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Keywords = leucite-reinforced ceramic

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15 pages, 2256 KiB  
Article
In Vivo Wear Analysis of Leucite-Reinforced Ceramic Inlays/Onlays After 14 Years
by Ragai-Edward Matta, Lara Berger, Oleksandr Sednyev, Dennis Bäuerle, Eva Maier, Werner Adler and Michael Taschner
Materials 2025, 18(15), 3446; https://doi.org/10.3390/ma18153446 - 23 Jul 2025
Viewed by 288
Abstract
Material wear significantly impacts the clinical success and longevity of dental ceramic restorations. This in vivo study aimed to assess the wear behavior of IPS Empress® glass-ceramic inlays and onlays over 14 years, considering the influence of different antagonist materials. Fifty-four indirect [...] Read more.
Material wear significantly impacts the clinical success and longevity of dental ceramic restorations. This in vivo study aimed to assess the wear behavior of IPS Empress® glass-ceramic inlays and onlays over 14 years, considering the influence of different antagonist materials. Fifty-four indirect restorations of 21 patients were available for comprehensive wear analysis, with complete follow-up data for up to 14 years. Three-dimensional measurements relied on digitized epoxy resin models produced immediately post-insertion (baseline) and subsequently at 2, 4, and 14 years. The occlusal region on the baseline model was delineated for comparative analysis. Three-dimensional superimpositions with models from subsequent time points were executed to assess wear in terms of average linear wear and volumetric loss. Statistical analyses were conducted in R (version 4.4.1), employing Mann–Whitney U tests (material comparisons) and Wilcoxon signed rank tests (time point comparisons), with a significance threshold of p ≤ 0.05. During the entire study period, an increase in wear was observed at each assessment interval, gradually stabilizing over time. Significant differences in substance loss were found between the follow-up time points, both for mean (−0.536 ± 0.249 mm after 14a) and integrated distance (−18,935 ± 11,711 mm3 after 14a). In addition, significantly higher wear was observed after 14 years with gold as antagonist compared to other materials (p ≤ 0.03). The wear behavior of IPS Empress® ceramics demonstrates clinically acceptable long-term outcomes, with abrasion characteristics exhibiting stabilization over time. Full article
(This article belongs to the Special Issue Advanced Dental Materials: From Design to Application, Second Volume)
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38 pages, 3106 KiB  
Review
Exploring the Properties and Indications of Chairside CAD/CAM Materials in Restorative Dentistry
by Codruţa-Eliza Ille, Anca Jivănescu, Daniel Pop, Eniko Tunde Stoica, Razvan Flueras, Ioana-Cristina Talpoş-Niculescu, Raluca Mioara Cosoroabă, Ramona-Amina Popovici and Iustin Olariu
J. Funct. Biomater. 2025, 16(2), 46; https://doi.org/10.3390/jfb16020046 - 1 Feb 2025
Cited by 4 | Viewed by 3178
Abstract
The present review provides an up-to-date overview of chairside CAD/CAM materials used in restorative dentistry, focusing on their classification, properties, and clinical applications. If CAD/CAM technology was only an aspiration in the past, a higher proportion of clinics are employing it nowadays. The [...] Read more.
The present review provides an up-to-date overview of chairside CAD/CAM materials used in restorative dentistry, focusing on their classification, properties, and clinical applications. If CAD/CAM technology was only an aspiration in the past, a higher proportion of clinics are employing it nowadays. The market is overflowing with biomaterials, and these materials are constantly evolving, making it challenging for practitioners to choose the most appropriate one, especially in correlation with patients’ medical diseases. The evolution of CAD/CAM technology has revolutionized dental practice, enabling the efficient fabrication of high-quality restorations in a single appointment. The main categories of chairside CAD/CAM materials include feldspathic ceramics, leucite-reinforced ceramics, lithium disilicate, zirconia, hybrid ceramics, and acrylic resins. The mechanical, physical, and aesthetic properties of these materials are discussed, along with their advantages and limitations for different clinical scenarios. Factors influencing material selection, such as strength, aesthetics, and ease of use, are also assessed. Ultimately, the guiding principle of dentistry is minimally invasive treatment following the particularity of the clinical case to obtain the envisioned result. Correlating all these factors, a simple, up-to-date classification is required to begin an individualized treatment. By synthesizing current evidence, this comprehensive review aims to guide clinicians in selecting appropriate chairside CAD/CAM materials to achieve optimal functional and aesthetic outcomes in restorative procedures. The integration of digital workflows and continued development of novel materials promise to further enhance the capabilities of chairside CAD/CAM systems in modern dental practice. Full article
(This article belongs to the Special Issue State-of-the-Art Dental Adhesives and Restorative Composites)
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16 pages, 3950 KiB  
Article
Are Dental Prophylaxis Protocols Safe for CAD-CAM Restorative Materials? Surface Characteristics and Fatigue Strength
by Lucas Saldanha da Rosa, Luiza Freitas Brum Souza, Rafaela Oliveira Pilecco, Thaís Andressa Cavalcante Kluch, Felipe Somavilla Binotto, Vitória Zanetti Henriques, Cornelis Johannes Kleverlaan, Gabriel Kalil Rocha Pereira and João Paulo Mendes Tribst
Coatings 2024, 14(12), 1510; https://doi.org/10.3390/coatings14121510 - 30 Nov 2024
Cited by 1 | Viewed by 1077
Abstract
The surface of dental materials is exposed to various prophylaxis protocols during routine dental care. However, the impact of these protocols on the functional properties of the material’s surface remains unclear. This study investigates the influence of different dental prophylaxis protocols on the [...] Read more.
The surface of dental materials is exposed to various prophylaxis protocols during routine dental care. However, the impact of these protocols on the functional properties of the material’s surface remains unclear. This study investigates the influence of different dental prophylaxis protocols on the surface properties and their effect on the mechanical performance of CAD-CAM restorative materials. Discs (Ø = 15 mm, thickness = 1.2 mm) were fabricated from resin composite (RC, Tetric CAD), leucite-reinforced (LEU, IPS Empress CAD), lithium disilicate (LD, IPS e.max CAD), and zirconia ceramics (ZIR, IPS e.max ZirCAD MT). The materials were subjected to six prophylactic treatments: untreated (CTRL), prophylactic paste fine (PPF), prophylactic paste coarse (PPC), pumice stone (PS), air abrasion with sodium bicarbonate jet (BJ), and ultrasonic scaling (US). Biaxial flexural fatigue tests, along with fractographic, roughness, and topographic analyses, were conducted. No significant changes in fatigue strength were observed for RC, LD, and ZIR under any prophylaxis protocols. However, LEU subjected to BJ treatment exhibited significantly reduced fatigue strength (p = 0.004), with a 22% strength reduction compared to the monotonic test and substantial surface alterations. Surface roughness analyses revealed increased roughness for RC treated with PPF, PPC, and PS compared to CTRL (p < 0.05), while LD exhibited decreased roughness following PPF, PS, and US treatments (p < 0.05). In ZIR, only the BJ protocol increased roughness (p = 0.001). In conclusion, dental prophylaxis protocols do not significantly affect the mechanical strength of RC, LD, and ZIR materials, thus allowing any protocol to be used for these materials. However, for LEU ceramics, the BJ protocol should be avoided due to its effect of reducing fatigue strength and damaging the surface. Full article
(This article belongs to the Special Issue Surface Properties of Dental Materials and Instruments, 3rd Edition)
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17 pages, 900 KiB  
Review
Survival Rates of Glass versus Hybrid Ceramics in Partial Prosthetic Restorations: A Scoping Review with Emphasis on Adhesive Protocols
by Manuela Manziuc, Alex Abbas Khechen, Marius Negucioiu, Irina Poiană, Andreea Kui, Anca Mesaroș and Smaranda Buduru
J. Clin. Med. 2023, 12(21), 6744; https://doi.org/10.3390/jcm12216744 - 25 Oct 2023
Cited by 4 | Viewed by 3443
Abstract
As dental practices and methodologies evolve, the emergence of novel materials adds complexity to clinical choices. While glass ceramics, particularly those based on lithium disilicate and leucite-reinforced variants, have been extensively researched and are well regarded for their attributes, hybrid ceramics remain relatively [...] Read more.
As dental practices and methodologies evolve, the emergence of novel materials adds complexity to clinical choices. While glass ceramics, particularly those based on lithium disilicate and leucite-reinforced variants, have been extensively researched and are well regarded for their attributes, hybrid ceramics remain relatively recent area of research that is less investigated. This review aims to evaluate the durability of glass and hybrid ceramics while assessing the role of various adhesive techniques on restoration longevity. Using a comprehensive search of PubMed and EMBASE, 84 articles from the past decade were found. Only eleven met the set criteria for analysis. The results underscore the urgent need for the extended monitoring of partial prosthetic restorations. The existing literature has significant gaps, hindering the attainment of dependable insights about these materials’ long-term performance. For a clearer understanding of how different ceramic systems affect restoration survival rates, rigorous research involving more participants and uniform outcome documentation is vital. Full article
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13 pages, 7217 KiB  
Article
The Influence of Hydrofluoric Acid Temperature and Application Technique on Ceramic Surface Texture and Shear Bond Strength of an Adhesive Cement
by Cristiana Cuzic, Anca Jivanescu, Radu Marcel Negru, Iosif Hulka and Mihai Rominu
Materials 2023, 16(12), 4303; https://doi.org/10.3390/ma16124303 - 10 Jun 2023
Cited by 7 | Viewed by 1734
Abstract
All-ceramic restorations are the foundation of modern esthetic dentistry. Clinical approaches for preparation, durability, aesthetics, and repair have been reformed by the idea of adhesive dentistry. The aim of the study and the objective question was to evaluate the impact of heated hydrofluoric [...] Read more.
All-ceramic restorations are the foundation of modern esthetic dentistry. Clinical approaches for preparation, durability, aesthetics, and repair have been reformed by the idea of adhesive dentistry. The aim of the study and the objective question was to evaluate the impact of heated hydrofluoric acid pretreatment and the application technique’s influence on the surface morphology and roughness of leucite-reinforced glass–ceramic materials (IPS Empress CAD, Ivoclar Vivadent), which is fundamental for understanding the adhesive cementation process. Scanning electron microscopy was used to observe the effectiveness of the two HF (Yellow Porcelain Etch, Cerkamed) application techniques and the HF’s temperature impact on the surface topography of the ceramic. Based on surface conditioning methods, the adhesive cement (Panavia V5, Kuraray Noritake Dental Inc., Tokyo, Japan) was applied to the conditioned ceramic samples and light-cured. Shear bond strength values were correlated with the micro-retentive surface texture of the ceramic. With universal testing equipment at a 0.5 mm/min crosshead speed, SBS values between the resin cement and the ceramic material were assessed until failure. Analyzing the fractured surfaces of the specimens by digital microscopy, the failure modes were divided into three categories: adhesive, cohesive, and mixed failure. Analysis of variance (ANOVA) was used to statistically analyze the collected data. The results show that alternative treatment methods affected the material’s surface characteristics and have an influence on the shear bond strength. Full article
(This article belongs to the Special Issue From Conventional towards Modern Biomaterials in Dentistry)
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11 pages, 1739 KiB  
Article
Ceramic versus Composite Resin Polishing Systems on the Surface Roughness of Milled Leucite-Reinforced Ceramics
by Carlos A. Jurado, Saad Alresayes, Silvia Rojas-Rueda, Ali Alqahtani, Akimasa Tsujimoto, Nicholas G. Fischer and Kelvin I. Afrashtehfar
Medicina 2023, 59(6), 1048; https://doi.org/10.3390/medicina59061048 - 29 May 2023
Cited by 3 | Viewed by 2402
Abstract
Background and Objective: This study aimed to compare the surface finish of milled leucite-reinforced ceramics polished with ceramic and composite polishing systems based on the manufacturers’ recommendations. Materials and Methods: Sixty subtractive computer-aided manufactured (s-CAM) leucite-reinforced glass-ceramic specimens (IPS-Empress-CAD) were assigned into six [...] Read more.
Background and Objective: This study aimed to compare the surface finish of milled leucite-reinforced ceramics polished with ceramic and composite polishing systems based on the manufacturers’ recommendations. Materials and Methods: Sixty subtractive computer-aided manufactured (s-CAM) leucite-reinforced glass-ceramic specimens (IPS-Empress-CAD) were assigned into six groups: no polishing, a ceramic polishing kit, and four composite kit groups. The roughness average (Ra) was evaluated in microns using a profilometer, and scanning electron micrographs were obtained for qualitative analysis. A Tukey HSD posthoc test (α = 0.05) was used to determine significant intergroup differences. Results: After surface evaluation of the ceramics, the Ra values of the polishing systems ranked OptraFine (0.41 ± 0.26) < Enhance (1.60 ± 0.54) < Shofu (2.14 ± 0.44) < Astropol (4.05 ± 0.72) < DiaComp (5.66 ± 0.62) < No Polishing (5.66 ± 0.74). Discussion: Composite polishing systems did not provide as smooth surfaces as the ceramic polishing kit for CAD-CAM leucite-reinforced ceramics. Thus, using ceramic polishing systems, polishing leucite ceramics is recommended, whereas composite polishing systems should not be considered as an alternative for use in minimally invasive dentistry. Full article
(This article belongs to the Special Issue Outcome of Minimally Invasive Techniques in Dentistry)
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12 pages, 6930 KiB  
Article
Effect of Different Scaling Methods on the Surface Topography of Different CAD/CAM Ceramic Compositions
by Passent Ellakany, Nourhan M. Aly, Maram M. Alghamdi, Shahad T. Alameer, Turki Alshehri, Sultan Akhtar and Marwa Madi
Materials 2023, 16(8), 2974; https://doi.org/10.3390/ma16082974 - 8 Apr 2023
Cited by 4 | Viewed by 2162
Abstract
This study evaluated the effect of ultrasonic and manual scaling using different scaler materials on the surface topography of computer-aided designing and computer-aided manufacturing (CAD/CAM) ceramic compositions. After scaling with manual and ultrasonic scalers, the surface properties of four classes of CAD/CAM ceramic [...] Read more.
This study evaluated the effect of ultrasonic and manual scaling using different scaler materials on the surface topography of computer-aided designing and computer-aided manufacturing (CAD/CAM) ceramic compositions. After scaling with manual and ultrasonic scalers, the surface properties of four classes of CAD/CAM ceramic discs: lithium disilicate (IPE), leucite-reinforced (IPS), advanced lithium disilicate (CT), and zirconia-reinforced lithium silicate (CD) of 1.5 mm thickness were evaluated. Surface roughness was measured before and after treatment, and scanning electron microscopy was used to evaluate the surface topography following the performed scaling procedures. Two-way ANOVA was conducted to assess the association of the ceramic material and scaling method with the surface roughness. There was a significant difference in the surface roughness between the ceramic materials subjected to different scaling methods (p < 0.001). Post-hoc analyses revealed significant differences between all groups except for IPE and IPS where no significant differences were detected between them. CD showed the highest surface roughness values, while CT showed the lowest surface roughness values for the control specimens and after exposure to different scaling methods. Moreover, the specimens subjected to ultrasonic scaling displayed the highest roughness values, while the least surface roughness was noted with the plastic scaling method. Full article
(This article belongs to the Special Issue Novel Resin Composites and Biomaterials)
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11 pages, 3140 KiB  
Article
Wear Behavior of Monolithic Zirconia after Staining, Glazing, and Polishing Opposing Dental Restorative Materials: An In Vitro Study
by Lívia Fiorin, Paulo Eduardo Barros Souza Oliveira, Allan Oliveira da Silva, Adriana Cláudia Lapria Faria, Ana Paula Macedo, Ricardo Faria Ribeiro and Renata Cristina Silveira Rodrigues
Coatings 2023, 13(2), 466; https://doi.org/10.3390/coatings13020466 - 18 Feb 2023
Cited by 5 | Viewed by 2992
Abstract
The purpose of this in vitro study was to compare the effect of staining, glazing, and polishing on the wear behavior of stabilized zirconia with 5 mol% of yttrium oxide (5Y-TZP) opposing 5Y-TZP, leucite-reinforced ceramic (LC), lithium disilicate (LD), and microhybrid composite resin [...] Read more.
The purpose of this in vitro study was to compare the effect of staining, glazing, and polishing on the wear behavior of stabilized zirconia with 5 mol% of yttrium oxide (5Y-TZP) opposing 5Y-TZP, leucite-reinforced ceramic (LC), lithium disilicate (LD), and microhybrid composite resin (MCR). Hemispheres of 5Y-TZP were divided into six groups (n = 10) according to the finishing procedure: C (control), S (staining), G (glazing), P (polishings), SG (staining plus glazing), and SP (staining plus polishing). The two-body wear test (2BW) was performed (20 N load, at 2 Hz, until 300,000 cycles). Vertical height loss of hemispheres (VHL) and wear depth of restorative materials (WD) were analyzed using a profile projector and laser confocal microscope, respectively. Data of VHL and WD were analyzed using a generalized linear model by the Wald test and t post hoc test with the Bonferroni adjustment (α = 0.05). The staining, glazing, polishing, and restorative material had a significant effect (p < 0.05) on VHL and WD. Polishing reduced VHL opposing MCR, LC, and LD. There was an increase in WD to G opposing LD and SG opposing MCR. The 5Y-TZP presented the highest wear resistance, while MCR presented the lowest. Polishing was recommended to promote staining durability and decrease wear rates opposing MCR and LD. Full article
(This article belongs to the Section Bioactive Coatings and Biointerfaces)
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14 pages, 4109 KiB  
Article
Influences of Different CAD/CAM Ceramic Compositions and Thicknesses on the Mechanical Properties of Ceramic Restorations: An In Vitro Study
by Passent Ellakany, Marwa Madi, Nourhan M. Aly, Turki Alshehri, Shahad T. Alameer and Fahad A. Al-Harbi
Materials 2023, 16(2), 646; https://doi.org/10.3390/ma16020646 - 9 Jan 2023
Cited by 11 | Viewed by 2981
Abstract
The aim of this study was to assess the influences of different CAD/CAM ceramic compositions and thicknesses on the surface roughness and hardness of ceramic restorations. Four different ceramics were used in the current study: lithium disilicate (LD), leucite reinforced (LE), advanced lithium [...] Read more.
The aim of this study was to assess the influences of different CAD/CAM ceramic compositions and thicknesses on the surface roughness and hardness of ceramic restorations. Four different ceramics were used in the current study: lithium disilicate (LD), leucite reinforced (LE), advanced lithium disilicate (ALD), and zirconia-reinforced lithium silicate (ZLS). Each group included 30 specimens subdivided into three different ceramic thicknesses (0.5, 1 and 1.5 mm thicknesses). The microhardness was measured for all the specimens using a microhardness testing machine, while the surface roughness was measured using a non-contact optical profilometer at three intervals (before toothbrushing and after toothbrushing, with and without toothpaste). Three-way and two-way ANOVA were used to determine the factors influencing the surface roughness and microhardness. There was a significant difference in the surface roughness between the studied groups for all the thicknesses. The findings showed that ALD had the lowest surface roughness, while ZLS showed the highest surface roughness. Moreover, ALD, followed by ZLS, had the highest hardness, while LD and LE had the lowest hardness values. Regarding the thicknesses, both the 0.5 and 1 mm ceramic thicknesses showed a significantly lower surface roughness than the 1.5 mm thickness, while the 1.5 mm thickness showed a significantly higher microhardness than the 0.5 mm thickness. The surface roughness and hardness were significantly affected by the ceramic composition and type of filler. It is recommended to use 1.5 mm-thick ceramic materials for the fabrication of definitive full-coverage ceramic restorations, while veneers require 0.5 mm-thick materials. ALD is a promising CAD/CAM material that can be used for the fabrication of restorations with a proper strength in both anterior and posterior regions. Full article
(This article belongs to the Special Issue Frontiers Research in Novel Dental Materials)
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12 pages, 2256 KiB  
Article
Factory Crystallized Silicates for Monolithic Metal-Free Restorations: A Flexural Strength and Translucency Comparison Test
by Alessandro Vichi, Zejiao Zhao, Gaetano Paolone, Nicola Scotti, Mahdi Mutahar, Cecilia Goracci and Chris Louca
Materials 2022, 15(21), 7834; https://doi.org/10.3390/ma15217834 - 6 Nov 2022
Cited by 30 | Viewed by 3222
Abstract
Flexural strength (FS) and translucency (Contrast Ratio-CR) of three different factory crystallized silica-based glass ceramics, Celtra Duo (CD), N!ce (NI) and Li-Si Block, a lithium disilicate, IPS e.max CAD (LD), and a leucite-reinforced feldspathic ceramic, Empress CAD (EM), in two different translucencies (HT [...] Read more.
Flexural strength (FS) and translucency (Contrast Ratio-CR) of three different factory crystallized silica-based glass ceramics, Celtra Duo (CD), N!ce (NI) and Li-Si Block, a lithium disilicate, IPS e.max CAD (LD), and a leucite-reinforced feldspathic ceramic, Empress CAD (EM), in two different translucencies (HT and LT) for use in chairside dental restorations have been compared. CAD blocks of the materials were cut into beams and tiles and processed following manufacturers’ instructions. The beams were tested (3-PBT) to determine flexural strength, Weibull characteristic strength, and Weibull modulus; and tiles were tested to determine CR. All data were statistically analyzed. In addition, SEM analysis of the materials was performed. Differences in flexural strength (FS) and translucency (CR) between the materials were found to be statistically significant. FS decreased as follows (MPa): LDHT 350.88 ± 19.77 (a) = LDLT 343.57 ± 18.48 (a) > LSLT 202.15 ± 17.41 (b) = LSHT 196.93 ± 8.87 > NIHT 186.69 ± 13.06 (c) = CDLT 184.73 ± 13.63 (c) = CDHT 174.15 ± 21.76 (c) = NILT 172.12 ± 11.98 (c) > EMHT 131.16 ± 13.33 (e) = EMLT 127.65 ± 11.09. CR decreased as follows (mean ± sd): CDLT 74.1 ± 1.1 (a); LSLT 74.0 ± 1.1 (ab); NILT 73.3 ± 0.8 (ab); EMLT 73.0 ± 1.5 (ab); NIHT 72.4 ± 1.0 (bc); LDLT 71.3 ± 1.1 (bc); LTHT 65.2 ± 0.9 (de); LSHT 63.8 ± 1.1 (def); EMHT 636 ± 1.2 (ef); CDHT 62.2 ± 0.8 (f). Our findings show that factory-crystallized lithium silicate glass ceramics fulfill ISO standards for Classes 1 and 2. Therefore, they can be considered viable alternatives to produce single-unit restorations with a chairside procedure not requiring thermal treatment. Full article
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13 pages, 4660 KiB  
Article
Effect of Different Etching Times with Hydrofluoric Acid on the Bond Strength of CAD/CAM Ceramic Material
by Liane Tabitha Avram, Sergiu-Valentin Galațanu, Carmen Opriș, Cristian Pop and Anca Jivănescu
Materials 2022, 15(20), 7071; https://doi.org/10.3390/ma15207071 - 11 Oct 2022
Cited by 17 | Viewed by 2868
Abstract
The objective of this study was to evaluate the influence of hydrofluoric acid (HF) and conditioning time on the micro-shear bond strength (µSBS) between dual-cure resin cement and glass-ceramic materials, such as lithium disilicate ceramic (IPS e.max CAD, Ivoclar Vivadent) (EX) and leucite-reinforced [...] Read more.
The objective of this study was to evaluate the influence of hydrofluoric acid (HF) and conditioning time on the micro-shear bond strength (µSBS) between dual-cure resin cement and glass-ceramic materials, such as lithium disilicate ceramic (IPS e.max CAD, Ivoclar Vivadent) (EX) and leucite-reinforced ceramic (IPS Empress CAD, Ivoclar Vivadent) (EP), and also a hybrid ceramic (Vita Enamic, Vita Zahnfabrik) (VE). Eighteen sections with 1 mm thickness were cut from each CAD/CAM material and randomly divided into three groups, according to the surface etching time (30 s, 60 s, 90 s). The surface treatment was performed using 9.5% HF acid gel, then resin cement was applied on the prepared ceramic plates and light cured. µSBS values between resin cement and the ceramic material were measured with a universal testing machine at a crosshead speed of 0.5 mm/min until the failure occurred. The fractured surfaces of specimens were microscopically evaluated, and failure modes were classified as: adhesive between resin cement and ceramic, cohesive within ceramic or cement and mixed failure. Surface roughness of etched samples was examined using a scanning electron microscope. Obtained data were statistically analysed using one-way analysis of variance (ANOVA) and Bonferroni post hoc test with a level of significance α = 0.05. The results of the statistical methods applied indicate that µSBS mean difference for leucite-reinforced ceramic (EP) was statistically significant (p < 0.05). However, µSBS values for hybrid ceramic (VE) and lithium disilicate ceramic (EX) were not affected, from a statistical point of view, by the conditioning time (p > 0.05). Full article
(This article belongs to the Section Advanced Materials Characterization)
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11 pages, 11460 KiB  
Article
Surface Morphology Changes of Bleached Dental Ceramics
by Giedrė Morkūnaitė, Rimantas Ožiūnas, Vytautas Čeplauskas, Simona Tučkutė, Jurgita Laurikaitienė and Diana Adlienė
Appl. Sci. 2022, 12(9), 4557; https://doi.org/10.3390/app12094557 - 30 Apr 2022
Cited by 3 | Viewed by 2159
Abstract
Tooth whitening is one of the most conservative procedures for increasing the aesthetics of patients, but the effect of bleaching on ceramic restorations has not been extensively studied. In this study, the bleaching effect on three dental restoration materials (polished/glazed lithium disilicate glass [...] Read more.
Tooth whitening is one of the most conservative procedures for increasing the aesthetics of patients, but the effect of bleaching on ceramic restorations has not been extensively studied. In this study, the bleaching effect on three dental restoration materials (polished/glazed lithium disilicate glass ceramic, leucite reinforced glass ceramic and zirconium dioxide ceramic) has been investigated in terms of surface roughness changes of the exposed samples. Philips Zoom NiteWhite 16% carbamide peroxide, Philips Zoom 6% hydrogen peroxide with following LED illumination and Pola Office 6% hydrogen peroxide have been used for ceramic bleaching. The experimental investigation and performed statistical analysis revealed that the highest surface roughness changes of all investigated ceramics were caused by the hydrogen peroxide and the lowest by carbamide peroxide. These findings correlated well with the colour changes observed in the same bleached dental ceramic samples indicating potential of carbamide peroxide as the most prospective bleaching agent. Full article
(This article belongs to the Special Issue Application of Restorative Dentistry)
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13 pages, 3282 KiB  
Article
Curing through Ceramics: Influence of Different Light-Curing Units and Curing Modes on Bond Strength
by Evonne Mei Jing Phua, John Neil Waddell and Joanne Jung Eun Choi
Oral 2022, 2(1), 62-74; https://doi.org/10.3390/oral2010008 - 17 Feb 2022
Cited by 4 | Viewed by 3837
Abstract
Objectives: To measure and compare the bond strength between three different types of ceramics and resin cement, as well as the degree of conversion of resin cement after using different light-curing units and curing modes. Methods: Three types of ceramics—Leucite-reinforced (Empress CAD), Lithium [...] Read more.
Objectives: To measure and compare the bond strength between three different types of ceramics and resin cement, as well as the degree of conversion of resin cement after using different light-curing units and curing modes. Methods: Three types of ceramics—Leucite-reinforced (Empress CAD), Lithium disilicate (Emax CAD), and Zirconia (Emax ZirCAD)—of varying thicknesses (1.5 mm and 2.0 mm) were bonded to a light-cure resin cement (Variolink Esthetic LC). Light-curing was carried out using a monowave LCU (3M Elipar DeepCure-S LED Curing Light with irradiance of 1470 mW/cm2) and with polywave LCU (Ivoclar Bluephase PowerCure) using High, Turbo, and 3 s curing modes, respectively (1200, 2100, 3000 mW/cm2). A chevron-notch bond strength test (total n = 288) was conducted to calculate the fracture energy and interfacial bond strength (J/m2). The degree of cure (%DC) of the residual resin cement on debonded surfaces was measured using Fourier Transform Infrared Spectroscopy (FTIR). Collected data were statistically analysed under SPSS ver. 27 by conducting an ANOVA and Bonferroni post hoc test. The mode of failure was established using a scanning electron microscope (SEM). Results: A significant difference in interfacial bond strength was found between the three types of ceramic material groups (p < 0.01). Cement cured through Empress that was 2 mm thick showed the highest bond strength (1.36 ± 0.46 J/m2), while the lowest was observed (0.26 ± 0.07 J/m2) in 2 mm Emax CAD using the 3 s mode. The use of different LCUs and curing modes had a significant influence on the %DC of resin cement seen in all groups, except 2 mm Emax ZirCAD. The dominant mode of failure for Empress, EmaxCAD, and EmaxZirCAD were cohesive, adhesive, and mixed, respectively. Conclusions: The type of ceramic and its thickness can significantly affect bond strength, and the results showed that polywave LCU is more effective than monowave LCU when curing through ceramics. Full article
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11 pages, 2081 KiB  
Article
Effect of CAD/CAM Ceramic Thickness on Shade Masking Ability of Discolored Teeth: In Vitro Study
by Passent Ellakany, Marwa Madi, Nourhan M. Aly, Zainb S. Al-Aql, Maher AlGhamdi, Abdulrahman AlJeraisy and Adel S. Alagl
Int. J. Environ. Res. Public Health 2021, 18(24), 13359; https://doi.org/10.3390/ijerph182413359 - 18 Dec 2021
Cited by 18 | Viewed by 3219
Abstract
Shade matching is a common challenge that dentists face during fabrication of esthetic dental restoration. Thus, the aim of the current study was to assess the masking ability of two types of CAD/CAM ceramics for gaining high esthetic prosthesis. This in vitro study [...] Read more.
Shade matching is a common challenge that dentists face during fabrication of esthetic dental restoration. Thus, the aim of the current study was to assess the masking ability of two types of CAD/CAM ceramics for gaining high esthetic prosthesis. This in vitro study used a total sample size of 66 lithium disilicate (LD) and leucite reinforced (LR) CAD/CAM ceramics sub-grouped into three thicknesses: 0.5, 1, and 1.5 mm. Nine shades of natural dentin die materials were prepared as a replica of the underlying tooth structure. The difference in color (ΔE) and translucency parameter (TP) were assessed for both tested ceramics at the three thicknesses. One-way ANOVA was performed to compare the three thicknesses of each ceramic, followed by multiple pairwise comparisons between both ceramics. LR had significantly higher ΔE than LD at all thicknesses used unlike the case in TP. Thickness of 0.5 mm exhibited the highest ΔE and TP, while 1.5 mm thickness showed the lowest ΔE and TP in both ceramics. Increase in ceramic thickness had a great impact on both color masking ability of the underlying tooth structure and its translucency. The higher the ceramic thickness, the better the masking ability and the lower the translucency was reported. Full article
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13 pages, 3756 KiB  
Article
Influence of Low-Pressure Plasma on the Surface Properties of CAD-CAM Leucite-Reinforced Feldspar and Resin Matrix Ceramics
by Pablo Sevilla, Carlos Lopez-Suarez, Jesús Pelaez, Celia Tobar, Veronica Rodriguez-Alonso and María J. Suarez
Appl. Sci. 2020, 10(24), 8856; https://doi.org/10.3390/app10248856 - 10 Dec 2020
Cited by 8 | Viewed by 2703
Abstract
The introduction of new ceramic materials for dental restorations is currently a reality; however, little information is available on their surface treatment for the bonding process. Furthermore, surface treatment with plasma on ceramic materials has been recently introduced, although not many studies are [...] Read more.
The introduction of new ceramic materials for dental restorations is currently a reality; however, little information is available on their surface treatment for the bonding process. Furthermore, surface treatment with plasma on ceramic materials has been recently introduced, although not many studies are available. The aim of this study was to evaluate the surface properties of a leucite-reinforced feldspar ceramic (LIC) and resin matrix ceramic (RMC) after low-pressure plasma treatment. From each material, 48 discs were prepared and subject to surface treatment. The LIC group was treated by hydrofluoric acid (HF) (LIC-HF), plasma with oxygen (LIC-O2), and plasma with argon (LIC-Ar). The RMC group was treated by sandblasting with alumina (RMC-SB), plasma with oxygen (RMC-O2), and plasma with argon (RMC-Ar). The groups whose surfaces were not subjected to treatment were considered as the control group. Surface wettability and roughness was analyzed. The results showed significant differences among the treatments for both ceramics regarding wettability and roughness. Plasma treatments increased the wettability and had a very low effect on the roughness. Plasma treatments achieved similar values for both surface properties in each ceramic group with no differences between both treatments. Plasma treatment seems to be a promising alternative for ceramic surface treatments since it increased the surface energy of the ceramics analyzed and hardly affects the roughness. Further studies are necessary to evaluate the effect of plasma treatment on the bond strength of ceramics. Full article
(This article belongs to the Section Applied Dentistry and Oral Sciences)
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