hardware and software) able to achieve an accuracy in the order of a few parts in 10⁹ in the determination of resonance frequencies. Herein we report the experimental assessment of the measurement stability, repeatability and resolution, and the calibration of the thermometer in the temperature range from −74 °C to 85 °C. The combined standard uncertainty for a single temperature calibration point is found to be within 5 mK (i.e., comparable with state-of-the-art for industrial thermometry), and is mainly due to the employed calibration setup. The uncertainty contribution of the WGM thermometer alone is within a millikelvin. Full article

The heat transfer analysis of hydrate-bearing sediment involved phase changes is one of the key requirements of gas hydrate exploitation techniques. In this paper, experiments were conducted to examine the heat transfer performance during hydrate formation and dissociation by a thermal method using a 5L volume reactor. This study simulated porous media by using glass beads of uniform size. Sixteen platinum resistance thermometers were placed in different position in the reactor to monitor the temperature differences of the hydrate in porous media. The influence of production temperature on the production time was also investigated. Experimental results show that there is a delay when hydrate decomposed in the radial direction and there are three stages in the dissociation period which is influenced by the rate of hydrate dissociation and the heat flow of the reactor. A significant temperature difference along the radial direction of the reactor was obtained when the hydrate dissociates and this phenomenon could be enhanced by raising the production temperature. In addition, hydrate dissociates homogeneously and the temperature difference is much smaller than the other conditions when the production temperature is around the 10 °C. With the increase of the production temperature, the maximum of ΔT_oi grows until the temperature reaches 40 °C. The period of ΔT_oi have a close relation with the total time of hydrate dissociation. Especially, the period of ΔT_oi with production temperature of 10 °C is twice as much as that at other temperatures. Under these experimental conditions, the heat is mainly transferred by conduction from the dissociated zone to the dissociating zone and the production temperature has little effect on the convection of the water in the porous media. Full article