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17 pages, 1171 KiB  
Article
An Innovative Metal–Synthetic Hybrid Thread for the Construction of Aquaculture Nets
by Alexis Conides, Efthimia Cotou, Dimitris Klaoudatos and Branko Glamuzina
J. Mar. Sci. Eng. 2025, 13(8), 1384; https://doi.org/10.3390/jmse13081384 - 22 Jul 2025
Viewed by 172
Abstract
Based on the experience gained worldwide from potential solutions to the fouling problem of fisheries and aquaculture infrastructure, we attempted to design, construct and test the antifouling efficiency of a new hybrid filament created from non-laminated copper wire braided with synthetic fibers made [...] Read more.
Based on the experience gained worldwide from potential solutions to the fouling problem of fisheries and aquaculture infrastructure, we attempted to design, construct and test the antifouling efficiency of a new hybrid filament created from non-laminated copper wire braided with synthetic fibers made of Dyneema. The design involved the creation of a hybrid twine substituting a percentage of the synthetic fibers with 0.1–0.15 mm diameter copper wire at 5%, 10%, 20% and 40% levels. There is limited information in the international literature for comparison with our results, since there has never been any attempt to create such a hybrid net. The results showed that for the 6 mm mesh, the maximum openness obtained after the 8-month experimental period was 8.72%, with Cu wire substitution at 35%. For the 12 mm mesh, these values were 27.07% at 26%, and for the 20 mm mesh, they were 33.68% at 28%. A conservative average independent from mesh size to achieve optimum openness in the long term is 30 ± 4.73% Cu wire substitution. In addition, we found that both the mesh size (mm) and the copper substitution percentage affected the fouling process during the experimental period, which lasted 8 months. Full article
(This article belongs to the Section Marine Aquaculture)
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12 pages, 778 KiB  
Article
Comparison of All-Suture Anchors and Metal Anchors in Arthroscopic Rotator Cuff Repair: Short-Term Clinical Outcomes and Anchor Pullout Risk
by Tolga Keçeci, Yusuf Polat, Abdullah Alper Şahin, Murat Alparslan, Serkan Sipahioğlu and Alper Çıraklı
J. Clin. Med. 2025, 14(8), 2619; https://doi.org/10.3390/jcm14082619 - 11 Apr 2025
Viewed by 769
Abstract
Objectives: Metal anchors (MA), commonly used in the early stages of rotator cuff surgical treatment development, are associated with a high risk of complications, especially in osteoporotic bone. As an alternative to rigid anchors, all-suture anchors (ASA) have been introduced for the medial [...] Read more.
Objectives: Metal anchors (MA), commonly used in the early stages of rotator cuff surgical treatment development, are associated with a high risk of complications, especially in osteoporotic bone. As an alternative to rigid anchors, all-suture anchors (ASA) have been introduced for the medial row, offering promising clinical outcomes and favorable biomechanical studies. We aimed to compare the clinical outcomes of MAs and ASAs in either single-row or in medial-row suture bridge techniques in arthroscopic rotator cuff repair. Our hypothesis was that in cases where ASA was used for at least 12 months of follow-up, more favorable results would be obtained as compared to rigid anchors, and intraoperative complications such as anchor pullout would be encountered less. Methods: In this retrospective cohort analysis, we reviewed patients who underwent arthroscopic rotator cuff repair between January 2020 and December 2022. Surgeries were performed by two senior surgeons in a single tertiary center. Patients who had undergone revision surgery, had a history of previous shoulder surgeries, had massive rotator cuff tears, and partial-thickness tears; or had concomitant subscapularis tears were excluded. Preoperative and postoperative scores, including Constant–Murley (CM), Disabilities of the Arm, Shoulder, and Hand (DASH), and visual analog scale (VAS), were compared. The minimum follow-up period was 12 months. Clinical assessment of shoulder range of motion included forward flexion, abduction, internal rotation, and external rotation. Intraoperative anchor-related complications were compared. All patients underwent the same surgical technique and postoperative rehabilitation protocol. Results: A total of 142 patients (89 females, 53 males; mean age: 57.4 years) were included in the study, with 67 patients in the ASA group and 75 in the MA group. The sex distribution and mean age were similar between groups. The ASA group had 15 traumatic tears, while the MA group had 13 (p < 0.05). The mean follow-up period was 21.6 months (range 12–40 months). Preoperative CM scores were statistically better in the ASA group, but this difference was not clinically relevant (p < 0.046). The mean CM score was 75.64, the mean DASH score was 8.57, and the mean VAS was 1.38 at the postoperative period in the MA group. The mean CM score was 78.40, the mean DASH score was 9.75, and VAS was 1.59 at the postoperative period in the ASA group. Seven cases experienced anchor pullout in the MA group, and thread breakage occurred in one patient of each group (p = 0.014). The mean age of the patients with anchor pullout was significantly higher (p = 0.002). This finding was not hypothesized in the initial study design but emerged during post-hoc analysis and highlights the importance of considering bone quality in elderly patients. Conclusions: The clinical outcomes of rotator cuff repairs using all-suture anchors or metal anchors are comparable. However, ASA use may offer an advantage in elderly patients by reducing the risk of anchor pullout. Further studies assessing tendon integrity and bone quality and incorporating long-term follow-up periods are recommended to support and validate the present findings. Full article
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25 pages, 4314 KiB  
Article
Textronic Sensors of Hazardous Gaseous Substances
by Ewa Skrzetuska, Paulina Rzeźniczak, Zuzanna Błaszkowska, Hubert Ciszek, Olga Kowalczyk and Michał Olecki
Materials 2025, 18(2), 341; https://doi.org/10.3390/ma18020341 - 14 Jan 2025
Cited by 1 | Viewed by 972
Abstract
Toxic materials are a threat in workplaces and the environment, as well as households. In them, gaseous substances are included, especially ones without any colour or fragrance, due to their non-detectability with the human senses. In this article, an attempt was made to [...] Read more.
Toxic materials are a threat in workplaces and the environment, as well as households. In them, gaseous substances are included, especially ones without any colour or fragrance, due to their non-detectability with the human senses. In this article, an attempt was made to find a solution for its detection in various conditions with the use of intelligent textiles. The approach was to perform modification on fifteen materials by screen printing using carbon nanotubes paste with expanded graphite and embroidery with stainless steel thread and then investigate their reaction with risky gases such as acetone, methanol and toluene. Four combinations of samples were tested: before tests, after the washing test and after the alkaline and acidic sweat contact test. Three materials can be highlighted. Para-aramid knitwear which reacted well to all tested gases. The biggest value of sensory percentage response was 144%. Screen-printed linen knitwear showed properly detecting skills after washing test for toluene. The biggest value of sensory percentage response was noted at 186%. The third most promising material was low surface mass cotton knitwear with embroidery which had a visible response at every stage of testing for acetone. The biggest value of sensory percentage response was 94% and the smallest one was 27%. For these three materials, repeated contact with harmful gases was tested. Simulations showed also repeated responses expressed in changes in surface resistance under changed conditions. After analysis, there is a possibility to create textile sensors for the detection of hazardous substances. Full article
(This article belongs to the Special Issue Smart Textile Materials: Design, Characterization and Application)
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14 pages, 4579 KiB  
Article
Development and Evaluation of Thread Transistor Based on Carbon-Nanotube Composite Thread with Ionic Gel and Its Application to Logic Gates
by Hiroki Kodaira and Takahide Oya
J. Compos. Sci. 2024, 8(11), 463; https://doi.org/10.3390/jcs8110463 - 8 Nov 2024
Viewed by 1233
Abstract
We propose a new type of flexible transistor based on carbon-nanotube (CNT) composite thread (CNTCT), i.e., a thread transistor, with ionic gel. In our previous study, we demonstrated that transistor operation was possible by combining metallic and semiconducting CNTCTs as gate and channel [...] Read more.
We propose a new type of flexible transistor based on carbon-nanotube (CNT) composite thread (CNTCT), i.e., a thread transistor, with ionic gel. In our previous study, we demonstrated that transistor operation was possible by combining metallic and semiconducting CNTCTs as gate and channel with an insulating material. However, its performance was not sufficient. Therefore, we here aim to improve it. For this, we tried to apply ionic gel as a dielectric layer to it. With this, the transistor was expected to be an electric-double-layer transistor. The transistor performance was improved, and the on/off ratio of the transistor increased by more than 4. This is a large value compared to our previous work. In addition, we not only evaluated the performance of the transistors, but also investigated whether they could be used as logic circuits. It was confirmed that the logic circuit composed of the thread transistor also operated correctly and stably for a long period of time. It was also confirmed that the output changed in response to weak external forces. These results indicate that it is a flexible transistor that can be used in a wide range of applications such as logic circuits and sensors. Full article
(This article belongs to the Special Issue Recent Progress in Hybrid Composites)
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19 pages, 4784 KiB  
Article
Manufacture and Analysis of a Textile Sensor Response to Chemical Stimulus Using Printing Techniques and Embroidery for Health Protection
by Ewa Skrzetuska, Paulina Szablewska and Aleksander Patalas
Sustainability 2024, 16(22), 9702; https://doi.org/10.3390/su16229702 - 7 Nov 2024
Cited by 2 | Viewed by 1356
Abstract
The development of the field of textronics covers many directions, but the neediest are safety, medicine, and environmental protection. The solutions developed can combine the needs of many people from different social groups and ages. This leads to sustainable socio-economic, scientific and integrated [...] Read more.
The development of the field of textronics covers many directions, but the neediest are safety, medicine, and environmental protection. The solutions developed can combine the needs of many people from different social groups and ages. This leads to sustainable socio-economic, scientific and integrated approaches to sustainable development. The authors, seeing the growing need to monitor air pollution in order to increase safety, decided to develop textronic chemical sensors based on carbon-based inks and metal thread embroidery, sensitive to harmful gases and vapors based on textiles. This was to limit the production of subsequent sensors made in plastic housings containing difficult-to-recycle materials and replace them with sensors incorporated into everyday materials such as clothing, which will inform us about emerging threats not only in the place where a large plastic sensor is placed, but in every place at home, at work and outside where we will be. The authors assume that the sensors can be incorporated into clothing, e.g. work clothes, and can also be fastened from one piece of clothing to another. This increases their economic aspect and usability on a larger scale. Three materials of different composition were tested: cotton, polyester and viscose. These materials were selected based on their properties, namely the easier determination of their ability to achieve full circularity of the final product.Functional and mechanical tests of resistance to factors occurring during everyday use were carried out for the use of systems in clothing materials and to produce roller blinds and curtains. To examine the durability of the systems, electrical conductivity was checked before and after the tests. The results showed changes in resistance values after individual tests and during contact with harmful gases. Particularly noticeable are the differences between samples with embroidery and samples with inkjet paste applied. It was shown that the selected materials are suitable for the intended application, and selected modifications together with conductive materials show proper functioning in detecting harmful gases. This project demonstrates the possibility of creating chemical sensors based on printing techniques using carbon printing pastes and embroidery with a metal thread with silver on a textile substrate. Possible applications considering health and environmental aspects are presented. Full article
(This article belongs to the Section Sustainable Materials)
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20 pages, 7498 KiB  
Article
Study on Joint Model Simplification for Finite Element Analysis of Bamboo/Wood-Oriented Strand Board Furniture
by Kaiting Zhang, Jun Zhang, Yong Guo and Yuxia Chen
Materials 2024, 17(17), 4395; https://doi.org/10.3390/ma17174395 - 6 Sep 2024
Cited by 2 | Viewed by 1107
Abstract
Board furniture’s performance and scientific design are making it popular. Research on simplifying furniture joints reduces design cycles and costs and improves structural safety. In this article, using a cantilever beam to calculate deflection theoretically simplifies the L-shaped component model and yields a [...] Read more.
Board furniture’s performance and scientific design are making it popular. Research on simplifying furniture joints reduces design cycles and costs and improves structural safety. In this article, using a cantilever beam to calculate deflection theoretically simplifies the L-shaped component model and yields a joint elastic modulus formula. Finite element analysis (FEA) confirms the effectiveness of this simplified model by comparing its results with experimental data. In simplified components, the joint elastic modulus increases with length (l2) and stabilizes at l2/b ≥ 6 (b is the board’s thickness). The variation pattern of the joint elastic modulus equals that of the stiffness, proving its usefulness in assessing component deformation resistance. Furthermore, the component strength and stiffness are also affected by the screw spacing and connector type. In particular, the connectors type affects bamboo-oriented strand board (BOSB) component performance more than wood-oriented strand board (WOSB). Compared to WOSB, BOSB components have superior strength and stiffness and are more stable. The recommended screw spacing for L-shaped components is 48 mm. BOSB components fixed with two-in-one and metal nuts utilizing threads embedded in the board have better strength and stiffness, while for WOSB components, nylon nuts, and wooden dowel pins are more appropriate for securing. Full article
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18 pages, 6689 KiB  
Article
Experimental Analysis of Stress Shielding Effects in Screw Spacers Placed in Porcine Spinal Tissue
by Elliot Alonso Alcántara-Arreola, Karla Nayeli Silva-Garcés, Jocabed Mendoza-Martínez, Miguel Antonio Cardoso-Palomares and Christopher René Torres-SanMiguel
J. Funct. Biomater. 2024, 15(8), 238; https://doi.org/10.3390/jfb15080238 - 22 Aug 2024
Cited by 4 | Viewed by 1473
Abstract
Bone cortical tissues reorganize and remodel in response to tensile forces acting on them, while compressive forces cause atrophy. However, implants support most of the payload. Bones do not regenerate, and stress shielding occurs. The aim is to analyze the biomechanical behavior of [...] Read more.
Bone cortical tissues reorganize and remodel in response to tensile forces acting on them, while compressive forces cause atrophy. However, implants support most of the payload. Bones do not regenerate, and stress shielding occurs. The aim is to analyze the biomechanical behavior of a lumbar cage to study the implant’s stress shielding. The ASTM E-9 standard was used with the necessary adjustments to perform compression tests on lumbar and thoracic porcine spinal vertebrae. Twelve cases were analyzed: six with the metal prosthesis and six with the PEEK implant. A mathematical model based on the Hertz contact theory is proposed to assess the stress shielding for endoprosthesis used in spine pathologies. The lumbar spacer (screw) helps to reduce the stress shielding effect due to the ACME thread. The best interspinous spacer is the PEEK screw. It does not embed in bone. The deformation capability increases by 11.5% and supports 78.6 kg more than a system without any interspinous spacer. Full article
(This article belongs to the Special Issue Biomaterials and Biomechanics Studies in Tissue Engineering)
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8 pages, 4119 KiB  
Review
Zirconia Implants: A Brief Review and Surface Analysis of a Lost Implant
by Eduardo Borie, Eduardo Rosas, Raphael Freitas de Souza and Fernando José Dias
Coatings 2024, 14(8), 995; https://doi.org/10.3390/coatings14080995 - 6 Aug 2024
Cited by 1 | Viewed by 3046
Abstract
Zirconia implants have emerged as a valuable alternative for clinical scenarios where aesthetic demands are high, as well as in cases of hypersensitivity to titanium or for patients who refuse metallic objects in their bodies due to personal reasons. However, these implants have [...] Read more.
Zirconia implants have emerged as a valuable alternative for clinical scenarios where aesthetic demands are high, as well as in cases of hypersensitivity to titanium or for patients who refuse metallic objects in their bodies due to personal reasons. However, these implants have undergone various changes in geometry, manufacturing techniques, and surface modifications since the introduction of the first zirconia implants. The present study aims to review the current evidence on zirconia implants, considering the changes they have undergone in recent years. Additionally, it aims to analyze the three-dimensional surface characteristics of a failed zirconia implant using scanning electron microscopy and elemental analysis with energy-dispersive X-ray spectrometry (EDX). A zirconia implant lost three weeks after placement was immediately assessed using VP-SEM equipment and chemically analyzed by EDX using a 410-M detector connected to the microscope. Sparse material depositions were found on all parts of the implant, with a notable concentration in the thread grooves. The elements identified in the sample included zirconium, oxygen, carbon, calcium, and phosphorus. This report demonstrates that the surface of zirconia implants can accumulate elements early in the process of bone matrix neoformation, which is consistent with the initial stage of osseointegration. Full article
(This article belongs to the Special Issue Surface Properties of Implants and Biomedical Devices)
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27 pages, 23574 KiB  
Article
Experimental and Numerical Analysis of the Damage Mechanism of an Aramid Fabric Panel Engaged in a Medium-Velocity Impact
by Larisa Chiper Titire and Cristian Muntenita
Polymers 2024, 16(13), 1920; https://doi.org/10.3390/polym16131920 - 5 Jul 2024
Viewed by 1713
Abstract
The aim of this study is to analyze the ballistic impact behavior of a panel made of Twaron CT736 fabric with a 9 mm Full Metal Jacket (FMJ) projectile. Three shots are fired at different velocities at this panel. The ballistic impact test [...] Read more.
The aim of this study is to analyze the ballistic impact behavior of a panel made of Twaron CT736 fabric with a 9 mm Full Metal Jacket (FMJ) projectile. Three shots are fired at different velocities at this panel. The ballistic impact test procedure was carried out in accordance with NIJ 010106. The NIJ-010106 standard is a document that specifies the minimum performance requirements that protection systems must meet to ensure performance. The 9 mm FMJ projectile is, according to NIJ 010106, in threat level II, but the impact velocity is in threat level IIIA. Analysis of macro-photographs of the impact of the Twaron CT736 laminated fabric panel with a 9 mm FMJ projectile involves a detailed examination of the images to gather information about the material performance and failure mechanisms at the macro- or even meso-level (fabric/layer, thread). In this paper, we analyze numerically and experimentally a panel consisting of 32 layers, made of a single material, on impact with a 9 mm FMJ projectile. The experimental results show that following impact of the panel with three projectiles, with velocities between 414 m/s and 428 m/s, partial penetration occurs, with a different number of layers destroyed, i.e., 15 layers in the case of the projectile velocity of 414 m/s, 20 layers of material in the case of the panel velocity of 422 m/s and 22 layers destroyed in the case of the projectile velocity of 428 m/s. Validation of the simulated model is achieved by two important criteria: the number of broken layers and the qualitative appearance. Four numerical models were simulated, of which three models validated the impact results of the three projectiles that impacted the panel. Partial penetration occurs in all four models, breaking the panel in the impact area, with only one exception, i.e., the number of layers destroyed, in which case the simulation did not validate the validation criterion. The performance of Twaron CT736 fabric is also given by the indentation depth values by two methods: according to NIJ 0101.06 and by 3D scanning. The NIJ 010106 standard specifies that a panel provides protection when the indentation depth values are less than 0.44 mm. Full article
(This article belongs to the Section Polymer Physics and Theory)
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28 pages, 12834 KiB  
Article
Natural Dyes in Embroideries of Byzantine Tradition, the Collection of Embroidered Aëres and Epitaphioi in the National Museum of Art of Romania
by Irina Petroviciu, Emanuela Cernea, Iolanda Turcu, Silvana Vasilca and Ina Vanden Berghe
Heritage 2024, 7(6), 3248-3275; https://doi.org/10.3390/heritage7060153 - 11 Jun 2024
Viewed by 1692
Abstract
The medieval textiles collection of the National Museum of Art of Romania (MNAR) has been in place since 1865 and nowadays preserves about 1000 medieval and pre-modern weavings and embroideries. These extremely valuable objects, dated between the 14th and the 19th centuries, are [...] Read more.
The medieval textiles collection of the National Museum of Art of Romania (MNAR) has been in place since 1865 and nowadays preserves about 1000 medieval and pre-modern weavings and embroideries. These extremely valuable objects, dated between the 14th and the 19th centuries, are mainly religious embroidered garments and veils with special significance in the Byzantine li-turgy. Ecclesiastical embroideries of Byzantine tradition are characterized by a complex technique: metallic threads with a silk core, metallic wires and coloured silk threads are couched over padding on layers of silk and cellulosic supports so as to create relief through light reflection. The silk sup-ports and the sewing threads are coloured, mainly in red, blue, green and yellow hues, and analytical investigations of the dyes used in embroideries preserved in the MNAR, in the Putna and Sucevița Monasteries, have been released in previous studies by the corresponding author. The present work continues the approach with research into dyes in about 25 aëres and epitaphioi from the MNAR collection. Considering their privileged function in the liturgical ritual, these luxurious pieces embroidered with silver, gilded silver or coloured silk threads and decorated with pearls, sequins or semi-precious stones are the most faithful description of the stylistic and technological evolution of the art of post-Byzantine embroidery in the Romanian provinces. The data resulting from the present research will improve the knowledge regarding this topic. Dye analysis was performed by liquid chromatography with diode array detection, while fibres were characterized by infrared spectroscopy (with attenuated total reflectance) and optical microscopy. The biological sources identified—carminic acid-based dyes, redwood, dyer’s broom, weld, indigo-based dyes––will be discussed in correspondence with their use in the embroidery technique: support, lining and embroidery threads, together with other sources previously reported on Byzantine embroideries in Romanian collections, and in similar objects preserved at Holy Mount Athos. Full article
(This article belongs to the Special Issue Dyes in History and Archaeology 42)
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17 pages, 8658 KiB  
Article
Characterization of Micro-Threaded Stem Taper Surfaces of Cementless Hip Endoprostheses
by Drago Dolinar, Boštjan Kocjančič, Klemen Avsec, Barbara Šetina Batič, Aleksandra Kocijan, Matjaž Godec, Marko Sedlaček, Mojca Debeljak, John T. Grant, Timon Zupanc and Monika Jenko
Materials 2024, 17(11), 2751; https://doi.org/10.3390/ma17112751 - 5 Jun 2024
Cited by 1 | Viewed by 1224
Abstract
We investigated micro-threaded stem taper surface and its impact on premature failures, aseptic loosening, and infection in cementless hip endoprostheses. Our study focused on the fretting, and crevice corrosion of micro-threaded tapers, as well as the characterization of the microstructure and surface properties [...] Read more.
We investigated micro-threaded stem taper surface and its impact on premature failures, aseptic loosening, and infection in cementless hip endoprostheses. Our study focused on the fretting, and crevice corrosion of micro-threaded tapers, as well as the characterization of the microstructure and surface properties of two new and three retrieved Zweymüller stem tapers. The retrieved samples were selected and examined based on the head–stem taper interface being the sole source of modularity with a metallic component, specifically between the Ti alloy taper stem and the ceramic head. To determine the surface chemistry and microstructures of both new and retrieved hip endoprostheses stem taper titanium alloy, scanning -electron microscopy (SEM) was employed for morphological and microstructural analyses. Energy dispersive spectroscopy (EDS) was utilized for characterizing chemical element distribution, and electron backscattered diffraction (EBSD) was used for phase analysis. The roughness of the micro-threated stem tapers from different manufacturers was investigated using an optical profilometer, with standard roughness parameters Ra (average surface roughness) and Rz (mean peak to valley height of the roughness profile) being measured. Electrochemical studies revealed no fretting corrosion in retrieved stem tapers with ceramic heads. Consequently, three retrieved tapers and two new ones for comparison underwent potentiodynamic measurements in Hank’s solution to determine the corrosion rate of new and retrieved stem taper surfaces. The results showed a low corrosion rate for both new and prematurely failed retrieved samples due to aseptic loosening. However, the corrosion rate was higher in infected and low-grade infected tapers. In conclusion, our study suggests that using ceramic heads reduces taper corrosion and subsequently decreases the incidence of premature failures in total hip arthroplasty. Full article
(This article belongs to the Special Issue Materials for Hard Tissue Repair and Regeneration (Third Edition))
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15 pages, 41098 KiB  
Article
Preparation, Characterization, and High-Temperature Anti-Seizing Application of CrAlN-Based Gradient Multilayer Coatings
by Chunmei Tang, Dingjun Li, Xiaohu Yuan, Wei Wang, Xianping Guo, Yu Fang, Xiufang Gong and Quande Li
Crystals 2024, 14(6), 509; https://doi.org/10.3390/cryst14060509 - 27 May 2024
Cited by 1 | Viewed by 1075
Abstract
High-temperature fasteners are metal parts of gas turbines and steam turbines, which work at high temperatures and under stress for a long time. However, the frequent seizures of fasteners bring great trouble to the normal maintenance of power plants. In this paper, three [...] Read more.
High-temperature fasteners are metal parts of gas turbines and steam turbines, which work at high temperatures and under stress for a long time. However, the frequent seizures of fasteners bring great trouble to the normal maintenance of power plants. In this paper, three kinds of dense and controllable CrAlN-based gradient multilayer coatings were prepared on the samples and screws by arc ion plating (AIP) technology. The morphology, composition, structure, nano hardness, adhesion, residual stress, and room temperature tribological performance of the coating were investigated. To evaluate the high-temperature, anti-seizing performance, coated screws were heated to 700 °C for 140 h with a torque of 20 N·m. The results indicate that the CrN/CrAlN multilayer coating shows better comprehensive properties. The characterization of coated screws proved that the coating structures obtained on the screws were similar to the flat samples. However, the as-prepared coating on the screws showed different thickness variation rules, which was related to the clamping method, deposition distance, and screw shape. After a simulation service, the thread of the screw remained intact with similar structure and thinner thickness. The above results indicate that the high-temperature seize prevention of fasteners can be successfully achieved by preparing a CrAlN-based multilayer coating, which is suitable for fasteners with service temperatures below 700 °C. Full article
(This article belongs to the Special Issue Advanced Surface Modifications on Materials)
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17 pages, 8175 KiB  
Article
Research and Optimization of Extrusion Tap Structure Based on Numerical Simulation and Experimental Analysis
by Yi Tao, Nian Wan, Daoming Xu and Qiang He
Materials 2024, 17(8), 1891; https://doi.org/10.3390/ma17081891 - 19 Apr 2024
Cited by 2 | Viewed by 1447
Abstract
In order to enhance the quality of thread processing by tap, a systematic analysis of its forming mechanism and factors affecting forming quality is conducted. Effects of the number of edges, the amount of shovel back, the extrusion cone, the calibration part and [...] Read more.
In order to enhance the quality of thread processing by tap, a systematic analysis of its forming mechanism and factors affecting forming quality is conducted. Effects of the number of edges, the amount of shovel back, the extrusion cone, the calibration part and the extrusion cone angle on the torque and temperature are achieved by finite element analysis and experiments. From the perspective of reducing torque and temperature during the forming process, the optimal combination of tap structural parameters for machining M22×2 internal threads on 42CrMo4 high-strength steel are further obtained through orthogonal optimization. The results show that, unlike the cutting process of threads, the extrusion forming process of threads is a net forming process in which metal undergoes plastic deformation in a limited space, and the metal material continuously flows along the edge of the V-shaped groove of the tap, gradually piling up to form the thread tooth shape. This also caused a noticeable lack of flesh at the top of the extruded thread teeth. Better quality threads can be obtained by machining with optimized structural parameters. The maximum torque and temperature during the machining process are reduced by 22.86% and 20.31%, respectively. The depth of the hardened layer increased by 0.05 mm, and the root and top hardness of the teeth increased by 10 HV0.2 and 5 HV0.2, respectively. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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16 pages, 8150 KiB  
Article
Modeling Surface Roughness and Flow of Gases in Threaded Connections to Analyze Sealing Performance
by Wenqi Zhu, Yu Liang and Lv Zhao
Processes 2024, 12(3), 574; https://doi.org/10.3390/pr12030574 - 14 Mar 2024
Cited by 1 | Viewed by 1483
Abstract
Oil casings and premium threaded connections play vital roles in the oil and gas extraction industry. The present work establishes an integrated modeling framework for the sealability assessment of premium threaded connections which can be easily implemented and employed by engineers. The framework [...] Read more.
Oil casings and premium threaded connections play vital roles in the oil and gas extraction industry. The present work establishes an integrated modeling framework for the sealability assessment of premium threaded connections which can be easily implemented and employed by engineers. The framework incorporates a part-scale finite element analysis of the make-up process, a micro-scale simulation of the contact behavior, and a mechanism-informed gap flow model. It is found that complete sealing can be achieved when the contact pressure exceeds 1540 MPa for Gaussian rough surfaces presenting a roughness of 1.6 μm. The seal surface fit is revealed to be critical for sealing performance, as it slightly changes the optimum make-up torque (up to 4%) but significantly changes contact pressure (up to 22%). At an optimum make-up torque, the connection with the loosest seal surface tolerance fit is prone to gas leakage when considering an inlet pressure of 110 MPa. The proposed modeling framework can be extended to other types of threaded connections with metal–metal contact sealing. Full article
(This article belongs to the Special Issue Oil and Gas Drilling Processes: Control and Optimization)
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23 pages, 9600 KiB  
Article
Multi-Analytical Techniques for the Study of Burial Clothes of Polish King Sigismund III Vasa (1566–1633) and His Wife Constance Habsburg (1588–1631)
by Magdalena Śliwka-Kaszyńska, Maria Cybulska, Anna Drążkowska, Sławomir Kuberski, Jakub Karczewski, Anna Marzec and Przemysław Rybiński
Molecules 2024, 29(1), 192; https://doi.org/10.3390/molecules29010192 - 28 Dec 2023
Cited by 1 | Viewed by 1496
Abstract
The subjects of this research are the burial clothes of Polish King Sigismund III Vasa and his wife Constance, which were woven and embroidered with silk and metal threads. Fragments of the textiles underwent spectroscopic, spectrometric, and thermogravimetric analyses. The hydrofluoric acid extraction [...] Read more.
The subjects of this research are the burial clothes of Polish King Sigismund III Vasa and his wife Constance, which were woven and embroidered with silk and metal threads. Fragments of the textiles underwent spectroscopic, spectrometric, and thermogravimetric analyses. The hydrofluoric acid extraction method was improved to isolate various classes of dyes from the textile samples that had direct contact with human remains. High-performance liquid chromatography, coupled with diode array and tandem mass spectrometry detectors with electrospray ionization (HPLC-DAD-ESI-MS/MS) facilitated the detection and identification of colorants present in the textiles. Cochineal, indigo-, madder-, orchil-, and tannin-producing plants were identified as the sources of dyes used. Scanning electron microscopy with an energy-dispersive X-ray detector (SEM-EDS) was employed to identify and characterize the silk fibers and mordants and the metal threads. The presence of iron, aluminum, sodium, and calcium in the silk threads suggests their potential use as mordants. The analysis of the metal threads revealed that most of them were made from flattened gilded silver wire, with only a few being cut from a sheet of metal. Typical degradation mechanisms of metal threads were shown, resulting from both burial environment and earlier manufacturing process, and the use of the textiles in clothing, i.e., a significant loss of the gold layer was observed in most of silver gilt threads, caused by abrasion and delamination. The results of the thermal analysis confirmed the presence of silk and silver threads in the examined textiles. Full article
(This article belongs to the Section Analytical Chemistry)
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