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22 pages, 9108 KB  
Article
Research on Application of High-Pressure Cyclic Grouting Technology in Soft Soil Layers
by Xiaolong Pei, Liwei Huang, Ping Fu and Zhanqing Xing
Coatings 2026, 16(2), 194; https://doi.org/10.3390/coatings16020194 - 4 Feb 2026
Abstract
Aiming at technical challenges such as the insufficient bearing capacity of orifice formation leading to slurry overflow and non-uniform formation reinforcement in soft soil layer grouting engineering, an external cyclic grouting process through the grouting pipe is innovatively proposed. Distinguished from traditional in-hole [...] Read more.
Aiming at technical challenges such as the insufficient bearing capacity of orifice formation leading to slurry overflow and non-uniform formation reinforcement in soft soil layer grouting engineering, an external cyclic grouting process through the grouting pipe is innovatively proposed. Distinguished from traditional in-hole circulation methods, this process achieves bottom-up cyclic grouting through a slurry return channel outside the grouting hole, which effectively reduces the risk of orifice fracturing and improves grouting uniformity. A grouting pressure loss equation is established to quantitatively analyze the relationships between the allowable grouting pressure and the side wall opening of the grouting pipe, slurry rheological parameters, surface consolidation depth, and surface consolidation strength. It is revealed that slurry with high viscosity and low yield stress is suitable for deep grouting, and a design criterion innovatively proposes that the side wall opening of the grouting hole should dynamically increase with the grouting depth. Based on the strain–pressure curve, a prediction model for the reinforcement radius of compaction grouting is established. Slurry rheological parameters and formation mechanical parameters are obtained through laboratory tests, and field grouting tests are conducted. The reinforcement effect is verified by means of ground-penetrating radar and standard penetration tests. The results show that, compared with traditional grouting processes, this process significantly improves the bearing capacity of the orifice and enhances the uniformity and compactness of formation reinforcement and that the theoretical prediction error of the reinforcement radius is less than 15%. The research results provide the theoretical basis and technical support for soft soil grouting engineering and have important engineering application value. Full article
(This article belongs to the Section Surface Characterization, Deposition and Modification)
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19 pages, 2369 KB  
Article
Numerical Simulation of Failure Modes of Solid Propellants with Internal Cavities Under Various Loading Conditions
by Kai Liu, Qingchun Yang, Liang Cao, Jianru Wang and Peng Cao
Polymers 2026, 18(3), 404; https://doi.org/10.3390/polym18030404 - 4 Feb 2026
Abstract
The reliability of solid rocket motors depends primarily on the structural integrity of their propellants. Internal cavity defects in the widely used hydroxyl-terminated polybutadiene (HTPB) propellant, formed during manufacturing and service, significantly degrade its mechanical properties and compromise motor safety. This study developed [...] Read more.
The reliability of solid rocket motors depends primarily on the structural integrity of their propellants. Internal cavity defects in the widely used hydroxyl-terminated polybutadiene (HTPB) propellant, formed during manufacturing and service, significantly degrade its mechanical properties and compromise motor safety. This study developed a constitutive model for HTPB propellant based on the generalized incremental stress–strain damage model (GISSMO). The validity of the constitutive model was verified through uniaxial tensile tests conducted at various tensile rates. Based on this constitutive model, numerical simulations were performed to examine the effects of initial modulus, impact rate, and cavity confining pressure on the failure modes of propellants containing cavities with radii from 40 to 100 mm. The results show that the simulation’s force–displacement curve agrees well with the test. The simulation accurately captures the propellant’s transition from elastic–plastic plateau at low rates to elastic response at high rates. The prediction error for the maximum tensile force is less than 5%. For cavities of 80 mm and 100 mm, local stress concentration causes damage to the inner wall, followed by rapid cavity extrusion, collapse, and possible cross-shaped matrix fracture. However, cavities of 40 mm and 60 mm show greater stability, experiencing only volume compression, which rarely causes overall damage. When the propellant’s initial modulus is higher than 24 MPa, damage propagation in large cavities over 80 mm is suppressed. A low modulus worsens structural deformation. At low impact velocity, cavity compression is significant, and the structure remains conformal. At high impact velocity (4000 MPa/s), the cavity stays conformal, the matrix collapses, and the damage value decreases. For 60 mm cavities, damage is localized, and the overall structure is most stable within a confining pressure of 5 to 9.5 MPa. This study clarifies the interaction between engineering parameters and cavity size, providing a basis for optimizing the safety of the propellant structure. Full article
(This article belongs to the Section Polymer Physics and Theory)
18 pages, 16964 KB  
Article
Tailoring Microstructure and Mechanical Properties of the Al-7Si-0.35Mg-0.35Fe Alloy by Cr Addition: A Study on Fe-Rich Phase Modification
by Chiteng Le, Wenjun Liu, Tiancai Yin, Shuai Zhao, Cong Gao, Mingbo Yang, Tiehu Li and Bin Jiang
Materials 2026, 19(3), 593; https://doi.org/10.3390/ma19030593 - 3 Feb 2026
Abstract
Fe-rich phases are unavoidable intermetallic compounds in aluminum alloys, particularly in recycled aluminum. Their needle-like morphology not only impairs the mechanical performance of the alloy by disrupting the continuity of the matrix but also significantly reduces the allowable addition of recycled aluminum materials. [...] Read more.
Fe-rich phases are unavoidable intermetallic compounds in aluminum alloys, particularly in recycled aluminum. Their needle-like morphology not only impairs the mechanical performance of the alloy by disrupting the continuity of the matrix but also significantly reduces the allowable addition of recycled aluminum materials. Based on this, this study focuses on the Al-7Si-0.35Mg-0.35Fe alloy with a high Fe content. The Cr was introduced to modify the characteristics of the Fe-rich phase, and the microstructural evolution and mechanical properties of the aluminum alloy with different Cr content (0–0.25 wt.%) were investigated. Experimental results show that the secondary dendrite arm spacing of the alloy is significantly refined after Cr addition. Meanwhile, the Fe-rich phase gradually transitions from β-Al5FeSi with needle-like morphology to α-Al15(Fe,Cr)3Si2 with short rod-like or blocky morphology as the Cr content increases. Notably, the Fe-rich phase in the 0.20Cr alloy exhibits an approximately 65% increase in sphericity and an 84% reduction in equivalent diameter compared to those in the 0Cr alloy. The morphological blunting and dispersed distribution of Fe-rich phases lead to a broad effective Cr addition range of 0.05–0.20 wt% in the alloy. Among them, the 0.20Cr alloy exhibited the best comprehensive mechanical properties, with its ultimate tensile strength and elongation approximately 19% and 107% higher than those of the 0Cr alloy, respectively. Furthermore, the fracture morphology and the relationship between the Fe-rich phase and microcracks in Al-7Si-0.35Mg-0.35Fe alloys with different Cr contents were also analyzed. Full article
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24 pages, 8605 KB  
Article
Numerical Investigation on Rotational Cutting of Coal Seam by Single Cutting Pick
by Ying Tian, Shengda Zhang, Qiang Zhang, Yan Song, Yongliang Han, Long Feng, Huaitao Liu, Yingchun Zhang and Xiangwei Dong
Processes 2026, 14(3), 531; https://doi.org/10.3390/pr14030531 - 3 Feb 2026
Abstract
Shearers and roadheaders are critical equipment in coal mining and roadway excavation, where the rock-breaking performance of cutting picks directly influences operational efficiency and economic outcomes. Complex geological conditions, such as hard coal seams and embedded inclusions like gangue or pyrite nodules, pose [...] Read more.
Shearers and roadheaders are critical equipment in coal mining and roadway excavation, where the rock-breaking performance of cutting picks directly influences operational efficiency and economic outcomes. Complex geological conditions, such as hard coal seams and embedded inclusions like gangue or pyrite nodules, pose significant challenges to cutting efficiency and tool wear. This study presents a numerical investigation into the rotational cutting process of a single pick in heterogeneous coal seams using the Smoothed Particle Hydrodynamics (SPH) method integrated with a mixed failure model. The model combines the Drucker–Prager criterion for shear failure and the Grady–Kipp damage model for tensile failure, enabling accurate simulation of crack initiation, propagation, and coalescence without requiring explicit fracture treatments. Simulations reveal that cutting depth significantly influences the failure mode: shallow depths promote tensile crack-induced spallation of hard nodules under compressive stress, while deeper cuts lead to shear-dominated failure. The cutting pick exhibits periodic force fluctuations corresponding to stages of compressive-shear crack initiation, propagation, and spallation. The results provide deep insights into pick–rock interaction mechanisms and offer a reliable computational tool for optimizing cutting parameters and improving mining equipment design under complex geological conditions. A key finding is the identification of a critical transition in failure mechanism from tensile-dominated spallation to shear-driven fragmentation with increasing cutting depth, which provides a theoretical basis for practitioners to select optimal cutting parameters that minimize tool wear and energy consumption in field operations. Full article
(This article belongs to the Section Chemical Processes and Systems)
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21 pages, 5381 KB  
Article
Dynamic Fracture Behaviour of Cracked H-Shaped Beam-Column Joints with Beam Ends Supported by Columns
by Kai Wang, Chengxiang Yang, Yan Dong, Tiejun Yuan, Yaodong Xue and Yonghui Huang
Buildings 2026, 16(3), 642; https://doi.org/10.3390/buildings16030642 - 3 Feb 2026
Abstract
The study of the mechanical response and crack propagation behaviour of H-shaped beam-column specimens is of great significance for ensuring the safety and stability of buildings. As a connection structure that has gained ubiquity in modern shopping malls and high-rise buildings, an in-depth [...] Read more.
The study of the mechanical response and crack propagation behaviour of H-shaped beam-column specimens is of great significance for ensuring the safety and stability of buildings. As a connection structure that has gained ubiquity in modern shopping malls and high-rise buildings, an in-depth exploration of the failure mechanisms of H-shaped beam-column components will facilitate more accurate technical support for building maintenance and service life prediction. The present study employs a combination of drop-weight impact tests and the caustic method to systematically investigate the dynamic fracture characteristics of H-shaped beam-column joints under various prefabricated crack configurations. The results demonstrate that the number and location of cracks in H-shaped beam-column specimens have a significant impact on the propagation path and velocity. Specifically, beam-end cracks are prone to bifurcation, while column-end cracks predominantly initiate from the beam-column intersection. This phenomenon is particularly evident in specimens with prefabricated cracks at both the beam ends and column ends. The propagation of cracks at the beam ends is arrested due to the presence of compressive stress when they reach the beam-column intersection. During this period, the stress intensity of the column-end cracks increases significantly, with a growth rate of 33%. Full article
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27 pages, 8433 KB  
Article
Polygonal Crack Evolution in Multilayered Rocks Under Cooling Contraction
by Tiantian Chen, Yu Jiang, Zhengzhao Liang, Chun’an Tang and Tao Geng
Fractal Fract. 2026, 10(2), 107; https://doi.org/10.3390/fractalfract10020107 - 3 Feb 2026
Abstract
Multilayered geological structures are common in geotechnical engineering, where cooling shrinkage induces polygonal cracks in interlayers, compromising rock mass strength, permeability, and long-term stability. Existing thermo-mechanical studies on layered rock cracking insufficiently address the combined effects of weak interlayer geometry or interface-regulated mechanisms. [...] Read more.
Multilayered geological structures are common in geotechnical engineering, where cooling shrinkage induces polygonal cracks in interlayers, compromising rock mass strength, permeability, and long-term stability. Existing thermo-mechanical studies on layered rock cracking insufficiently address the combined effects of weak interlayer geometry or interface-regulated mechanisms. To address this gap, based on meso-damage mechanics and thermodynamics, this study adopts a thermo-mechanical coupling simulation method considering rock heterogeneity, innovatively focusing on the understudied stress transfer effect at strong–weak interlayer interfaces. Systematic investigations were conducted on the initiation, propagation, and saturation of polygonal cracks in plate-like layered rocks under surface cooling, analyzing the influences of weak interlayer thickness, number, and position, and comparing surface vs. inner interlayer behaviors. Results showed that stress transfer interruption at weak–strong layer interfaces can inhibit crack propagation. Inter weak interlayers produce significantly more cracks and fragments than surface weak interlayers, with a stratified crack length distribution, and the maximum fragment area increases exponentially with weak interlayer thickness. Crack development is strongly influenced by weak interlayer thickness, with thinner layers dominated by non-penetrating cracks and thicker layers tending to develop penetrating lattice-like cracks. The inter layer stress and crack distribution exhibit fractal characteristics, with crack density decreasing layer by layer and no new cracks forming after saturation. This study clarifies the regulatory mechanism of weak interlayer features and surface cooling on crack evolution, quantifies interface effects and fractal characteristics, and provides a theoretical basis for instability prediction of layered rock structures in low-temperature geotechnical engineering. Full article
(This article belongs to the Special Issue Applications of Fractal Dimensions in Rock Mechanics and Geomechanics)
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15 pages, 3487 KB  
Article
Investigation of Microstructure and Mechanical Behavior of Nanomodified Cement-Based Materials
by Spyridoula G. Farmaki, Dimitrios A. Exarchos, Vasileios Dracopoulos, Anastasios Gkotzamanis, Konstantinos G. Dassios and Theodore E. Matikas
Appl. Mech. 2026, 7(1), 13; https://doi.org/10.3390/applmech7010013 - 3 Feb 2026
Abstract
Recent advances in nanotechnology have highlighted the transformative potential of carbon-based nanomaterials, such as carbon nanofibers, carbon nanotubes, and graphene, in cementitious systems. These materials have shown a remarkable ability to enhance the mechanical strength, fracture toughness, and overall functional performance of cementitious [...] Read more.
Recent advances in nanotechnology have highlighted the transformative potential of carbon-based nanomaterials, such as carbon nanofibers, carbon nanotubes, and graphene, in cementitious systems. These materials have shown a remarkable ability to enhance the mechanical strength, fracture toughness, and overall functional performance of cementitious composites. Their nanoscale dimensions and exceptional intrinsic properties allow for effective stress bridging, crack arrest, and matrix densification. Despite these promising features, the current understanding remains limited, particularly regarding their application to concrete. Furthermore, literature lacks systematic, parallel evaluations of their respective effectiveness in improving both mechanical performance and long-term durability, as well as their potential to impart true multifunctionality to concrete structures. It is worth noting that significant and statistically significant improvements in fracture behavior were observed at specific nanofiller concentrations, suggesting strong potential for the material system in next-generation innovative infrastructure applications. Experimental results demonstrated that both CNTs and GNPs significantly enhanced the mechanical performance of concrete, with flexural strength increases of approximately 49% and 38%, and compressive strength improvements of 22% and 47%, respectively, at optimum contents of 0.6 wt.% CNTs and 0.8 wt.% GNPs. SEM analyses confirmed improved matrix densification and interfacial bonding at these concentrations, while higher dosages led to agglomeration and reduced performance. This gap highlights the need for targeted experimental studies to elucidate the structure-property relationships governing these advanced materials. Full article
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20 pages, 8306 KB  
Article
Damage Characteristics and Residual Strength of UAV Aluminum-Alloy Plate Structures Under High-Velocity Impact
by Yitao Wang, Teng Zhang, Hanzhe Zhang, Yuting He and Liying Ma
Drones 2026, 10(2), 111; https://doi.org/10.3390/drones10020111 - 2 Feb 2026
Abstract
To address the increasing vulnerability of unmanned aerial vehicle (UAV) lightweight airframe structures to high-velocity fragment impacts in complex operational environments, this study combines high-velocity impact penetration tests, quasi-static strength tests, fracture-surface microanalysis, and finite-element simulation to systematically reveal the formation mechanism of [...] Read more.
To address the increasing vulnerability of unmanned aerial vehicle (UAV) lightweight airframe structures to high-velocity fragment impacts in complex operational environments, this study combines high-velocity impact penetration tests, quasi-static strength tests, fracture-surface microanalysis, and finite-element simulation to systematically reveal the formation mechanism of typical penetration damage and its influence on residual strength. Results show that such penetration induces damage such as adiabatic-shear local melting zones, spall cracks, and grain-boundary separation, significantly weakening static strength and shifting the fracture mode from ductility- to brittleness-dominated. A modified fracture-mechanics criterion with higher prediction accuracy than the traditional net-section criterion is proposed, and a high-precision simulation model based on explicit–quasi-static coupling is established, which well reproduces damage morphology and tensile-failure processes. Compared with conventional manned aircraft structures, UAV airframes characterized by thinner skins and higher lightweighting ratios exhibit more pronounced sensitivity to penetration-induced micro-defects, making rapid residual-strength assessment essential for operational recovery and field-level repair decision-making. The research reveals the damage mechanism and provides an engineering-applicable residual-strength assessment method, offering a reliable theoretical basis and simulation tool for rapid UAV damage evaluation and fast-turnaround repair planning for civil and industrial UAV platforms. Full article
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21 pages, 9521 KB  
Article
Slotted Charge Blasting Technology: A Review of Mechanisms, Applications, and Future Directions
by Xiaohua Zhang, Shiqian Yan, Guangquan Li, Yang Yang, Jianguo Wang and Xianglong Li
Appl. Sci. 2026, 16(3), 1510; https://doi.org/10.3390/app16031510 - 2 Feb 2026
Abstract
The drilling and blasting method remains fundamental to mining and tunneling projects, prized for its simplicity and economy. However, conventional techniques are increasingly challenged by modern safety and environmental standards, particularly in complex geological settings. Slotted charge blasting technology addresses these limitations by [...] Read more.
The drilling and blasting method remains fundamental to mining and tunneling projects, prized for its simplicity and economy. However, conventional techniques are increasingly challenged by modern safety and environmental standards, particularly in complex geological settings. Slotted charge blasting technology addresses these limitations by offering exceptional control over fracture propagation and damage. This paper provides a comprehensive review of the field, synthesizing global research on its theoretical foundations, advanced diagnostic methodologies, key performance parameters, and engineering applications. We critically analyze the current challenges facing the technology, particularly in weak rock conditions, where extensive plastic deformation and rapid energy dissipation often compromise directional control, and identify promising trends for its future development. Specifically, the integration of intelligent adaptive control and additive manufacturing is highlighted as a key direction. By mapping out a clear trajectory for future research, this work provides a scientific basis to advance the efficacy and safety of slotted charge blasting in demanding engineering environments. Full article
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29 pages, 1797 KB  
Systematic Review
Head-to-Head: AI and Human Workflows for Single-Unit Crown Design—Systematic Review
by Andrei Vorovenci, Viorel Ștefan Perieanu, Mihai Burlibașa, Mihaela Romanița Gligor, Mădălina Adriana Malița, Mihai David, Camelia Ionescu, Ruxandra Stănescu, Mona Ionaș, Radu Cătălin Costea, Oana Eftene, Cristina Maria Șerbănescu, Mircea Popescu and Andi Ciprian Drăguș
Oral 2026, 6(1), 16; https://doi.org/10.3390/oral6010016 - 2 Feb 2026
Abstract
Objectives: To compare artificial intelligence (AI) crown design with expert or non-AI computer-aided (CAD) design for single-unit tooth and implant-supported crowns across efficiency, marginal and internal fit, morphology and occlusion, and mechanical performance. Materials and Methods: This systematic review was conducted and reported [...] Read more.
Objectives: To compare artificial intelligence (AI) crown design with expert or non-AI computer-aided (CAD) design for single-unit tooth and implant-supported crowns across efficiency, marginal and internal fit, morphology and occlusion, and mechanical performance. Materials and Methods: This systematic review was conducted and reported in accordance with PRISMA 2020. PubMed MEDLINE, Scopus, Web of Science, IEEE Xplore, and Dentistry and Oral Sciences Source were searched from 2016 to 2025 with citation chasing. Eligible studies directly contrasted artificial intelligence-generated or artificial intelligence-assisted crown designs with human design in clinical, ex vivo, or in silico settings. Primary outcomes were design time, marginal and internal fit, morphology and occlusion, and mechanical performance. Risk of bias was assessed with ROBINS-I for non-randomized clinical studies, QUIN for bench studies, and PROBAST + AI for computational investigations, with TRIPOD + AI items mapped descriptively. Given heterogeneity in settings and endpoints, a narrative synthesis was used. Results: A total of 14 studies met inclusion criteria, including a clinical patient study, multiple ex vivo experiments, and in silico evaluations. Artificial intelligence design reduced design time by between 40% and 90% relative to expert computer-aided design or manual workflows. Marginal and internal fit for artificial intelligence and human designs were statistically equivalent in multiple comparisons. Mechanical performance matched technician designs in load-to-fracture testing, and modeling indicated stress distributions similar to natural teeth. Overall risk of bias was judged as some concerns across tiers. Conclusions: Artificial intelligence crown design delivers efficiency gains while showing short-term technical comparability across fit, morphology, occlusion, and strength for single-unit crowns in predominantly bench and in silico evidence, with limited patient-level feasibility data. Prospective clinical trials with standardized, preregistered endpoints are needed to confirm durability, generalizability, and patient-relevant outcomes, and to establish whether short-term technical advantages translate into clinical benefit. Full article
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29 pages, 1920 KB  
Article
Surface Characterisation of Retrieved Orthopaedic Knee Liners
by Supriya Wakale and Tarun Goswami
Appl. Sci. 2026, 16(3), 1501; https://doi.org/10.3390/app16031501 - 2 Feb 2026
Viewed by 17
Abstract
Total knee arthroplasty (TKA) is one of the most frequently performed surgical procedures for patients with advanced knee joint disease, which is intended to relieve pain and restore normal joint function. A critical component of the TKA system is the ultra-high-molecular-weight polyethylene knee [...] Read more.
Total knee arthroplasty (TKA) is one of the most frequently performed surgical procedures for patients with advanced knee joint disease, which is intended to relieve pain and restore normal joint function. A critical component of the TKA system is the ultra-high-molecular-weight polyethylene knee liner, which acts as the bearing surface between the metallic components. Despite continuous improvements in material processing and implant design, these liners remain vulnerable to several damage mechanisms such as wear, fatigue, delamination, oxidative degradation, pitting, embedded debris, overload, creep, edge damage, backside wear, and fracture. This study introduces a new quadrant-based characterization system to evaluate retrieved knee liners through non-destructive methods. The liners, collected from revision surgeries, were divided into nine anatomical zones labelled Q1 to Q9 to systematically identify and map surface damage. Damage density was determined manually as well as by using computational image analysis through MATLAB R2024a and Python 3.13. The computational methods demonstrated greater accuracy and reproducibility, showing a strong correlation with manual evaluation, with p equalling 0.41 for Python and p equalling 1.00 for MATLAB. The proposed quadrant-based system, together with computational validation, offers a more reliable framework in studying wear and damage patterns in retrieved implants. This approach contributes to an enhanced understanding of how different damage modes interact and offers useful guidance for enhancing implant design, material durability, and clinical outcome improvement in total knee arthroplasty. Full article
17 pages, 4803 KB  
Communication
Effect of Lap Joint Configuration and Seam Strategy in Green-Laser Welding on Multi-Layer Cu Foil Stacks to Lead-Tab Joints for Pouch Cell Application
by Seong Min Hong, Bum-Su Go and Hee-Seon Bang
Materials 2026, 19(3), 573; https://doi.org/10.3390/ma19030573 - 2 Feb 2026
Viewed by 14
Abstract
This study examines the joining characteristics of Cu foil stacks to lead tabs using green-laser welding in the main-welding step of a sequential welding process for lithium-ion pouch cells. The influence of lap configuration, line and wobble seam strategies, and process parameters was [...] Read more.
This study examines the joining characteristics of Cu foil stacks to lead tabs using green-laser welding in the main-welding step of a sequential welding process for lithium-ion pouch cells. The influence of lap configuration, line and wobble seam strategies, and process parameters was systematically investigated in terms of bead morphology, mechanical performance, metallurgical characteristics, and electrical resistance. Under the present line-welding parameter window (2.0 kW, 100–200 mm/s), humping, pinholes, and porosity were observed, particularly in the upper lead-tab configuration, which is attributed to melt-pool/keyhole instability under the applied conditions. Wobble welding effectively suppressed these defects in the foil-stack configuration by promoting stable melt flow and efficient bubble expulsion. Mechanical tests revealed that the wobble-based seam strategy achieved a maximum tensile–shear load of approximately 1.28 kN at a wobble amplitude of 0.8 mm. Fracture analysis confirmed a transition from seam-type interfacial failure in line welding to ductile tearing in the heat-affected zone with wobble welding. In electrical performance, wobble welding reduced resistance to as low as 45 µΩ at a wobble amplitude of 1.2 mm, while line welding yielded higher and scattered values. These results should be interpreted as the combined outcome of the wobble-based seam strategy (beam oscillation together with overlapped stitch welding at a lower travel speed) under the present processing windows. A strictly matched A/B comparison at identical linear energy density and seam layout will be investigated in future work to isolate the effect of oscillation. Full article
(This article belongs to the Collection Welding and Joining Processes of Materials)
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13 pages, 4498 KB  
Article
Fracture Energy Reduction Caused by Water at the Crack Front of an Aluminum/Epoxy Resin Interface
by Aoto Seki, Tetsuto Terabayashi, Kazumasa Shimamoto, Chiaki Sato and Yu Sekiguchi
Adhesives 2026, 2(1), 4; https://doi.org/10.3390/adhesives2010004 - 2 Feb 2026
Viewed by 31
Abstract
A detailed understanding of interface degradation in humid environments is essential for improving the reliability of adhesive bonding technologies. Water absorption within the adhesive layer significantly affects joint strength, a factor considered to be long-term degradation. However, even if water does not approach [...] Read more.
A detailed understanding of interface degradation in humid environments is essential for improving the reliability of adhesive bonding technologies. Water absorption within the adhesive layer significantly affects joint strength, a factor considered to be long-term degradation. However, even if water does not approach the interface from the inside due to absorption, it can reach the interface from the outside through the crack tip and instantaneously affect the fracture behavior of the interface, highlighting the need to investigate short-term degradation mechanisms. In this study, the effect of water at the aluminum/epoxy resin interface on crack propagation was quantitatively evaluated by measuring the mode I energy release rate through double cantilever beam (DCB) tests. By changing the surface condition of the adherend, interfacial and cohesive failures were achieved, and DCB tests were conducted in air and underwater conditions to compare the effect of water on the fracture energy. Results showed that the interfacial fracture energy decreased by more than 50% when the crack propagated in water, but no significant reduction was observed in the cohesive fracture energy. The decrease in interfacial fracture energy in the presence of water indicates the immediate disruption of chemical bonding. Full article
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21 pages, 18415 KB  
Article
Graded Brittle–Ductile Transition via Laser-Induced Thermal Gradient for Broaching of Z10C13 Steel
by Guozhen Liu, Zhen Meng, Junqiang Zheng, Weiguang Liu, Xinghua Wu, Jing Ni and Haohan Zhang
Micromachines 2026, 17(2), 204; https://doi.org/10.3390/mi17020204 - 2 Feb 2026
Viewed by 23
Abstract
This paper presents a breakthrough in activating the skin effect at conventional broaching speeds (1–8 m/min) by using laser defocus gradient modification to induce surface embrittlement in martensitic stainless steel Z10C13. Through controlled defocusing, a 50 μm gradient remelting layer was created, which [...] Read more.
This paper presents a breakthrough in activating the skin effect at conventional broaching speeds (1–8 m/min) by using laser defocus gradient modification to induce surface embrittlement in martensitic stainless steel Z10C13. Through controlled defocusing, a 50 μm gradient remelting layer was created, which features ultrafine grains (0.8 μm) and a high-density geometrically necessary dislocation (GND) zone (ρGND = 2.27 μm−3). The quasi-cleavage fracture was triggered via dislocation pinning by non-oriented low-angle grain boundaries (28.4% LAGBs). Multiscale characterization confirms that this microstructural transformation enhances surface hardness by 12.95% (reaching 31.4 HRC), reduces cutting force by 34.07%, and improves surface roughness by 63.74% (Sz = 28.80 μm). Simultaneously, a parallel crack-deflection mechanism restricts subsurface damage propagation, resulting in a crack-free subsurface zone. These results demonstrate the effectiveness of the embrittlement–toughening dichotomy for precision machining of difficult-to-cut materials under low-speed constraints. Full article
(This article belongs to the Section D:Materials and Processing)
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14 pages, 3019 KB  
Article
Imbibition and Oil Drainage Mechanisms of Nanoparticle Compound Polymer Fracturing Fluids
by Herui Fan, Tianyu Jiang, Ruoxia Li, Yu Si, Yunbo Dong, Mingwei Zhao, Zhongzheng Xu and Lin Li
Gels 2026, 12(2), 136; https://doi.org/10.3390/gels12020136 - 2 Feb 2026
Viewed by 38
Abstract
Unconventional low-permeability reservoirs present significant production challenges due to the poor imbibition and displacement efficiency of conventional polymer fracturing fluids. The injection of nanoparticle (NP) compounds into polymer fracturing fluid base systems, such as linear gels or slickwater, has garnered significant research interest [...] Read more.
Unconventional low-permeability reservoirs present significant production challenges due to the poor imbibition and displacement efficiency of conventional polymer fracturing fluids. The injection of nanoparticle (NP) compounds into polymer fracturing fluid base systems, such as linear gels or slickwater, has garnered significant research interest due to their superior performance. However, previous studies have primarily focused on evaluating the fluid’s properties, while its imbibition and oil displacement mechanisms within reservoirs remain unclear. Herein, the imbibition mechanism of nanoparticle composite polymer fracturing fluid was systematically investigated from macro and micro perspectives using low-field nuclear magnetic resonance (LF-NMR), atomic force microscopy (AFM), interfacial rheology, and other technical means. The results showed that the imbibition recovery using polymer fracturing fluid was 10.91% higher than that achieved with conventional slickwater. Small and medium pores were identified as the primary contributors to oil drainage. Nanoparticles can be adsorbed on the rock wall in the deep reservoir to realize wettability reversal from oil-wet to water-wet, reducing crude oil adhesion. Furthermore, a strong interaction between the adsorbed NPs and cleanup agents at the oil–water interface was observed, which reduces interfacial tension to 0.95 mN·m−1, mitigates the Jamin effect, and enhances interfacial film deformability. NPs increase the interfacial dilatational modulus from 6.0 to 14.4 mN·m−1, accelerating fluid exchange and oil stripping. This work provides a consolidated mechanistic framework linking NP-induced interfacial modifications to enhanced pore-scale drainage, offering a scientific basis for designing next-generation fracturing fluids. We conclude that NP-compound systems hold strong potential for low-permeability reservoir development, and future efforts must focus on optimizing NP parameters for specific reservoir conditions and overcoming scalability challenges for field deployment. Full article
(This article belongs to the Section Gel Applications)
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