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Keywords = large area fabrication

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13 pages, 4131 KiB  
Article
MBE Growth of High-Quality HgCdSe for Infrared Detector Applications
by Zekai Zhang, Wenwu Pan, Gilberto A. Umana Membreno, Shuo Ma, Lorenzo Faraone and Wen Lei
Materials 2025, 18(15), 3676; https://doi.org/10.3390/ma18153676 - 5 Aug 2025
Abstract
HgCdSe has recently been proposed as a potential alternative material to HgCdTe for fabricating high-performance infrared detectors. This work presents a study on the growth of high-crystalline-quality HgCdSe materials on GaSb (211)B substrates via molecular beam epitaxy and demonstration of the first prototype [...] Read more.
HgCdSe has recently been proposed as a potential alternative material to HgCdTe for fabricating high-performance infrared detectors. This work presents a study on the growth of high-crystalline-quality HgCdSe materials on GaSb (211)B substrates via molecular beam epitaxy and demonstration of the first prototype HgCdSe-based mid-wave infrared detectors. By optimizing the MBE growth parameters, and especially the thermal cleaning process of the GaSb substrate surface prior to epitaxial growth, high-quality HgCdSe material was achieved with a record XRD full width at half maximum of ~65 arcsec. At a temperature of 77 K, the mid-wave infrared HgCdSe n-type material demonstrated a minority carrier lifetime of ~1.19 µs, background electron concentration of ~2.2 × 1017 cm−3, and electron mobility of ~1.6 × 104 cm2/Vs. The fabricated mid-wave infrared HgCdSe photoconductor presented a cut-off wavelength of 4.2 µm, a peak responsivity of ~40 V/W, and a peak detectivity of ~1.2 × 109 cmHz1/2/W at 77 K. Due to the relatively high background electron concentration, the detector performance is lower than that of state-of-the-art low-doped HgCdTe counterparts. However, these preliminary results indicate the great potential of HgCdSe materials for achieving next-generation IR detectors on large-area substrates with features of lower cost and larger array format size. Full article
(This article belongs to the Section Optical and Photonic Materials)
13 pages, 3292 KiB  
Article
Topological Large-Area Waveguide States Based on THz Photonic Crystals
by Yulin Zhao, Feng Liang, Jingsen Li, Jianfei Han, Jiangyu Chen, Haihua Hu, Ke Zhang and Yuanjie Yang
Photonics 2025, 12(8), 791; https://doi.org/10.3390/photonics12080791 - 5 Aug 2025
Abstract
Terahertz (THz) has attracted substantial attention owing to its unique advantages in high-speed communications. However, conventional THz waveguide systems are inherently constrained by high transmission losses, stringent fabrication precision requirements, and extreme sensitivity to structural defects. Topological edge states with topological protection have [...] Read more.
Terahertz (THz) has attracted substantial attention owing to its unique advantages in high-speed communications. However, conventional THz waveguide systems are inherently constrained by high transmission losses, stringent fabrication precision requirements, and extreme sensitivity to structural defects. Topological edge states with topological protection have driven significant advancements in THz wave manipulation. Nevertheless, the width of the topological waveguide based on edge states remains restricted. In this work, we put forward a type of spin photonic crystal with three-layer heterostructures, where large-area topological waveguide states are demonstrated. The results show that these topological waveguide states are localized within the region of Dirac photonic crystals. They also display spin-momentum-locking characteristics and maintain strong robustness against defects and sharp bends. Furthermore, a THz beam splitter and a topological beam modulator are implemented. The designed heterostructures expand the applications of multi-functional topological devices and provide a prospective pathway for overcoming the waveguide bottleneck in THz applications. Full article
(This article belongs to the Section Optoelectronics and Optical Materials)
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42 pages, 4490 KiB  
Review
Continuous Monitoring with AI-Enhanced BioMEMS Sensors: A Focus on Sustainable Energy Harvesting and Predictive Analytics
by Mingchen Cai, Hao Sun, Tianyue Yang, Hongxin Hu, Xubing Li and Yuan Jia
Micromachines 2025, 16(8), 902; https://doi.org/10.3390/mi16080902 (registering DOI) - 31 Jul 2025
Viewed by 356
Abstract
Continuous monitoring of environmental and physiological parameters is essential for early diagnostics, real-time decision making, and intelligent system adaptation. Recent advancements in bio-microelectromechanical systems (BioMEMS) sensors have significantly enhanced our ability to track key metrics in real time. However, continuous monitoring demands sustainable [...] Read more.
Continuous monitoring of environmental and physiological parameters is essential for early diagnostics, real-time decision making, and intelligent system adaptation. Recent advancements in bio-microelectromechanical systems (BioMEMS) sensors have significantly enhanced our ability to track key metrics in real time. However, continuous monitoring demands sustainable energy supply solutions, especially for on-site energy replenishment in areas with limited resources. Artificial intelligence (AI), particularly large language models, offers new avenues for interpreting the vast amounts of data generated by these sensors. Despite this potential, fully integrated systems that combine self-powered BioMEMS sensing with AI-based analytics remain in the early stages of development. This review first examines the evolution of BioMEMS sensors, focusing on advances in sensing materials, micro/nano-scale architectures, and fabrication techniques that enable high sensitivity, flexibility, and biocompatibility for continuous monitoring applications. We then examine recent advances in energy harvesting technologies, such as piezoelectric nanogenerators, triboelectric nanogenerators and moisture electricity generators, which enable self-powered BioMEMS sensors to operate continuously and reducereliance on traditional batteries. Finally, we discuss the role of AI in BioMEMS sensing, particularly in predictive analytics, to analyze continuous monitoring data, identify patterns, trends, and anomalies, and transform this data into actionable insights. This comprehensive analysis aims to provide a roadmap for future continuous BioMEMS sensing, revealing the potential unlocked by combining materials science, energy harvesting, and artificial intelligence. Full article
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26 pages, 1247 KiB  
Review
Recent Progress in the Application of Electrospinning Technology in the Biomedical Field
by Qun Wang, Peng Ji, Tian Bu, Yating Mao, Hailun He and Naijing Ge
J. Funct. Biomater. 2025, 16(7), 266; https://doi.org/10.3390/jfb16070266 - 18 Jul 2025
Cited by 1 | Viewed by 713
Abstract
Electrospinning has emerged as a highly effective technique for fabricating micro- and nanofibers, which are characterized by high porosity, large surface area, and structural mimicry of the extracellular matrix (ECM). These properties render it particularly suitable for biomedical applications. This review provides a [...] Read more.
Electrospinning has emerged as a highly effective technique for fabricating micro- and nanofibers, which are characterized by high porosity, large surface area, and structural mimicry of the extracellular matrix (ECM). These properties render it particularly suitable for biomedical applications. This review provides a comprehensive overview of recent developments in electrospinning-based strategies across various biomedical fields, including tissue engineering, drug delivery, wound healing, enzyme immobilization, biosensing, and protective materials. The distinctive advantages of electrospun fibers—such as excellent biocompatibility, tunable architecture, and facile surface functionalization—are discussed, alongside challenges such as the toxicity of organic solvents and limitations in scalability. Emerging approaches, including environmentally benign electrospinning techniques and integration with advanced technologies such as 3D printing and microfluidics, present promising solutions for intelligent and personalized biomedical applications. Full article
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13 pages, 1563 KiB  
Article
A Sensitive and Accurate Electrochemical Sensor Based on Biomass-Derived Porous Carbon for the Detection of Ascorbic Acid
by Yashuang Hei, Lisi Ba, Xingwei Shi, Huanhuan Guo, Sisi Wen, Bingxiao Zheng, Wenjie Gu and Zhiju Zhao
Molecules 2025, 30(14), 2980; https://doi.org/10.3390/molecules30142980 - 15 Jul 2025
Viewed by 312
Abstract
Ascorbic acid (AA) is a vital biomarker for human metabolic processes, and many diseases are strongly linked to aberrant variations in its content. It is crucial to detect the levels of AA with sensitivity, speed, and accuracy. In this work, three-dimensional honeycomb-like porous [...] Read more.
Ascorbic acid (AA) is a vital biomarker for human metabolic processes, and many diseases are strongly linked to aberrant variations in its content. It is crucial to detect the levels of AA with sensitivity, speed, and accuracy. In this work, three-dimensional honeycomb-like porous carbons derived from discarded walnut (green) husks (DWGH-HCPCs) were synthesized using a process involving hydrothermal treatment, freeze-drying, and carbonization. The DWGH-HCPCs, with a high specific surface area of 419.72 m2 g−1, large pore volume of 0.35 cm3 g−1 and high density of defective sites, are used to fabricate the electrochemical sensor for the detection of AA. The electrochemical performance of the DWGH-HCPC-modified glassy carbon electrode (GCE) (DWGH-HCPC/GCE) was investigated through chronoamperometry, differential pulse voltammetry, and cyclic voltammetry. Compared with the GCE, the DWGH-HCPC/GCE exhibits higher sensitivities (34.7 μA mM−1 and 22.7 μA mM−1), a wider linear range (10–1040 μM and 1040–3380 μM), and a lower detection limit (0.26 μM) for AA detection. Specifically, the real sample concentrations of AA in beverages and artificial urine were successfully identified by DWGH-HCPC/GCE. Additionally, the DWGH-HCPC/GCE demonstrated great feasibility in the simultaneous detection of AA, dopamine (DA), and uric acid (UA). Therefore, as a green, eco-friendly, and low-cost electrode modifier, DWGH-HCPCs have broad prospects in the development of electrochemical sensing platforms for food and medical applications. Full article
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38 pages, 5046 KiB  
Review
Photonics on a Budget: Low-Cost Polymer Sensors for a Smarter World
by Muhammad A. Butt
Micromachines 2025, 16(7), 813; https://doi.org/10.3390/mi16070813 - 15 Jul 2025
Viewed by 581
Abstract
Polymer-based photonic sensors are emerging as cost-effective, scalable alternatives to conventional silicon and glass photonic platforms, offering unique advantages in flexibility, functionality, and manufacturability. This review provides a comprehensive assessment of recent advances in polymer photonic sensing technologies, focusing on material systems, fabrication [...] Read more.
Polymer-based photonic sensors are emerging as cost-effective, scalable alternatives to conventional silicon and glass photonic platforms, offering unique advantages in flexibility, functionality, and manufacturability. This review provides a comprehensive assessment of recent advances in polymer photonic sensing technologies, focusing on material systems, fabrication techniques, device architectures, and application domains. Key polymer materials, including PMMA, SU-8, polyimides, COC, and PDMS, are evaluated for their optical properties, processability, and suitability for integration into sensing platforms. High-throughput fabrication methods such as nanoimprint lithography, soft lithography, roll-to-roll processing, and additive manufacturing are examined for their role in enabling large-area, low-cost device production. Various photonic structures, including planar waveguides, Bragg gratings, photonic crystal slabs, microresonators, and interferometric configurations, are discussed concerning their sensing mechanisms and performance metrics. Practical applications are highlighted in environmental monitoring, biomedical diagnostics, and structural health monitoring. Challenges such as environmental stability, integration with electronic systems, and reproducibility in mass production are critically analyzed. This review also explores future opportunities in hybrid material systems, printable photonics, and wearable sensor arrays. Collectively, these developments position polymer photonic sensors as promising platforms for widespread deployment in smart, connected sensing environments. Full article
(This article belongs to the Section A:Physics)
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14 pages, 3449 KiB  
Article
Superhydrophobic Coating on 6061 Aluminum Alloy Fabricated by Femtosecond Laser Etching and Anodic Oxidation
by Quanlv Liu and Yuxin Wang
Coatings 2025, 15(7), 816; https://doi.org/10.3390/coatings15070816 - 11 Jul 2025
Viewed by 456
Abstract
A superhydrophobic surface with hierarchical micro/nano-array structures was successfully fabricated on 6061 aluminum alloy through a combination of femtosecond laser etching and anodic oxidation. Femtosecond laser etching formed a regularly arranged microscale “pit-protrusion” array on the aluminum alloy surface. After modification with a [...] Read more.
A superhydrophobic surface with hierarchical micro/nano-array structures was successfully fabricated on 6061 aluminum alloy through a combination of femtosecond laser etching and anodic oxidation. Femtosecond laser etching formed a regularly arranged microscale “pit-protrusion” array on the aluminum alloy surface. After modification with a fluorosilane ethanol solution, the surface exhibited superhydrophobicity with a contact angle of 154°. Subsequently, the anodic oxidation process formed an anodic oxide film dominated by an array of aluminum oxide (Al2O3) nanopores at the submicron scale. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses revealed that the nanopore structures uniformly and continuously covered the laser-ablated layer. This hierarchical structure significantly increased the surface water contact angle to 162°. Wettability analysis showed that the prepared composite coating formed an air layer accounting for 91% of the surface area. Compared with the sample only treated by femtosecond laser etching, the presence of the Al2O3 nanopore structure significantly enhanced the mechanical durability, superhydrophobic durability, and corrosion resistance of the superhydrophobic surface. The proposed multi-step fabrication strategy offers an innovative method for creating multifunctional, durable superhydrophobic coatings and has important implications for their large-scale industrial use. Full article
(This article belongs to the Special Issue Superhydrophobic Coatings, 2nd Edition)
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28 pages, 4234 KiB  
Review
A Review on Laser-Induced Graphene-Based Electrocatalysts for the Oxygen Reduction Reaction in Electrochemical Energy Storage and Conversion
by Giulia Massaglia and Marzia Quaglio
Nanomaterials 2025, 15(14), 1070; https://doi.org/10.3390/nano15141070 - 10 Jul 2025
Viewed by 470
Abstract
The increasing demand for efficient and sustainable energy conversion technologies has driven extensive research into alternative electrocatalysts for the oxygen reduction reaction (ORR). Platinum-based catalysts, while highly efficient, suffer from high costs, scarcity, and long-term instability Laser-Induced Graphene (LIG) has recently attracted considerable [...] Read more.
The increasing demand for efficient and sustainable energy conversion technologies has driven extensive research into alternative electrocatalysts for the oxygen reduction reaction (ORR). Platinum-based catalysts, while highly efficient, suffer from high costs, scarcity, and long-term instability Laser-Induced Graphene (LIG) has recently attracted considerable interest as an effective metal-free electrocatalyst for oxygen reduction reaction (ORR), owing to its remarkable electrical conductivity, customizable surface functionalities, and multi-scale porous architecture. This review explores the synthesis strategies, physicochemical properties, and ORR catalytic performance of LIG. Additionally, this review offered a detailed overview regarding the effective pole of heteroatom doping (N, S, P, B) and functionalization techniques to enhance catalytic activity. Finally, we highlight the current challenges and future perspectives of LIG-based ORR catalysts for fuel cells and other electrochemical energy applications. Furthermore, laser-induced-graphene (LIG) has emerged as a highly attractive candidate for electrochemical energy conversion systems, due to its large specific surface area, tunable porosity, excellent electrical conductivity, and cost-effective fabrication process. This review discusses recent advancements in LIG synthesis, its structural and electrochemical properties, and its applications in supercapacitors, batteries, fuel cells, and electrocatalysis. Despite its advantages, challenges such as mechanical stability, electrochemical degradation, and large-scale production remain key areas for improvement. Additionally, this review explores future perspectives on optimizing LIG for next-generation energy storage and conversion technologies. Full article
(This article belongs to the Special Issue Nanomaterials Based (Bio) Electrochemical Energy and Storage Sytems)
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13 pages, 1504 KiB  
Article
Mapping and Potential Risk Assessment of Marine Debris in Mangrove Wetlands in the Northern South China Sea
by Peng Zhou, Zhongchen Jiang, Li Zhao, Huina Hu and Dongmei Li
Sustainability 2025, 17(14), 6311; https://doi.org/10.3390/su17146311 - 9 Jul 2025
Viewed by 384
Abstract
Mangrove wetlands, acting as significant traps for marine debris, have received insufficient attention in previous research. Here, we conduct the first comprehensive investigation into the magnitude, accumulation, source, and fate of marine debris across seven mangrove areas in the northern South China Sea [...] Read more.
Mangrove wetlands, acting as significant traps for marine debris, have received insufficient attention in previous research. Here, we conduct the first comprehensive investigation into the magnitude, accumulation, source, and fate of marine debris across seven mangrove areas in the northern South China Sea (MNSCS) during 2019–2020. Systematic field surveys employed stratified random sampling, partitioning each site by vegetation density and tidal influence. Marine debris were collected and classified in sampling units by material (plastic, fabric, styrofoam), size (categorized into small, medium, and large), and origin (distinguishing between land-based and sea-based). Source identification and potential risk assessment were achieved through the integration of debris feature analysis. The results indicate relatively low debris levels in MNSCS mangroves, with plastics dominant. More than 70% of all debris weight with plastics (48.34%) and fabrics (14.59%) is land-based, and more than 70% comes from coastal/recreational activities. More than 90% of all debris items with plastics (52.50%) and Styrofoam (36.32%) are land-based, and more than 90% come from coastal/recreational activities. Medium/large-sized debris are trapped in mangrove wetlands under the influencing conditions of local tidal level, debris item materials, and sizes. Our study quantifies marine debris characteristics, sources, and ecological potential risks in MNSCS mangroves. From environmental, economic, and social sustainability perspectives, our findings are helpful for guiding marine debris management and mangrove conservation. By bridging research and policies, our work balances human activities with ecosystem health for long-term sustainability. Full article
(This article belongs to the Section Sustainable Oceans)
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21 pages, 3395 KiB  
Review
Advancements in Titanium Dioxide Nanotube-Based Sensors for Medical Diagnostics: A Two-Decade Review
by Joydip Sengupta and Chaudhery Mustansar Hussain
Nanomaterials 2025, 15(13), 1044; https://doi.org/10.3390/nano15131044 - 5 Jul 2025
Viewed by 1019
Abstract
Over the past two decades, titanium dioxide nanotubes (TiO2 NTs) have gained considerable attention as multifunctional materials in sensing technologies. Their large surface area, adjustable morphology, chemical stability, and photoactivity have positioned them as promising candidates for diverse sensor applications. This review [...] Read more.
Over the past two decades, titanium dioxide nanotubes (TiO2 NTs) have gained considerable attention as multifunctional materials in sensing technologies. Their large surface area, adjustable morphology, chemical stability, and photoactivity have positioned them as promising candidates for diverse sensor applications. This review presents a broad overview of the development of TiO2 NTs in sensing technologies for medical diagnostics over the last two decades. It further explores strategies for enhancing their sensing capabilities through structural modifications and hybridization with nanomaterials. Despite notable advancements, challenges such as device scalability, long-term operational stability, and fabrication reproducibility remain. This review outlines the evolution of TiO2 NT-based sensors for medical diagnostics, highlighting both foundational progress and emerging trends, while providing insights into future directions for their practical implementation across scientific and industrial domains. Full article
(This article belongs to the Special Issue The Future of Nanotechnology: Healthcare and Manufacturing)
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16 pages, 2745 KiB  
Article
Next-Generation Nafion Membranes: Synergistic Enhancement of Electrochemical Performance and Thermomechanical Stability with Sulfonated Siliceous Layered Material (sSLM)
by Valeria Loise and Cataldo Simari
Polymers 2025, 17(13), 1866; https://doi.org/10.3390/polym17131866 - 3 Jul 2025
Viewed by 491
Abstract
Nafion, while a benchmark proton exchange membrane (PEM) for fuel cells, suffers from significant performance degradation at elevated temperatures and low humidity due to dehydration and diminished mechanical stability. To address these limitations, this study investigated the development and characterization of Nafion nanocomposite [...] Read more.
Nafion, while a benchmark proton exchange membrane (PEM) for fuel cells, suffers from significant performance degradation at elevated temperatures and low humidity due to dehydration and diminished mechanical stability. To address these limitations, this study investigated the development and characterization of Nafion nanocomposite membranes incorporating sulfonated silica layered materials (sSLMs). The inherent lamellar structure, high surface area, and abundant sulfonic acid functionalities of sSLMs were leveraged to synergistically enhance membrane properties. Our results demonstrate that sSLM incorporation significantly improved ion exchange capacity, water uptake, and dimensional stability, leading to superior water retention and self-diffusion at higher temperatures. Critically, the nanocomposite membranes exhibited remarkably enhanced proton conductivity, particularly under demanding conditions of 120 C and low relative humidity (i.e., 20% RH), where filler-free Nafion largely ceases to conduct. Single H2/O2 fuel cell tests confirmed these enhancements, with the optimal sSLM-Nafion nanocomposite membrane (N-sSLM5) achieving a two-fold power density improvement over pristine Nafion at 120 C and 20% RH (340 mW cm−2 vs. 117 mW cm−2 for Nafion). These findings underscore the immense potential of sSLM as a functional filler for fabricating robust and high-performance PEMs, paving the way for the next generation of fuel cells capable of operating efficiently under more challenging environmental conditions. Full article
(This article belongs to the Section Polymer Membranes and Films)
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28 pages, 3287 KiB  
Review
Recent Progress in Photocatalytic Hydrogen Production Using 2D MoS2 Based Materials
by Khursheed Ahmad and Tae Hwan Oh
Catalysts 2025, 15(7), 648; https://doi.org/10.3390/catal15070648 - 2 Jul 2025
Viewed by 712
Abstract
Due to the increase in energy demand, photocatalytic hydrogen (H2) production has received enormous interest from the scientific community due to its simplicity and cost-effectiveness. The photocatalyst (PC) plays a vital role in H2 evolution, and it is well understood [...] Read more.
Due to the increase in energy demand, photocatalytic hydrogen (H2) production has received enormous interest from the scientific community due to its simplicity and cost-effectiveness. The photocatalyst (PC) plays a vital role in H2 evolution, and it is well understood that an efficient PC should have a larger surface area and better charge separation and transport properties. Previously, extensive efforts were made to prepare the efficient PC for photocatalytic H2 production. In some cases, pristine catalyst could not catalyze the catalytic reactions due to a fast recombination rate or poor catalytic behavior. Thus, cocatalysts can be explored to boost the photocatalytic H2 production. In this regard, a promising cocatalyst should have a large surface area, more active sites, decent conductivity, and improved catalytic properties. Molybdenum disulfide (MoS2) is one of the two-dimensional (2D) layered materials that have excellent optical, electrical, and physicochemical properties. MoS2 has been widely utilized as a cocatalyst for the photocatalytic H2 evolution under visible light. Herein, we have reviewed the progress in the fabrication of MoS2 and its composites with metal oxides, perovskite, graphene, carbon nanotubes, graphitic carbon nitrides, polymers, MXenes, metal-organic frameworks, layered double hydroxides, metal sulfides, etc. for photocatalytic H2 evolution. The reports showed that MoS2 is one of the desirable cocatalysts for photocatalytic H2 production applications. The challenges and future perspectives are also mentioned. This study may be beneficial for the researchers working on the design and fabrication of MoS2-based PCs for photocatalytic H2 evolution applications. Full article
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13 pages, 6820 KiB  
Article
An Exploration of SPS Fabrication and the Sliding Wear Properties of γ-TiAl-Ag Self-Lubrication Materials
by Na Xiao, Chenglong Yang, Shengfei Zhou, Yuliang Yin, Dian Zhao, Yulong Shi and Kang Yang
Surfaces 2025, 8(3), 45; https://doi.org/10.3390/surfaces8030045 - 30 Jun 2025
Viewed by 341
Abstract
To promote the optimization of the anti-friction and anti-wear behavior of lightweight TiAl alloys, γ-TiAl-10 wt.% Ag self-lubricating composites were fabricated, and their mechanical and tribological properties were tested. The results showed that the silver in TiAl-10 wt.% Ag slightly reduced its mechanical [...] Read more.
To promote the optimization of the anti-friction and anti-wear behavior of lightweight TiAl alloys, γ-TiAl-10 wt.% Ag self-lubricating composites were fabricated, and their mechanical and tribological properties were tested. The results showed that the silver in TiAl-10 wt.% Ag slightly reduced its mechanical properties compared with those of pure TiAl alloys. A silver-enriched lubrication film formed on a wear scar, which was helpful in improving the friction and wear behavior. It was found that a large amount of silver gathered at a wear scar, gradually spread out under the action of the sliding friction force, and then increased the silver distribution areas on the wear scar, leading to the good formation of a silver-rich film. Furthermore, an identification model was established to calculate the specific area η of the silver film. A quantitative relationship indicated that an increase in the Ag distribution area improved the tribological behavior of γ-TiAl-10 wt.% Ag. When the specific area η of a silver-rich film was maintained at 44–51%, the small friction coefficient (almost 0.28) and wear rate (about 2.25 × 10−4 mm3·N−1·m−1) were well stabilized. This provides a new research method to improve the tribological performance of TiAl-Ag samples. Full article
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12 pages, 3013 KiB  
Article
Investigation of Poling for Pb(Zr, Ti)O3/Pb(Zr, Ti)O3 Sol–Gel Composite
by Mako Nakamura, Ryota Ono and Makiko Kobayashi
Micromachines 2025, 16(7), 760; https://doi.org/10.3390/mi16070760 - 28 Jun 2025
Viewed by 485
Abstract
Phased-array ultrasonic transducers using sol–gel composites face challenges in terms of polarization uniformity when using conventional corona poling. Pb(Zr, Ti)O3 (PZT)/PZT composites with a thickness of 25 µm were fabricated on 3 mm thick titanium substrates, and the samples were poled by [...] Read more.
Phased-array ultrasonic transducers using sol–gel composites face challenges in terms of polarization uniformity when using conventional corona poling. Pb(Zr, Ti)O3 (PZT)/PZT composites with a thickness of 25 µm were fabricated on 3 mm thick titanium substrates, and the samples were poled by AC poling, DC poling, and corona discharge poling at RT. It was found that the polarization direction could be controlled by the voltage off-phase angle. When poling was performed with a voltage off-phase angle of 90°, applied voltage of 200 V (rms), 10 cycles, and frequency of 1 Hz, average values and standards of measured piezoelectric constant d33 of −35.1 ± 0.8 pC/N and ultrasonic sensitivity of 11.4 ± 0.1 dB were obtained. Furthermore, the AC-poled samples demonstrated smaller variations in d33 and ultrasonic sensitivity compared with the corona-poled samples, and higher values of d33 and ultrasonic sensitivity compared with the DC-poled samples, indicating the potential of AC poling for PZT/PZT sol–gel composites with large areas. Full article
(This article belongs to the Special Issue Acoustic Transducers and Their Applications, 2nd Edition)
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12 pages, 5010 KiB  
Article
Same Day Microfluidics: From Design to Device in Under Three Hours
by Raymond J. Arebalo, Augustin J. Sanchez and Nathan Tompkins
Nanomanufacturing 2025, 5(3), 9; https://doi.org/10.3390/nanomanufacturing5030009 - 27 Jun 2025
Viewed by 331
Abstract
Microfluidic devices are used in numerous scientific fields and research areas, but device fabrication is still a time- and resource-intensive process largely confined to the cleanroom or a similarly well-equipped laboratory. This paper presents a method to create microfluidic devices in under three [...] Read more.
Microfluidic devices are used in numerous scientific fields and research areas, but device fabrication is still a time- and resource-intensive process largely confined to the cleanroom or a similarly well-equipped laboratory. This paper presents a method to create microfluidic devices in under three hours using the silicone polymer polydimethylsiloxane (PDMS) and a laser cut positive master using PDMS double casting without a cleanroom or other large capital equipment. This method can be utilized by an undergraduate student with minimal training in a laboratory with a modest budget. This paper presents “Same Day Microfluidics” as a fabrication method accessible to research groups not currently fabricating their own microfluidic devices and as an option for established research groups to more quickly create prototype devices. The method is described in detail with timing, materials, and technical considerations for each step and demonstrated in the context of a Y-channel coflow device. Full article
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