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Keywords = drilling mud property

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40 pages, 3997 KB  
Review
Advances in Polymer Nanocomposites for Drilling Fluids: A Review
by Shahbaz Wakeel, Ammara Aslam and Jianhua Zhang
Materials 2025, 18(20), 4809; https://doi.org/10.3390/ma18204809 - 21 Oct 2025
Viewed by 778
Abstract
Hydrocarbon exploration and extraction increasingly rely on drilling fluids that guarantee operating safety and efficiency, particularly in ultra-deep, high-temperature, and unconventional reservoirs. Traditional drilling fluids, especially for water-based muds (WBMs), have several problems, including excessive fluid loss, severe swelling in shale and instability [...] Read more.
Hydrocarbon exploration and extraction increasingly rely on drilling fluids that guarantee operating safety and efficiency, particularly in ultra-deep, high-temperature, and unconventional reservoirs. Traditional drilling fluids, especially for water-based muds (WBMs), have several problems, including excessive fluid loss, severe swelling in shale and instability in high-pressure/high-temperature (HPHT) conditions. Polymer nanocomposites (PNCs) are new types of drilling fluid additives that combine the vast surface area and reactivity of nanoparticles (NPs) with the structural flexibility and stability of polymers. This combination enhances rheology, reduces filtrate loss, and, most importantly, creates hydrophobic and pore-blocking barriers that prevent shale from swelling. This review highlights important improvements in drilling fluids with PNCs regarding exceptional rheological properties, low fluid loss, and improved suppression of the shale swelling. The particular focus was placed on the specific mechanisms and role that PNCs play in enhancing shale stability, as well as their responsibilities in improving rheology, heat resistance, and salt tolerance. Current advancements, persistent hurdles, and prospective prospects are rigorously evaluated to emphasize the scientific and industrial trajectories for the development of next-generation, high-performance drilling fluids. Moreover, the current challenges and future opportunities of PNCs in drilling fluids are discussed to motivate future contributions and explore new possibilities. Full article
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22 pages, 3800 KB  
Article
Study on Carboxymethylation Modification of Konjac Gum and Its Effect in Drilling Fluid and Fracturing Fluid
by Yongfei Li, Pengli Guo, Kun Qu, Weichao Du, Yanling Wang and Gang Chen
Gels 2025, 11(10), 792; https://doi.org/10.3390/gels11100792 - 2 Oct 2025
Viewed by 594
Abstract
With the continuous progress and innovation of petroleum engineering technology, the development of new oilfield additives with superior environmental benefits has attracted widespread attention. Konjac glucomannan (KGM) is a natural resource characterized by abundant availability, low cost, biodegradability, and environmental compatibility. Konjac gum [...] Read more.
With the continuous progress and innovation of petroleum engineering technology, the development of new oilfield additives with superior environmental benefits has attracted widespread attention. Konjac glucomannan (KGM) is a natural resource characterized by abundant availability, low cost, biodegradability, and environmental compatibility. Konjac gum easily forms a weak gel network in water, but its water solubility and thermal stability are poor, and it is easily degraded at high temperatures. Therefore, its application in drilling fluid and fracturing fluid is limited. In this paper, a method of carboxymethyl modification of KGM was developed, and a carboxymethyl group was introduced to adjust KGM’s hydrogel forming ability and stability. Carboxymethylated Konjac glucomannan (CMKG) is a water-soluble anionic polysaccharide derived from natural Konjac glucomannan. By introducing carboxymethyl groups, CMKG overcomes the limitations of the native polymer, such as poor solubility and instability, while retaining its safe and biocompatible nature, making it an effective natural polymer additive for oilfield applications. The results show that when used as a drilling fluid additive, CMKG can form a stable three-dimensional gel network through molecular chain cross-linking, significantly improving the rheological properties of the mud. Its unique gel structure can enhance the encapsulation of clay particles and inhibit clay hydration expansion. When used as a fracturing fluid thickener, the viscosity of the gel system formed by CMKG at 0.6% (w/v) is superior to that of the weak gel system of KGM. The heat resistance/shear resistance tests confirm that the gel structure remains intact under high-temperature and high-shear conditions, meeting the sand-carrying capacity requirements for fracturing operations. The gel-breaking experiment shows that the system can achieve controlled degradation within 300 min, in line with on-site gel-breaking specifications. This modification process not only improves the rheological properties and water solubility of the CMKG gel but also optimizes the gel stability and controlled degradation through molecular structure adjustment. Full article
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13 pages, 985 KB  
Article
Experimental Study on the Effect of Drilling Fluid Rheological Properties on the Strength of Brittle Mud Shale
by Wei Wang, Yi Zhang, Fengke Dou, Chengyun Ma, Jianguo Chen, Tongtong Li, Hui Zhang and Wenzhen Yuan
Processes 2025, 13(10), 3059; https://doi.org/10.3390/pr13103059 - 25 Sep 2025
Viewed by 532
Abstract
To investigate the mechanism by which the rheological properties of drilling fluids affect the stability of the wellbore in brittle mud shale, this study systematically examines the influence of drilling fluids with different rheological properties on the hydration dispersion and rock strength of [...] Read more.
To investigate the mechanism by which the rheological properties of drilling fluids affect the stability of the wellbore in brittle mud shale, this study systematically examines the influence of drilling fluids with different rheological properties on the hydration dispersion and rock strength of brittle mud shale through a series of laboratory experiments, including thermal rolling tests and uniaxial compressive strength tests on core samples. The results reveal that for weakly dispersible brittle mud shale, the rheological properties of drilling fluids have a minor effect on hydration dispersion, with rolling recovery rates consistently above 90%. However, the rheological properties of drilling fluids significantly influence the strength of brittle mud shale, and this effect is coupled with multiple factors, including rock fracture intensity index, soaking time, and confining pressure. Specifically, as the viscosity of the drilling fluid increases, the reduction in rock strength decreases; for instance, at 5 MPa confining pressure with an FII of 0.46, the strength reduction after 144 h was 69.8% in distilled water (from an initial 133.2 MPa to 40.2 MPa) compared to 36.3% with 3# drilling fluid (from 133.2 MPa to 88.7 MPa, with 100 mPa·s apparent viscosity). Both increased soaking time and confining pressure exacerbate the reduction in rock strength; a 5 MPa confining pressure, for example, caused an additional 60.9% strength reduction compared to 0 MPa for highly fractured samples (FII = 0.46) in distilled water after 144 h. Rocks with higher fracture intensity indices are more significantly affected by the rheological properties of drilling fluids. Based on the experimental results, this study proposes a strength attenuation model for brittle mud shale that considers the coupled effects of fracture intensity index, soaking time, and drilling fluid rheological properties. Additionally, the mechanism by which drilling fluid rheological properties influence the strength of brittle mud shale is analyzed, providing a theoretical basis for optimizing drilling fluid rheological parameters and enhancing the stability of wellbores in brittle mud shale formations. Full article
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16 pages, 2715 KB  
Article
Hydrate Formation and Mitigation Methods Under Multiple Operational Conditions in Deepwater Drilling
by Yanjun Li, Deli Gao, Shujie Liu, Ying Zhao, Lei Li and Shuzhan Li
Processes 2025, 13(9), 3008; https://doi.org/10.3390/pr13093008 - 21 Sep 2025
Viewed by 550
Abstract
During deepwater drilling operations, when influx gas invades the wellbore, gas hydrates may form through the combination of the gas with free water in the drilling fluid under favorable temperature and pressure conditions. This process can alter the physical properties and flow behavior [...] Read more.
During deepwater drilling operations, when influx gas invades the wellbore, gas hydrates may form through the combination of the gas with free water in the drilling fluid under favorable temperature and pressure conditions. This process can alter the physical properties and flow behavior of the wellbore fluid, potentially leading to safety incidents. To prevent natural gas hydrate formation, mitigate wellbore blockages caused by hydrates, and address the associated safety hazards, this study conducted laboratory experiments to investigate hydrate formation and remediation under multiple deepwater drilling conditions. The hydrate formation boundaries for four different drilling fluid systems—seawater-based bentonite mud, seawater polymer mud, Plus/KCl mud, and HEM mud—were determined for varying well depths and pressure–temperature conditions, and corresponding trend lines were fitted. Key results reveal that a higher carbon content promotes hydrate formation, and the phase equilibrium curves also reveal significant differences among the four drilling fluids. The hydrate aggregation states and blockage processes were clarified for three typical drilling scenarios: drilling, well killing, and drilling suspension. Hydrate formation risk is negligible during normal circulation but increases dramatically during well-killing operations, significantly shrinking the safe operational window. A comparative analysis identified that adding 1% P(M-VCL), a kinetic hydrate inhibitor, to the drilling fluid was the most effective solution, demonstrating superior performance in delaying hydrate nucleation and preventing agglomeration. The study established a complete formation–inhibition–remediation approach for hydrate management in deepwater drilling, thereby enhancing operational safety and efficiency. Full article
(This article belongs to the Section Chemical Processes and Systems)
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16 pages, 4133 KB  
Article
Preparation, Performance Evaluation and Mechanisms of a Diatomite-Modified Starch-Based Fluid Loss Agent
by Guowei Zhou, Xin Zhang, Weijun Yan and Zhengsong Qiu
Processes 2025, 13(8), 2427; https://doi.org/10.3390/pr13082427 - 31 Jul 2025
Cited by 1 | Viewed by 715
Abstract
Natural polymer materials are increasingly utilized in drilling fluid additives. Starch has come to be applied extensively due to its low cost and favorable fluid loss reduction properties. However, its poor temperature resistance and high viscosity limit its application in high-temperature wells. This [...] Read more.
Natural polymer materials are increasingly utilized in drilling fluid additives. Starch has come to be applied extensively due to its low cost and favorable fluid loss reduction properties. However, its poor temperature resistance and high viscosity limit its application in high-temperature wells. This study innovatively introduces for the first time diatomite as an inorganic material in the modification process of starch-based fluid loss additives. Through synergistic modification with acrylamide and acrylic acid, we successfully resolved the longstanding challenge of balancing temperature resistance with viscosity control in existing modification methods. The newly developed fluid loss additive demonstrates remarkable performance: It remains effective at 160 °C when used independently. When added to a 4% sodium bentonite base mud, it achieves an 80% fluid loss reduction rate—significantly higher than the 18.95% observed in conventional starch-based products. The resultant filter cake exhibits thin and compact characteristics. Moreover, this additive shows superior contamination resistance, tolerating 30% NaCl and 0.6% calcium contamination, outperforming other starch-based treatments. With starch content exceeding 75%, the product not only demonstrates enhanced performance but also achieves significant cost reduction compared to conventional starch products (typically containing < 50% starch content). Full article
(This article belongs to the Section Food Process Engineering)
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15 pages, 1622 KB  
Article
An Evaluation of the Rheological and Filtration Properties of Cow Bone Powder and Calcium Carbonate as Fluid-Loss Additives in Drilling Operations
by Humphrey Nwenenda Dike, Light Nneoma Chibueze, Sunday Ipinsokan, Chizoma Nwakego Adewumi, Oluwasanmi Olabode, Damilola Deborah Olaniyan, Idorenyen Edet Pius and Michael Abidemi Oke
Processes 2025, 13(7), 2205; https://doi.org/10.3390/pr13072205 - 10 Jul 2025
Cited by 2 | Viewed by 1712
Abstract
Some additives currently used to enhance drilling mud’s rheological qualities have a substantial economic impact on society. Carboxymethyl cellulose (CMC) and calcium carbonate (CaCO3) are currently imported. Food crops have influences on food security; hence, this research explored the potential of [...] Read more.
Some additives currently used to enhance drilling mud’s rheological qualities have a substantial economic impact on society. Carboxymethyl cellulose (CMC) and calcium carbonate (CaCO3) are currently imported. Food crops have influences on food security; hence, this research explored the potential of utilizing cow bone powder (CBP), a bio-waste product and a renewable resource, as an environmentally friendly fluid-loss additive for drilling applications, in comparison with CaCO3. Both samples (CBP and CaCO3) were evaluated to determine the most efficient powder sizes (coarse, medium, and fine powder), concentrations (5–15 g), and aging conditions (before or after aging) that would offer improved rheological and fluid-loss control. The results obtained showed that CBP had a significant impact on mud rheology when compared to CaCO3. Decreasing the particle size (coarse to fine particles) and increasing the concentration from 5 to 15 g positively impacted mud rheology. Among all the conditions analyzed, fine-particle CBP with a 15 g concentration produced the best characteristics, including in the apparent viscosity (37 cP), plastic viscosity (29 cP), and yield point (25.5 lb/100 ft2), and a gel strength of 16 lb/100 ft2 (10 s) and 28 lb/100 ft2 (10 min). The filtration control ability of CaCO3 was observed to be better than that of the coarse and medium CBP particle sizes; however, fine-particle-size CBP demonstrated a 6.1% and 34.6% fluid-loss reduction at 10 g and 15 g concentrations when compared to respective amounts of CaCO3. The thermal behavior of the Mud Samples demonstrated that it positively impacted rheology before aging. In contrast, after aging, it exhibited a negative effect where samples grew more viscous and exceeded the API standard range for mud properties. Therefore, CBP’s excellent rheological and fluid-loss control ability makes it a potential, sustainable, and economically viable alternative to conventional materials. This superior performance enhances the thinning properties of drilling muds in stationary and circulating conditions. Full article
(This article belongs to the Section Environmental and Green Processes)
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24 pages, 4242 KB  
Article
Numerical Simulation of Drilling Fluid-Wellbore Interactions in Permeable and Fractured Zones
by Diego A. Vargas Silva, Zuly H. Calderón, Darwin C. Mateus and Gustavo E. Ramírez
Math. Comput. Appl. 2025, 30(3), 60; https://doi.org/10.3390/mca30030060 - 30 May 2025
Viewed by 1051
Abstract
In well drilling operations, interactions between drilling fluid water-based and the well-bore present significant challenges, often escalating project costs and timelines. Particularly, fractures (both induced and natural) and permeable zones at the wellbore can result in substantial mud loss or increased filtration. Addressing [...] Read more.
In well drilling operations, interactions between drilling fluid water-based and the well-bore present significant challenges, often escalating project costs and timelines. Particularly, fractures (both induced and natural) and permeable zones at the wellbore can result in substantial mud loss or increased filtration. Addressing these challenges, our research introduces a novel coupled numerical model designed to precisely calculate fluid losses in fractured and permeable zones. For the permeable zone, fundamental variables such as filtration velocity, filtrate concentration variations, permeability reduction, and fluid cake growth are calculated, all based on the law of continuity and convection-dispersion theory. For the fracture zone, the fluid velocity profile is determined using the momentum balance equation and both Newtonian and non-Newtonian rheology. The model was validated against laboratory data and physical models, and adapted for field applications. Our findings emphasize that factors like mud particle size, shear stress, and pressure differential are pivotal. Effectively managing these factors can significantly reduce fluid loss and mitigate formation damage caused by fluid invasion. Furthermore, the understanding gathered from studying mud behavior in both permeable and fractured zones equips drilling personnel with valuable information related to the optimal rheological properties according to field conditions. This knowledge is crucial for optimizing mud formulations and strategies, ultimately aiding in the reduction of non-productive time (NPT) associated with wellbore stability issues. Full article
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15 pages, 1786 KB  
Article
Comparison and Application of Pore Pressure Prediction Methods for Carbonate Formations: A Case Study in Luzhou Block, Sichuan Basin
by Wenzhe Li, Pingya Luo, Yatian Li, Jinghong Zhou, Xihui Hu, Qiutong Wang, Yiguo He and Yi Zhang
Energies 2025, 18(10), 2647; https://doi.org/10.3390/en18102647 - 20 May 2025
Viewed by 804
Abstract
The Luzhou Block in the Sichuan Basin hosts a widely distributed high-quality shale gas reservoir. However, the overlying carbonate strata pose considerable engineering challenges, including severe risks of subsurface fluid loss and wellbore collapse. These challenges are primarily attributed to inaccuracies in pore [...] Read more.
The Luzhou Block in the Sichuan Basin hosts a widely distributed high-quality shale gas reservoir. However, the overlying carbonate strata pose considerable engineering challenges, including severe risks of subsurface fluid loss and wellbore collapse. These challenges are primarily attributed to inaccuracies in pore pressure prediction, which significantly constrains the safety and efficiency of drilling operations in carbonate formations. To address this issue, this study systematically investigates and compares three classical pore pressure prediction approaches—namely, the equivalent depth method, the Eaton method, and the effective stress method—within the geological context of the Luzhou Block. A novel fitting strategy based on laboratory core experimental data is introduced, whereby empirical relationships between field-measured parameters and rock mechanical properties are established to improve model robustness in geologically complex formations. The optimized effective stress model is subsequently applied to the carbonate reservoir interval, and its prediction outcomes are evaluated against measured pore pressure data. The results demonstrate that the effective stress method achieves the highest prediction accuracy, with a maximum deviation of 8.4% and an average deviation of 5.3%. In comparison, the equivalent depth and Eaton methods yield average errors of 12.5% and 12.2%, respectively. These findings suggest that the effective stress method exhibits superior adaptability and reliability for pore pressure prediction in carbonate formations of the Luzhou Block, and holds significant potential for guiding mud density design and improving the operational safety of drilling programs. Full article
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12 pages, 1944 KB  
Article
An Experimental Study on Mud Adhesion Performance of a PDC Drill Bit Based on a Biomimetic Non-Smooth Surface
by Ming Chen and Qingchao Li
Processes 2025, 13(5), 1464; https://doi.org/10.3390/pr13051464 - 10 May 2025
Viewed by 1271
Abstract
In recent years, polycrystalline diamond compact (PDC) drill bits have seen significant advancements. They have replaced over 90% of the workload traditionally handled by roller cone bits and have become the predominant choice in energy drilling due to their superior efficiency and durability. [...] Read more.
In recent years, polycrystalline diamond compact (PDC) drill bits have seen significant advancements. They have replaced over 90% of the workload traditionally handled by roller cone bits and have become the predominant choice in energy drilling due to their superior efficiency and durability. However, PDC drill bits are susceptible to adhesion of rock cuttings during drilling in muddy formations, leading to mud accumulation on the bit surface. This phenomenon can cause drill bit failure and may contribute to downhole complications, including tool failure and borehole instability. The adhesion issue between PDC drill bits and mud rock cuttings underground is primarily influenced by the normal adhesion force between the drill bit surface and the mud rock cuttings. Therefore, biological non-smooth surface technology is applied to the prevention and control of drill bit balling. It is an optimal selection of biomimetic non-smooth surface structures with reduced adhesion and detachment properties. A non-smooth surface model for the PDC drill bit body is established through the analysis of the morphological characteristics of natural biological non-smooth surfaces. An experimental platform is designed and manufactured to evaluate the adhesion performance of non-smooth surface specimens. Indoor experiments are conducted to test the normal adhesion force of non-smooth surface specimens under varying morphologies, sizes, and contact times with clay. Finally, the anti-adhesion performance of the non-smooth surface unit structures is then analyzed. The normal adhesion force with a contact time of 12 h is as follows: 340 Pa of big square raised, 250 Pa of middle square raised, 190 Pa of small square raised, 315 Pa of big circular groove, 280 Pa of middle circular groove, 200 Pa of small circular groove, 225 Pa of big dot pit, 205 Pa of middle dot pit, and 130 Pa of small dot pit. Compared with the normal adhesion force of 550 Pa for smooth surface specimens with a contact time of 12 h, the anti-adhesion properties of the three non-smooth surface unit structure specimens designed in this paper were verified. We analyzed the anti-adhesion performance of non-smooth surface unit structures. At the critical contact time when the adhesion force tends to stabilize, the adhesion forces of different specimens are as follows: 330 Pa of big square raised, 237.5 Pa of middle square raised, 175 Pa of small square raised, 290 Pa of big circular groove, 250 Pa of middle circular groove, 160 Pa of small circular groove, 210 Pa of big dot pit, 185 Pa of middle dot pit, and 115 Pa of small dot pit. The results indicate that the anti-adhesion effect of small dot pit structures is the most effective, while the anti-adhesion effect of large square convex structures is the least effective. As the size of the unit structure decreases, it becomes more similar to the surface size of the organism. Additionally, a shorter contact time with clay leads to a better anti-adhesion effect. These findings provide new insights and research directions for the effective prevention and control of mud wrapping on PDC drill bits. Full article
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22 pages, 112804 KB  
Article
Lacustrine Gravity-Flow Deposits and Their Impact on Shale Pore Structure in Freshwater Lake Basins: A Case Study of Jurassic Dongyuemiao Member, Sichuan Basin, SW China
by Qingwu Yuan, Yuqiang Jiang, Zhujiang Liu, Xiangfeng Wei and Yifan Gu
Minerals 2025, 15(5), 473; https://doi.org/10.3390/min15050473 - 30 Apr 2025
Viewed by 708
Abstract
In recent years, the successful application of gravity-flow deposit theory in major petroliferous basins in China had attracted extensive attention in the field of sedimentology and had become a key research frontier. This study utilized core, drilling, logging, and microphotograph data, along with [...] Read more.
In recent years, the successful application of gravity-flow deposit theory in major petroliferous basins in China had attracted extensive attention in the field of sedimentology and had become a key research frontier. This study utilized core, drilling, logging, and microphotograph data, along with low-temperature nitrogen adsorption and high-pressure mercury injection experiments. It discussed the characteristics of gravity-flow deposits, sedimentary microfacies, sedimentary models, and the significance of gravity-flow deposits to pore heterogeneity in shale reservoirs, focusing on the first submember of the Dongyuemiao Member (referred to as the Dong 1 Member) in the Fuling area of the Sichuan Basin. The results indicated the development of four types of mudrock in the Dong 1 Member: massive to planar laminated shell mudrock (F1), planar laminated bioclastic mudrock (F2), planar laminated silty mudrock (F3), and massive mudrock (F4). These corresponded to debris flow deposits (F1, F2), turbidite deposits (F3), and suspension deposits (F4). According to the characteristics of lithofacies combinations and sedimentary features, four sedimentary microfacies were identified: gravity-flow channel, tongue-shaped, lobate, and semi-deep lake mud. The Shell Banks were disturbed by earthquakes, tides, storms, and other activities. Silt, clay, fossil fragments, plant debris, and other materials were deposited under the influence of gravity, mixing with surrounding water to form an unbalanced and unstable fluid. When pore pressure exceeded viscous resistance, the mixed fluid became unbalanced, and gravity flow began to migrate from the slope to the center of the lake basin. A sedimentary unit of gravity-flow channel-tongue-shaped-lobate was developed in the Fuling area. The Fuling area’s gravity-flow depositional system resulted in distinct microfacies within the Dongyuemiao Member, each exhibiting characteristic lithofacies associations. Notably, lobate deposits preferentially developed lithofacies F3, which is distinguished by significantly higher clay mineral content (60.8–69.1 wt%) and elevated TOC levels (1.53–2.45 wt%). These reservoir properties demonstrate statistically significant positive correlations, with clay mineral content strongly influencing total pore volume and TOC content specifically enhancing mesopore development (2–50 nm pores). Consequently, the F3 lithofacies within lobe deposits emerges as the most prospective shale gas reservoir unit in the study area, combining optimal geochemical characteristics with favorable pore-structure attributes. Full article
(This article belongs to the Special Issue Element Enrichment and Gas Accumulation in Black Rock Series)
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28 pages, 8440 KB  
Article
Feasibility Study of Biodegradable Vegetable Peels as Sustainable Fluid Loss Additives in Water-Based Drilling Fluids
by Olajide Ibrahim Oladipo, Foad Faraji, Hossein Habibi, Mardin Abdalqadir, Jagar A. Ali and Perk Lin Chong
J 2025, 8(1), 10; https://doi.org/10.3390/j8010010 - 1 Mar 2025
Cited by 5 | Viewed by 3318
Abstract
Drilling fluids are vital in oil and gas well operations, ensuring borehole stability, cutting removal, and pressure control. However, fluid loss into formations during drilling can compromise formation integrity, alter permeability, and risk groundwater contamination. Water-based drilling fluids (WBDFs) are favored for their [...] Read more.
Drilling fluids are vital in oil and gas well operations, ensuring borehole stability, cutting removal, and pressure control. However, fluid loss into formations during drilling can compromise formation integrity, alter permeability, and risk groundwater contamination. Water-based drilling fluids (WBDFs) are favored for their environmental and cost-effective benefits but often require additives to address filtration and rheological limitations. This study explored the feasibility of using vegetable waste, including pumpkin peel (PP), courgette peel (CP), and butternut squash peel (BSP) in fine (75 μm) and very fine (10 μm) particle sizes as biodegradable WBDF additives. Waste vegetable peels were processed using ball milling and characterized via FTIR, TGA, and EDX. WBDFs, prepared per API SPEC 13A with 3 wt% of added additives, were tested for rheological and filtration properties. Results highlighted that very fine pumpkin peel powder (PP_10) was the most effective additive, reducing fluid loss and filter cake thickness by 43.5% and 50%, respectively. PP_10 WBDF maintained mud density, achieved a pH of 10.52 (preventing corrosion), and enhanced rheological properties, including a 50% rise in plastic viscosity and a 44.2% increase in gel strength. These findings demonstrate the remarkable potential of biodegradable vegetable peels as sustainable WBDF additives. Full article
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19 pages, 11104 KB  
Article
Microbially Induced Calcite Precipitation (MICP) Improved Drilling Fluid Optimization for Gravel Stratum
by Rui Pan, Zhou Shu, Yumin Chen, Xiaobing Sha, Xinquan Zhang and Yi Han
Processes 2025, 13(1), 162; https://doi.org/10.3390/pr13010162 - 9 Jan 2025
Viewed by 1972
Abstract
During the exploration of the gravel stratum, incidents such as wellbore leakage, stuck drilling, and unstable wellbore walls frequently occur. These issues lead to diminished drilling efficiency and prolonged construction timelines, ultimately adversely affecting the core recovery rate, resulting in a significant waste [...] Read more.
During the exploration of the gravel stratum, incidents such as wellbore leakage, stuck drilling, and unstable wellbore walls frequently occur. These issues lead to diminished drilling efficiency and prolonged construction timelines, ultimately adversely affecting the core recovery rate, resulting in a significant waste of manpower and material resources. To address the issue of hole collapse during drilling, the microbially induced calcite carbonate precipitation (MICP) technique was employed to enhance the properties of bentonite mud drilling fluids. This study analyzed the effects of three factors, i.e., bentonite, biological solution, and barite powder, on the bentonite mud bio-cementation effectiveness through an orthogonal experiment and response surface methodology (RSM). The biological mechanism was examined using scanning electron microscopy (SEM). The experimental results indicated that optimal formulation was achieved when the mass fraction of bentonite was 13.96%, the biological solution comprised 0.6% xanthan gum and 0.4% carboxymethyl cellulose, and the mass fraction of barite was 25%. This research explores the application potential of MICP in enhancing the rheological properties of bentonite mud drilling fluids, which provides new insights and technical references for optimizing their performance. Full article
(This article belongs to the Section Chemical Processes and Systems)
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12 pages, 5172 KB  
Article
Synthesis and Mechanism Study of an Environmental Additive Used in Water-Based Drilling Fluids from Bovine Bone Glue
by Lei Guo, Jie Yang, Lubin Yu, Bingqian Song and Weichao Du
Materials 2024, 17(22), 5547; https://doi.org/10.3390/ma17225547 - 13 Nov 2024
Viewed by 1047
Abstract
At present, animal bone glue has been widely used in industry, but there are no relevant research reports on its application in the petroleum industry. In this paper, the rheological properties, inhibition, filtration, and temperature resistance performance of modified bone glue (Mbg) were [...] Read more.
At present, animal bone glue has been widely used in industry, but there are no relevant research reports on its application in the petroleum industry. In this paper, the rheological properties, inhibition, filtration, and temperature resistance performance of modified bone glue (Mbg) were evaluated in water-based drilling fluids, and the results showed that Mbg can significantly affect the performance of water-based muds with minimal dosage, and temperature resistance of Mbg could reach up to 130 °C. The inhibition mechanism of Mbg in drilling fluids was investigated by infrared spectroscopy (FT-IR), X-ray diffraction (XRD), zeta potential, thermogravimetric analysis (TGA), and scanning electron microscope (SEM). Results revealed that when 2% Mbg was added, a three-dimensional network structure was formed in an aqueous solution, which reduced the water content from 4.83% to 4.23%. FT-IR analysis showed that Mbg strongly adsorbed onto clay through hydrogen bonding, which reduced the clay particles in based muds from 1.251 µm to 0.789 µm and effectively controlled the filtration loss of the drilling fluids. Full article
(This article belongs to the Special Issue Environmentally Friendly Materials)
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16 pages, 9965 KB  
Article
Factors Influencing Radiation Sound Fields in Logging While Drilling Using an Acoustic Dipole Source
by Jingji Cao, Ruibao Qin, Xiongyan Li, Xinyu Ye, Chuang Hei, Zhongxu Yin and Peng Wang
Processes 2024, 12(10), 2118; https://doi.org/10.3390/pr12102118 - 29 Sep 2024
Viewed by 1406
Abstract
With the increasing number of complex well types in the development stage of oil and gas fields, it is becoming increasingly urgent to use remote detection logging while drilling (LWD) to explore the geological structures in a formation. In this paper, the feasibility [...] Read more.
With the increasing number of complex well types in the development stage of oil and gas fields, it is becoming increasingly urgent to use remote detection logging while drilling (LWD) to explore the geological structures in a formation. In this paper, the feasibility and reliability of the dipole remote detection of logging while drilling are demonstrated theoretically. For this purpose, we use an asymptotic solution of elastic wave far-field displacement to derive the calculation formula for the radiation pattern and energy flux of an LWD dipole source. The effects of influencing factors, including the source frequency, formation property, drill collar size, and mud parameter, on the radiation pattern and energy flux are analyzed. The results show that the horizontally polarized shear wave (SH-wave) has a greater advantage in imaging the reflector compared with the cases of the compressive wave (P-wave) and vertically polarized shear wave (SV-wave), which indicates the dominance of the SH-wave in dipole remote detection while drilling. The optimal source excitation frequency of 2.5 kHz and inner and outer radii of the drill collar of 0.02 and 0.1 m, respectively, should be considered in the design of an LWD dipole shear wave reflection tool. However, the heavy drilling mud is not conducive to remote detection during logging while drilling. In addition, the reflection of the SH-wave for the LWD condition is simulated. Under the conditions of optimal source frequency, drill collar size, and mud parameters, the reflection of the SH-wave signal is still detected under the fast formation. Full article
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16 pages, 964 KB  
Article
Experimental Investigations of Assessment of Acute Toxicity of Drilling Mud
by Arstan Mamyrbayev, Saule Bermagambetova, Kuanysh Baytenov, Zhanat Komekbay, Laura Sakebayeva, Umit Satybaldiyeva, Gulmira Yerimbetova and Kulyash Zhilisbayeva
Toxics 2024, 12(10), 700; https://doi.org/10.3390/toxics12100700 - 27 Sep 2024
Cited by 4 | Viewed by 1740
Abstract
At present, the main technological stages of oil production related to drilling operations require the use of a wide variety of drilling mud, which has a complex, multicomponent chemical composition. The drilling mud used and the resulting drilling waste must be safe for [...] Read more.
At present, the main technological stages of oil production related to drilling operations require the use of a wide variety of drilling mud, which has a complex, multicomponent chemical composition. The drilling mud used and the resulting drilling waste must be safe for human health and the environment. The toxicity and hazard of drilling mud at this point in time remain poorly understood scientific problems and require detailing and studying in toxicological terms. The real degree of hazard and toxicity of drilling mud can only be determined by an experimental method, since its composition, which changes depending on the nature of the technological process and its degree of depletion, is not constant, which can change the toxicological properties. In an experiment conducted on adult male rats, under conditions of a single intragastric injection of drilling mud, new data were obtained regarding the parameters of its toxicity and hazard. The use of a wide variety of methods for determining lethal doses of drilling mud, including the probit analysis method, made it possible not only to substantiate the mean lethal dose of drilling mud but also other parameters of toxicity and survival of animals in the experimental groups. Features of eating behavior and body weight dynamics and the nature of the behavioral reactions revealed by the number and duration of stands and frequency and duration of grooming also indicate the presence of dose-dependent effects. Full article
(This article belongs to the Special Issue Occupational Exposure to Chemicals, Aerosols and Toxic Materials)
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