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Keywords = isotropic conductive adhesive

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21 pages, 17034 KB  
Article
From CT Imaging to 3D Representations: Digital Modelling of Fibre-Reinforced Adhesives with Image-Based FEM
by Abdul Wasay Khan, Kaixin Xu, Nikolas Manousides and Claudio Balzani
Adhesives 2025, 1(4), 14; https://doi.org/10.3390/adhesives1040014 - 3 Dec 2025
Viewed by 907
Abstract
Short fibre-reinforced adhesives (SFRAs) are increasingly used in wind turbine blades to enhance stiffness and fatigue resistance, yet their heterogeneous microstructure poses significant challenges for predictive modelling. This study presents a fully automated digital workflow that integrates micro-computed tomography (µCT), image processing, and [...] Read more.
Short fibre-reinforced adhesives (SFRAs) are increasingly used in wind turbine blades to enhance stiffness and fatigue resistance, yet their heterogeneous microstructure poses significant challenges for predictive modelling. This study presents a fully automated digital workflow that integrates micro-computed tomography (µCT), image processing, and finite element modelling (FEM) to investigate the mechanical response of SFRAs. Our aim is also to establish a computational foundation for data-driven modelling and future AI surrogates of adhesive joints in wind turbine blades. High-resolution µCT scans were denoised and segmented using a hybrid non-local means and Gaussian filtering pipeline combined with Otsu thresholding and convex hull separation, enabling robust fibre identification and orientation analysis. Two complementary modelling strategies were employed: (i) 2D slice-based FEM models to rapidly assess microstructural effects on stress localisation and (ii) 3D voxel-based FEM models to capture the full anisotropic fibre network. Linear elastic simulations were conducted under inhomogeneous uniaxial extension and torsional loading, revealing interfacial stress hotspots at fibre tips and narrow ligaments. Fibre clustering and alignment strongly influenced stress partitioning between fibres and the matrix, while isotropic regions exhibited diffuse, matrix-dominated load transfer. The results demonstrate that image-based FEM provides a powerful route for structure–property modelling of SFRAs and establish a scalable foundation for digital twin development, reliability assessment, and integration with physics-informed surrogate modelling frameworks. Full article
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15 pages, 3772 KB  
Article
Effects of Build Orientation and Loading Direction on the Compressive Behavior of Additively Manufactured Re-Entrant Auxetic Materials
by Mehmet Ermurat and Mevlut Safa Dag
Polymers 2025, 17(23), 3123; https://doi.org/10.3390/polym17233123 - 25 Nov 2025
Cited by 3 | Viewed by 1052
Abstract
Additive manufacturing (AM) technologies, particularly Fused Deposition Modeling (FDM) and Digital Light Processing (DLP), offer viable solutions for producing Auxetic materials characterized by their negative Poisson’s ratio. This study investigates the influence of build orientation and loading direction on the mechanical behavior of [...] Read more.
Additive manufacturing (AM) technologies, particularly Fused Deposition Modeling (FDM) and Digital Light Processing (DLP), offer viable solutions for producing Auxetic materials characterized by their negative Poisson’s ratio. This study investigates the influence of build orientation and loading direction on the mechanical behavior of re-entrant honeycomb auxetic structures fabricated using both FDM- and LCD-based DLP techniques. Specimens were produced in three principal build orientations (X, Y, and Z) and subjected to compression along two directions (X and Y) to capture the anisotropic mechanical response. Standard PLA filament was used for FDM, while standard and tough resins were used for DLP. Uniaxial compression tests were conducted to evaluate maximum compressive stress, Poisson’s ratio, and energy absorption behavior. The results reveal significant anisotropy in mechanical performance depending on build orientation and printing technology. DLP-printed specimens exhibited more isotropic behavior compared to FDM due to superior interlayer adhesion. Furthermore, build orientation was found to have a pronounced effect on auxetic response and load-bearing capacity. This study highlights the critical importance of considering build orientation and loading direction during the design and manufacturing of auxetic structures, especially for applications requiring targeted mechanical performance. Full article
(This article belongs to the Section Polymer Processing and Engineering)
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17 pages, 8487 KB  
Article
Strength Optimisation of Hybrid Bolted/Bonded Composite Joints Based on Finite Element Analysis
by Raphael Blier, Leila Monajati, Masoud Mehrabian and Rachid Boukhili
Materials 2024, 17(13), 3354; https://doi.org/10.3390/ma17133354 - 6 Jul 2024
Cited by 7 | Viewed by 2556
Abstract
A finite element analysis (FEA) was conducted to examine the behaviour of single-lap quasi-isotropic (QI) and cross-ply (CP) hybrid bolted/bonded (HBB) configurations subjected to tensile shear loading. Several critical design factors influencing the composite joint strength, failure conditions, and load-sharing mechanisms that would [...] Read more.
A finite element analysis (FEA) was conducted to examine the behaviour of single-lap quasi-isotropic (QI) and cross-ply (CP) hybrid bolted/bonded (HBB) configurations subjected to tensile shear loading. Several critical design factors influencing the composite joint strength, failure conditions, and load-sharing mechanisms that would optimise the joining performance were assessed. The study of the stress concentration around the holes and along the adhesive layer highlights the fact that the HBB joints benefit from significantly lower stresses compared to only bolted joints, especially for CP configurations. The simulation results confirmed the redundancy of the middle bolt in a three-bolt HBB joint. The stiffness and plastic behaviour of the adhesive were found to be important factors that define the transition of the behaviour of the joint from a bolted type, where load sharing is predominant, to a bonded joint. The load-sharing potential, known as an indicator of the joint’s performance, is improved by reducing the overlap length, using a low-stiffness, high-plasticity adhesive, and using thicker laminates in the QI layup configuration. Enhancing both the ratio of the edge distance to the hole diameter and washer size proves advantageous in reducing stresses within the adhesive layer, thereby improving the joint strength. Full article
(This article belongs to the Special Issue Manufacturing and Mechanics of Materials, Volume II)
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16 pages, 6039 KB  
Article
Preparations and Thermal Properties of PDMS-AlN-Al2O3 Composites through the Incorporation of Poly(Catechol-Amine)-Modified Boron Nitride Nanotubes
by Arni Gesselle Pornea, Duy Khoe Dinh, Zahid Hanif, Numan Yanar, Ki-In Choi, Min Seok Kwak and Jaewoo Kim
Nanomaterials 2024, 14(10), 847; https://doi.org/10.3390/nano14100847 - 13 May 2024
Cited by 9 | Viewed by 4917
Abstract
As one of the emerging nanomaterials, boron nitride nanotubes (BNNTs) provide promising opportunities for diverse applications due to their unique properties, such as high thermal conductivity, immense inertness, and high-temperature durability, while the instability of BNNTs due to their high surface induces agglomerates [...] Read more.
As one of the emerging nanomaterials, boron nitride nanotubes (BNNTs) provide promising opportunities for diverse applications due to their unique properties, such as high thermal conductivity, immense inertness, and high-temperature durability, while the instability of BNNTs due to their high surface induces agglomerates susceptible to the loss of their advantages. Therefore, the proper functionalization of BNNTs is crucial to highlight their fundamental characteristics. Herein, a simplistic low-cost approach of BNNT surface modification through catechol-polyamine (CAPA) interfacial polymerization is postulated to improve its dispersibility on the polymeric matrix. The modified BNNT was assimilated as a filler additive with AlN/Al2O3 filling materials in a PDMS polymeric matrix to prepare a thermal interface material (TIM). The resulting composite exhibits a heightened isotropic thermal conductivity of 8.10 W/mK, which is a ~47.27% increase compared to pristine composite 5.50 W/mK, and this can be ascribed to the improved BNNT dispersion forming interconnected phonon pathways and the thermal interface resistance reduction due to its augmented compatibility with the polymeric matrix. Moreover, the fabricated composite manifests a fire resistance improvement of ~10% in LOI relative to the neat composite sample, which can be correlated to the thermal stability shift in the TGA and DTA data. An enhancement in thermal permanence is stipulated due to a melting point (Tm) shift of ∼38.5 °C upon the integration of BNNT-CAPA. This improvement can be associated with the good distribution and adhesion of BNNT-CAPA in the polymeric matrix, integrated with its inherent thermal stability, good charring capability, and free radical scavenging effect due to the presence of CAPA on its surface. This study offers new insights into BNNT utilization and its corresponding incorporation into the polymeric matrix, which provides a prospective direction in the preparation of multifunctional materials for electric devices. Full article
(This article belongs to the Special Issue Thermally Conductive Nanomaterials and Their Applications)
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13 pages, 6269 KB  
Article
A Printing Strategy for Embedding Conductor Paths into FFF Printed Parts
by Timo Banko, Stefan Grünwald, Rainer Kronberger and Hermann Seitz
Polymers 2023, 15(17), 3498; https://doi.org/10.3390/polym15173498 - 22 Aug 2023
Cited by 5 | Viewed by 2452
Abstract
A novel approach to manufacture components with integrated conductor paths involves embedding and sintering an isotropic conductive adhesive (ICA) during fused filament fabrication (FFF). However, the molten plastic is deposited directly onto the adhesive path which causes an inhomogeneous displacement of the uncured [...] Read more.
A novel approach to manufacture components with integrated conductor paths involves embedding and sintering an isotropic conductive adhesive (ICA) during fused filament fabrication (FFF). However, the molten plastic is deposited directly onto the adhesive path which causes an inhomogeneous displacement of the uncured ICA. This paper presents a 3D printing strategy to achieve a homogeneous cross-section of the conductor path. The approach involves embedding the ICA into a printed groove and sealing it with a wide extruded plastic strand. Three parameter studies are conducted to obtain a consistent cavity for uniform formation of the ICA path. Specimens made of polylactic acid (PLA) with embedded ICA paths are printed and evaluated. The optimal parameters include a groove printed with a layer height of 0.1 mm, depth of 0.4 mm, and sealed with a PLA strand of 700 µm diameter. This resulted in a conductor path with a homogeneous cross-section, measuring 660 µm ± 22 µm in width (relative standard deviation: 3.3%) and a cross-sectional area of 0.108 mm2 ± 0.008 mm2 (relative standard deviation 7.2%). This is the first study to demonstrate the successful implementation of a printing strategy for embedding conductive traces with a homogeneous cross-sectional area in FFF 3D printing. Full article
(This article belongs to the Special Issue 3D Printing of Polymer-Based Composite Materials)
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12 pages, 6014 KB  
Article
Development of 3D-Printed Self-Healing Capsules with a Separate Membrane and Investigation of Mechanical Properties for Improving Fracture Strength
by Taeuk Lim, Hao Cheng, Jie Hu, Yeongjun Lee, Sangyou Kim, Jangheon Kim and Wonsuk Jung
Materials 2023, 16(16), 5687; https://doi.org/10.3390/ma16165687 - 18 Aug 2023
Cited by 5 | Viewed by 2212
Abstract
Studies on self-healing capsules embedded in cement composites to heal such cracks have recently been actively researched in order to improve the dimensional stability of concrete structures. In particular, capsule studies were mainly conducted to separately inject reactive healing solutions into different capsules. [...] Read more.
Studies on self-healing capsules embedded in cement composites to heal such cracks have recently been actively researched in order to improve the dimensional stability of concrete structures. In particular, capsule studies were mainly conducted to separately inject reactive healing solutions into different capsules. However, with this method, there is an important limitation in that the probability of self-healing is greatly reduced because the two healing solutions must meet and react. Therefore, we propose three-dimensional (3D) printer-based self-healing capsules with a membrane structure that allows two healing solutions to be injected into one capsule. Among many 3D printing methods, we used the fusion deposition modeling (FDM) to design, analyze, and produce new self-healing capsules, which are widely used due to their low cost, precise manufacturing, and high-speed. However, polylactic lactic acid (PLA) extruded in the FDM has low adhesion energy between stacked layers, which causes different fracture strengths depending on the direction of the applied load and the subsequent performance degradation of the capsule. Therefore, the isotropic fracture characteristics of the newly proposed four types of separated membrane capsules were analyzed using finite element method analysis. Additionally, capsules were produced using the FDM method, and the compression test was conducted by applying force in the x, y, and z directions. The isotropic fracture strength was also analyzed using the relative standard deviation (RSD) parameter. As a result, the proposed separated membrane capsule showed that the RSD of isotropic fracture strength over all directions fell to about 18% compared to other capsules. Full article
(This article belongs to the Section Construction and Building Materials)
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12 pages, 5003 KB  
Article
Assembly of Surface-Mounted Devices on Flexible Substrates by Isotropic Conductive Adhesive and Solder and Lifetime Characterization
by Rafat Saleh, Sophie Schütt, Maximilian Barth, Thassilo Lang, Wolfgang Eberhardt and André Zimmermann
Micromachines 2022, 13(8), 1240; https://doi.org/10.3390/mi13081240 - 1 Aug 2022
Cited by 8 | Viewed by 2901
Abstract
The assembly of passive components on flexible electronics is essential for the functionalization of circuits. For this purpose, adhesive bonding technology by isotropic conductive adhesive (ICA) is increasingly used in addition to soldering processes. Nevertheless, a comparative study, especially for bending characterization, is [...] Read more.
The assembly of passive components on flexible electronics is essential for the functionalization of circuits. For this purpose, adhesive bonding technology by isotropic conductive adhesive (ICA) is increasingly used in addition to soldering processes. Nevertheless, a comparative study, especially for bending characterization, is not available. In this paper, soldering and conductive adhesive bonding of 0603 and 0402 components on flexible polyimide substrates is compared using the design of experiments methods (DoE), considering failure for shear strength and bending behavior. Various solder pastes and conductive adhesives are used. Process variation also includes curing and soldering profiles, respectively, amount of adhesive, and final surface metallization. Samples created with conductive adhesive H20E, a large amount of adhesive, and a faster curing profile could achieve the highest shear strength. In the bending characterization using adhesive bonding, samples on immersion silver surface finish withstood more cycles to failure than samples on bare copper surface. In comparison, the samples soldered to bare copper surface finish withstood more cycles to failure than the soldered samples on immersion silver surface finish. Full article
(This article belongs to the Special Issue Structural Analyses and Designs for Flexible/Stretchable Electronics)
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13 pages, 2500 KB  
Article
Property Prediction of Ag-Filled Isotropic Conductive Adhesive through the Analysis of Its Curing and Decomposition Kinetics
by Han Jiang, Minbo Zhou and Xinping Zhang
Catalysts 2022, 12(2), 185; https://doi.org/10.3390/catal12020185 - 1 Feb 2022
Cited by 3 | Viewed by 2442
Abstract
In this study, various thermal analyses were carried out on a self-developed and commerce-oriented Ag-filled isotropic conductive adhesive (ICA) and its unfilled matrix resin through which glass transition temperature (Tg) and thermal endurance could be quantitatively predicted. An autocatalyzed kinetic [...] Read more.
In this study, various thermal analyses were carried out on a self-developed and commerce-oriented Ag-filled isotropic conductive adhesive (ICA) and its unfilled matrix resin through which glass transition temperature (Tg) and thermal endurance could be quantitatively predicted. An autocatalyzed kinetic model was used to describe the curing reaction, which was proven to be in good consistency with the experimental data. The activation energies for the curing reaction of the ICA and the matrix resin were determined to be 68.1 kJ/mol and 72.9 kJ/mol, respectively, which means that the reaction of the ICA was easier to occur than its unfilled matrix resin. As a result, the time–temperature profile could be calculated for any Tg requested based on the kinetic model of curing and the DiBenedetto equation. Further, the thermal decomposition stability of the ICA and its unfilled matrix resin were also studied. The activation energies for the thermal decomposition of the ICA and the matrix resin were calculated to be 134.1 kJ/mol and 152.7 kJ/mol, respectively, using the Ozawa–Flynn–Wall method, which means that the decomposition of ICA was easier to occur. The service life of the resin system at a specific temperature could therefore be calculated with their activation energy. The addition of micro-scale Ag flakes did not change the curing and decomposition mechanisms by much. Full article
(This article belongs to the Special Issue New Advances in Self-Catalysis Technology)
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12 pages, 2197 KB  
Article
Enhancing Acoustic Emission Characteristics in Pipe-Like Structures with Gradient-Index Phononic Crystal Lens
by Gorkem Okudan, Hrishikesh Danawe, Lu Zhang, Didem Ozevin and Serife Tol
Materials 2021, 14(6), 1552; https://doi.org/10.3390/ma14061552 - 22 Mar 2021
Cited by 9 | Viewed by 3914
Abstract
Phononic crystals have the ability to manipulate the propagation of elastic waves in solids by generating unique dispersion characteristics. They can modify the conventional behavior of wave spreading in isotropic materials, known as attenuation, which negatively influences the ability of acoustic emission method [...] Read more.
Phononic crystals have the ability to manipulate the propagation of elastic waves in solids by generating unique dispersion characteristics. They can modify the conventional behavior of wave spreading in isotropic materials, known as attenuation, which negatively influences the ability of acoustic emission method to detect active defects in long-range, pipe-like structures. In this study, pipe geometry is reconfigured by adding gradient-index (GRIN) phononic crystal lens to improve the propagation distance of waves released by active defects such as crack growth and leak. The sensing element is designed to form a ring around the pipe circumference to capture the plane wave with the improved amplitude. The GRIN lens is designed by a special gradient-index profile with varying height stubs adhesively bonded to the pipe surface. The performance of GRIN lens for improving the amplitude of localized sources is demonstrated with finite element numerical model using multiphysics software. Experiments are conducted using pencil lead break simulating crack growth, as well as an orifice with pressured pipe simulating leak. The amplitude of the burst-type signal approximately doubles on average, validating the numerical findings. Hence, the axial distance between sensors can be increased proportionally in the passive sensing of defects in pipe-like geometries. Full article
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